Chemical Engineering - Teerthanker Mahaveer University
Chemical Engineering - Teerthanker Mahaveer University
Chemical Engineering - Teerthanker Mahaveer University
You also want an ePaper? Increase the reach of your titles
YUMPU automatically turns print PDFs into web optimized ePapers that Google loves.
Study & Evaluation Scheme<br />
of<br />
Bachelor of Technology<br />
(<strong>Chemical</strong> <strong>Engineering</strong>)<br />
[Applicable w.e.f. Academic Session 2012-13 till revised]<br />
TEERTHANKER MAHAVEER UNIVERSITY<br />
N.H.-24, Delhi Road, Moradabad, Uttar Pradesh-244001<br />
Website: www.tmu.ac.in<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 1
TEERTHANKER MAHAVEER UNIVERSITY<br />
(Established under Govt. of U. P. Act No. 40, 2008)<br />
Delhi Road, Bagarpur, Moradabad (U.P)-244001<br />
Study & Evaluation Scheme<br />
Bachelor of Technology<br />
SUMMARY<br />
Programme : B.Tech ( <strong>Chemical</strong> <strong>Engineering</strong>)<br />
Duration : Four year full time (Eight Semesters)<br />
Medium : English<br />
Minimum Required Attendance : 75 %<br />
Credit :<br />
Maximum Credit<br />
:<br />
:<br />
194<br />
Minimum credit required for the degree : 190<br />
Assessment- Theory (Other than<br />
Professional Communication)<br />
Internal Evaluation (Theory Papers)<br />
Evaluation of Practical/Project Reports,<br />
Seminar & Professional Communication<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
:<br />
Internal External Total<br />
30 70 100<br />
Class Class Class<br />
Other<br />
Test Test Test Assignment(s) Activity<br />
I II III<br />
(including Total<br />
Best two out of the<br />
three<br />
Mini-3 attendance)<br />
10 10 10 5 5 30<br />
:<br />
Internal External Total<br />
50 50 100<br />
External Internal<br />
Duration of Examination :<br />
3 hrs. 1 ½ hrs<br />
To qualify the course a student is required to secure a minimum of 40 marks in aggregate including the<br />
semester end examination and teachers continuous evaluation.(i.e. both internal and external).<br />
A Candidate who secures less than of 40% of marks in a course shall be deemed to have failed in that<br />
course. The student should have at least 50% marks in aggregate to clear the semester. In case a student<br />
has more than 40% in each course, but less than 50% overall in a semester , he/she shall re-appear in<br />
courses where the marks are less than 50% to achieve the required aggregate percentage of 50% in the<br />
semester.<br />
Question Paper Structure<br />
1. The question paper shall consist of eight questions. Out of which first question shall be of short answer<br />
type (not exceeding 50 words) and will be compulsory. Question No. 1 shall contain 8 parts<br />
representing all units of the syllabus and students shall have to answer any five (weightage 4 marks<br />
each).<br />
2. Out of the remaining seven questions, student shall be required to attempt any five questions. There<br />
will be minimum one and maximum two questions from each unit of the syllabus. The weightage of<br />
Question No. 2 to 8 shall be 10 marks each.<br />
3. Usually each question in the examination Study should & be Evaluation designed to have Scheme a numerical component.<br />
Programme: B.Tech. (<strong>Chemical</strong> <strong>Engineering</strong>)<br />
Semester I<br />
Page 2
S. Course<br />
Subject<br />
Periods Credit Evaluation Scheme<br />
No Code<br />
L T P Internal External Total<br />
1 EAS101 <strong>Engineering</strong> Mathematics-I 3 1 - 4 30 70 100<br />
2<br />
3<br />
EAS102/202 Physics - I<br />
EAS103/203 Chemistry<br />
EME101/201 <strong>Engineering</strong> Mechanics<br />
EME102/202 Manufacturing Science<br />
3 - - 3 30 70 100<br />
3 - - 3 30 70 100<br />
4 ECS101/201 Computer Basics & C Programming 3 - - 3 30 70 100<br />
EAS 104/204 Environmental Science<br />
5 EEE101/201 Basic Electrical <strong>Engineering</strong> 3 - - 3 30 70 100<br />
EEC101/201 Basic Electronics <strong>Engineering</strong><br />
6 EHM101 Foundation English-I 2 - 2 3 30 70 100<br />
7<br />
8<br />
9<br />
10<br />
S.<br />
No<br />
.<br />
EAS151/251 Physics (Lab)<br />
EAS152/252 Chemistry (Lab)<br />
EME151/251 <strong>Engineering</strong> Mechanics (Lab)<br />
ECS151/251 Computer Basics & C Programming<br />
(Lab)<br />
EME152/252 <strong>Engineering</strong> Drawing (Lab)<br />
- - 3 1.5 50 50 100<br />
- - 3 1.5 50 50 100<br />
- - 4 2 50 50 100<br />
EME153/253 Workshop Practice (Lab)<br />
EEE151/251 Basic Electrical <strong>Engineering</strong> (Lab) - - 3 1.5 50 50 100<br />
EEC151/251 Basic Electronics <strong>Engineering</strong> (Lab)<br />
Total 17 1 15 25.5 440 560 1000<br />
Course<br />
Code<br />
Subject<br />
Semester II<br />
Periods Credit Evaluation Scheme<br />
L T P Internal External Total<br />
1 EAS201 <strong>Engineering</strong> Mathematics-II 3 1 - 4 30 70 100<br />
2<br />
3<br />
EAS102/202 Physics - I<br />
EAS103/203 Chemistry<br />
EME101/201 <strong>Engineering</strong> Mechanics<br />
3 - - 3 30 70 100<br />
3 - - 3 30 70 100<br />
EME102/202 Manufacturing Science<br />
4 ECS101/201 Computer Basics & C Programming 3 - - 3 30 70 100<br />
EAS 104/204 Environmental Science<br />
5 EEE101/201 Basic Electrical <strong>Engineering</strong><br />
3 - - 3 30 70 100<br />
EEC101/201 Basic Electronics <strong>Engineering</strong><br />
6 EHM201 Foundation English-II 2 - 2 3 30 70 100<br />
7 EAS151/251 Physics (Lab)<br />
- - 3 1.5 50 50 100<br />
EAS152/252 Chemistry (Lab)<br />
8 EME151/251 <strong>Engineering</strong> Mechanics (Lab)<br />
- - 3 1.5 50 50 100<br />
ECS151/251 Computer Basics & C Programming<br />
(Lab)<br />
9 EME152/252 <strong>Engineering</strong> Drawing (Lab) - - 4 2 50 50 100<br />
EME153/253 Workshop Practice (Lab)<br />
10 EEE151/251 Basic Electrical <strong>Engineering</strong> (Lab) - - 3 1.5 50 50 100<br />
EEC151/251 Basic Electronics <strong>Engineering</strong> (Lab)<br />
Total 17 1 15 25.5 440 560 1000<br />
S.<br />
No.<br />
Subject<br />
Code<br />
Subject<br />
Semester III<br />
Periods Credit Evaluation Scheme<br />
L T P Intern External Total<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 3
1 ECH301 <strong>Chemical</strong> <strong>Engineering</strong><br />
Thermodynamics-I<br />
3 - - 3<br />
al<br />
30 70 100<br />
2 ECH302 Physical <strong>Chemical</strong><br />
Technology<br />
3 - - 3 30 70 100<br />
3 ECH303 Applied Chemistry 3 - - 3 30 70 100<br />
4 ECH304 <strong>Chemical</strong> Process<br />
Calculations<br />
3 - - 3 30 70 100<br />
5 EME 305 Industrial <strong>Engineering</strong> 3 - - 3 30 70 100<br />
6 EAS301/ Mathematics –III / Physics 3 1 - 4 30 70 100<br />
EAS302 II<br />
7 ECH351 <strong>Chemical</strong> <strong>Engineering</strong><br />
Thermodynamics-I (Lab)<br />
- - 4 2 50 50 100<br />
8 ECH352 Physical <strong>Chemical</strong><br />
Technology (Lab)<br />
- - 4 2 50 50 100<br />
9 ECH353 Applied Chemistry (Lab) - - 3 1.5 50 50 100<br />
Total 18 1 11 24.5 330 570 900<br />
Additional Courses for Lateral Entry Students with B.Sc. background, to be taken in III and IV<br />
semester and all should pass with minimum of 40% marks: credits will not be added.<br />
1 EME152/252 <strong>Engineering</strong> Drawing Lab - - 3 1.5 50 50 100<br />
2 EME101/201<br />
EME102/202<br />
<strong>Engineering</strong> Mechanics<br />
Manufacturing Science<br />
3 - - 3 30 70 100<br />
3 EME153/253<br />
EME151/251<br />
Workshop Practice<br />
(Lab)<br />
<strong>Engineering</strong> Mechanics<br />
(Lab)<br />
- - 3 1.5 50 50 100<br />
S. Subject<br />
Subject<br />
Semester IV<br />
Periods Credit Evaluation Scheme<br />
No. Code<br />
L T P<br />
Internal External Total<br />
1 ECH401 Heat Transfer 3 - - 3 30 70 100<br />
2 ECH 402 Inorganic <strong>Chemical</strong><br />
Technology<br />
3 - - 3 30 70 100<br />
3 ECH403 Material Science &<br />
Technology<br />
3 - - 3 30 70 100<br />
4 ECH404 <strong>Chemical</strong> <strong>Engineering</strong><br />
Thermodynamics-II<br />
3 - - 3 30 70 100<br />
5 ECH405 Numerical Methods in<br />
<strong>Chemical</strong> <strong>Engineering</strong><br />
3 1 - 4 30 70 100<br />
6 EAS401/ Mathematics –III / Physics 3 1 - 4 30 70 100<br />
EAS402 II<br />
7 ECH451 Heat Transfer (Lab) - - 4 2 50 50 100<br />
8 ECH452 Inorganic <strong>Chemical</strong><br />
Technology (Lab)<br />
- - 4 2 50 50 100<br />
Total 18 1 8 24 280 520 800<br />
Semester V<br />
S. Subject Subject Periods Credit Evaluation Scheme<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 4
No. Code L T P Internal External Total<br />
1 ECH501 Process Instrumentation 3 - - 3 30 70 100<br />
2 ECH502 Organic <strong>Chemical</strong><br />
Technology<br />
3 - - 3 30 70 100<br />
3 ECH503 Mass Transfer –I 3 - - 3 30 70 100<br />
4 ECH504 Spectroscopy Techniques 3 - - 3 30 70 100<br />
5 ECH505 Environmental <strong>Engineering</strong> 3 - - 3 30 70 100<br />
6<br />
EHM503<br />
<strong>Engineering</strong> and Managerial<br />
Economics<br />
3 - - 3 30 70 100<br />
7 ECH551 Process Instrumentation<br />
(Lab)<br />
- - 4 2 50 50 100<br />
8 ECH552 Organic <strong>Chemical</strong><br />
Technology (Lab)<br />
- - 4 2 50 50 100<br />
9 ECH553 Mass Transfer-I (Lab) - - 3 1.5 50 50 100<br />
10 ECH 591 Industrial Training<br />
(4 Weeks) & Presentation<br />
- - - 2 50 50 100<br />
Total 18 - 11 25.5 380 620 1000<br />
Semester VI<br />
S. Subject<br />
Subject<br />
Periods Credit Evaluation Scheme<br />
No. Code<br />
L T P<br />
Internal External Total<br />
1 ECH601 <strong>Chemical</strong> Reaction<br />
<strong>Engineering</strong>-I<br />
3 - - 3 30 70 100<br />
2 ECH602 Mass Transfer -II 3 - - 3 30 70 100<br />
3 ECH603 Petroleum Refining 3 - - 3 30 70 100<br />
4 ECH604 Biochemical Technology 3 - - 3 30 70 100<br />
5 EHM601 Technical Writing 2 - 2 3 30 70 100<br />
6 EHM 602 Industrial Psychology 3 - - 3 30 70 100<br />
7 ECH651 <strong>Chemical</strong> Reaction<br />
<strong>Engineering</strong>-I (Lab)<br />
- - 3 1.5 50 50 100<br />
8 ECH652 Mass Transfer –II (Lab) - - 3 1.5 50 50 100<br />
ECH605<br />
Elective I – Select any one course<br />
<strong>Chemical</strong> Plant Safety and<br />
Occupational Hazard<br />
9 ECH606 Fertilizer Technology 3 - - 3 30 70 100<br />
ECH607 Rubber Science &<br />
Technology<br />
Total 20 - 18 24 310 590 900<br />
Semester VII<br />
S. Subject Subject Periods Credit Evaluation Scheme<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 5
No. Code L T P Internal External Total<br />
1 ECH701 <strong>Chemical</strong> Reaction Eng. II 3 - - 3 30 70 100<br />
2 ECH702 Introduction to Oil/Fat<br />
Technology<br />
3 - - 3 30 70 100<br />
3 ECH703 Bioprocess <strong>Engineering</strong> 3 - - 3 30 70 100<br />
4 ECH704 Sugar Technology 3 - - 3 30 70 100<br />
5 ECH751 <strong>Chemical</strong> Reaction-II (Lab) - - 4 2 50 50 100<br />
6<br />
ECH752 Introduction to Oil/Fat<br />
Technology (Lab)<br />
- - 4 2 50 50 100<br />
ECH705<br />
Elective II* – Select any one course<br />
Process Equipment Design<br />
7<br />
8<br />
9<br />
ECH706 Air Pollution and Control<br />
Equipments<br />
ECH707 Industrial Pollution Control<br />
Industrial Training & - - - 3 50<br />
100<br />
ECH791 Presentation(6 Weeks)<br />
Project Work Phase-1<br />
50<br />
(Synopsis, Literature Survey - - 6 3 100<br />
100<br />
ECH799 & Presentation)<br />
-<br />
Total 15 - 14 25 400 500 900<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
3 - - 3 30 70 100<br />
Semester VIII<br />
S. Subject<br />
Subject<br />
Periods Credit Evaluation Scheme<br />
No. Code<br />
L T P<br />
Internal External Total<br />
1<br />
ECH801 Polymer Science &<br />
Technology<br />
3 - - 3 30 70 100<br />
2 ECH802 Pulp and Paper Technology 3 - - 3 30 70 100<br />
3<br />
ECH 851 Polymer Science &<br />
Technology (Lab)<br />
- - 4 2 50 50 100<br />
ECH 899 Project Work Phase-2 - - 18 9 50 50 100<br />
4<br />
(Report, Analysis,<br />
Implementation/ Simulation<br />
and Presentation)<br />
ECH803<br />
Elective III* – Select any one course<br />
Industrial Safety & Hazard<br />
Management<br />
5<br />
ECH804<br />
ECH 805<br />
Energy Management<br />
Catalysis Processes<br />
3 - - 3<br />
30 70 100<br />
ECH 806 Industrial Pollution<br />
Abatement & Waste<br />
Management<br />
Total 9 - 22 20 190 310 500<br />
Semester I<br />
ENGINEERING MATHEMATICS-I<br />
Course Code: EAS101 L T P C<br />
Page 6
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
3 1 0 4<br />
Objective:<br />
• To familiarize the basics of matrices, differential calculus, multiple integrals and vector calculus.<br />
• To solve all problems related to matrices, calculus and vectors.<br />
Course Contents<br />
Unit I (Lectures 08)<br />
Matrices: Elementary row and column transformation; Rank of matrix; Linear dependence; Consistency<br />
of linear system of equations; Characteristic equation; Cayley-Hamilton Theorem; Eigen values and<br />
Eigen vectors; Diagonalization; Complex and unitary matrices.<br />
Unit II (Lectures 08)<br />
Differential Calculus-I: Successive differentiation; Leibnitz theorem; Partial differentiation; Euler’s<br />
theorem; Curve tracing; Change of variables; Expansion of function of several variables<br />
Unit III (Lectures 08)<br />
Differential Calculus–II: Jacobian; Approximation of errors; Extrema of functions of several variables;<br />
Lagrange’s method of multipliers (Simple applications).<br />
Unit IV (Lectures 08)<br />
Multiple Integrals: Double and triple integral; Change of order & Change of variables; Beta and Gamma<br />
functions; Applications to area, volume; Dirichlet integral and applications.<br />
Unit V (Lectures 08)<br />
Vector Calculus: Point functions; Gradient, Divergence and Curl of a vector and their physical<br />
interpretations; Line, Surface and Volume integrals; Green’s & Stokes’ theorem; Gauss’ divergence<br />
theorem.<br />
Text Books<br />
1. Grewal B.S., Higher <strong>Engineering</strong> Mathematics, Khanna Publishers.<br />
2. Prasad C., <strong>Engineering</strong> Mathematics for Engineers, Prasad Mudralaya.<br />
3. Dass H.K., <strong>Engineering</strong> Mathematics Vol-I, S. Chand.<br />
Reference Books<br />
1. Kreyszig E., Advanced <strong>Engineering</strong> Mathematics, Wiley Eastern.<br />
2. Piskunov N, Differential & Integral Calculus, Moscow Peace Publishers.<br />
3. Narayan Shanti, A Text book of Matrices, S. Chand.<br />
Page 7
Semester I/II<br />
PHYSICS-I<br />
Course Code: EAS102/EAS 202 L T P C<br />
3 0 0 3<br />
Objective:<br />
• To understand the fundamentals of physics like interference, diffraction, lasers etc.<br />
Course Contents<br />
Unit I (Lectures 08)<br />
Semiconductor Physics: Distinction among metal, insulator & semiconductor on the basis of band<br />
theory; Intrinsic and Extrinsic semiconductors; Basic concepts of Fermi level; Electron and hole<br />
mobilities; Electrical conductivity and Hall effect; Basics of p-n Junction.<br />
Unit II (Lectures 08)<br />
Interference: Basics of interference of light; coherent Sources, Conditions of Interference; Interference<br />
by division of wave front and amplitude (Fresnel’s bi-prism, Newton’s Rings).<br />
Diffraction: Single and multiple slit Diffraction; Diffraction Grating; Rayleigh’s criterion of resolution;<br />
Resolving Power of Telescope, Microscope and Grating.<br />
Unit III (Lectures 08)<br />
Polarization: Phenomenon of double refraction; Ordinary and extra-ordinary rays; Nicol Prism;<br />
Production and analysis of Plane, Circularly and Elliptically Polarized Light; Optical Activity; Specific<br />
Rotation, Polarimeter.<br />
Laser: Principle of Laser action; Einstein’s Coefficients; Construction and working of He-Ne and Ruby<br />
Laser.<br />
Unit IV (Lectures 08)<br />
Fiber Optics and Holography: Fundamentals of fiber optics; Types of fibers; Acceptance angle ;<br />
Numerical aperture; Attenuation, signal loss in optical fiber and dispersion; Propagation mechanism and<br />
communication in optical fiber.<br />
Basic principle of holography; Construction of a hologram and wave reconstruction; Applications of<br />
holography.<br />
Unit V (Lectures 08)<br />
Electromagnetics: Ampėre’s law and displacement current; Maxwell’s equations in Integral and<br />
Differential Forms; Equation of continuity; Electromagnetic Wave Propagation in Free Space and<br />
Conducting Media; Poynting Theorem.<br />
Text Books<br />
1. Malik K. H., <strong>Engineering</strong> Physics, Tata McGraw Hill.<br />
2. Subramanyam N, Optics, Tata McGraw Hill.<br />
Reference Book<br />
1. Yadav V. S., <strong>Engineering</strong> Physics, Tata McGraw Hill.<br />
2. Mehta Neeraj, <strong>Engineering</strong> Physics Vol. I & II, Prentice Hall of India Pvt. Ltd.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 8
Semester I/II<br />
CHEMISTRY<br />
Course Code: EAS103/EAS203 L T P C<br />
3 0 0 3<br />
Objective:<br />
• To understand the fundamentals of chemistry like Bonding, Pollution, Polymers, Water Chemistry, etc.<br />
Course Contents<br />
Unit I (Lectures 08)<br />
<strong>Chemical</strong> bonding & Solid State Chemistry:<br />
Molecular theory of diatomic hetero-molecules; Band theory of bonding in metals; Hydrogen bonding;<br />
Radius Ratio Rule; Space lattice (only cubes); Type of unit cell, Bragg’s Law, Calculation of Density of<br />
unit cell; One & Two Dimensional solids; graphite as two dimensional solid and its conducting<br />
properties; Fullerene & its applications.<br />
Unit II (Lectures 08)<br />
Polymers , Reaction Kinetics, Phase rule & Electrochemistry:<br />
Structures of the following polymers, viz, Natural and synthetic rubbers, Polyamide and Polyester fibres,<br />
polymethylmethacrylate, poly acrylonitrile and polystyrene; A brief account of conducting polymers<br />
(polypyrrole & polytriphene) & their applications.<br />
Order & Molecularity of reactions; First & Second order reactions; Energy of activation.<br />
Phase Rule: Its application to one component system (Water). Equilibrium Potential, Introduction of<br />
electrochemical cells & Types: Galvanic & Concentration cells, Electrochemical theory of corrosion &<br />
protection of corrosion.<br />
Unit III (Lectures 08)<br />
Water Chemistry & Fuels:<br />
Hardness of water; water softening by Lime Soda Process, Calgon process, Zeolites and ion-exchange<br />
resins; Reverse osmosis;<br />
Classification of fuels, Coal, Biomass & Biogas; Determination of gross and net calorific values using<br />
Bomb Calorimeter.<br />
Unit IV (Lectures 08)<br />
Glass & Ceramics:<br />
Concept of glass & its constituents; Classification & uses of different glasses; Elementary idea of<br />
manufacturing process of glass; Introduction to Ceramics materials & its constituents, Industrial<br />
application of glass & ceramics.<br />
Unit V (Lectures 08)<br />
Lubricants:<br />
Introduction to lubricants; Mechanism of lubrication; Classification of lubricants; Flash and fire points,<br />
Selection of lubricants.<br />
Text Books<br />
1. Agarwal R. K., <strong>Engineering</strong> Chemistry, Krishna Prakashan.<br />
2. Morrison & Boyd, Organic Chemistry, Prentice Hall<br />
3. Chawla Shashi, <strong>Engineering</strong> Chemistry, Dhanpat Rai Publication.<br />
Reference Books<br />
1. Barrow Gordon M., Physical Chemistry, McGraw-Hill.<br />
2. Manahan Stanley E., Environmental Chemistry, CRC Press.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 9
Semester I/II<br />
ENGINEERING MECHANICS<br />
Course Code: EME101/EME201 L T P C<br />
3 0 0 3<br />
Objective:<br />
To study about mechanics, force system, torsion, beams, trusses, frames etc.<br />
Course Contents<br />
Unit I (Lectures 08)<br />
Force systems and analysis: Basic concept; Newton’s laws of motion; Transfer of force to a parallel<br />
position; Determination of resultant of planer force system; Free body diagrams; Equilibrium of forces<br />
and its equations.<br />
Friction: Introduction; Coulomb’s law of friction; Equilibrium of bodies involving dry fiction; Belt<br />
Friction.<br />
Unit II (Lectures 08)<br />
Structural Analysis: Beams; Introduction; Shear force and Bending Moment; shear force and Bending<br />
Moment Diagram for statically determinate beams.<br />
Trusses: Introduction; Simple Trusses; Determination of Forces in simple trusses members; methods of<br />
joints and method of section.<br />
Unit III (Lectures 08)<br />
Centroid and Moment of Inertia: Centroid of plane; curve, area, volume and composite bodies;<br />
Moment of inertia of plane area; Parallel Axes Theorem; Perpendicular axes theorems; Principal Moment<br />
Inertia; Mass Moment of Inertia of Circular Ring, Disc, Cylinder, Sphere and Cone about their axis of<br />
symmetry<br />
Unit IV (Lectures 08)<br />
Simple stress and strain: Introduction; Normal shear stresses; stress-strain diagrams for ductile and<br />
brittle materials; Elastic constants; one dimensional loading of members of varying cross sections.<br />
Unit V (Lectures 08)<br />
Pure Bending of Beams: Introduction; Simple bending theory; Stress in Beams of different cross<br />
sections.<br />
Torsion: Introduction; Torsion of shafts of circular section; Torque and Twist; Shear stress due to<br />
Torque.<br />
Text Books<br />
1. Bansal R. K., <strong>Engineering</strong> Mechanics, Laxmi Publications.<br />
2. Kumar D. S., <strong>Engineering</strong> Mechanic, S. K. Kataria & Sons.<br />
3. Kumar K. L., Kumar V., <strong>Engineering</strong> Mechanics, Tata McGraw Hill Publication.<br />
4. Khurmi R. S., <strong>Engineering</strong> Mechanics, S. Chand Publications.<br />
Reference Books<br />
1. Shames, <strong>Engineering</strong> Mechanics, Prentice Hall of India Pvt. Ltd.<br />
2. Ryder G. H., Strength of Materials, Macmillan Publishers India Ltd.<br />
3. Ramamruthams, Strength of materials, Dhanpat Rai Publications.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 10
Semester I/II<br />
MANUFACTURING SCIENCE<br />
Course Code: EME102/EME202 L T P C<br />
3 0 0 3<br />
Objective: To expose the students about basics of manufacturing processes as applicable in Mechanical<br />
<strong>Engineering</strong>.<br />
Course Contents<br />
Unit I (Lectures 08)<br />
Basic Metals & Alloys: Properties and Applications; Properties of Materials: Strength, elasticity,<br />
stiffness, malleability, ductility, brittleness, toughness, and hardness; Elementary ideas of fracture fatigue<br />
& creep.<br />
Unit II (Lectures 10)<br />
Metal Forming: Basic metal forming operations & uses of such as: Forgoing, Rolling, Wire<br />
drawing/making and Extrusion, and its products/application; Press-work; die & punch assembly, cutting<br />
and forming, its application; Hot-working versus cold-working; Introduction to Plastics: Types,<br />
Machines: Injection Moulding.<br />
Casting: Pattern & allowance; Molding sands its desirable properties; Mould making with the use of<br />
core; Gating system, Casting defects & remedies; Cupola Furnace, Die-casting and its uses.<br />
Unit III (Lectures 10)<br />
Machining: Basic principles of Lathe-machine and operations performed on it; basic description of<br />
machines and operations of Shaper-Planner, Drilling, Milling & Grinding.<br />
Welding: Importance & basic concepts of welding; Classification of welding processes: Gas-welding,<br />
types of flames and principle; Electric-Arc welding; Resistance welding; Soldering, & Brazing and its<br />
uses.<br />
Unit IV (Lectures 8)<br />
Unconventional Manufacturing Process: Limitations of conventional manufacturing process; need of<br />
unconventional manufacturing processes; Basic Principles and working of unconventional manufacturing<br />
process and their applications; Electro-Discharge machining; Electro-chemical machining; Ultrasonic<br />
machining; Abrasive jet machining; Water jet machining;, Laser cutting and Laser beam welding.<br />
Unit V (Lectures 04)<br />
Super Finishing Processes: Introduction; Lapping; Honing; Buffing; Burnishing; Powder coating;<br />
Polishing<br />
Text Books<br />
1. Hajra & Bose, Workshop Technology, Vol 1 & 2, Roy Media Promoters.<br />
2. Pandey & Singh, Production <strong>Engineering</strong> Science, Standard Publishers.<br />
3. R.K. Jain, Production technology, Khanna publishers.<br />
Reference Books<br />
1. Raghuvanshi, B.S., Workshop Technology, Vol 1 & 2, Dhanpat Rai & Sons.<br />
2. Laxmi Narayan & Vaish W, A Text Book of Practical Geometrical Drawing, Pearson Education.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 11
Semester I/II<br />
COMPUTER BASICS & ‘C’ PROGRAMMING<br />
Course Code: ECS101/ECS201 L T P C<br />
3 0 0 3<br />
Objective:<br />
• To learn the basics of computers & C programming language.<br />
Course Contents:<br />
Unit I (Lectures 08)<br />
Concepts in Computer Application: Definition of Electronic Computer; History; Generations;<br />
Characteristics and Application of Computers; Classification of Computers; Functional Component of<br />
Computer: CPU, I/O devices, Type of Memory & Memory Hierarchy, Firmware and Human ware.<br />
Data and data types: Definitions, data, data types: Integer, Character, Float, String, etc.; Constants<br />
and Variable Declaration; Token; Keyboard; Identifier.<br />
Unit II (Lectures 08)<br />
Programming Language Classification & Computer Languages: Generation of Languages;<br />
Introduction to 4GLs; Translators; Assemblers; Compilers; Interpreters.<br />
Number System: Decimal, Octal, Binary and Hexadecimal & their Conversions; Various Code: BCD,<br />
ASCII and EBCDIC and Gray Code.<br />
Operators and Expressions: Numeric and relation operators; logical operator; bit operator; operator<br />
precedence and associativity.<br />
Unit III (Lectures 08)<br />
Internet and Web Technologies: Hypertext Markup Language; WWW; Gopher; FTP; Telnet; Web<br />
Browsers; Search Engines; Email.<br />
Control Structure: while statement, if, else, Nested if else statement. Nested logic: for loop, do- while<br />
loop, loop inside a loop structure, Switch Statement. Break and default with switch.<br />
Unit IV (Lectures 08)<br />
Concepts in Operating Systems: Elementary Concepts in Operating Systems; Textual Vs GUI Interface.<br />
Arrays: Notation and representation; Manipulation of array elements; Multidimensional arrays.<br />
Unit V (Lectures 08)<br />
Functions & Strings: Definition; Declaration; Call by Value; Call by Reference; Returns values and<br />
their types; Function calls<br />
Text Books<br />
1. Sinha P. K., Computer Fundamentals, BPB Publications.<br />
2. Yadav, DS, Foundations of IT, New Age.<br />
3. Curtin, Information Technology: Breaking News, Tata McGraw Hill.<br />
4. Rajaraman,R, Introduction to Computers, Prentice Hall of India.<br />
Reference Books<br />
1. Peter Nortans, Introduction to Computers, Tata McGraw Hill.<br />
2. Leon & Leon, Fundamental of Information Technology, Vikas Publishing.<br />
3. Kanter, Managing Information System, Prentice-Hall.<br />
4. CISTems, Internet: An Introduction, Tata McGraw Hill.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 12
Semester I/II<br />
ENVIRONMENTAL SCIENCE<br />
Course Code: EAS104/EAS204 L T P C<br />
3 0 0 3<br />
Objective: To create awareness among students about environment protection.<br />
Unit I (Lectures 08)<br />
Introduction: Definition, Scope, Segments of Environment and its Multidisciplinary Nature; Some Major<br />
Environmental Problems; Definition and Scope of Ecology.<br />
Unit II (Lectures 08)<br />
Ecology And Environment: Concept of an Ecosystem- its components and functions; Trophic Levels-<br />
Producer; Consumer and Decomposer; Energy Flow in an Ecosystem; Biogeochemical Cycles; Food<br />
Chain; Food Web and Ecological Pyramid.<br />
Unit III (Lectures 08)<br />
Air & water pollution: Various segments of Atmosphere and their Significance; Sources and Effects of<br />
Air Pollution; Sources of Air Pollution: Photochemical Smog, Acid Rain, Global Warming, Ozone Layer -<br />
Its Depletion and Control Measures; Sources of Water Pollution; Treatment of Water Pollution;<br />
Eutrophication.<br />
Unit IV (Lectures 08)<br />
Soil & Thermal pollution: Soil pollution: Sources and Consequences; Solid Wastes – Pollution;<br />
Treatment & Disposal.<br />
Thermal - sources and consequences; Sustainable Development; Dams and Reservoirs- Their Benefits and<br />
Problems.<br />
Unit V (Lectures 08)<br />
Biodiversity & its conservation<br />
Bio-Diversity Hot-spots of Biodiversity in India and World; Conservation; Importance and Factors<br />
Responsible for Loss of Biodiversity; Deforestation- causes and effects; Biogeographical Classification of<br />
India; Environment Conservation Movement in India (Chipko Movement, Appiko Movement),<br />
Bioremediation; Biological Magnification.<br />
Text Books<br />
1. De A.K., Environmental Chemistry, New Age Publishers Pvt. Ltd.<br />
2. Masters, G.M., Introduction to Environmental <strong>Engineering</strong> and Science, Prentice Hall India Pvt. Ltd.<br />
3. Odum, E.P., Fundamentals of Ecology, W. B. Sannders Co.<br />
Reference Books<br />
1. Bryant,P.J., Biodiversity and Conservation, Hypertext Book.<br />
2. Tewari, Khulbe & Tewari, Textbook of Environment Studies, I.K. Publication.<br />
3. Trivedi, R.K., Handbook of Environmental Laws, Rules, Guidelines, Compliances and Standards, Vol<br />
I and II, Environment Media.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 13
Semester I/II<br />
BASIC ELECTRICAL ENGINEERING<br />
Course Code: EEE101/EEE201 L T P C<br />
3 0 0 3<br />
Objective<br />
• To understand the fundamental concept of Electrical <strong>Engineering</strong> like DC Network, AC Network,<br />
Measuring Instruments, Energy Conversion Devices etc.<br />
Course Contents<br />
Unit I (Lectures 08)<br />
D.C. Network Theory: Circuit theory concepts-Mesh and node analysis; Network Theorems-<br />
Superposition theorem, Thevenin’s theorem, Norton’s theorem and Maximum Power Transfer theorem;<br />
Star Delta transformation.<br />
Unit II (Lectures 08)<br />
Steady State Analysis of A.C. Circuits: Sinusoidal and phasor representation of voltage and current;<br />
Single phase A.C. circuit behaviour of resistance, inductance and capacitance and their combination in<br />
series & parallel; Power factor; Series and parallel resonance; Band width and quality factor; magnetic<br />
circuit.<br />
Unit III (Lectures 08)<br />
Measuring Instruments: Construction and principles of operation of voltage and current measuring<br />
instruments; introduction to power and energy meters.<br />
Three Phase A.C. Circuits: Star-Delta connections; Line and phase voltage/current relations; Three<br />
phase power and its measurement.<br />
Unit IV (Lectures 08)<br />
Transformer: Principle of operation; Types of construction; Phasor diagram; Equivalent circuit;<br />
Efficiency and voltage regulation of single phase transformer; Open and short circuit tests.<br />
D.C. Machines: Principles of electromechanical energy conversion; Types of D.C. machines; E.M.F.<br />
equation; Magnetization and load characteristics; Losses and efficiency; Starter and speed control of D.C.<br />
Motors; Motor applications.<br />
Unit V (Lectures 08)<br />
Three phase induction Motor: Principle of operation; Types and methods of starting; slip-torque<br />
characteristics; Applications.<br />
Synchronous Machines: Principle of Operation of Alternator and synchronous motor<br />
Single phase Motors: Principle of operation and methods of starting of induction motor,<br />
Text Books<br />
1. V. Del Toro, Principles of Electrical <strong>Engineering</strong>, Prentice-Hall International.<br />
2. W.H. Hayt & J.E. Kemmerly, <strong>Engineering</strong> Circuit Analysis, McGraw Hill.<br />
Reference Books<br />
1. Nagrath I.J., Basic Electrical <strong>Engineering</strong>, Tata McGraw Hill.<br />
2. Fitzgerald A.E & Higginbotham ., D.E., Basic Electrical <strong>Engineering</strong>, McGraw Hill.<br />
3. A Grabel, Basic Electrical <strong>Engineering</strong>, McGraw Hill.<br />
4. Cotton H., Advanced Electrical Technology, Wheeler Publishing.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 14
Semester I/II<br />
BASIC ELECTRONICS ENGINEERING<br />
Course Code: EEC101/EEC201 L T P C<br />
3 0 0 3<br />
Objective<br />
• To understand the basic concept of Electronics <strong>Engineering</strong> like p-n Junction, Bipolar Junction<br />
Transistor, Field Effect Transistor, Operational Amplifier etc.<br />
Course Contents<br />
Unit I (Lectures 08)<br />
p-n Junction: Properties of Elements; Crystal Structure; Energy band diagram; Introduction to PN-<br />
Junction; Depletion layer; V-I characteristics Diode Ratings (average current, peak-inverse voltage); p-n<br />
junction as rectifiers (half wave and full wave) & filter; calculation of ripple factor and load regulation;<br />
clipping and clamping circuits; Zener diode and its application as shunt regulator.<br />
Unit II (Lectures 08)<br />
Bipolar Junction Transistor (BJT): Basic construction; transistor action; CB, CE and CC<br />
configurations; input/output characteristics; Biasing of transistors: Fixed bias, emitter bias, potential<br />
divider bias; Graphical analysis of CE amplifier; concept of Voltage gain current gain; λ-parameter model<br />
(low frequency); Computation of Ai, Av, Ri & Ro of single transistor CE amplifier configuration.<br />
Unit III (Lectures 08)<br />
Field Effect Transistor (FET): Basic construction of JFET; Principle of working; concept of pinch-off<br />
maximum drain saturation current; input and transfer characteristics; Characteristics equation; CG, CS<br />
and CD Configuration; fixed and self biasing of JFET amplifier Introduction of MOSFET; Depletion and<br />
Enhancement type MOSFET- Construction; Operation and Characteristics.<br />
Unit IV (Lectures 08)<br />
Operational Amplifier (Op-Amp): Concept of ideal operational amplifier; ideal and practical Op-Amp<br />
parameters; inverting, non-inverting and unity gain configurations; Applications of Op-Amp as adders,<br />
difference amplifiers, integrators and differentiator.<br />
Unit V (Lectures 08)<br />
Switching Theory: Number system; conversion of bases (decimal, binary, octal and hexadecimal<br />
numbers); Adder & Subtraction; BCD numbers; Seven Segment Display; Boolean Algebra; Logic gates;<br />
Concept of universal gates; Canonical forms; minimization using K-Map<br />
Text Books<br />
1. Robert Boylestad & Louis Nashelsky, Electronic Circuit and Devices, Pearson India.<br />
2. Millman & Halkias, Integrated Electronics, McGraw Hill.<br />
3. Millman & Halkias, Electronics Devices and Circuits, McGraw Hill.<br />
4. Morris Mano M., Digital Design, Prentice Hall.<br />
Reference Books<br />
1. Sedra and Smith, Microelectronic Circuits, Oxford <strong>University</strong> Press .<br />
2. Gayakwad, R A, Operational Amplifiers and Linear Integrated circuits, Prentice Hall of India Pvt.<br />
Ltd.<br />
3. Chattopadhyay D and P C Rakshit, Electronics Fundamentals and Applications, New Age<br />
International.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 15
Semester-I<br />
FOUNDATION ENGLISH - I<br />
Course code: EHM101 L T P C<br />
2 0 2 3<br />
(Common with BPH105/BED105/BAL101/AR107/BHM101/BFS106/BCA106/BBA106/ BCH106/<br />
BFA103)<br />
Course Contents:<br />
Unit I (Lectures 10)<br />
Functional Grammar: Patterns & Parts of speech Subject, Predicate, Noun, Pronoun, Adjective,<br />
Adverb, Verb, Verb phrases, Conjunction, Interjection.<br />
Unit II (Lectures 10)<br />
Vocabulary: Word formation, Prefix, Suffix, Compound words, Conversion, Synonyms, Antonyms,<br />
Homophones and Homonyms, How to look up a dictionary.<br />
Unit III (Lectures 10)<br />
Communication: Meaning & importance of communication, Barriers to effective communication,<br />
Channels of communication, Language as a tool of communication<br />
Unit IV (Lectures 10)<br />
Requisites of Sentence writing: Fragmented sentences, A good sentence, expletives, Garbled sentences,<br />
Rambling sentences, Loaded sentences, Parallel Comparison, Squinting construction, Loose & periodic<br />
sentences.<br />
Text Books:<br />
1. Martin & Wren - High School English Grammar & Composition, S.Chand & Co.<br />
2. Lewis Norman - Word Power made easy, W.R.Goyal Publication & Distributors.<br />
3. Better Your English: A Workbook for 1 st year Students, Macmillan India.<br />
Reference Books:<br />
1. Raman Meenakshi & Sharma Sangeeta, Technical Communication: Principles & Practices, Oxford<br />
<strong>University</strong> Press, New Delhi.<br />
2. Mohan Krishna & Banerji Meera, Developing Communication Skills, Macmillan India Ltd.<br />
3. Rosen Blum M., How to Build Better Vocabulary, Bloomsbury Publication. London.<br />
NOTE:<br />
This syllabus has been designed to improve the oral and written communication skills of students.<br />
The faculty members should put emphasis on practical (oral) activities for generating students’<br />
interest in language learning.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 16
Semester I/II<br />
PHYSICS (LAB)<br />
Course Code: EAS151/EAS251 L T P C<br />
0 0 3 1.5<br />
LIST OF EXPERIMENTS<br />
1. To determine the wavelength of Sodium light by Newton’s rings.<br />
2. To determine the wavelength of Sodium light by Fresnel’s Biprism.<br />
3. To determine the Specific Rotation of the Cane sugar solution with the help of Polari meter.<br />
4. To determine the wavelength of the sodium light by Michelson’s interferometer.<br />
5. To study the PN junction characteristics.<br />
6. To determine the high resistance by Leakage method.<br />
7. To study the energy band gap by four probe method.<br />
8. To study the variation of magnetic field using Stewart and Gee’s apparatus.<br />
9. To determine the frequency of A.C. mains by means of a Sonometer.<br />
10. To study the Hall Effect.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 17
Semester I/II<br />
CHEMISTRY (LAB)<br />
Course Code: EAS152/EAS252 L T P C<br />
0 0 3 1.5<br />
LIST OF EXPERIMENTS<br />
1. To determine total alkalinity in the given water sample.<br />
2. To determine the temporary and permanent hardness in water sample using EDTA as standard<br />
solution.<br />
3. To determine the available chlorine in bleaching powder solution.<br />
4. To determine the chloride content in the given water sample by Mohr’s method.<br />
5. To determine the pH of the given solution using pH meter and pH-metric titration.<br />
6. To determine the Equivalent weight of Iron by the chemical displacement method.<br />
7. To determine the Viscosity of an addition polymer like polyester by Viscometer.<br />
8. To determine the dissolved oxygen present in a water sample.<br />
9. To prepare the Bakelite resin polymer.<br />
10. To determine the viscosity of a given sample of a lubricating oil using Redwood Viscometer.<br />
11. To determine the carbon dioxide content in polluted water sample.<br />
12. To find chemical oxygen demand of waste water sample by potassium dichromate.<br />
13. To determine the total hardness in water sample using complexometric method.<br />
14. To determine the iron content in the given sample using external indicator.<br />
15. To determine the strength of given HCL solution by titrating against N/10 Standard Sodium<br />
hydroxide solution.<br />
Note: Minimum of 10 experiments has to be completed for completion of curriculum.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 18
Semester I/II<br />
ENGINEERING MECHANICS (LAB)<br />
Course Code: EME151/EME251 L T P C<br />
0 0 3 1.5<br />
(Any 10 experiments of the following or such experiments suitably designed)<br />
LIST OF EXPERIMENTS<br />
1. To conduct the tensile test and determine the ultimate tensile strength, percentage elongation for a steel<br />
specimen.<br />
2. To conduct the compression test and determine the ultimate compressive strength for a specimen.<br />
3. To conduct the Impact test on Impact-testing machine to find the toughness by Charpy impact test.<br />
4. To conduct the Impact-test on Impact-testing machine to find the toughness by Izod impact Test.<br />
5. To determine the hardness of the given specimen using Rockwell hardness testing machine.<br />
6. To determine the hardness of the given specimen using Brinell hardness testing machine.<br />
7. To determine gear ratio of simple and compound gear train.<br />
8. To determine the mechanical advantage of worm and worm wheel for load lifting.<br />
9. To find the coefficient of friction on inclined plane.<br />
10. To perform torsion test for rod on torsion testing machine.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva voce taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 19
Semester I/II<br />
COMPUTER BASICS & C PROGRAMMING (LAB)<br />
Course Code: ECS 151/ 251 L T P C<br />
0 0 3 1.5<br />
Perform any ten experiments.<br />
Course Contents<br />
1. To write a program to calculate Sum & average of N numbers.<br />
2. To write a program to convert integer arithmetic to a given number of day and month.<br />
3. To write a program to find maximum and minimum out of 3 numbers a, b & c.<br />
4. To write a program to find factorial of positive integer.<br />
5. To write a program to find sum of series up to n number, 2+5+8+…………………+n.<br />
6. To write a program to print all the number between 1 to 100 which are dividing by 7.<br />
7. To write a program to generate Fibonacci series up to n.<br />
8. To write a program to implement a function to calculate area of a circle.<br />
9. To write a program to implement a recursive function to calculate factorial of given number.<br />
10. To write a program to find whether number is prime or not.<br />
11. To write a program to find that the enter character is a letter or digit.<br />
12. To write a program to find addition of two matrix of n*n order.<br />
13. To write a program to find multiplication of two matrix of n*n order.<br />
14. To write a program to add 6 digit numbers in even case & multiple 6 digit number in odd case.<br />
15. To write a program to find even or odd up to a given limit n.<br />
16. To write a program to find whether a given no is palindrome or not.<br />
17. To write a program to joining & Comparing the 2 string.<br />
Evaluation of Practical Examination:<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 20
Semester I/II<br />
ENGINEERING DRAWING (LAB)<br />
Course Code: EME152/EME252 L T P C<br />
0 0 4 2<br />
1. To write all Numbers (0 to 9) and alphabetical Letters (A to Z) as per the standard dimensions.<br />
2. To draw the types of lines and conventions of different materials.<br />
3. To draw and study dimensioning and Tolerance.<br />
4. To construction geometrical figures of Pentagon and Hexagon<br />
5. To draw the projection of points and lines<br />
6. To draw the Orthographic Projection of given object in First Angle<br />
7. To draw the Orthographic Projection of given object in Third Angle<br />
8. To draw the sectional view of a given object<br />
9. To draw the development of the lateral surface of given object<br />
10. To draw the isometric projection of the given orthographic projection.<br />
Reference Books<br />
1. Bhatt. N.D., Elementary <strong>Engineering</strong> Drawing, Charothar Publishing.<br />
2. Narayana K.L. & Vaish W., A Text Book of Practical Geometry on Geometrical Drawing, Pearson<br />
Education.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each sheet prepared would be evaluated by the faculty concerned on the date of preparing the sheet on a<br />
5 point scale which would include the sheet drawn by the students and a Viva voce taken by the faculty<br />
concerned. The marks shall be entered on the index sheet.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 21
Semester I/II<br />
WORKSHOP PRACTICE (LAB)<br />
Course Code: EME153/EME253 L T P C<br />
0 0 4 2<br />
List of Experiments<br />
Perform any ten experiments selecting at least one from each shop.<br />
Carpentry Shop:<br />
1. To prepare half-lap corner joint.<br />
2. To prepare mortise & tenon joint.<br />
3. To prepare a cylindrical pattern on woodworking lathe.<br />
Fitting Bench Working Shop:<br />
1. To prepare a V-joint fitting<br />
2. To prepare a U-joint fitting<br />
3. To prepare a internal thread in a plate with the help of tapping process<br />
Black Smithy Shop:<br />
1. To prepare a square rod from given circular rod<br />
2. To prepare a square U- shape from given circular rod<br />
Welding Shop:<br />
1. To prepare a butt and Lap welded joints using arc welding machine.<br />
2. To prepare a Lap welded joint Gas welding equipment.<br />
3. To prepare a Lap welded joint using spot welding machine.<br />
Sheet-metal Shop:<br />
1. To make round duct of GI sheet using ‘soldering’ process.<br />
2. To prepare a tray of GI by fabrication<br />
Machine Shop:<br />
1. To prepare a bolt on the lathe machine as per given. diagram<br />
2. To prepare a job on the lathe machine as per given diagram.<br />
Foundry Shop:<br />
1. To prepare core as per given size.<br />
2. To prepare a mould for given casting.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
Page 22
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
Semester I/II<br />
BASIC ELECTRICAL ENGINEERING (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
TOTAL EXTERNAL<br />
(50 MARKS)<br />
Course Code: EEE151/EEE251 L T P C<br />
0 0 3 1.5<br />
LIST OF EXPERIMENTS<br />
1. To verify the Kirchhoff’s current and voltage laws.<br />
2. To verify the Superposition theorem.<br />
3. To verify the Thevenin’s theorem.<br />
4. To verify the Norton’s theorem.<br />
5. To verify the maximum power transfer theorem.<br />
6. To determine the efficiency of single-phase transformer by load test.<br />
7. To determine the external characteristics of DC Shunt generator.<br />
8. To measure current and speed for speed control of D.C. Shunt Motor.<br />
9. To measure the power in a 3-phase system by two-wattmeter method<br />
10. To measure the power factor in an RLC by varying the capacitance.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 23
Semester I/II<br />
BASICS ELECTRONICS ENGINEERING (LAB)<br />
Course Code: EEC151/EEC251 L T P C<br />
0 0 3 1.5<br />
LIST OF EXPERIMENTS<br />
1. To study the V-I characteristics of p-n junction diode.<br />
2. To study the diode as clipper and clamper.<br />
3. To study the half-wave & full-wave rectifier using silicon diode.<br />
4. To study transistor in Common Base configuration & plot its input/output characteristics.<br />
5. To study transistor in Common Emitter configuration & plot its input/output characteristics. .<br />
6. To study the operational amplifier in inverting & non inverting modes using IC 741.<br />
7. To study the operational amplifier as differentiator & integrator.<br />
8. To study the Zener diode as a shunt regulator.<br />
9. To study various logic gates & verify their truth tables.<br />
10. To study half adder/full adder & verify their truth tables.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 24
Semester II<br />
ENGINEERING MATHEMATICS- II<br />
Course Code: EAS201 L T P C<br />
3 1 0 4<br />
Objective: To familiarize the basic concept of Differential Equations, Laplace Transform, Fourier series<br />
and Partial Differential Equations etc.<br />
Course Contents<br />
Unit I (Lectures 08)<br />
Differential Equations: Ordinary differential equations of first order; Exact differential equations;<br />
Linear differential equations of first order, Linear differential equations of nth order with constant<br />
coefficients; Complementary functions and particular integrals; Simultaneous linear differential<br />
equations; Solutions of second order differential equations by changing dependent and independent<br />
variables; Method of variation of parameters; Applications to engineering problems (without derivation).<br />
Unit II (Lectures 08)<br />
Series Solutions and Special Functions: Series solutions of ODE of 2nd order with variable coefficients<br />
with special emphasis to differential equations of Legendre and Bessel; Legendre polynomials; Bessel’s<br />
functions and their properties.<br />
Unit III (Lectures 10)<br />
Partial Differential Equations and applications: Introduction of partial differential equations; Linear<br />
partial differential equations with constant coefficients of 2nd order and their classifications – parabolic;<br />
elliptic and hyperbolic with illustrative examples.<br />
Method of separation of variables for solving partial differential equations; Wave equation up to two<br />
dimensions; Laplace equation in two-dimensions; Heat conduction equations up to two-dimensions;<br />
Equations of transmission Lines.<br />
Unit IV (Lectures 06)<br />
Fourier Series: Periodic functions, Trigonometric series; Fourier series; Euler’s formulae; Even and odd<br />
functions, Half range sine and cosine series.<br />
Unit V (Lectures 08)<br />
Laplace Transform: Laplace transform; Existence theorem; Laplace transform of derivatives and<br />
integrals; Inverse Laplace transform; Unit step function; Diracth delta function; Laplace transform of<br />
periodic functions; Convolution theorem; Application to solve simple linear and simultaneous differential<br />
equations.<br />
Text Books<br />
1. Grewal B.S., Higher <strong>Engineering</strong> Mathematics, Khanna Publishers.<br />
2. Prasad C., <strong>Engineering</strong> Mathematics for Engineers, Prasad Mudralaya.<br />
3. Das H.K., <strong>Engineering</strong> Mathematics Vol-II, S. Chand.<br />
Reference Books<br />
1. Kreyszig E., Advanced <strong>Engineering</strong> Mathematics, Wiley Eastern.<br />
2. Piskunov N, Differential & Integral Calculus, Moscow Peace Publishers.<br />
3. Narayan Shanti, A Text book of Matrices, S. Chand<br />
4. Bali N.P., <strong>Engineering</strong> Mathematics-II, Laxmi Publications.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 25
Semester-II<br />
FOUNDATION ENGLISH - II<br />
Course code: EHM 201 L T P C<br />
2 0 2 3<br />
(Common with BPH206/BBA206/BCA206/BHM201/AR207/BCH206/BFA203)<br />
Unit I (Lectures 10)<br />
Functional Grammar: Articles, Preposition, Tenses: Functions, Synthesis, Transformation, Spotting<br />
errors and correction of sentences.<br />
Unit II (Lectures 10)<br />
Pre- Requisites of Technical written Communication: One word substitution, Spelling rules, Words<br />
often confused & misused, Phrases.<br />
Unit III (Lectures 10)<br />
The Structure of sentences/ clauses: Adverb clause, Adjective clause, Noun clause. Sentences: Simple,<br />
Double, Multiple and complex, Transformation of sentences: simple to complex & vice versa, simple to<br />
compound & vice-versa, Interrogative to assertive & negative & vice-versa.<br />
Unit IV (Lectures 10)<br />
Technical Communication: Nature, Origin and Development, Salient features, Scope & Significance,<br />
Forms of Technical Communication, Difference between Technical Communication & General writing,<br />
Objective Style vs. Literary Composition<br />
Text-Books:<br />
1. Wren & Martin, High School English Grammar & Composition – S. Chand & Co.<br />
2. Raman Meenakshi & Sharma Sangeeta, Technical Communication-Principles & Practice, Oxford<br />
<strong>University</strong> Press, New Delhi, 2007.<br />
3. Mitra Barum K., Effective Technical Communication, Oxford <strong>University</strong> Press, New Delhi.<br />
4. Better Your English- A Workbook for 1 st year Students- Macmillan India.<br />
Reference Books:<br />
1. Horn A.S., Guide to Patterns & Usage in English, Oxford <strong>University</strong> Press, New Delhi.<br />
NOTE:<br />
This syllabus has been designed to improve the oral and written communication skills of students.<br />
The faculty members should put emphasis on practical (oral) activities for generating students’<br />
interest in language learning.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 26
Course Code: ECH-301<br />
Semester-III<br />
CHEMICAL ENGINEERING THERMODYNAMICS-I<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I (Lectures 08)<br />
Introduction; Definitions and Concepts - System, Surroundings, Property, Intensive and Extensive<br />
Energy, Work, Thermodynamic equilibrium, stability of equilibrium states; Zeroth Law of<br />
Thermodynamics; Perfect Gas scale.<br />
Unit – II (Lectures 08)<br />
First law of Thermodynamics and Its Applications; First law analysis of processes; Control mass and<br />
control volume analysis; Steady state and Transient state flow processes.<br />
Thermodynamic properties of fluids - pure substance, Concept of Phase, Ideal gas equation of state, Van<br />
der Waals’ equation of state, two parameter corresponding states principle, Compressibility charts; Steam<br />
Tables and applications.<br />
Unit – III (Lectures 08)<br />
Second law of Thermodynamics - Limitation of First Law, Kelvin-Planck and Clausius Statements,<br />
Reversible and Irreversible Processes, Carnot cycle, Entropy; Second Law analysis of a control volume;<br />
Heat Engine and Heat Pump; Fundamental Thermodynamic Relations; Maxwell Relations; Clapeyron’s<br />
Equation; Kirchoff’s equation; Phase Rule.<br />
Unit – IV (Lectures 08)<br />
Ideal gas mixture ; Air-Water mixture; Humidity; Psychrometric chart and its applications.<br />
Power Cycles - Rankine cycle and its modifications, Otto cycle, Diesel cycle; Refrigeration Cycles -<br />
Vapor Compression Refrigeration cycle, Absorption Refrigeration cycle<br />
Unit – V (Lectures 08)<br />
Statistical Thermodynamics - Postulates, Macrostates and microstates, Partition Function, Maxwell-<br />
Boltzmann, Bose-Einstein and Fermi-Dirac statistics; Applications of Statistical Thermodynamics - Ideal<br />
gas, Maxwell speed distribution, Einstein & Debye Models of a solid.<br />
Text Books:<br />
1. Rao, Y. V. C., “An Introduction to Thermodynamics,” John Wiley, 1993.<br />
2. Van Wylen, G. J. and Sonntag, R. E., “Fundamentals of Classical Thermodynamics,” 2nd ed., John<br />
Wiley, New Delhi.<br />
Reference Books:<br />
1. Yannes & Smith. John , <strong>Chemical</strong> Engg. Thermdynamics Wiley, New Delhi.<br />
2. Yunus A. Cengel Michael A. Boles, An-thermodyanamic Engg, John Wiley, New Delhi.<br />
3. Gordon Rogers Yon Mayhew. Engg- thermodyanamic , John Wiley, New Delhi.<br />
Page 27
Semester-III<br />
PHYSICAL CHEMICAL TECHNOLOGY<br />
Course Code: ECH-302<br />
L T P C<br />
3 0 0 3<br />
Unit I (Lectures 08)<br />
Liquid State: Liquefaction of Gases; Critical constants; Classius-Clayperon Equation; Vapor pressure of<br />
Liquids.<br />
Unit II (Lectures 08)<br />
Physical Properties of Liquids: Surface tension - Explanation, Measurement, Effect of temperature on<br />
surface tension, Applications; Viscosity - Definition, Measurement, Applications; Intermolecular forces<br />
in liquids; Hydrogen Bond.<br />
Unit III (Lectures 08)<br />
Thermodynamics and Thermochemistry: First law - Internal Energy, Work and Heat changes,<br />
Enthalpy, reversible changes, maximum work; Heat capacities at constant pressure and volume;<br />
Adiabatic changes; Heat of Reaction; Heat of Formation; Heat of Combustion; Second law - Entropy and<br />
Entropy change for an ideal gas, Gibb’s Free Energy and applications.<br />
Unit IV (Lectures 08)<br />
Phase Rule: Definition and explanation of terms involved in Phase Rule; Derivation of the Phase Rule;<br />
One component systems (water system) and two component system (Ag-Pb and KI-H2O) - Eutectic point<br />
and its significance.<br />
Unit V (Lectures 08)<br />
<strong>Chemical</strong> Kinetics and Catalysis: Order and molecularity of a reaction; Specific reaction rate and its<br />
determination; First Order and Second Order reactions - Half-Life period. Effect of temperature on<br />
reaction rate; Energy of Activation - Elementary treatment of collision theory and activated complex<br />
theory.<br />
Text Books:<br />
1. Samuel Glasstone and David Lewis, Elements of Physical Chemistry, Macmillan & Co.Ltd.,<br />
London.<br />
2. P.W.Atkins, Physical Chemistry (3 rd. Edition), Oxford <strong>University</strong> Press, New Delhi.<br />
Reference Books:<br />
1. Bahl & Tuli, Text Book of Physical Chemistry, S. Chand and Co, New Delhi.<br />
2. Puri, Sharma and Pathania, Principles of Physical Chemistry, VISHAL PUBLISHING Company,<br />
Delhi.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 28
Course Code: ECH-303<br />
Semester-III<br />
APPLIED CHEMISTRY<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
UNIT-I (Lectures 08)<br />
Electrochemistry: Specific, equivalent and molecular conductance and their determination; Debye-<br />
Huckel theory of strong electrolytes; Galvanic cells; Standard cell; Standard electrode potential;<br />
Determination of dissociation constants of acids and bases - Solubility product, Hydrolysis constant,<br />
Hydrogen ion concentration, Complex formation.<br />
UNIT –II (Lectures 08)<br />
Photochemistry: Photochemical Reactions; Laws of Photochemistry.<br />
Reactions and their Mechanism: Types of mechanism; Types of reactions and method of determination<br />
of mechanism.<br />
UNIT-III (Lectures 08)<br />
<strong>Chemical</strong> Bonding: Basic concepts of bonding; Types of bonding - covalent bonding, multiple bonding;<br />
Inductive and field effects and bond energy; Aromaticity and Huckle’s rule of electrons;<br />
Hyperconjugation and Tautomerism; Bonding weaker than covalent, resonance and field effects<br />
UNIT-IV (Lectures 08)<br />
Aromatic Chemistry: Structure of benzene resonance and orbital picture; Orientation and directive<br />
influence of substituents.<br />
Heterocyclic Compounds: Heterocyclic compounds containing one heteroatom - Pyrrole; Thiophene;<br />
Furan, Pyridine and their aromatic character.<br />
UNIT-V (Lectures 08)<br />
Carbohydrates: Introduction; Definition and classification; Structure of glucose and fructose.<br />
Stereochemistry: A brief account of stereochemistry - optical activity and chirality, configuration and<br />
strain.<br />
Text Book:<br />
1. Jerry March, “Organic Chemistry,” John Wiley, New York.<br />
2. Finar, I. L.,“Organic Chemistry,” ELBS, New Delhi.<br />
3. Morrison and Boyd, “Organic Chemistry,” MacMillan, New Delhi.<br />
Reference Books:<br />
1. Glasstone, S., “A Textbook of Physical Chemistry,” MacMillan, New Delhi.<br />
2. Bahl and Tuli, “Essentials of Physical Chemistry,” S. Chand and Co, New Delhi.<br />
Page 29
Course Code: ECH-305<br />
Semester-III<br />
CHEMICAL PROCESS CALCULATIONS<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
UNIT-I (Lectures 08)<br />
Introduction to <strong>Chemical</strong> <strong>Engineering</strong>: Calculations, Definition and Strichiometry - Units and<br />
dimensions, the mole unit, conventions in methods of analysis and measurement, basis, temperature,<br />
pressure, the chemical equation and chemical formulae.<br />
UNIT –II<br />
Gases, Vapours, Liquids and Solids: Ideal gas law and its related calculations; Real gas relationships;<br />
Vapour pressure and liquids;Saturation, partial saturation and humidity; Introduction to vapour-liquid<br />
equilibria for multicomponent systems; Material balances involving condensation and vaporization.<br />
UNIT-III (Lectures 08)<br />
Material Balances: Material balance of physical processes with and without chemical reaction, including<br />
recycle, purge and bypass.<br />
UNIT-IV (Lectures 08)<br />
Energy Balances: Concept and Units; Calculation of enthalpy changes; General balance with and<br />
without reactions; Heats of solution and mixing.<br />
UNIT-V (Lectures 08)<br />
Unsteady-state material and energy balances: Solids, liquids and gaseous fuels; Some industrial<br />
examples of the above; Simple estimation of physical properties (transport, thermodynamic) of fluids and<br />
mixtures.<br />
Text Book:<br />
1. Himmelblau, D. M., “Basic Principles and Calculations in <strong>Chemical</strong> <strong>Engineering</strong>,”<br />
6th ed., Prentice-Hall of India, New Delhi.<br />
2. Bhatt and Vora, “Stoichiometry,” 3rd ed., Tata McGraw-Hill, New Delhi.<br />
3. Hougen, Watson and Ragatz, “<strong>Chemical</strong> Process Principles,” Vol. 1, Asia Publishing House, New<br />
Delhi.<br />
Reference Books:<br />
1. Saha, S. N., “Fundamentals of <strong>Chemical</strong> <strong>Engineering</strong>,” Dhanpat Rai Publishing Co., New Delhi.<br />
Page 30
Semester-III<br />
INDUSTRIAL ENGINEERING<br />
Course Code: EME305 L T P C<br />
3 0 0 3<br />
Objective: To know about productivity, work study, production planning and control techniques in<br />
industry.<br />
Unit I (Lectures 8)<br />
Productivity: Introduction, Definition, Measurement, Productivity index, Productivity improvement;<br />
Types of Production Systems.<br />
Work study: Meaning and benefits of work study, Time & motion study; Micro-motion study Pre<br />
determine motion time study Man machine Diagram flow chart; Motion economy; Method study; Work<br />
measurement; Work sampling; Standard time.<br />
Unit II (Lectures 8)<br />
Plant layout and materials Handling: Plant location; Type of layout; Principles of facility layout;<br />
Principles of material handling; Material Handling equipments.<br />
Production planning and control: Objectives; Forecasting; Product design and development functions;<br />
steps in PPC; Planning routine, scheduling, Dispatching & follow-up; Effectiveness of PPC; Introduction<br />
of JIT.<br />
Unit III (Lectures 8)<br />
Managerial Economics : Introduction; Assumptions; Time Value of money; Step-in Break Even<br />
Analysis; Purpose; Costs: Overheads, Fixed & variable costs; Margin of safety; Angle of incidence;<br />
Profit volume graph.<br />
Depreciation Analysis: Causes; Obsolescence; Methods.<br />
Maintenance Management: Maintenance, Planning & Control; Maintenance Strategy.<br />
Unit IV (Lectures 8)<br />
Inventory Control: Inventory; Function; Cost; Deterministic models; Introduction to MRP; Supplychain<br />
Management<br />
Quality Control: Introduction; Process control; SQC control Charts; Single, double & sequential<br />
sampling; Introduction to TQM & bench marking.<br />
Unit V (Lectures 8)<br />
Industrial Ownership: Proprietorship; Partnership; Joint stock & co-operative stores.<br />
Manpower Planning: Process.<br />
Organization: Principles of organization; Development of Organizational charts like line, staff, line and<br />
staff & Functional types.<br />
Job Evaluation & Merit rating: Job analysis; Job description; Job simplification and job evaluation<br />
methods & description; Merit rating; Wage incentive plans.<br />
Text Books<br />
1. Koontz H. Donnel C.O., Principles of Management: An Analysis of Management Functions, Tata<br />
McGraw Hill.<br />
2. Moore J., Manufacturing Management”, Prentice Hall.<br />
3. Mahajan, Industrial <strong>Engineering</strong>, Dhanpat Rai & Sons.<br />
Reference Books<br />
1. Khanna O.P., Industrial <strong>Engineering</strong> & Management, Dhanpat Rai & Sons .<br />
2. Shanker. Ravi, Industrial <strong>Engineering</strong>, Galgotia Publications.<br />
3. Buffa E.S., Modern Production Operations Management, Wiley Eastern<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 31
Semester-III/IV<br />
MATHEMATICS-III<br />
Course Code: EAS301/EAS 401 L T P C<br />
3 1 0 4<br />
Unit I (Lectures 08)<br />
Integral Transforms: Fourier integral, Fourier complex transform, Fourier sine and cosine transforms and<br />
applications to simple heat transfer equations.<br />
Z – Transform and its application to solve difference equations.<br />
Unit II (Lectures 08)<br />
Functions of a Complex Variable: Analytic functions; C-R equations and harmonic functions; Line<br />
integral in the complex plane; Cauchy's integral theorem, Cauchy's integral formula for derivatives of<br />
analytic functions; Liouvilles theorem.<br />
Unit III (Lectures 08)<br />
Functions of a Complex Variable II: Representation of a function by power series; Taylor's and<br />
Laurent's series; Singularities, zeroes and poles; Residue theorem, evaluation of real integrals; conformal<br />
mapping and bilinear transformations.<br />
Unit IV (Lectures 08)<br />
Statistical Techniques: Moments, Moment generating functions, Skewness, Kurtosis, Curve Fitting and<br />
Solution of Equations: Method of least squares and curve fitting of straight line and parabola, Solution of<br />
cubic and bi-quadratic equations, Correlation and Regression, Binomial distribution, Poisson distribution,<br />
Normal distribution.<br />
Unit V (Lectures 08)<br />
Numerical Technique: Bisection method, Regula – Falsi method, Newton - Raphson method.<br />
Interpolation: Finite difference, Newton’s forward and backward interpolation, Lagrange’s and<br />
Newton’s divided difference formula for unequal intervals; Numerical Differentiation, Numerical<br />
Integration; Trapezoidal, Simpson’s 1/3 and 3/8 rule.<br />
Text Books<br />
1. Grewal B.S., Higher <strong>Engineering</strong> Mathematics, Khanna Publishers.<br />
2. Prasad C., <strong>Engineering</strong> Mathematics for Engineers, Prasad Mudralaya.<br />
3. Das H.K., <strong>Engineering</strong> Mathematics Vol-II, S. Chand.<br />
Reference Books<br />
1. Kreyszig E., Advanced <strong>Engineering</strong> Mathematics, Wiley Eastern.<br />
2. Piskunov N, Differential & Integral Calculus, Moscow Peace Publishers.<br />
3. Narayan Shanti, A Text book of Matrices, S. Chand.<br />
4. Bali N.P., <strong>Engineering</strong> Mathematics-III, Laxmi Publications.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 32
Semester-III/IV<br />
PHYSICS II<br />
Course Code: EAS302/EAS 402 L T P C<br />
3 1 0 4<br />
Objective: To understand modern physics like nanotechnology, cryogenics etc.<br />
Course Contents<br />
Unit I (Lectures 08)<br />
Relativistic Mechanics: Inertial and Non- inertial Frames; Michelson-Morley Experiment;<br />
Postulates of Special Theory of Relativity; Galilean and Lorentz Transformation; Length Contraction<br />
and Time Dilation; Addition of Velocities; Mass Energy Equivalence and Variation of Mass with<br />
Velocity.<br />
Unit II (Lectures 08)<br />
Modern Physics: Bragg’s Law; Compton Effect; Wave Particle Duality; De Broglie matter wave;<br />
Davisson and Germer's Experiment; Phase and Group velocities; Uncertainty Principle and<br />
application.<br />
Unit III (Lectures 08)<br />
Quantum Mechanics II : Physical Interpretation of Wave Function and its Normalization;<br />
Expectation Value; Schrodinger Equation in One Dimension; Solutions of Time-Independent<br />
Schrodinger Equation for Free Particle; Particle in an Infinite Square Well; Potential Barrier and<br />
Tunneling; Hydrogen atom (qualitative<br />
Unit IV (Lectures 08)<br />
Superconductivity: Temperature dependence of resistivity; Meissner effect; Penetration depth; Type<br />
I and Type II superconductors; Temperature dependence of critical filed; BCS theory of<br />
superconductors; applications of superconductors.<br />
Introduction to Nanomaterials: Basic principles of nanoscience and technology; creation and use of<br />
buckyballs; properties and use of carbon nanotubes; applications of nanomaterials.<br />
Unit V (Lectures 08)<br />
Vacuum Physics: Mean free path; rotary and diffusion pumps; Pirani and Penning Gauges.<br />
Nuclear Physics: Nuclear Forces; Binding Energy; Liquid Drop Model; Fission; Nuclear Reactors;<br />
Fusion and Energy Processes in Stars, Controlled Thermonuclear Reactions.<br />
Text Books:<br />
1. Robert Resmick, Introduction to Special Theory of Relativity, Wiley.<br />
2. A. Beiser, Perspectives of Modern Physics, McGraw Hill.<br />
3. R. Booker and E. Boysen, Nanotechnology, Wiley.<br />
4. G. G. Haselden, Cryogenic Fundamentals, Academic Press.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 33
Course Code: ECH-351<br />
Semester-III<br />
CHEMICAL ENGINEERING THERMODYNAMIC-I (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
1. To find indicated power of four stroke petrol engine by Morse Test.<br />
2. To prepare heat balance sheet of petrol engine test ring.<br />
3. To prepare the heat balance sheet for diesel engine test ring.<br />
4. To identify the differences between two stroke and four stroke S.I. engine.<br />
5. To determine the calorific value of a liquid fuel using Bomb Calorimeter.<br />
6. To determine the calorific value of a liquid fuel using Gas Calorimeter.<br />
7. To find out the COP (Coefficient of Performance) of a Vapour Compression Refrigeration<br />
system.<br />
8. To study the working of velocity compounded Steam Turbine.<br />
9. Study of steam Engine model.<br />
10. Study of Gas Turbine Model<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 34
Semester-III<br />
PHYSICAL CHEMICAL TECHNOLOGY (LAB)<br />
Course Code: ECH-352<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
1. To study the adsorption of acetic acid on dispersed charcoal.<br />
2. To determine pH of a solution using pH-meter and pH-metric titration.<br />
3. Determination of the strength of HCl solution using a standard solution of Sodium Hydroxide pH<br />
metrically.<br />
4. To find out the rate constant for the inversion of sugar cane in acid medium and to show that<br />
inversion follows the first order kinetics.<br />
5. To estimate Mohrs salt by titrating against a standard solution of potassium dichromate<br />
potentiometrically.<br />
6. To determine the partition coefficient of iodine between carbon tetrachloride and water.<br />
7. To determine the reaction rate constant of an acid catalyzed hydrolysis of an ester- titrimetry.<br />
8. To determine the coefficient of viscosity of the given liquid at room temperature by using<br />
Ostwald’s viscometer.<br />
9. To determine the surface tension of the given liquid by drop number method.<br />
10. To find out the molecular weight of a given substance by Rast’s camphor method.<br />
11. To determine the solubility of potassium nitrate at different temperatures.<br />
12. To determine the transition temperature of Glauber’s salt by thermometric method.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 35
Course Code: ECH-353<br />
Semester-III<br />
APPLIED CHEMISTRY (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
1. Estimation of Glucose.<br />
2. Freundlich adsorption isotherm verification.<br />
3. Conductivity: (i) Conductivity titration strength of strong acid vs. strong base, (ii) Dissociation<br />
constant of a weak acid (CH3COOH).<br />
4. Applications of TLC in the organic chemistry.<br />
5. Determination of dissolved oxygen percent in a given water sample (Winkler’s method)<br />
6. Determination of iron by spectrophotometric method.<br />
7. Determination of the strength of HCl solution using a standard solution of sodium hydroxide p H<br />
metrically.<br />
8. Estimation of mohrs salt by titrating against a standard solution of potassium dichromate<br />
potentiometrically.<br />
9. Determination of conductance of a given sample of water with a conductivity meter.<br />
10. Determination of partition coefficient of iodine between carbon tetrachloride and water.<br />
11. Determination of reaction rate constant of an acid catalyzed hydrolysis of an ester.<br />
12. Determination of the coefficient of viscosity of the given liquid by Ostwald viscometer.<br />
13. Identification of organic compounds in the mixture.<br />
14. Functional group test of organic compounds.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 36
Course Code: ECH-401<br />
Semester-IV<br />
HEAT TRANSFER<br />
L T P C<br />
3 0 0 3<br />
Unit – I (Lectures 08)<br />
Introduction: Modes of heat transfer - Conduction, convection, radiation.<br />
Steady-State Conduction in One Dimension: Fourier’s Law; Thermal conductivity; Steady-state<br />
conduction of heat through a single and composite solid - cylinder and sphere; Steady-state heat<br />
conduction in bodies with heat sources - plane wall, cylinder and sphere.<br />
Heat Transfer Coefficient: Convective heat transfer and the concept of heat transfer coefficient; Overall<br />
heat transfer coefficient; Heat transfer from extended surfaces; Thermal contact resistance; Critical and<br />
optimum insulation thickness.<br />
Unit – II (Lectures 08)<br />
Forced Convection: Flow over a flat plate; Thermal boundary layer; Flow across a cylinder;<br />
Dimensional analysis - Buckingham Pi theorem, Dimensionless groups in heat transfer; Correlations for<br />
the heat transfer coefficient - Laminar flow through a circular pipe, turbulent flow through a non-circular<br />
duct, flow over flat plate, flow across a cylinder, flow past a sphere, flow across a bank of tubes, heat<br />
transfer coefficient in a packed and fluidized bed; Double-pipe heat exchanger in parallel and countercurrent<br />
flow.<br />
Free Convection: Introduction; Heat transfer correlations for free convection - flat surface, cylinder,<br />
sphere, enclosure; Combined free and forced convection.<br />
Unit – III (Lectures 08)<br />
Boiling and Condensation: Boiling phenomenon; Nucleate boiling; Correlations for pool boiling heat<br />
transfer - Nucleate boiling, critical heat flux, stable film boiling; Forced convection boiling;<br />
Condensation phenomena - Film condensation on a vertical surface, turbulent film condensation,<br />
condensation outside a horizontal tube and tube bank, Condensation inside a horizontal tube, effect of<br />
non-condensable gases, Dropwise condensation.<br />
Unit – IV (Lectures 08)<br />
Radiation Heat Transfer: Basic concepts of radiation from a surface - Black body radiation, Planck’s<br />
Law, Wien’s Displacement Law, Stefan-Boltzmann Law, Kirchoff’s Law, Gray body; Radiation intensity<br />
of a black body; Spectral emissive power of a black body over a hemisphere; Radiation heat exchange<br />
between surfaces – the view factor; Radiation exchange between black bodies and between diffuse gray<br />
surfaces.<br />
Unit – V (Lectures 08)<br />
Heat Exchangers: Construction of a shell and tube heat exchanger; Fouling of a heat exchanger; LMTD;<br />
Temperature distribution in multi-pass heat exchangers; Individual heat transfer coefficients and their<br />
relations with overall H.T. coefficients; Types of shell and tube heat exchanger.<br />
Evaporators: Types of evaporators – Natural circulation evaporators, forced circulation evaporators,<br />
falling film evaporators, climbing film evaporators, agitated thin film evaporators and plate evaporators;<br />
Principles of evaporation and evaporators; Single and multiple effect evaporators; Capacity and<br />
economy; Boiling point rise; Enthalpy balance of a solution; Calculations of single effect and multieffect<br />
evaporators; Methods of feeding to multieffect evaporators.<br />
Unsteady-State Heat Conduction: Mathematical formulations and initial and boundary conditions;<br />
Analytical solution; Numerical solution.<br />
Text Books:<br />
1. Dutta, B. K., “Heat Transfer: Principles and Applications,” PHI, New Delhi,<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 37
2001.<br />
2. Holman, J. P., “Heat Tansfer,” 8th ed., McGraw-Hill,New Delhi<br />
3. A.J. Chapman, “Heat Transfer,” Maxwell Macmillan, 1984. New Delhi<br />
4. Kern D.Q., “Process Heat Transfer”, Tata McGraw Hill, 1950. New Delhi<br />
Reference Books:<br />
1. Hewitt, G. F., Shires, G.L. and Bott, T. R., “Process Heat Transfer”, CRC Press,1994, New Delhi<br />
2. Rao, Y. V. C., “Heat Transfer”. New Age International, Delhi<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 38
Course Code: ECH-402<br />
Semester-IV<br />
INORGANIC CHEMICAL TECHNOLOGY<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I (Lectures 08)<br />
Water: Sources of water; Hardness; Treatment for different end-uses; Municipal water conditioning;<br />
Industrial waste and water treatment.<br />
Unit – II (Lectures 08)<br />
Sulphur and sulphuric acid: Sources of sulphur; Sulphuric acid; Different processes of manufacturing -<br />
Contact process, DCDA process.<br />
Nitrogen based compounds: Manufacture of ammonia; Nitric acid; Urea and ammonium nitrate.<br />
Unit – III (Lectures 08)<br />
Phosphorous and phosphoric acid: Methods for production of phosphorous and phosphoric acid;<br />
Manufacture of super phosphate and triple super phosphate.<br />
Chloro-alkali : - Manufacture of soda ash; Caustic soda and chlorine.<br />
Unit – IV (Lectures 08)<br />
Cement: Types of cement; Manufacture of ordinary Portland cement; Slag cement.<br />
Fuel and industrial gases: Production of water gas; producer gas and coke oven gas; Production of<br />
acetylene, oxygen and nitrogen.<br />
Unit – V (Lectures 08)<br />
Metallurgy: Manufacture of pig iron; Cast iron; Methods of making steel - open hearth process;<br />
Production of aluminium by electrolytic process.<br />
Textbooks:<br />
1. Gopala Rao, M & Marshall Sitting, “Dryden’s Outlines of <strong>Chemical</strong> Technology” .Affiliated East<br />
West Press Pvt. Ltd. New Delhi<br />
2. Austin, G.T., “Shreve’s <strong>Chemical</strong> Process Industries” McGraw Hill Book. New Delhi<br />
Reference Books:<br />
1. Kirk, R.E. & Othmer, D.F.“ Encyclopedia of <strong>Chemical</strong> Technology” John Wiley. New Delhi.<br />
Page 39
Semester-IV<br />
MATERIAL SCIENCE AND TECHNOLOGY<br />
Course Code: ECH-403<br />
L T P C<br />
3 0 0 3<br />
Unit- I (Lectures 08)<br />
Introduction to Materials<br />
<strong>Engineering</strong> materials - Classification, Characteristics and basic principles for their selection; Structure of<br />
atom; Types of bonds; Crystal structure - Defects in crystal structure and their influence on properties of<br />
a material.<br />
Unit- II (Lectures 08)<br />
Metals and Their Alloys<br />
Phase equilibrium diagram for Iron-carbon and Copper-zinc system; Ferrous and nonferrous alloys; Mild<br />
steels; Special steels; Stainless steels; Brasses; Bronzes; Aluminum alloys; Titanium alloys; Methods for<br />
fabrications - Rolling, Forging, Extrusion and Joining.<br />
Unit- III (Lectures 08)<br />
Polymers<br />
Types of plastics; Structure; Properties; Correlations of important plastics; Polymerization processes and<br />
additives; Fibre-reinforced plastics; Rubbers & elastomers and Applications.<br />
Unit- IV (Lectures 08)<br />
Ceramics and Glass<br />
Structure – Properties, Correlations, Oxide and non-oxide ceramics, Vitreous and borosilicate glasses,<br />
glass-ceramics and enamels; Major electrical, optical and mechanical properties of ceramics and glasses;<br />
Enameling and glass lining.<br />
Unit- V (Lectures 08)<br />
Corrosion and its Control<br />
Types of corrosion; <strong>Chemical</strong> and electrochemical reactions; Methods of corrosion prevention;<br />
Corrosion-resistant materials.<br />
Text Books:<br />
1. James, F. Shackelford, “Introduction to Materials Science”, Macmillan Pub. Co., NY, 1990<br />
2. Jestrazebaski, D.Z., “ Properties of <strong>Engineering</strong> Materials”, 3rd ed., Toppen Co. Ltd.<br />
3. Smith, W. F., “Foundations of Materials Science and <strong>Engineering</strong>,” 2nd ed., McGraw-Hill, 1993.<br />
Reference Books:<br />
1. Raghavan, V., “Materials Science and <strong>Engineering</strong>,” PHI, New Delhi.<br />
2. Van Vlack, L. H., “Materials Science and <strong>Engineering</strong>,” Addison Wesley. New Delhi.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 40
Semester-IV<br />
CHEMICAL ENGINEERING THERMODYNAMICS-II<br />
Course Code: ECH-404<br />
L T P C<br />
3 0 0 3<br />
Unit – I (Lectures 08)<br />
Review: First and second laws of thermodynamics<br />
Volumetric Properties of Pure Fluids: PVT behavior of pure substances; Virial equation and its<br />
applications; Cubic equations of state; Generalized correlations for gases and liquids.<br />
Heat Effects: Sensible heat effect; Heat effects accompanying phase changes of pure substances;<br />
Standard heats of reaction, formation and combustion; Effect of temperature on the standard heat of<br />
reaction.<br />
Unit – II (Lectures 08)<br />
Thermodynamic Properties of Fluids: Fundamental relations; Maxwell’s equations; Residual<br />
properties; Clapeyron’s Equation; Generalized correlations for thermodynamic properties of gases.<br />
Unit – III (Lectures 08)<br />
Multicomponent Systems: <strong>Chemical</strong> potential; Ideal-gas mixture; Ideal solution; Raoult’s Law; Partial<br />
properties; Fugacity and fugacity coefficient; Generalized correlations for the fugacity coefficient; Excess<br />
Gibbs’ energy; Activity coefficient.<br />
Unit – IV (Lectures 08)<br />
Phase Equilibria at low to moderate pressures - Phase rule, Phase behavior for vapor liquid systems;<br />
Margules equation; Van laar equation; Wilson equation; NRTL equation; Dew point; Bubble point and<br />
flash calculations.<br />
Solution Thermodymics: Ideal solution; Fundamental residual – property relation; Fundamental excess<br />
– property relation; Evaluation of partial properties; Heat effects of mixing processes; Partially miscible<br />
systems.<br />
Unit – V (Lectures 08)<br />
<strong>Chemical</strong> Reaction Equilibria: Reaction coordinate; Equilibrium criteria to chemical reactions;<br />
Standard Gibbs’ energy change and the equilibrium constant; Effect of temperature on the equilibrium<br />
constant; Evaluation of equilibrium constants; Relations between equilibrium constants and compositions<br />
- gas-phase reactions, liquid- phase reactions; Calculation of equilibrium compositions for single-phase<br />
reactions; Multireaction equilibria.<br />
Text Books:<br />
1. McCabe, W.L., Smith, J.C., and Harriott, P., “Unit Operations of <strong>Chemical</strong> <strong>Engineering</strong>”, 6th ed.,<br />
McGraw Hill. New Delhi<br />
2. Brown, G. G., et al, “Unit Operations,” CBS Publications, Delhi.<br />
3. Coulson, J. H. and Richardson, J. F., “<strong>Chemical</strong> <strong>Engineering</strong>,” Vol. 2, Asian Books<br />
Private Ltd., New Delhi.<br />
Reference Books:<br />
1. Perry, R. H., et al, “<strong>Chemical</strong> Engineers’ Handbook,” 7th ed., McGraw-Hill. New Delhi.<br />
2. Foust, A.S., et al., “Unit Operations”, 2nd ed., John Wiley. New Delhi.<br />
3. Bhattacharya, “Unit Operations”, Vol. 1., Khanna Publishers. New Delhi.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 41
Semester-IV<br />
NUMERICAL METHODS IN CHEMICAL ENGINEERING<br />
Course Code: ECH-405<br />
L T P C<br />
3 1 0 4<br />
Unit – I (Lectures 08)<br />
Linear Algebraic Equations: Introduction; Gauss-Elimination; Gauss-Siedel and LU Decomposition<br />
Methods; Thomas’ algorithm.<br />
Eigen Values and Eigen Vectors of Matrices: Introduction; Fadeev Leverrier’s method; Power method;<br />
Householder’s and Givens’ method.<br />
Unit – II (Lectures 08)<br />
Nonlinear, Algebraic Equations: Single variable and multivariable successive substitution method;<br />
Single variable and multivariable Newton-Raphson technique; Polynomial root finding methods.<br />
Unit – III (Lectures 08)<br />
Ordinary Differential Equations: Initial Value Problems; Explicit Adams–Bashforth technique;<br />
Implicit Adams-Moulton technique; Predictor-corrector technique; Runge-Kutta method; Stability of<br />
algorithms.<br />
Unit – IV (Lectures 08)<br />
Ordinary Differential equations: Boundary Value Problems; Finite difference technique; Orthogonal<br />
collocation (OC); Orthogonal collocation on finite Elements (OCFE); Galerkin Finite Element (GFE)<br />
technique; Shooting techniques.<br />
Unit – V (Lectures 08)<br />
Partial differential Equations: Partial Differential Equations (PDE); Classification of PDE; Finite<br />
difference technique (Method of lines); Orthogonal collocation; Case Studies; Use of spreadsheets in<br />
<strong>Chemical</strong> <strong>Engineering</strong>.<br />
Text Books:<br />
1. Gupta, S.K., “Numerical Methods for Engineers”, New Age International Ltd. New Delhi,1995.<br />
Reference Books:<br />
1. Hanna, O.T. and Sandall, O.C., “Computational Methods in <strong>Chemical</strong> <strong>Engineering</strong>” Prentice-Hall,<br />
New Delhi 1975.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 42
Course Code: ECH-451<br />
Semester-IV<br />
HEAT TRANSFER (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
1. To determine total thermal resistance and thermal conductivity of composite wall.<br />
2. To determine the thermal conductivity of a metal rod.<br />
3. To determine the natural convective heat transfer coefficient for a vertical tube.<br />
4. To determine critical heat flux point for pool boiling of water.<br />
5. To determine forced convective heat transfer coefficient for air flowing through a pipe.<br />
6. To determine over-all heat transfer coefficient in double pipe heat exchanger.<br />
7. To study temperature distribution along the length of a pin fin under natural and forced<br />
convection conditions.<br />
8. To determine Stefan-Boltzmann constant.<br />
9. To determine emissivity of a given plate at various temperatures.<br />
10. To determine radiation constant of a given surface.<br />
11. To study shell and tube heat exchanger.<br />
12. Estimation of unsteady state film heat transfer coefficient between the medium in which the body<br />
is cooled.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 43
Course Code: ECH-452<br />
Semester-IV<br />
INORGANIC CHEMICAL TECHNOLOGY (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
1. To analyze the given inorganic mixture containing five radicals by semi micro technique.<br />
2. To find out the chemical oxygen demand of a waste water sample using potassium dichromate.<br />
3. To determine the chlorine concentration in a supplied water sample using silver nitrate method.<br />
4. To find out the strength of the supplied magnesium salt solution using EDTA as an intermediate<br />
solution.<br />
5. To find out the strength of the supplied calcium salt solution using EDTA as an intermediate<br />
solution by substitution method.<br />
6. To determine the carbon dioxide content in polluted water.<br />
7. To estimate barium as barium sulphate from the solution of barium chloride.<br />
8. To prepare the micro-cosmic salt.<br />
9. To prepare sodium thiosulphate by using sodium sulphate with powdered roll sulphur.<br />
10. To prepare tetra ammine copper (II) sulphate.<br />
11. To determine the percentage of available chlorine in a given sample of bleaching powder.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 44
Course Code: ECH-501<br />
Semester-V<br />
PROCESS INSTRUMENTATION<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Introduction, general principles of measurement, its classification by physical characteristics, direct and<br />
inferential measurement.<br />
(Lectures 08)<br />
Unit – II<br />
Static and dynamic characteristics of instruments. Measurement of temperature, pH, pressure, vacuum,<br />
flow rate, liquid level, differential pressure<br />
(Lectures 08)<br />
Unit – III<br />
Viscosity, conductivity, nuclear radiation, humidity and gas composition, spectroscopy.<br />
(Lectures 08)<br />
Unit – IV<br />
Classification of sensors and transducers. Building blocks of an instrument, transducer, amplifier signal<br />
conditioner, signal isolation, transmission, display, data acquisition modules, interfaces, recording.<br />
(Lectures 08)<br />
Unit – V<br />
Control centre, instrumentation diagram, On line instrumentation in modern plants.<br />
Text Books:<br />
1. Nakra, “Instrumentation, Measurement and Analysis”; Tata McGraw Hill,<br />
New Delhi.<br />
2. Patranabis, D., “Principles of Industrial Instrumentation” 2nd ed. Tata McGraw<br />
Hill, New Delhi.<br />
3. Eckman, D.P., “Industrial Instrumentation” Wiley Eastern, 1978.<br />
4. Liptak, B.G., “Industrial Engineers’ Handbook” Vol.1 and 2, CRC Press,<br />
1994.<br />
Reference Books:<br />
1. Andrew, W.G., et al., “Applied Instrumentation in the Process Industries,”<br />
Gulf Pub.1993.<br />
2. Wightman, E.J., “Instrumentation in Process Control,” Butterworth, 1972.<br />
3. Doebelin, E., “Measurement Systems: Applications and Design,” 4th ed.,<br />
McGraw Hill, 1990<br />
(Lectures 08)<br />
Page 45
Course Code: ECH-502<br />
Semester-V<br />
ORGANIC CHEMICAL TECHNOLOGY<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit I<br />
Coal and Coal chemicals: Types of coal, different uses, distillation of coal, treatment of products, low<br />
and high temperature carbonization of coal, coal tar distillation,<br />
Petroleum: Origin, classification, composition of crude oil, production of crude oil, distillation of crude<br />
petroleum, refining-methods, uses of products, (Lectures 08)<br />
Unit II<br />
Extraction of vegetable oils: Purification, acid value, hydrogenation of oils,<br />
Iodine value: Manufacture of fatty acids and soaps, saponification value, detergents- classification and<br />
manufacture. (Lectures 08)<br />
Unit III<br />
Paints and varnishes: Constituents of paints, functions of paint, manufacturing procedures, Pigmentsmanufacture<br />
of lithophone, varnishes, (Lectures 08)<br />
Unit IV<br />
Manufacture of pulp: Kraft process and sulphite process, production of paper.<br />
Manufacture of cane sugar: Refining, manufacture of starch, dextrin and dextrose, production of<br />
ethanol by fermentation, manufacture of pencillin, (Lectures 08)<br />
Unit V<br />
Polymerisation: Different methods, manufacture of polyethylene, phenol formaldehyde, SBR, synthetic<br />
fibres, rayon, 6-nylon, 6,6-nylon, polyesters. (Lectures 08)<br />
Text books:<br />
1.`Dryden’s out lines of chemical Technology’ by Gopala Rao, M. & Marshall Sitting, .Affilated East<br />
West Press Pvt.Ltd.<br />
2.`Shreve’s <strong>Chemical</strong> Process Industries’ Austin,G.T,,. Mcgraw Hill Publishers<br />
Reference book:<br />
1.`Encyclopedia of <strong>Chemical</strong> Technology’ by Kirk.R.E & othmer,D.F., Inter Science.<br />
Page 46
Course Code: ECH-503<br />
Semester-V<br />
MASS TRANSFER – I<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Diffusion phenomenon: Molecular and eddy diffusion in gases, liquids and solids, interface mass<br />
transfer Mass transfer theories: Film theory penetration theory and surface renewal theory.<br />
(Lectures 08)<br />
Unit – II<br />
Concept of Mass transfer coefficient: Individual and film coefficients, overall mass transfer co-efficient<br />
and their inter relationships. Continuous contact and differential contact, mass transfer concepts of NTU<br />
and HTU, their inter relationship.<br />
Interphase Mass Transfer: Equilibrium, diffusion between phases, material balances, stages and<br />
concept of operating line and tie line.<br />
(Lectures 08)<br />
Unit – III<br />
Equipment for gas liquid contact: Sparged vessel, mechanically agitated vessel, tray towers, venture<br />
scrubber, wetted wall towers, spray towers and packed towers, tray tower vs packed tower.<br />
Absorption: Absorption in continuous contact columns, Co-current, Counter current and cross current<br />
contacting of fluids, calculation of NTU and HTU, concept of HETP.<br />
(Lectures 08)<br />
Unit – IV<br />
Adsorption: Adsorption theories, types of adsorbent, activated carbon silica, silica and molecular sieves,<br />
Batch and column adsorption. Break through curves, gas adsorption, BDST models for adsorption<br />
calculation.<br />
(Lectures 08)<br />
Unit – V<br />
Drying: Equilibrium mechanism theory of drying, drying rate curve, Batch and continuous drying,<br />
working principle of different types of dryers such as tray driers, Drum dryers, spray and tunnel dryers.<br />
(Lectures 08)<br />
Text Books:<br />
1. Treybal, R.E.; “Mass Transfer Operation”, McGraw-Hill, 1980.<br />
2 King, C.J. “Separation Processes”, McGraw – Hill, NY.<br />
3 Smith, B.D., “Design of Equilibrium stage Processes”, McGraw-Hill, NY<br />
Reference Books:<br />
1. McCabe, W.L. Smith, J.C. and Harriot, P., “Unit Operations of <strong>Chemical</strong> <strong>Engineering</strong>”, 6th ed,<br />
McGraw-Hill, NY.<br />
2. Coulson, J.M. and Richardson, J.F., “<strong>Chemical</strong> <strong>Engineering</strong>”, Vol. I and II, Asian<br />
Books Pvt., New Delhi..<br />
Page 47
Course Code: ECH-504<br />
Semester-V<br />
SPECTROSCOPY TECHNIQUES<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Components of instruments for optical spectroscopy : Components and configuration of instruments<br />
for optical spectroscopy, radiation sources, sample contains, radiation detection, signal processor and<br />
vadouts.<br />
An Introduction to absorption Spectroscopy : Terms employed in absorption spectroscopy,<br />
quantitative aspects of absorption measurements (Lectures 08)<br />
Unit – II<br />
Application of Ultraviolet and visible Spectroscopy: Absorption species, typical instruments,<br />
application of absorption measurements to qualitative and quantitative Measurement.<br />
Infra Red Absorption Spectroscopy : Theory of infrared absorption, infrared instruments qualitative<br />
and quantitative application. (Lectures 08)<br />
Unit – III<br />
Raman Spectroscopy: Theory of Raman spectroscopy, instrumentation application of Raman<br />
spectroscopy<br />
Nuclear Magnetic Resonance Spectroscopy : Theory of instrumentation of NMR, application of protein<br />
NMR to analysis of compounds. (Lectures 08)<br />
Unit – IV<br />
Mass Spectroscopy : Theory of Flame Spectroscopy, flame characteristics, atomizer for<br />
atomic spectroscopy atomic absorption spectroscopy. (Lectures 08)<br />
Unit – V<br />
Atomic Spectroscopy : Theory of Flame Spectroscopy, flame characteristics, atomizer for<br />
atomic spectroscopy, atomic absorption spectroscopy. (Lectures 08)<br />
Text Books:<br />
1. D. Holen and H.Peck, “Analytical Biochemistry” Longman, 1983.<br />
Reference Books:<br />
1. Wilson and J. Walker, “Practical Biochemistry” <strong>University</strong> Press, 2000<br />
Page 48
Course Code: ECH-505<br />
Semester-V<br />
ENVIRONMENTAL ENGINEERING<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Atmosphere- Introduction, structure of the atmosphere, chemical and photochemical reaction in the<br />
atmosphere, primary air pollutants-sources. Carbon, Nitrogen & Sulfur Cycle. (Lectures 08)<br />
Unit – II<br />
Wastewater Treatment: Characterization of industrial wastewater, primary, secondary and tertiary<br />
treatment. Segregation, screening, equalization, coagulation, flocculation, precipitation, flotation,<br />
sedimentation, aerobic treatment, anaerobic treatment, absorption, ion exchange, membrane filtration,<br />
electrodialysis, sludge dewatering and disposal methods. (Lectures 08)<br />
Unit – III<br />
Air Pollution Control: Sources and classification of air pollutants, nature and characteristics of gaseous<br />
and particulate pollutants, from automobiles. Air pollution meteorology, plume and its behavior and<br />
atmospheric dispersion, control of particulate emission by gravity settling chamber, cyclones , wet<br />
scrubbers, bag filters and electrostatic precipitators (General Explanation). Control of gaseous<br />
emission by absorption, adsorption, chemical transformation and combustion.<br />
(Lectures 08)<br />
Unit – IV<br />
Solid Waste Management: solid waste, waste disposal methods, recycling of solid waste and its<br />
management. Hazardous and non-hazardous waste, methods of treatment and disposal, land filling,<br />
leachate treatment and incineration of solid wastes. (Lectures 08)<br />
Unit – V<br />
Environmentally Pollution Monitoring Legislation, standards for water and air, Effects of air pollutants<br />
on human health, vegetation and materials, Air pollution monitoring instruments COx, NOx, SOx,<br />
Hydrocarbon and Ozone. Hydrocarbons particulates, sampling techniques. Global warming, Green house<br />
effect, depletion of ozone layer, human activity and meteorology.<br />
(Lectures 08)<br />
Text Books:<br />
1. Dhameja, S.K., “Environmental <strong>Engineering</strong> and Management”, S.K. Kataria & Sons,<br />
Delhi, 2002.<br />
2. Masters, G.M., “Introduction to Environmental <strong>Engineering</strong> and Science”, Prentice Hall of<br />
India, New Delhi, 2001.<br />
3. Bhatia, S.C., “Environmental Pollution and Control in <strong>Chemical</strong> Process Industries”,<br />
Khanna Publishers, Delhi, 2001.<br />
Reference Books:<br />
1. Pandey G.N. and Karney, “Environmental <strong>Engineering</strong>” Tata McGraw Hill, Delhi.<br />
2. Instrumentation by Khandpur. Metcalf & Eddy, Inc., “Wastewater <strong>Engineering</strong>: Treatment and<br />
Reuse”, 4th ed., Tata McGraw Hill, New Delhi, 2003.<br />
3. Modi, P.N. “Sewage Treatment and disposal and Waste Water <strong>Engineering</strong>,” Vol.II, Standard<br />
book house, Delhi, 2001.<br />
Page 49
Semester V<br />
<strong>Engineering</strong> and Managerial Economics<br />
Course Code: EHM503<br />
L T P C<br />
3 0 0 3<br />
Objective:<br />
• To understand the Scope of Economics, Demand Forecasting and Market Study.<br />
Unit-I<br />
Introduction: Meaning, Nature and Scope of Economics, Meaning of Science, <strong>Engineering</strong> and<br />
Technology; Managerial Economics and its scope in engineering perspective.<br />
Unit-II<br />
Demand: Basic Concepts Demand Analysis, Law of Demand, Determinates of Demand; Elasticity of<br />
Demand-Price; Income and cross Elasticity; Uses of concept of elasticity of demand in managerial<br />
decision.<br />
Unit-III<br />
Forecasting: Demand forecasting Meaning, significance and methods of demand forecasting; production<br />
function; Laws of returns to scale & Law of Diminishing returns scale.<br />
Short and Long run Cost curves: fixed cost, variable cost, average cost, marginal cost, Opportunity<br />
cost.<br />
Unit-IV<br />
Market Study: Market Structure Perfect Competition; Imperfect competition: Monopolistic, Oligopoly,<br />
Duopoly sorbent features of price determination and various market conditions.<br />
Unit-V<br />
Inflation: National Income; Inflation and Business Cycles Concept of N.I. and Measurement; Meaning<br />
of Inflation; Type causes & prevention methods; Phases of business cycle.<br />
Text Books:<br />
1. Koutsoyiannis, A : Modern Microeconomics, ELBS.<br />
2. Kakkar, D.N., Managerial Economics for <strong>Engineering</strong>, New Age International Publication.<br />
Reference Books:<br />
1. Dwivedi, D.N., Managerial Economics, Vikas Publishing.<br />
2. Maheshwari, Y., Managerial Economics, Prentice Hall of India.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 50
Course Code: ECH-551<br />
Semester-V<br />
PROCESS INSTRUMENTATION (LAB)<br />
1. Calibration of thermocouple.<br />
2. Calibration of Bimetallic thermocouple.<br />
3. Calibration of Resistance thermocouple.<br />
4. Calibration of Pressure gauge.<br />
5. Calibration of Pnuematic pressure recorder.<br />
6. Calibration of Differential pressure recorder.<br />
7. Calibration of Orificemeter<br />
8. Calibration of Venturimeter / Rotameter/ Gas flow meter.<br />
9. Estimation of viscosity by Redwood/ Saybolt/<br />
10. Estimation of viscosity by Ostwald viscometer.<br />
11. Calibration of pH meter.<br />
12. Calibration of Conductivity meter.<br />
13. Calibration of Turbidity meter.<br />
14. Estimation of surface tension by Tensiometer.<br />
Evaluation of Practical Examination:<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 51
Course Code: ECH-552<br />
Semester-V<br />
ORGANIC CHEMICAL TECHNOLOGY (LAB)<br />
A. Analysis of water:<br />
1. Total solids, dissolved solids,pH<br />
2. Chlorides and sulphates<br />
3. Temporary, permanent and total hardness.<br />
B. Analysis of oils:<br />
4. Acid value<br />
5. Iodine value<br />
6. Saponification value<br />
C. Miscellaneous analysis:<br />
7. Analysis of coal: Proximate analysis and ultimate analysis.<br />
8. Analysis of lime: Estimation of acid insolubles, available lime and<br />
calcium carbonate<br />
9. Analysis of bleaching powder: Estimation of chlorine content.<br />
10. Analysis of starch/glucose: Estimation of total reducing sugars<br />
11. Analysis of saw dust: Estimation of total cellulose and –cellulose<br />
E. Miscellaneous preparations:<br />
12. Preparation of soap<br />
13. Preparation of copper pigment<br />
14. Preparation of chrome yellow pigment<br />
15. Preparation of phenol formaldehyde resin<br />
16. Prepare nitrobenzene from benzene<br />
17. Prepare m-dinitro benzene from nitro benzene<br />
18. Prepare p-nitro acetanilide from acetanilide<br />
Evaluation of Practical Examination:<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE & VIVA<br />
DURING THE SEMESTER (40 MARKS)<br />
EXPERIMENT FILE WORK VIVA<br />
(10 MARKS) (10 MARKS) (10 MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5 MARKS)<br />
VIVA<br />
(10 MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50 MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
Page 52
Course Code: ECH-553<br />
Semester-V<br />
MASS TRANSFER-I (LAB)<br />
1. To study the steam distillation.<br />
2. To study differential distillation.<br />
3. To estimate the height equivalent to a theoretical plate .<br />
4. To study vapor-liquid equilibria.<br />
5. To determine the liquid diffusion coefficient.<br />
6. To determine the vapor diffusion coefficient.<br />
7. To study the surface evaporation.<br />
8. To estimate the height of a transfer unit.<br />
9. To study the absorption unit.<br />
10. To study the evaporator (Feed forward and Feed backward).<br />
11. To study the drying unit.<br />
Evaluation of Practical Examination:<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 53
Semester V<br />
INDUSTRIAL TRAINING<br />
(PRESENTATION BASED ON INDUSTRIAL TRANING DONE AFTER THE IV<br />
SEMESTER EXAMINATION IN SUMMER)<br />
Course Code: ECH-591<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 0 2<br />
Students will attend Industrial training of four weeks in any industry or reputed organization after the IV<br />
semester examination in summer vacation. The evaluation of this training shall be included in the V<br />
semester evaluation.<br />
The student will be assigned a faculty guide who would be the supervisor of the student. The faculty<br />
would be identified before the end of the IV semester and shall be the nodal officer for coordination of<br />
the training.<br />
Students will also be required to prepare an exhaustive technical report of the training undertaken during<br />
the V semester which will be duly signed by the officer under whom training was taken in the industry/<br />
organization. The covering format shall be signed by the concerned office in-charge of the training in the<br />
industry. The officer-in-charge of the trainee would also give his rating of the student in the standard<br />
<strong>University</strong> format in a sealed envelope to the Director of the college.<br />
The student at the end of the V semester will present his report about the training before a committee<br />
constituted by the Director of the College which would be comprised of at least three members<br />
comprising of the Department Coordinator, Class Coordinator and a nominee of the Director. The<br />
students guide would be a special invitee to the presentation. The seminar session shall be an open house<br />
session. The internal marks would be the average of the marks given by each member of the committee<br />
separately in a sealed envelope to the Director.<br />
The marks by the external examiner would be based on the report submitted by the student which shall be<br />
evaluated by the external examiner and cross examination done of the student concerned.<br />
Not more than three students would form a group for such industrial training/ project submission.<br />
The marking shall be as follows.<br />
Internal: 50 marks<br />
By the Faculty Guide - 25 marks<br />
By Committee appointed by the Director – 25 marks<br />
External: 50 marks<br />
By Officer-in-charge trainee in industry – 25 marks<br />
By External examiner appointed by the <strong>University</strong> – 25 marks<br />
Page 54
Course Code: ECH-601<br />
Unit – I<br />
Semester-VI<br />
CHEMICAL REACTION ENGINEERING – I<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Introduction: Definition of reaction rates, variable affecting reaction rates, classification of reactions,<br />
order, molecularity.<br />
(Lectures 08)<br />
Unit – II<br />
Kinetics of Homogenous Reactions: Concentration dependent term of a rate equation, temperature<br />
dependent term of a rate equation, searching for a mechanism.<br />
Interpretation of Batch Reactor Data: Constant volume batch reactor, variable volume batch reactor,<br />
temperature and reaction rate.<br />
(Lectures 08)<br />
Unit – III<br />
Introduction to Reactor Design: Ideal reactors for single reaction: Ideal batch reactor, steady state<br />
mixed flow Reactor, steady state PFR, Holding time and space time for flow systems.<br />
Design for single reactions: Size comparison, multiple reactor systems, recycle reactor, auto catalytic<br />
reactions.<br />
Design for multiple reactions: Reactions in parallel, reactions in series, series – parallel reactions.<br />
(Lectures 08)<br />
Unit – IV<br />
Temperature and Pressure Effects on Reactions: Single reactions: Heat of reaction, equilibrium<br />
constants, graphical design procedure, optimum temperature progression, adiabatic operations. Multiple<br />
reactions: Product distribution and temperature.<br />
(Lectures 08)<br />
Unit – V<br />
Stability of Multiple Steady – States: Multiple steady-states of a CSTR with a first order reaction,<br />
Ignition – extinction curve.<br />
(Lectures 08)<br />
Texts Books:<br />
1. Levenspiel, O., “<strong>Chemical</strong> Reaction <strong>Engineering</strong>” 3rd ed., John Wiley & Sons,<br />
Singapore 1999.<br />
2. Fogler, H.S., “Elements of <strong>Chemical</strong> Reaction <strong>Engineering</strong>” 3rd ed., Prentice Hall of<br />
India, 2003.<br />
3. Smith, J.M. “<strong>Chemical</strong> <strong>Engineering</strong> Kinetics”, 3rd McGraw-Hill, 1981.<br />
Reference Books:<br />
1. Dawande S.D. “Principles of <strong>Chemical</strong> Reaction <strong>Engineering</strong>,” 2nd ed., Central Techno<br />
Publications, Nagpur, 2003.<br />
2. Richardson, J.F. and peacock D.G., “Coulson and Richardson’s <strong>Chemical</strong><br />
<strong>Engineering</strong>,” Vol.3, 3rd ed. Asian Books Pvt. Ltd. New Delhi 1998.<br />
Page 55
Course Code: ECH-602<br />
Semester-VI<br />
MASS TRANSFER–II<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Distillation : Vapor liquid Equilibria, Boiling point diagram, Relative volatility, flash and differential<br />
distillation for two component mixture, steam distillation, azeotropic distillation, extractive distillation.<br />
Continuous and differential contact distillation: Rectification, reflux ratio and its importance,<br />
Minimum reflux, total and optimum reflux ration, material balance and Q-line equation, open steam,<br />
multiple feed and multiple product calculations, Enthalpy concentration diagram, panchon-Savarit and<br />
McCabe Theile method for calculation of number of plates. Approximate wquation; Fensky and<br />
underwood equation for minimum reflux and minimum number of plate calculation, Batch distillation.<br />
(Lectures 08)<br />
Unit – II<br />
Liquid – Liquid extraction : Liquid-Liquid equilibrium, packed and spray column, conjugate curve and<br />
tie line data, plait-point, ternary liquid-liquid extraction, co-current, counter current and parallel current<br />
system, selection of solvent for extraction.<br />
(Lectures 08)<br />
Unit – III<br />
Leaching : Solid-liquid equilibrium, Equipment, principles of leaching, co-current and counter current<br />
systems and calculation of number of stage required.<br />
Unit – IV<br />
Humidification : General theory, psychometric chart, fundamental concepts in humidification and<br />
dehumidification, drybulb and wet bulb temperature, adiabatic saturation temperature, measurement of<br />
humidity calculation of humidification operation, cooling towers and related equipments.<br />
(Lectures 08)<br />
Unit – V<br />
Crystallization : Supersaturation, methods to achieve supersaturation, Factors governing nucleation and<br />
crystal growth rates, controlled-growth of crystals, super saturation curve, principle and design of batch<br />
and continuous type crystallizers, Inverted soliability, fractional crystallization.<br />
(Lectures 08)<br />
Text Books:<br />
1. Treybal, R.E; “Mass Transfer Operation”, McGraw-Hill,1980.<br />
2. King, C.J. “Separation Process”, McGraw-Hill, NY.<br />
3. Smith, B.D., “Design of Equilibrium stage Processes”, McGraw-Hill, NY.<br />
References Books:<br />
1. McCabe, W.L., Smith, J.C. and Harriot, P., “Unit Operation of <strong>Chemical</strong> <strong>Engineering</strong>”, 6th<br />
ed, McGraw-Hill, NY.<br />
2. Coulson, J.M. and Richardson, J.F., “<strong>Chemical</strong> <strong>Engineering</strong>”, Vol. I and II, Asian Books<br />
Pvt., New Delhi.<br />
Page 56
Course Code: ECH-603<br />
Semester-VI<br />
PETROLEUM REFINING<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Introduction: World Petroleum resources, petroleum industry in India, origin, exploration, drilling,<br />
composition and classification of petroleum crude, ASTM, TBP and FEV and production of petroleum<br />
crude, transportation and pretreatment of crude oil. (Lectures 08)<br />
Unit – II<br />
Distillation of crude oil Atmospheric and Vacuum distillation. Properties and specification of petroleum<br />
products-LPG, Gasoline, naphtha, kerosene, diesel oil, lubricating oil, wax etc Testing and uses of<br />
petroleum products. Safety and pollution considerations in refineries. (Lectures 08)<br />
Unit – III<br />
Conversion process: Thermal and catalytic in vapor, liquid and mixed phases, Hydro cracking, Thermal<br />
reforming, Polyforming and plat forming, Catalytic reforming. (Lectures 08)<br />
Unit – IV<br />
Conversion of petroleum gases into motor fuel with reference to Alkylation, Polymerization,<br />
Isomerisation, Hydrogenation, Production of aviation gasoline, motor fuel, kerosene, diesel oil and jet<br />
fuel. (Lectures 08)<br />
Unit – V<br />
Vacuum distillation: Design and operation of topping and vacuum distillation units. Tube still furnaces<br />
solvent extraction, uses of lubricating oils & waxes, <strong>Chemical</strong> & clay treatment of petroleum products,<br />
Desulphurization. (Lectures 08)<br />
Text Books:<br />
1. Nelson, W.L., “Petroleum Refinery <strong>Engineering</strong>,” 4th Ed., McGraw Hill,<br />
1987<br />
2. Garry, J.H. and Handwrek, G.E. “Petroleum Refining, Technology and Economics” 2nd Ed.,<br />
Marcel-Dekker<br />
3. Prasad, R., “Petroleum Refining Technology” Khanna Publishers, Delhi, 2000<br />
4. Kobe, K.A., and Mcketta, J.J. “Advances in Petroleum Chemistry and Refining”, Wiley<br />
Interscience<br />
Reference Books:<br />
1. Gruse, W.A. and Steven, D.R. “<strong>Chemical</strong> Technology of Petreleum” McGraw Hill<br />
2. Rao, M.G. and sitting, M. “Dryden’s Outlines of <strong>Chemical</strong> Technology”, East West Press,<br />
1997<br />
Page 57
Course Code: ECH-604<br />
Semester-VI<br />
BIOCHEMICAL TECHNOLOGY<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Biochemical : Introduction, Biochemical <strong>Engineering</strong>, Biological Process, Definition of Fermentation,<br />
Overview of industrial bioprocesses with emphasis on new material.<br />
(Lectures 08)<br />
Unit – II<br />
Enzyme Kinetics: Introduction, Simple Enzyme Kinetics, Evaluation of Kinetic Parameters, Enzyme<br />
Reactor with Simple Kinetics, Inhibition of Enzyme Reactions, Influences on Enzyme Activity, Industrial<br />
Applications of Enzymes.<br />
(Lectures 08)<br />
Unit – III<br />
Downstream Processing, Solid-Liquid Separation, Cell Rupture, Recovery, Purification, Sterilization,<br />
Sterilization Methods, Batch Sterilization, Air Sterilization, Continuous Sterilization, Design Criterion.<br />
(Lectures 08)<br />
Unit – IV<br />
Sulfa drugs, antibiotic and vitamins-introduction, use- vitamins C, vitamins K. Side effect of sulfa drugs<br />
antibiotic and vitamins. (Lectures 08)<br />
Unit – V<br />
Pharmaceutical products- introduction, preparation, uses, environmental impact Effect of Pharmaceutical<br />
products on human health. (Lectures 08)<br />
Text Books:<br />
1. Atkinson, B. andMavituna, F., “Biochemical <strong>Engineering</strong> and Biotechnology<br />
Handbook,” Nature Press, Macmillan, 1983<br />
2. Glazer, A.N. and Nikaido, H., “Microbial Biotechnology: Fundamentals of Applied<br />
Microbiology,” WH Freeman & Co., New York, 1995<br />
References Books:<br />
1.Reed, G. (Ed.), “Prescott & Dunn’s Industrial Microbiology” 4th Ed., CBS Publishers &<br />
Distributors, New Delhi, 1999.<br />
Semester VI<br />
Page 58
Technical Writing<br />
Course code: EHM601 L T P C<br />
2 0 2 3<br />
Course Contents:<br />
Unit I<br />
Forms of Technical Communication: Report writing, Definition and characteristics, Steps towards<br />
report writing, Structure, style of Report writing, Types & forms of Reports, Presentation of Reports,<br />
importance of Report writing.<br />
Unit II<br />
Technical Paper writing: Definition and purpose, essentials of a good technical paper/Article,<br />
Scientific Article writing, Difference between Technical paper/Article and scientific article,<br />
elements/steps in writing Technical paper & Scientific Article, Methods of writing technical paper &<br />
Scientific article.<br />
Unit III<br />
Technical Proposal: Definition and meaning of Technical Proposal, Significance of Proposal, Kinds,<br />
Types of proposal, Characteristics of a good Proposal, Structure, Parts, Format of Proposal,<br />
Supplementary parts, Uses of Proposals.<br />
Unit IV<br />
Writing Skills: Reporting events, Writing News paper, Reports, Essentials of essay writing –writing an<br />
essay of about 300 words on a given topic. Bio-Data Making, Writing of CV & Resumes, Difference<br />
between CV and Resume, Writing Job application etc.<br />
Unit V<br />
Value-based Text Reading: R.K. Narayan- A Bookish Topic.<br />
1. Francis Bacon- of studies.<br />
2. CEM Joad – The Civilization of Today.<br />
(Note: The two periods per week may be utilized in Language Lab covering the above syllabus.)<br />
Text Books:<br />
1. Singh R.P., An Anthology of English Easy O.U.P. New Delhi.<br />
2. Raman Meenakshi & Sharma Sangeeta, Technical Communication-Principles & Practice O.U.P.<br />
New Delhi. 2007.<br />
Reference Books:<br />
1. Monippally Matthukutty M., Business Communication Strategies Tata- Mc Graw Hill Publications<br />
Company, New Delhi.<br />
2. Mohan K. & Sharma R.C., Business Correspondence of Report Writing,TMH, New Delhi.<br />
Semester VI<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 59
Industrial Psychology<br />
Course code: EHM602 L T P C<br />
3 0 0 3<br />
Unit I<br />
Sociology in the industrial Perspective: Concept of Sociology, Sociology as a Science, Sociology of<br />
work & industry, Perspectives for sociological analysis of work, Class- Conflict in Industry, Social<br />
impact of industrialization, Corporate skills in the fast growing multinational set up.<br />
(Lectures 08)<br />
Unit II<br />
Work and Social change: Nature of modern societies, emergence of industrial capitalism, Technology &<br />
Social change, the information society after the industrial society, post-modernity, globalization &<br />
Convergence, Significance of the service sector today, work restructuring and corporate management.<br />
(Lectures 08)<br />
Unit III<br />
Work experience in Industry: The concept of alienation, Work satisfaction, Technology & work<br />
experience, and Social background of workers, Work orientations, Stress & anxiety of the worker, Work<br />
& Leisure, Unemployment, Conflicts in the work place. (Lectures 08)<br />
Unit IV<br />
General and Applied Ethics- Ethics and the professions – Standard of right and wrong, problems of<br />
Ethical Certainty, Significance of professional Ethics for Engineers, New Technology and Ethics,<br />
Applied Ethics - Cases in professional <strong>Engineering</strong> Practice, Principles of business ethics, Individual in<br />
the organization. (Lectures 08)<br />
Unit V<br />
Ethical Leadership: Decision making, corporate culture and reputation management, corporate social<br />
responsibility and social reporting. (Lectures 08)<br />
Text Books:<br />
1. Sheth N.R., Social Frame Work of Indian Factory, O.U.P. Bombay.<br />
2. Gisbert P., Fundamentals of Industrial Sociology, O.U.P. New Delhi.<br />
3. Watson Tony J., Sociology: Work & Industry, New York. Routledge.<br />
4. Schinzinger, Roland & Mike W. Martin, Introduction to <strong>Engineering</strong> Ethics- Boston, McGraw<br />
Hill.<br />
Reference Books:<br />
1. Fleddermann Charles, <strong>Engineering</strong> Ethics, Upper Saddle River- N.J. Prentice Hall.<br />
2. Miller & Form, Industrial Sociology, London Harper & Row.<br />
3. Parsons Richard D., The Ethics of Professional Practice- Allyn & Bacon, London.<br />
4. Govindarajan - <strong>Engineering</strong> Ethics- Prentice Hall (India) New Delhi.<br />
Bhatia S.K. - Business Ethics & Management Values- Deep & Deep Publication. N. Delhi<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 60
Course Code: ECH-651<br />
Semester-VI<br />
CHEMICAL REACTION ENGINEERING-I (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
1. To determine the relative rates of reaction of iodide ion with hydrogen peroxide at room temperature<br />
using different concentrations of the iodide ion.<br />
2. To separate Organic Compounds by Paper Chromatography.<br />
3. To study the effect of temperature, concentration of the reactants and a catalyst on the rate of chemical<br />
reaction.<br />
4. To study the activity results or oxidation-reduction replacement reaction.<br />
5. To purify water by ion -exchange.<br />
6. To determine the order and rate constant of esterification reaction at room temperature.<br />
7. To determine the order and rate constant of saponification reaction at room temperature.<br />
8. To study the residence time distribution (R.T.D.) in a stirred tank reactor.<br />
9. To study the residence time distribution (R.T.D.) in a plug flow reactor.<br />
10. To study the decomposition of calcium carbonate<br />
11. To determine the energy of activation of a given chemical reaction.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
Semester-VI<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 61
Course Code: ECH-652<br />
MASS TRASNFER-II (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
1. To determine the ternary liquid equillibria (Binodal curve).<br />
2. To study the liquid-liquid equilibria.<br />
3. To determine the limiting flow rates in spray tower.<br />
4. To determine the hydrodynamics of perforated plate tower.<br />
5. To determine the volumetric mass transfer coefficients in perforated plate tower.<br />
6. To determine the dynamics of liquid drops (Single drop extraction tower).<br />
7. To studies of axial mixing characteristics in a packed bed.<br />
8. To determine the gas-liquid mass transfer in packed tower.<br />
9. To determine the drying characteristics of a given material.<br />
10. To determine the Mass balance and Energy balance in Feed forward and Feed backward Evaporator.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
Semester-VI<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 62
CHEMICAL PLANT SAFETY & OCCUPATIONAL HAZARD (ELECTIVE)<br />
Course Code: ECH-605<br />
Unit-I<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
INDUSTRIAL SAFETY<br />
<strong>Chemical</strong> process Industries - First degree and second-degree hazards. Lines of defense-first, second and<br />
third line defense-chemical and physical job safety analysis-high pressure - high temperature operationdangerous<br />
and toxic chemicals-highly radio active materials-Safe handling and operation of materials and<br />
machineriesplanning layout-safety slogans. (Lectures 08)<br />
Unit-II<br />
SAFETY PROGRAMS IN INDUSTRIES<br />
Effective steps to implement safety procedures-Periodic Advice and checking to follow safety procedures<br />
and rules-proper selection and replacement of handling equipment-personnel safety and protective<br />
equipment. (Lectures 08)<br />
Unit-III<br />
ACCIDENTS<br />
Industrial accident costs-Identification of accident spots, Remedial measures, Identification and analysis<br />
of causes of injury to men and machineries- Accident prevention -accident proneness-vocational<br />
guidance, fire prevention and fire protection. (Lectures 08)<br />
Unit-IV<br />
HEALTH HAZARD Hazard identification and Assessment-involvement of human factors and errorsoccupational<br />
and industrial health hazards. (Lectures 08)<br />
Unit-V<br />
Role of Government, Safety Organization, Management and trade unions in promoting industrial safety-<br />
On-site and Off-site safety provisions. (Lectures 08)<br />
Text Book:<br />
1. Krishnan, Safety Management in Industry, Jaico Publishers, New Delhi, 1997<br />
2. Fawcett H.H. and Wood W.S., Safety and Accident Prevention in <strong>Chemical</strong> Operations, John<br />
Wiley & sons, U.S.A.,1965<br />
3. Anton, Occupational Safety and Health Management, McGraw Hill Book Co., New York, 1998<br />
References Books:<br />
1. William, Industrial Safety Handbook, McGraw Hill, 2001<br />
Page 63
Course Code: ECH-606<br />
Semester-VI<br />
FERTILISER TECHNOLOGY (ELECTIVE)<br />
Unit – I<br />
Introduction: Plant nutrients, different types of fertilizers and their production in India.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
(Lectures 08)<br />
Unit – II<br />
Nitrogenous Fertilizers: Different feed stocks, synthesis gas production by steamnaptha reforming and<br />
gas purification. Ammonia synthesis, Urea manufacturing processes. Manufacture of sulphuric acid and<br />
ammonium sulphate. Nitric acid and ammonium nitrate manufacture.<br />
(Lectures 08)<br />
Unit – III<br />
Phosphatic Fertilizers : Availability and grinding of rock phosphate, manufacturing processes for single<br />
and triple super-phosphate and phosphoric acid. (Lectures 08)<br />
Unit – IV<br />
Mixed fertilizers: Availability and manufacture of muriate of potash.<br />
Mixed Fertilizers: Mono and di-ammonium phosphate, ure ammonium phosphates, NPK complex<br />
fertilizers, granulation techniques. (Lectures 08)<br />
Unit – V<br />
<strong>Engineering</strong> Problems: Fertilizers Storage and handling. Corrosion problems in fertilizers industries.<br />
Fertilizer plant effluent treatment and disposal. (Lectures 08)<br />
Text Books:<br />
1. Slack A.V. “Chemistry and Technology of Fertilizers”, Wiley linter science Publishers.<br />
2. Waggaman W.H., “Phosphoric Acid, Phosphates and Phosphatic Fertilizers”<br />
Hafner Pub.<br />
3. Austin G.T., “Shreve’s <strong>Chemical</strong> Processes Industries”, 5th Ed. McGraw Hill.<br />
Reference Books:<br />
1.Rao M.G. and Sittig M., “Dryden’s Outlines of <strong>Chemical</strong> Technology”,<br />
Affiliated East West Press, Delhi.<br />
Page 64
Course Code: ECH-607<br />
Semester-VI<br />
RUBBER SCIENCE AND TECHNOLOGY (ELECTIVE)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Rubber Science : Classification of polymers – Thermoplastic, elastomers (rubber), thermosets,<br />
Description of elastomers- rubber vulcanizates, classification of rubbers, glass rubber transition behavior,<br />
Rubber physics-elastic behaviour. (Lectures 08)<br />
Unit – II<br />
Rubber Rheology: Flow behaviour of unvulcanized rubber compounds, measurement of plasticity,<br />
viscoelasticity and relaxation properties, Rheological models. (Lectures 08)<br />
Unit – III<br />
Natural Rubber : Hevea Brasiliensis, Preservation and concentration of NR latex, Comparison of<br />
natural rubber and synthesis CIS 1,4 polyisoprene, Special features and uses of natural rubber<br />
Synthetic Rubber: Polymerization methods, addition polymerization and condensation polymerization.<br />
(Lectures 08)<br />
Unit – IV<br />
Rubber Compounding : Introduction to rubber compounding bulcanization and its effects, vulcanization<br />
systems, vulcanizate physical properties and their significance, properties desired for different rubber<br />
compounds, compounding ingredients and formulations.<br />
(Lectures 08)<br />
Unit – V<br />
Rubber Processing : Mixing, extrusion, and molding techniques.<br />
Manufacture of Rubber Products : Pneumatic tyres, lates products, rubber footwear and rubber<br />
moulded products<br />
Rubber Characterization : Rubber Compound analysis and identification of rubber.Behavior in service.<br />
(Lectures 08)<br />
Text Book:<br />
1. Blow, C.M. and Hepburn, “Rubber Technology and Manufacture” 2nd ed.<br />
Butterworth, London, 1982.<br />
2. Evans, C.M. “Practical Rubber Compounding and processing” Elsevier<br />
Applied Science Publisher, 1981.<br />
Reference Books:<br />
1. “Rubber <strong>Engineering</strong>” by Indian Rubber Institute published by Tata McGraw-<br />
Hill, 1998<br />
Page 65
Course Code: ECH-701<br />
Semester-VII<br />
CHEMICAL REACTION ENGINEERING – II<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 2 0 3<br />
Unit – I<br />
Catalysts : Description, method of preparation and manufacture; catalyst characterization – BET surface<br />
area, pore volume, pore size distribution.<br />
Catalyst Reaction Kinetic Models : Physical and chemical absorption; determination of rate expressions<br />
using absorption, surface reaction and desorption as rate-controlling steps. (Lectures 08)<br />
Unit – II<br />
Determination of Global Rate of Reaction : Heterogeneous laboratory reactors; Determination of rate<br />
expressions from experimental data. (Lectures 08)<br />
Unit – III<br />
Effect of Intrapellet Diffusion on Reaction Rates in Isothermal Pellets : Concept of effectiveness<br />
factor, Thiele modulus, experimental determination of effectiveness factor- wesiz-Prater criteria, Non-<br />
Isothermal effectiveness factor; Prater number, maximum temperature rise in a pellet, multiple steady<br />
states in heterogeneous reactors. (Lectures 08)<br />
Unit – IV<br />
Non-catalytic Gas-Solid Reactions : Progressive conversion model, Shrinking core model; various<br />
controlling regimes, design of gas-solid reactors.<br />
(Lectures 08)<br />
Unit – V<br />
Gas-Liquid Reactions : Effect of diffusion on rate of reaction, enhancement factor.<br />
Introduction to Design of Heterogeneous Reactors : One dimensional model for fixed-bed reactors,<br />
parametric sensitivity; design of fluidized bed reactors.<br />
(Lectures 08)<br />
Text Book:<br />
1. Levenspiel, O., “<strong>Chemical</strong> Reaction <strong>Engineering</strong>” 3rd Ed., John Wiley, 1999.<br />
2. Smith, J.M., “<strong>Chemical</strong> <strong>Engineering</strong> Kinetics” 3rd Ed., Mc Graw-Hill, 1981.<br />
3. Fogler, H.S., “Elements of <strong>Chemical</strong> Reaction <strong>Engineering</strong>” 3rd Ed.,<br />
Prentice-Hall of India, Delhi, 2003.<br />
4. Carberry, J.J., “Catalytic Reaction <strong>Engineering</strong>” Mc Graw-Hill, 1976.<br />
Reference Books:<br />
1. Dawande, S.D., “Principles of Reaction <strong>Engineering</strong>” Central Techno Pub.,<br />
Nagpur, 2001.<br />
6. Levenspiel, O., “The <strong>Chemical</strong> Reactor Omnibook” OSU Bookstores,<br />
Corvallis Oregon, 1996.<br />
Page 66
Course Code: ECH-702<br />
Semester-VII<br />
INTRODUCTION TO OIL/FAT TECHNOLOGY<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 2 0 3<br />
Unit – I<br />
Fats and Oils: An Overview, Properties of Fats and Oils, Sources of Fats and Oils, Characteristics of<br />
Oilseed, Oils and fats Oil Milling and Solvent Extraction, Nutritional and Health Aspects of Dietary<br />
Lipids, Oil Trading. (Lectures 08)<br />
Unit – II<br />
Fats and Oils Processing, Recovery of Fats and Oils from Plant and Animal Sources, Refining of Fats and<br />
Oils, Bleaching, Hydrogenation, Fractionation, Processes and Products of Interesterification,<br />
Deodorization Specialty Fats and Oils. (Lectures 08)<br />
Unit – III<br />
Packaging and Bulk Handling of Edible Fats and Oils, , Regulatory Considerations for Oilseed<br />
Processors and Oil Refiners, Economics of Fats and Oils Plants, Flavor Quality of Fats and Oils, Oil<br />
Quality Improvement through Processing.<br />
(Lectures 08)<br />
Unit – IV<br />
Managing Oil Quality, Utilization of Fats and Oils, Shortening Technology, Margarine Types and<br />
Preparation Technology, Oil and Fats Derivatives, Liquid Oils Technology.<br />
(Lectures 08)<br />
Unit – V<br />
Environmental Considerations in Fats and Oils Technologies, Design and Application of Fat-Based<br />
Surfactants, By-Product Utilization, Strategies for Replacement of Fat in Food Products, Genetically<br />
Engineered and Identity Preserved Oils, Health and Nutrition. (Lectures 08)<br />
Text Books:<br />
1. Swern, D. (ed.) “Bailey’s Industrial Oil and Fat Products,” 4th Ed. John Wiley and Sons, NY 1982<br />
2. Hilditch, T.P., “The Industrial Chemistry of Fats and Waxes,” 3rd ed. Bailliere,<br />
Tindall and Cox, London, 1949<br />
References Books:<br />
1. Patterson, H.B.W. “Handling and storage of Oilseeds, Oils Fats and Meat”<br />
Elsevier Applied Science, Landon 1989<br />
2. O'Brien, Richard D.; Farr, Walter E.; Wan, Peter J. ‘Introduction to Fats and Oils Technology (2nd<br />
Edition)’ AOCS Press, New Delhi.<br />
Page 67
Course Code: ECH-703<br />
Semester-VII<br />
BIOPROCESS ENGINEERING<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Introduction to Bioprocesses<br />
Historical development of bioprocess technology, an overview of traditional and modern applications of<br />
biotechnology industry, outline of an integrated bioprocess and the various (upstream and down stream)<br />
unit operations involved in bioprocess, generalized process flow sheets.<br />
(Lectures 08)<br />
Unit – II<br />
Fermentation Process-I : General requirements of fermentation processes, Basic design and<br />
construction of fermentor and ancillaries, Main parameters to be monitored and controlled in<br />
fermentation process;<br />
Fermentation Process-II : An overview of aerobic and anaerobic fermentation processes and their<br />
application in the biotechnology industry, solid-substrate, slurry fermentation and its applications, whole<br />
cell immobilization, behaviour of microbes in different reactors (air lift, fluidized, batch, continuous fed<br />
batch condition). (Lectures 08)<br />
Unit – III<br />
Media Design : Medium requirements for fermentation process, Carbon, nitrogen, minerals, vitamins<br />
and other complex nutrients, oxygen requirements, medium formulation for optimal growth and product<br />
formation, examples of simple and complex media, design and usage of various commercial media for<br />
industrial fermentations.<br />
Sterilization : Thermal death kinetics of microorganisms, batch and continuous heat. Sterilization of<br />
liquid media, filter sterilization of liquid media, Air, Design of sterilization equipment.<br />
(Lectures 08)<br />
Unit – IV<br />
Metabolic Stoichiometry : Stoichiometry of Cell growth and product formation, elemental balances,<br />
degrees of reduction of substrate and biomass, available electron balances, yield coefficients of biomass<br />
and product formation, maintenance coefficients.<br />
Energetics : Energetic analysis of microbial growth and product formation, oxygen consumption and<br />
heat evolution in aerobic cultures thermodynamic efficiency of growth.<br />
(Lectures 08)<br />
Unit – V<br />
Kinetics of Microbial Growth and Product Formation : Phases of cell growth in batch cultures.<br />
Simple unstructured kinetic models for microbial growth, Monod Model, Growth of Filamentous<br />
organisms, Growth associated (Primary) and non growth associated (secondary) product formation<br />
Kinteics. Leudeking-Piret models, substrate and product inhibition on cell growth and product formation,<br />
introduction to Structured Models for growth and product formation.<br />
(Lectures 08)<br />
Text Books:<br />
1. Biochemical <strong>Engineering</strong> Fundamentals Balley and Ollis, McGraw Hill (2nd<br />
Ed.), 1986.<br />
2. Bioprocess <strong>Engineering</strong>, Shule and Kargi, Prentice Hall, 1992.<br />
References Books:<br />
1. Stanbury, P.F., Whitaker, A., & Hall, S.J., (1998), Principles of fermentation Technology,<br />
2nd ed., Elsevier Science Publishers, BV, Amsterdam.<br />
Page 68
Course Code: ECH-704<br />
Semester-VII<br />
SUGAR TECHNOLOGY<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Sugar Industry and sugar scenario in India and world. Raw materials such as Sugar cane and beet root<br />
and their availability. Raw materials and their preparation, continuous operations, cane processing,<br />
weighment, chopping, grading crushing, milling and imbibition. Seeparation of bagase and bagacillo.<br />
(Lectures 08)<br />
Unit – II<br />
Juice purification – screening filtration, chemical treatment, sulfitation, carbonization, precipitation and<br />
clarification. Working of filter press, vacuum filtration and dorrclarifier settler.<br />
(Lectures 08)<br />
Unit – III<br />
Concentration of clarified juice in multi effect evaporation, triple and quadruple effect, and capacity,<br />
stream economy, Co-current and countercurrent flow of juice in the evaporators.<br />
(Lectures 08)<br />
Unit – IV<br />
Operations of vacuum pan. Theory of sugar crystallization, strike- pans sugar crystallizers. Crystal<br />
drying, screening and grading. (Lectures 08)<br />
Unit – V<br />
Sugar Industry bye products – bagasse, press mud, molasses; mud wax captive power and their<br />
utilization. (Lectures 08)<br />
Text Books:<br />
1. Birch and Parket, “Sugar Sciences and Technology” App. Sci Pub.<br />
2. Hong. P. “Principles of Sugar Technology” 3rd ed., Elsevier New York<br />
3. Gopal Rao and Marshal Sitting, “Dryden Outlines of <strong>Chemical</strong> Technology,” East-West<br />
Press, 3rd ed., New Delhi 1977<br />
Reference Books:<br />
1. Austin, G.T., “Shreve’s <strong>Chemical</strong> Process Industries,” 5th Ed. McGraw Hill Book Co. Singapore.<br />
Page 69
Course Code: ECH-751<br />
1. Preparation of Aspirin.<br />
2. Preparation of Benzanilide.<br />
3. Preparation of m-dinitrobenzene.<br />
4. Preparation of Benzoic acid.<br />
5. Preparation of Phthalimide.<br />
6. Preparation of Methyl Orange.<br />
7. Preparation of Parabenzoquinone.<br />
8. Preparation of nerolin.<br />
9. Detection of Extra elements.<br />
10. Analysis of Compound -1<br />
11. Analysis of Compound -2<br />
12. Analysis of Compound -3<br />
13. Analysis of Compound -4<br />
14. Analysis of Compound -5<br />
15. Analysis of Compound -6<br />
Evaluation of Practical Examination:<br />
Semester VII<br />
CHEMICAL REACTION ENGINEERING-II (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 70
Course Code: ECH-752<br />
Semester VII<br />
INTRODUCTION TO OIL/FAT TECHNOLOGY (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
a) Determine various properties of fuels (diesel, petrol and kerosene) by measuring:<br />
Flash point and fire point, carbon residue, viscosity test, ASTM distillation, corrosion test (copper strip<br />
and silver strip), Annealing point, specific gravity, pore point and cloud pont.<br />
b) Analysis of oilseeds and oil bearing materials for following:<br />
Moisture content, oil content, protein content, fiber content, ash content etc.<br />
c) Determination of physical characteristics of oils and fats derived from oilseeds and cake:<br />
Refractive index, color, specific gravity, titre, melting point, gel test, cloud point, carbon residue,<br />
viscosity test.<br />
d) Determination of chemical characteristics of oils and fats derived from oilseeds and cake: Acid<br />
value, saponification value, Iodine value, hydroxyl value, Acetyl value, peroxide value, Anisidine<br />
value, R.M., P and K value, Diene value, thicocynagen value etc.<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 71
Course Code: ECH-705<br />
Semester-VII<br />
PROCESS EQUIPMENT DESIGN (ELECTIVE)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Heat Exchangers: Auxiliary calculations; Review of Kern method; Bell’s method and HTRI method of<br />
Shell-and-tube heat exchanger design; Plate heat exchanger design; finned tube heat exchanger;<br />
Optimization of shell-and-tube exchanger. (Lectures 08)<br />
Unit – II<br />
Reboliers: Design of Kettle and thermosyphon reboilers.<br />
Evaporators : Sizing of drum; central core pipe size and number of tubes for short and long tube<br />
evaporators. (Lectures 08)<br />
Unit – III<br />
Agitated Vessels: Design of mixing vessels, gas-spraying systems; impellers, propellers, anchors and<br />
helical ribbon-type agitators. (Lectures 08)<br />
Unit – IV<br />
Gas Liquid Contact Systems: Distillation column, Absorption tower, tray hydraulics of sieve and valve<br />
trays; Design of packed bed columns. (Lectures 08)<br />
Unit – V<br />
Design of Reactors: CSTR, Batch and packed bed. (Lectures 08)<br />
Text Books:<br />
1. Sinnott, R.K., “Coulson and Richardson’s <strong>Chemical</strong> <strong>Engineering</strong>” Vol. 6, 3rd<br />
Ed., Butterworth Heinmann, New Delhi, 2002.<br />
2. Kern, D.Q., “Process Heat Transfer” McGraw-Hill, 1950.<br />
3. Evans, F.I., “Equipment Design Handbook” 2nd Ed., Vol.2, Gulf Publishing, 1980.<br />
Reference Books:<br />
1. Smith,B.D., “Design of Equilibrium Stage Process” Mc Graw-Hill, 1963.<br />
2.. Dawande, S.D., “Process Design of Equipments,” 2nd Ed., Central Techno Publications,<br />
Nagpur, 2000.<br />
Page 72
Course Code: ECH-706<br />
Semester-VII<br />
AIR POLLUTION AND CONTROL EQUIPMENTS (ELECTIVE)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit I<br />
Air Pollutant Sources, Effects and Clean Air Acts: Pollution of air: Sources and effects of air pollutants<br />
on physical environment and living systems, Monitoring of air pollution, Air pollution Laws and national<br />
standards. (Lectures 08)<br />
Unit II<br />
Air Pollutant Formation, Dipersion, Analysis: Formation of pollutants through large-scale combustion of<br />
fossil fuels, mineral processing, automobiles in urban areas and at source minimisation of release -<br />
Meteorological aspects of air pollutant dispersion. <strong>Chemical</strong> reactions in a contaminated atmosphere,<br />
urban air pollution, acid rain, Air sampling and measurement, Analysis of air pollutants.<br />
(Lectures 08)<br />
Unit III<br />
Air Pollution Control Methods for Particulates Removal: Control Methods – Source Correction methods -<br />
Particulate emission control: Dry techniques: Design of industrial dust collectors, gravity settling<br />
chambers, cyclone and multiclone separators, fabric & Fibrous filters, electrostatic precipitators, relative<br />
merits and demerits, overall selection of gas cleaning equipment, economics. Wet techniques: Design of<br />
wet dust collection, wet cyclone, empty scrubber, column (packed) scrubber, ventury scrubber,<br />
suitability, merits and demerits, economics. (Lectures 08)<br />
Unit IV<br />
Control of Specific Gaseous Pollutants: Cleaning of Gaseous effluents - Control of sulphur dioxide<br />
emission by various methods - Control of nitrogen oxides in combustion products - Control of release of<br />
carbon monoxide and hydrocarbons to the atmosphere; Case studies: Role of APC techniques in coal<br />
fired thermal power plants,cement plant and petroleum refinery. (Lectures 08)<br />
Unit V<br />
Noise Pollution and Control: Sound pressure, Power and Intensity - Measures of Noise-Outdoor noise<br />
propagation- Indoor Noise propagation- Noise Control.<br />
(Lectures 08)<br />
Texts Books:<br />
1. B.G. Verma, H. Brauer," Air Pollution Control Equipments", Springer, Verlag Berlin, 1981<br />
2. M.N. Rao and H.V.N. Rao, "Air Pollution", Tata McGraw Hill, New Delhi, 1993<br />
3. Rao C .S. "Environmental Pollution Control <strong>Engineering</strong>,” 2nd Edition, New Age International<br />
Publishers, 2006<br />
References Books:<br />
1.A. P. Sincero and G.A. Sincero Environmental <strong>Engineering</strong>: A Design Approach, Prentice Hall of India<br />
Pvt Ltd, N.Delhi, 1996<br />
2. Air Pollution Control Equipment: Selection, Design, Operation and Maintenance, Louis Theodore<br />
(Editor), Anthony J. Buonicore (Editor), Springer-Verlag Telos, 1994.<br />
Page 73
Course Code: ECH-707<br />
Semester VII<br />
INDUSTRIAL POLLUTION CONTROL (ELECTIVE)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit-I<br />
INTRODUCTION Definition of pollutant, types of pollution; Air, Water, Land, noise- adverse effects of<br />
pollutants eco system and human health - need for effluent treatment and toxicity, control. Water<br />
standards for portable, agricultural and left-off streams- air standards for cities, industrial areas, resorts.<br />
(Lectures 08)<br />
Unit-II<br />
AIR POLLUTION CONTROL METHODS Particulate emission control- gravitational settling chambers-<br />
cyclone separators, fabric filters, electrostatic precipitators, wet scrubbers, absorbers. Control of sulphur<br />
di oxide, oxides of nitrogen, carbon monoxide and hydrocarbons. Noise pollution measurements and its<br />
control. (Lectures 08)<br />
Unit-III<br />
WASTE WATER Origin of waste water, types of water pollutants and their effects, waste water sampling<br />
and analysis, determination of organic and inorganic matters, physical characteristics, bacteriological<br />
measurements. (Lectures 08)<br />
Unit-IV<br />
BASIC PROCESS OF WATER TREATMENT Primary , secondary and tertiary treatments - advanced<br />
waste water treatments; recovery of metals from process effluents. (Lectures 08)<br />
Unit-V<br />
POLLUTION CONTROL ASPECTS IN TYPICAL CHEMICAL PROCESS INDUSTRIES Fertilizer,<br />
petroleum refinery, petrochemical, pulp and paper, tanning, sugar, distilleries, textile industries.<br />
Text Book:<br />
1. Rao C.S., Environmental Pollution Control <strong>Engineering</strong>, Wiley Eastern Limited, 1991<br />
(Lectures 08)<br />
Reference Book:<br />
1.Rose G.R.D., Air pollution and Industry, Van Nostrand Reinhold Co., New York 1972.<br />
2. Pandey G.N. and Carney G.C., Environmental <strong>Engineering</strong>, Tata McGraw Hill, New Delhi,1989<br />
3.Kapoor B.S., Environmental <strong>Engineering</strong>, 3rd Edn., Khanna publishers,1997<br />
4.Mahajan S.P., Pollution Control in Process Industries, 1st Edn., Tata McGraw Hill Publishing<br />
Company Ltd., New Delhi, 1995<br />
Page 74
Semester VII<br />
INDUSTRIAL TRAINING PRESENTATION<br />
(BASED ON INDUSTRIAL TRAINING DONE AFTER THE VI SEMESTER<br />
EXAMINATION IN SUMMER)<br />
Course Code: ECH-791<br />
L T P C<br />
0 0 0 3<br />
Students will have to undergo industrial training of six weeks in any industry or reputed organization<br />
after the VI semester examination in summer. The evaluation of this training shall be included in the VII<br />
semester evaluation.<br />
The student will be assigned a faculty guide who would be the supervisor of the student. The faculty<br />
would be identified before the end of the VI semester and shall be the nodal officer for coordination of<br />
the training.<br />
Students will prepare an exhaustive technical report of the training during the VII semester which will be<br />
duly signed by the officer under whom training was undertaken in the industry/ organization. The<br />
covering format shall be signed by the concerned office in-charge of the training in the industry. The<br />
officer-in-charge of the trainee would also give his rating of the student in the standard <strong>University</strong> format<br />
in a sealed envelope to the Director of the college.<br />
The student at the end of the VII semester will present his report about the training before a committee<br />
constituted by the Director of the College which would comprise of at least three members comprising of<br />
the Department Coordinator, Class Coordinator and a nominee of the Director. The students guide would<br />
be a special invitee to the presentation. The seminar session shall be an open house session. The internal<br />
marks would be the average of the marks given by each member of the committee separately in a sealed<br />
envelope to the Director.<br />
The marks by the external examiner would be based on the report submitted by the student which shall be<br />
evaluated by the external examiner and cross examination done of the student concerned.<br />
Not more than three students would form a group for such industrial training/ project submission.<br />
The marking shall be as follows.<br />
Internal: 50 Marks<br />
By the faculty guide - 25 marks<br />
By committee appointed by the director – 25 marks<br />
External: 50 Marks<br />
By officer-in-charge trainee in industry – 25 marks<br />
By external examiner appointed by the university – 25 marks<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 75
Semester VII<br />
PROJECT WORK PHASE- 1<br />
(Synopsis, Literature Survey & Presentation)<br />
Course Code: ECH-799 L T P C<br />
0 0 6 3<br />
A group of students, not more than three, will be assigned a faculty guide who would be the supervisor of<br />
the student. The faculty would be identified in the starting of the VII semester.<br />
The group will carry out the literature search and collect required material for carrying out the project.<br />
The group will prepare a report not exceeding 15 pages at the end of semester.<br />
The assessment of performance of students should be made at least twice in each semester i.e. VII and<br />
VIII. In this semester the student shall present the progress of project live as also using overheads project<br />
or power point presentation on LCD to the internal committee as also the external examiner.<br />
The evaluation committee shall consist of faculty members constituted by the college which would<br />
comprise of at-least three members comprising of the Department Coordinator, Class Coordinator and a<br />
nominee of the Director. The students guide would be a special invitee to the presentation. The seminar<br />
session shall be an open house session. The internal marks would be the average of the marks given by<br />
each member of the committee separately in a sealed envelope to the Director.<br />
The marking shall be as follows.<br />
Internal: 100 Marks<br />
By The Faculty Guide - 50 Marks<br />
By Committee Appointed By the Director – 50 Marks<br />
Semester VIII<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 76
Course Code: ECH-801<br />
POLYMER SCIENCE AND TECHNOLOGY<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Chemistry of Polymerization Reactions : Functionality, polymerization reactions, polycondensation,<br />
addition free radical and chain polymerization. Copolymerization, block and graft polymerizations,<br />
stereospecific polymerization. (Lectures 08)<br />
Unit – II<br />
Polymerization Kinetics : Kinetics of radical, chain and ionic polymerization and copolymerization<br />
systems. (Lectures 08)<br />
Unit – III<br />
Molecular Weight Estimation : Average molecular weight: number average and weight average.<br />
Theoretical distributions, methods for the estimation of molecular weight. (Lectures 08)<br />
Unit – IV<br />
Polymerization Processes : Bulk, solution, emulsion and suspension polymerization. Thermoplastic<br />
composites, fibre reinforcement fillers, surface treatment reinforced thermoset composites – Resins,<br />
Fibres, additives, fabrication methods. (Lectures 08)<br />
Unit – V<br />
Rheology : Simple Rheological response, simple linear viscoelastic models – Maxwell,, Voigt, material<br />
response time, temperature dependence of viscosity, Rheological studies. (Lectures 08)<br />
Text Books:<br />
1. Rodringuez, “Principles of Polymer Systems”, Tata McGraw Hill, 1960<br />
2. Billmayer Jr. and Fred. W., “Textbook of Polymer Science”, Wiley Tappers, 1965<br />
3. David, J.W., “Polymer Science and <strong>Engineering</strong>”, Prentice Hall, 1971<br />
4. Schmidt, A.K. and Marlies, G.A., “High Polymers – Theory and Practice”, McGraw<br />
Hill, 1948.<br />
Reference Book:<br />
1. McKelvey, J.M., “Polymer Processing, “John Wiley, 1962<br />
2. Manoriffs, R.W., “Man-made Fibres,” Wiley Inter Science.<br />
Semester VIII<br />
Page 77
Course Code: ECH-802<br />
PULP AND PAPER TECHNOLOGY<br />
Unit – I<br />
Introduction: Present status of pulp industries: Fivrous raw materials, Fibre Chemistry.<br />
Raw Material Preparation: Debarking, chipping, chip screening, storage.<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
(Lectures 08)<br />
Unit – II<br />
Pulping : <strong>Chemical</strong>, semi chemical, mechanical, chemimechanical and nonconventional.<br />
Secondary fibre pulping. Advances and recent trends in pulping.<br />
Pulp Manufacture: Stock preparation, beating and refining, functional and control additives for<br />
papermaking, wet-end chemistry, polymer chemistry, retention sizing.<br />
(Lectures 08)<br />
Unit – III<br />
Bleaching : Objective of bleaching, bleachability measurement, bio-bleaching<br />
<strong>Chemical</strong> Recovery: Composition and properties of black liquor, oxidation and desilication,<br />
concentration of black liquor and its incineration, causticizing and clarification sludge washing and<br />
burning. (Lectures 08)<br />
Unit – IV<br />
Paper Manufacture: Approach flow system, wire part, sheet forming process, sheet transfer mechanism,<br />
press part, theory of pressing, dryer part, paper drying process, calendering, cylinder mould machine,<br />
finishing, fibre recovery systems, recent developments in paper making. Coating and lamination.<br />
(Lectures 08)<br />
Unit – V<br />
Paper Properties: Physical (Optical, strength and resistance) <strong>Chemical</strong> and electrical properties, paper<br />
defects<br />
Paper Grades: Types, composition, manufacturing techniques, properties and uses<br />
(Lectures 08)<br />
Text Books:<br />
1. Britt, K.W. (Ed.) “Handbook of Pulp and paper Technology” 2nd ed., CBS<br />
Publishers & Distributors, Delhi, 1984.<br />
2. Casey, J.P. “Pulp and paper Chemistry and <strong>Chemical</strong> Technology” Vol.1, 3rd ed. Wiley<br />
Interscience.<br />
3. Rydholm. S.A. “Pulping Processes” Wiley Interscience.<br />
4. Libby, C.E. “Pulp and paper Science and Technology” Vol.1, McGraw-Hill.<br />
5. Clark, JDA, “Pulp Technology and Treatment for Paper” 2nd ed. Miller Freeman.<br />
Reference Books:<br />
1. McDonald, R.G., “Pulp and Paper Manufacture,” Vol.1, 2nd ed. McGraw-Hill.<br />
2. Biermann, C.J. “Essentials of Pulpingand Paper Making,” Academic Press.<br />
3. Saltman, D., “Paper Basics” Van Nostrand, 1978.<br />
Semester VIII<br />
Page 78
Course Code: ECH-851<br />
POLYMER SCIENCE & TECHNOLOGY (LAB)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
0 0 4 2<br />
a) Identification of following polymers<br />
Polyethylene, Polypropylene, Polystyrene, Polyamide, Polyvinyl chloride, PMMA, PE, UF, MF<br />
Analysis of following polymers PVA, Alkyd resin, PVAc, Epoxy resin<br />
b) Synthesis of following polymers (at least five)<br />
1. Polyvinyl acetate by bulk polymerization, 2. Polyvinyl chloride by emulsion polymerization,<br />
3. Polystyrene by solution polymerization, 4.PMMA by Suspension polymerization, 5. Epoxy resin by<br />
condensation polymerization, 6. UF by condensation polymerization,7 PF by condensation<br />
polymerization, 8. MF by condensation polymerization<br />
c) Determine CAC and CMC of polymer-surfactant mixture by conductivity test using conductivity<br />
meter and surface tension test by using Tensiometer.<br />
d) Characterization (at least Five)<br />
1. Acid value, 2.Hydroxyl value, 3. Iodine value 5. Epoxy value and epoxy content, 6. Amine value,<br />
7. K-value, 8. Chlorine content<br />
Evaluation of Practical Examination:<br />
Internal Evaluation (50 marks)<br />
Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />
scale which would include the practical conducted by the students and a Viva taken by the faculty<br />
concerned. The marks shall be entered on the index sheet of the practical file.<br />
Evaluation scheme:<br />
PRACTICAL PERFORMANCE &<br />
VIVA DURING THE SEMESTER (30<br />
EXPERIMENT<br />
(10 MARKS)<br />
MARKS)<br />
FILE<br />
WORK<br />
(10<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
ATTENDANCE<br />
(5 MARKS)<br />
QUIZ<br />
(5<br />
MARKS)<br />
VIVA<br />
(10<br />
MARKS)<br />
TOTAL<br />
INTERNAL<br />
(50<br />
MARKS)<br />
External Evaluation (50 marks)<br />
The external evaluation would also be done by the external Examiner based on the experiment conducted<br />
during the examination.<br />
EXPERIMENT<br />
(20 MARKS)<br />
FILE WORK<br />
(10 MARKS)<br />
VIVA<br />
(20 MARKS)<br />
TOTAL<br />
EXTERNAL<br />
(50 MARKS)<br />
Page 79
Semester VIII<br />
PROJECT WORK PHASE-2<br />
(Report, Analysis, Implementation/Simulation and Presentation)<br />
Course Code: ECH-899 L T P C<br />
0 0 18 9<br />
Students should devote themselves to prepare something tangible, which could be a working model of<br />
their thoughts based on their subject of choice.<br />
The project shall be finalized by the students based on the VII semester project work report and shall be<br />
completed and submitted at least one month before the last teaching day of the VIII semester, date of<br />
which shall be notified in the academic calendar.<br />
The assessment of performance of students should be made at least twice in each semester i.e. VII and<br />
VIII. In this semester student shall present the final project live as also using overheads project or power<br />
point presentation on LCD to the internal committee as also the external examiner.<br />
The evaluation committee shall consist of faculty members constituted by the college which would<br />
comprise of at-least three members comprising of the Department Coordinator, Class Coordinator and a<br />
nominee of the Director. The students guide would be a special invitee to the presentation. The seminar<br />
session shall be an open house session. The internal marks would be the average of the marks given by<br />
each member of the committee separately in a sealed envelope to the Director.<br />
The marking shall be as follows.<br />
Internal: 50 Marks<br />
By The Faculty Guide - 25 Marks<br />
By Committee Appointed By the Director – 25 Marks<br />
External: 50 Marks<br />
By External Examiner Appointed By the <strong>University</strong> – 50 Marks<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
Page 80
Course Code: ECH-803<br />
Semester VIII<br />
INDUSTRIAL SAFETY & HAZARD MANAGEMENT (ELECTIVE)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit I<br />
Industrial safety, Industrial hygiene and safety aspects related to toxicity, noise, pressure, temperature,<br />
vibrations, radiation etc. Explosions including dust, vapor, cloud and mist explosion.<br />
(Lectures 08)<br />
Unit II<br />
Elements of safety, safety aspects related to site, plant layout, process development and design stages,<br />
identification of hazards and its estimation, risk, risk analysis and assessment methods; fault free method,<br />
event free method, scope of risk assessment, controlling toxic chemicals and flammable materials.<br />
(Lectures 08)<br />
Unit III<br />
Toxic substances and degree of toxicity, its estimation, their entry routes into human system, their doses<br />
and responses, control techniques for toxic substances exposure, use of respirators, ventilation systems<br />
(Lectures 08)<br />
Unit IV<br />
Prevention of losses, pressure relief, provision for fire fighting, release of hazardous materials from tanks,<br />
pipes through holes and cracks , relief systems : types and location of reliefs.<br />
(Lectures 08)<br />
Unit V<br />
Handling, transportation and storage of of flammable liquids, gases, and toxic materials and wastes,<br />
regulation and legislation, government role, risk management routines, emergency preparedness, disaster<br />
planning and management.<br />
(Lectures 08)<br />
Text Books:<br />
1. D. A. Crowl and J.F. Louvar – <strong>Chemical</strong> Process Safety (Fundamentals with Applications), Prentice<br />
Hall (1990)<br />
2. H.H. Fawcett and W.S. Wood – Safety and Accident prevention in <strong>Chemical</strong> Operations, 2 nd Edition,<br />
John Wiley &Sons,New York, 1982.<br />
3. Coulson & Richardson’s <strong>Chemical</strong> <strong>Engineering</strong> – Vol. 6 – R.K. Sinnott, Butterworth – Heinmann Ltd.,<br />
1996.<br />
Reference Books:<br />
1. Sanjoy Banerjee, Industrial Hazards & Plant Safety, Taylor & Francis Group<br />
Page 81
Course Code: ECH-804<br />
Semester VIII<br />
ENERGY MANAGEMENT (ELECTIVE)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit I<br />
Energy Scenario : Commercial & Non commercial energy, primary energy resources, commercial<br />
energy production, final energy consumption, energy need of growing economy, long term energy<br />
scenario, energy pricing, energy sector reform, energy & environment, energy conservation and its<br />
importance, re- structuring of the energy supply sector, energy strategy for future, energy conservation<br />
act. (Lectures 08)<br />
Unit II<br />
Energy Management & Energy Planing : Definition & significance, energy strategy, energy policy &<br />
energy planning, two sides of energy management, sectors of supply side energy management, objective<br />
of energy management, hierarchical levels of supply side energy management, trade off b/w energy<br />
management, energy strategies & energy planning, energy & economy, essential imperatives & steps in<br />
supply side energy planning, energy planning flow for supply side, essential data for supply side energy<br />
planing, infrastructure planning, transportation of energy, per capita energy consumption, imperatives &<br />
steps in user side energy planning, energy management & control system for demand side, seven<br />
principal of energy management, energy policy of a supply organization & demand side organization,<br />
organization for energy management, training & human resource development, motivation.<br />
(Lectures 08)<br />
Unit III<br />
Energy Audit & Energy Monitoring, Targeting and Conservation: Introduction, need, types &<br />
procedure of energy audits, modern techniques and instruments for energy audit. Defining monitoring &<br />
targeting, element of monitoring & targeting, data & information analysis, techniques- energy<br />
consumption, production & cumulative sum of differences (CUSUM). Energy conservation opportunity,<br />
electrical & thermodynamic ECOs, ECOs in chemical process industries, waste management & recycling<br />
of discard material and energy. (Lectures 08)<br />
Unit IV<br />
Advancement In Technologies & Future Energy Alternatives: Recent advancement in energy<br />
technology towards 21st century, transport of energy, ethanol as a fuel. Fusion – introduction potential,<br />
condition for fusion, magnetic confinement fusion reactor, cold fusion laser induced fusion. Biomass –<br />
introduction, municipal waste, biomass conversion, wood combustion Geothermal energy – introduction,<br />
origin, nature, resources and exploration, environment impact, low temperature geothermal resources.<br />
(Lectures 08)<br />
Unit V<br />
Case Studies: Energy conservation in alcohol industry. Energy conservation in fertilizer industry and<br />
pulps & paper industry. Energy conservation in different units of refinery likes FCCU, HCU & ADU.<br />
(Lectures 08)<br />
Text Books:<br />
1. Murphy W.R. and Mckay G., Energy Management(BH)<br />
2. Hinrich & Kleinbach “Energy : its use and the environment” III ed. Harcourt.<br />
3. Boyle “Renewable Energy : Power for a sustainable future” Oxford.<br />
Reference Books:<br />
1. Rao S. & Parulckar B.B. ”Energy technology” khhanna publisher<br />
2. Capenart & Turner “ Guide to energy management ” 6 ed. Keinnedu fairmant press.<br />
Page 82
Course Code: ECH-805<br />
Semester VIII<br />
CATALYTIC PROCESSES (ELECTIVE)<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit – I<br />
Review of Heterogeneous Catalysis. (Lectures 08)<br />
Unit – II<br />
Transport Processes : Analysis of external transport processes in heterogeneous reactions in fixed ed,<br />
fluidized bed and slurry reactors, Intrapellet mass transfer, heat transfer, mass transfer with chemical<br />
reaction and simultaneous mass and heat transfer with chemical reaction. (Lectures 08)<br />
Unit – III<br />
Catalyst Selectivity: Effect of intrapellet diffusionon on selectivities in complex reactions, effect of<br />
external mass transfer on selectivities. (Lectures 08)<br />
Unit – IV<br />
Catalyst Deactivation: Modes of deactivation – poisoning, fouling and sintering. Determination of<br />
deactivation routes, combined effect of deactivation and diffusion on reaction rates, effect of deactivation<br />
on selectivity. (Lectures 08)<br />
Unit – V<br />
Reactor Design: Design calculation for ideal catalytic reactor operating at isothermal, adiabatic and nonadiabatic<br />
conditions. Deviations from ideal reactor performance. Design of industrial fixed-bed, fluidized<br />
bed and slurry reactors, Thermal stability of packed bed and fluidized bed reactors. (Lectures 08)<br />
Text Books:<br />
1. Smith, J.M., “<strong>Chemical</strong> <strong>Engineering</strong> Kinetics,” 3rd ed., McGraw-Hill, 1981<br />
2. Carberry, J.J., “Catalytic Reaction <strong>Engineering</strong>,” McGraw-Hill, 1977.<br />
3. Lee, H.H., “Heterogeneous Catalytic Reactors,” Butterworth<br />
4. Tarhan, M.O., “Catalytic Reactor Design,” McGraw-Hill, NY 1983<br />
Reference Book:<br />
1. Anderson, J.R. and Boudart, M., “Catalysis, Science and Technology,” Vol.7., Springer Verlag. N.Y.<br />
2 . Thomas, J.M. and Thomas, W.J., “Introduction to the Principles of Heterogeneous Catalysis,”<br />
Academic Press, 1967.<br />
Page 83
Semester VIII<br />
INDUSTRIAL POLLUTION ABATEMENT & WASTE MANAGEMENT (ELECTIVE)<br />
Course Code: ECH-806<br />
B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />
L T P C<br />
3 0 0 3<br />
Unit I<br />
Introduction: Environment and environmental pollution from chemical process industries,<br />
characterization of emission and effluents, environmental Laws and rules, standards for ambient air, noise<br />
emission and effluents.<br />
(Lectures 08)<br />
Unit II<br />
Pollution Prevention: Process modification, alternative raw material, recovery of by co-product from<br />
industrial emission effluents, recycle and reuse of waste, energy recovery and waste utilization. Material<br />
and energy balance for pollution minimization. Water use minimization, Fugitive emission/effluents and<br />
leakages and their control-housekeeping and maintenance.<br />
(Lectures 08)<br />
Unit III<br />
Air Pollution Control: Particulate emission control by mechanical separation and electrostatic<br />
precipitation, wet gas scrubbing, gaseous emission control by adsorption and adsorption, Design of<br />
cyclones, ESP, fabric filters and absorbers.<br />
Water Pollution Control: Physical treatment, pre-treatment, solids removal by setting and<br />
sedimentation, filtration centrifugation, coagulation and flocculation.<br />
(Lectures 08)<br />
Unit IV<br />
<strong>Chemical</strong> Treatment: Anaerobic and aerobic treatment biochemical kinetics, trickling filter, activated<br />
sludge and lagoons, aeration systems, sludge separation and drying.<br />
(Lectures 08)<br />
Unit V<br />
Waste management: Characterization of wastes-hazardous and non-hazardous wastes. Waste disposal<br />
and management laws and guidelines. Non-hazardous industrial wastes-treatment, disposal, utilization<br />
and management. Value-extraction from the wastes. Handling, storage and disposal of hazardous wastes.<br />
Case studies of a few real scenarios of waste management – sugar, pulp and paper, and fertilizer units<br />
(Lectures 08)<br />
Text Books:<br />
1. Pollution Control Acts, Rules and Notifications, CPCB, Delhi. 1995<br />
2. Vallero D., “Fundamentals of Air Pollution”, 4th Ed., Academic Press, 2007<br />
3. Eckenfelder W. W., “Industrial Water Pollution Control”, 2nd Ed., Mc Graw Hill, 1999<br />
4. Kreith F. and Tchobanoglous G., “Handbook of Solid Waste Management”, 2nd Ed., Mc Graw Hill,<br />
2002<br />
Reference Books:<br />
1. Pichtel J., “Waste Management Practices: Municipal, Hazardous and Industrial”, CRC, 2005<br />
2. Conway R.A. & Ross R.D., “Handbook of Industrial Waste Disposal”, Van-Nostrand Reinhold, 1980<br />
3. Tchobanoglous G., Theisen H. & Vigil S.A., “Integrated Solid Waste Management : <strong>Engineering</strong><br />
Principles and Management Issues”, McGraw Hill, 1993.<br />
Page 84