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Chemical Engineering - Teerthanker Mahaveer University

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Study & Evaluation Scheme<br />

of<br />

Bachelor of Technology<br />

(<strong>Chemical</strong> <strong>Engineering</strong>)<br />

[Applicable w.e.f. Academic Session 2012-13 till revised]<br />

TEERTHANKER MAHAVEER UNIVERSITY<br />

N.H.-24, Delhi Road, Moradabad, Uttar Pradesh-244001<br />

Website: www.tmu.ac.in<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 1


TEERTHANKER MAHAVEER UNIVERSITY<br />

(Established under Govt. of U. P. Act No. 40, 2008)<br />

Delhi Road, Bagarpur, Moradabad (U.P)-244001<br />

Study & Evaluation Scheme<br />

Bachelor of Technology<br />

SUMMARY<br />

Programme : B.Tech ( <strong>Chemical</strong> <strong>Engineering</strong>)<br />

Duration : Four year full time (Eight Semesters)<br />

Medium : English<br />

Minimum Required Attendance : 75 %<br />

Credit :<br />

Maximum Credit<br />

:<br />

:<br />

194<br />

Minimum credit required for the degree : 190<br />

Assessment- Theory (Other than<br />

Professional Communication)<br />

Internal Evaluation (Theory Papers)<br />

Evaluation of Practical/Project Reports,<br />

Seminar & Professional Communication<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

:<br />

Internal External Total<br />

30 70 100<br />

Class Class Class<br />

Other<br />

Test Test Test Assignment(s) Activity<br />

I II III<br />

(including Total<br />

Best two out of the<br />

three<br />

Mini-3 attendance)<br />

10 10 10 5 5 30<br />

:<br />

Internal External Total<br />

50 50 100<br />

External Internal<br />

Duration of Examination :<br />

3 hrs. 1 ½ hrs<br />

To qualify the course a student is required to secure a minimum of 40 marks in aggregate including the<br />

semester end examination and teachers continuous evaluation.(i.e. both internal and external).<br />

A Candidate who secures less than of 40% of marks in a course shall be deemed to have failed in that<br />

course. The student should have at least 50% marks in aggregate to clear the semester. In case a student<br />

has more than 40% in each course, but less than 50% overall in a semester , he/she shall re-appear in<br />

courses where the marks are less than 50% to achieve the required aggregate percentage of 50% in the<br />

semester.<br />

Question Paper Structure<br />

1. The question paper shall consist of eight questions. Out of which first question shall be of short answer<br />

type (not exceeding 50 words) and will be compulsory. Question No. 1 shall contain 8 parts<br />

representing all units of the syllabus and students shall have to answer any five (weightage 4 marks<br />

each).<br />

2. Out of the remaining seven questions, student shall be required to attempt any five questions. There<br />

will be minimum one and maximum two questions from each unit of the syllabus. The weightage of<br />

Question No. 2 to 8 shall be 10 marks each.<br />

3. Usually each question in the examination Study should & be Evaluation designed to have Scheme a numerical component.<br />

Programme: B.Tech. (<strong>Chemical</strong> <strong>Engineering</strong>)<br />

Semester I<br />

Page 2


S. Course<br />

Subject<br />

Periods Credit Evaluation Scheme<br />

No Code<br />

L T P Internal External Total<br />

1 EAS101 <strong>Engineering</strong> Mathematics-I 3 1 - 4 30 70 100<br />

2<br />

3<br />

EAS102/202 Physics - I<br />

EAS103/203 Chemistry<br />

EME101/201 <strong>Engineering</strong> Mechanics<br />

EME102/202 Manufacturing Science<br />

3 - - 3 30 70 100<br />

3 - - 3 30 70 100<br />

4 ECS101/201 Computer Basics & C Programming 3 - - 3 30 70 100<br />

EAS 104/204 Environmental Science<br />

5 EEE101/201 Basic Electrical <strong>Engineering</strong> 3 - - 3 30 70 100<br />

EEC101/201 Basic Electronics <strong>Engineering</strong><br />

6 EHM101 Foundation English-I 2 - 2 3 30 70 100<br />

7<br />

8<br />

9<br />

10<br />

S.<br />

No<br />

.<br />

EAS151/251 Physics (Lab)<br />

EAS152/252 Chemistry (Lab)<br />

EME151/251 <strong>Engineering</strong> Mechanics (Lab)<br />

ECS151/251 Computer Basics & C Programming<br />

(Lab)<br />

EME152/252 <strong>Engineering</strong> Drawing (Lab)<br />

- - 3 1.5 50 50 100<br />

- - 3 1.5 50 50 100<br />

- - 4 2 50 50 100<br />

EME153/253 Workshop Practice (Lab)<br />

EEE151/251 Basic Electrical <strong>Engineering</strong> (Lab) - - 3 1.5 50 50 100<br />

EEC151/251 Basic Electronics <strong>Engineering</strong> (Lab)<br />

Total 17 1 15 25.5 440 560 1000<br />

Course<br />

Code<br />

Subject<br />

Semester II<br />

Periods Credit Evaluation Scheme<br />

L T P Internal External Total<br />

1 EAS201 <strong>Engineering</strong> Mathematics-II 3 1 - 4 30 70 100<br />

2<br />

3<br />

EAS102/202 Physics - I<br />

EAS103/203 Chemistry<br />

EME101/201 <strong>Engineering</strong> Mechanics<br />

3 - - 3 30 70 100<br />

3 - - 3 30 70 100<br />

EME102/202 Manufacturing Science<br />

4 ECS101/201 Computer Basics & C Programming 3 - - 3 30 70 100<br />

EAS 104/204 Environmental Science<br />

5 EEE101/201 Basic Electrical <strong>Engineering</strong><br />

3 - - 3 30 70 100<br />

EEC101/201 Basic Electronics <strong>Engineering</strong><br />

6 EHM201 Foundation English-II 2 - 2 3 30 70 100<br />

7 EAS151/251 Physics (Lab)<br />

- - 3 1.5 50 50 100<br />

EAS152/252 Chemistry (Lab)<br />

8 EME151/251 <strong>Engineering</strong> Mechanics (Lab)<br />

- - 3 1.5 50 50 100<br />

ECS151/251 Computer Basics & C Programming<br />

(Lab)<br />

9 EME152/252 <strong>Engineering</strong> Drawing (Lab) - - 4 2 50 50 100<br />

EME153/253 Workshop Practice (Lab)<br />

10 EEE151/251 Basic Electrical <strong>Engineering</strong> (Lab) - - 3 1.5 50 50 100<br />

EEC151/251 Basic Electronics <strong>Engineering</strong> (Lab)<br />

Total 17 1 15 25.5 440 560 1000<br />

S.<br />

No.<br />

Subject<br />

Code<br />

Subject<br />

Semester III<br />

Periods Credit Evaluation Scheme<br />

L T P Intern External Total<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 3


1 ECH301 <strong>Chemical</strong> <strong>Engineering</strong><br />

Thermodynamics-I<br />

3 - - 3<br />

al<br />

30 70 100<br />

2 ECH302 Physical <strong>Chemical</strong><br />

Technology<br />

3 - - 3 30 70 100<br />

3 ECH303 Applied Chemistry 3 - - 3 30 70 100<br />

4 ECH304 <strong>Chemical</strong> Process<br />

Calculations<br />

3 - - 3 30 70 100<br />

5 EME 305 Industrial <strong>Engineering</strong> 3 - - 3 30 70 100<br />

6 EAS301/ Mathematics –III / Physics 3 1 - 4 30 70 100<br />

EAS302 II<br />

7 ECH351 <strong>Chemical</strong> <strong>Engineering</strong><br />

Thermodynamics-I (Lab)<br />

- - 4 2 50 50 100<br />

8 ECH352 Physical <strong>Chemical</strong><br />

Technology (Lab)<br />

- - 4 2 50 50 100<br />

9 ECH353 Applied Chemistry (Lab) - - 3 1.5 50 50 100<br />

Total 18 1 11 24.5 330 570 900<br />

Additional Courses for Lateral Entry Students with B.Sc. background, to be taken in III and IV<br />

semester and all should pass with minimum of 40% marks: credits will not be added.<br />

1 EME152/252 <strong>Engineering</strong> Drawing Lab - - 3 1.5 50 50 100<br />

2 EME101/201<br />

EME102/202<br />

<strong>Engineering</strong> Mechanics<br />

Manufacturing Science<br />

3 - - 3 30 70 100<br />

3 EME153/253<br />

EME151/251<br />

Workshop Practice<br />

(Lab)<br />

<strong>Engineering</strong> Mechanics<br />

(Lab)<br />

- - 3 1.5 50 50 100<br />

S. Subject<br />

Subject<br />

Semester IV<br />

Periods Credit Evaluation Scheme<br />

No. Code<br />

L T P<br />

Internal External Total<br />

1 ECH401 Heat Transfer 3 - - 3 30 70 100<br />

2 ECH 402 Inorganic <strong>Chemical</strong><br />

Technology<br />

3 - - 3 30 70 100<br />

3 ECH403 Material Science &<br />

Technology<br />

3 - - 3 30 70 100<br />

4 ECH404 <strong>Chemical</strong> <strong>Engineering</strong><br />

Thermodynamics-II<br />

3 - - 3 30 70 100<br />

5 ECH405 Numerical Methods in<br />

<strong>Chemical</strong> <strong>Engineering</strong><br />

3 1 - 4 30 70 100<br />

6 EAS401/ Mathematics –III / Physics 3 1 - 4 30 70 100<br />

EAS402 II<br />

7 ECH451 Heat Transfer (Lab) - - 4 2 50 50 100<br />

8 ECH452 Inorganic <strong>Chemical</strong><br />

Technology (Lab)<br />

- - 4 2 50 50 100<br />

Total 18 1 8 24 280 520 800<br />

Semester V<br />

S. Subject Subject Periods Credit Evaluation Scheme<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 4


No. Code L T P Internal External Total<br />

1 ECH501 Process Instrumentation 3 - - 3 30 70 100<br />

2 ECH502 Organic <strong>Chemical</strong><br />

Technology<br />

3 - - 3 30 70 100<br />

3 ECH503 Mass Transfer –I 3 - - 3 30 70 100<br />

4 ECH504 Spectroscopy Techniques 3 - - 3 30 70 100<br />

5 ECH505 Environmental <strong>Engineering</strong> 3 - - 3 30 70 100<br />

6<br />

EHM503<br />

<strong>Engineering</strong> and Managerial<br />

Economics<br />

3 - - 3 30 70 100<br />

7 ECH551 Process Instrumentation<br />

(Lab)<br />

- - 4 2 50 50 100<br />

8 ECH552 Organic <strong>Chemical</strong><br />

Technology (Lab)<br />

- - 4 2 50 50 100<br />

9 ECH553 Mass Transfer-I (Lab) - - 3 1.5 50 50 100<br />

10 ECH 591 Industrial Training<br />

(4 Weeks) & Presentation<br />

- - - 2 50 50 100<br />

Total 18 - 11 25.5 380 620 1000<br />

Semester VI<br />

S. Subject<br />

Subject<br />

Periods Credit Evaluation Scheme<br />

No. Code<br />

L T P<br />

Internal External Total<br />

1 ECH601 <strong>Chemical</strong> Reaction<br />

<strong>Engineering</strong>-I<br />

3 - - 3 30 70 100<br />

2 ECH602 Mass Transfer -II 3 - - 3 30 70 100<br />

3 ECH603 Petroleum Refining 3 - - 3 30 70 100<br />

4 ECH604 Biochemical Technology 3 - - 3 30 70 100<br />

5 EHM601 Technical Writing 2 - 2 3 30 70 100<br />

6 EHM 602 Industrial Psychology 3 - - 3 30 70 100<br />

7 ECH651 <strong>Chemical</strong> Reaction<br />

<strong>Engineering</strong>-I (Lab)<br />

- - 3 1.5 50 50 100<br />

8 ECH652 Mass Transfer –II (Lab) - - 3 1.5 50 50 100<br />

ECH605<br />

Elective I – Select any one course<br />

<strong>Chemical</strong> Plant Safety and<br />

Occupational Hazard<br />

9 ECH606 Fertilizer Technology 3 - - 3 30 70 100<br />

ECH607 Rubber Science &<br />

Technology<br />

Total 20 - 18 24 310 590 900<br />

Semester VII<br />

S. Subject Subject Periods Credit Evaluation Scheme<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 5


No. Code L T P Internal External Total<br />

1 ECH701 <strong>Chemical</strong> Reaction Eng. II 3 - - 3 30 70 100<br />

2 ECH702 Introduction to Oil/Fat<br />

Technology<br />

3 - - 3 30 70 100<br />

3 ECH703 Bioprocess <strong>Engineering</strong> 3 - - 3 30 70 100<br />

4 ECH704 Sugar Technology 3 - - 3 30 70 100<br />

5 ECH751 <strong>Chemical</strong> Reaction-II (Lab) - - 4 2 50 50 100<br />

6<br />

ECH752 Introduction to Oil/Fat<br />

Technology (Lab)<br />

- - 4 2 50 50 100<br />

ECH705<br />

Elective II* – Select any one course<br />

Process Equipment Design<br />

7<br />

8<br />

9<br />

ECH706 Air Pollution and Control<br />

Equipments<br />

ECH707 Industrial Pollution Control<br />

Industrial Training & - - - 3 50<br />

100<br />

ECH791 Presentation(6 Weeks)<br />

Project Work Phase-1<br />

50<br />

(Synopsis, Literature Survey - - 6 3 100<br />

100<br />

ECH799 & Presentation)<br />

-<br />

Total 15 - 14 25 400 500 900<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

3 - - 3 30 70 100<br />

Semester VIII<br />

S. Subject<br />

Subject<br />

Periods Credit Evaluation Scheme<br />

No. Code<br />

L T P<br />

Internal External Total<br />

1<br />

ECH801 Polymer Science &<br />

Technology<br />

3 - - 3 30 70 100<br />

2 ECH802 Pulp and Paper Technology 3 - - 3 30 70 100<br />

3<br />

ECH 851 Polymer Science &<br />

Technology (Lab)<br />

- - 4 2 50 50 100<br />

ECH 899 Project Work Phase-2 - - 18 9 50 50 100<br />

4<br />

(Report, Analysis,<br />

Implementation/ Simulation<br />

and Presentation)<br />

ECH803<br />

Elective III* – Select any one course<br />

Industrial Safety & Hazard<br />

Management<br />

5<br />

ECH804<br />

ECH 805<br />

Energy Management<br />

Catalysis Processes<br />

3 - - 3<br />

30 70 100<br />

ECH 806 Industrial Pollution<br />

Abatement & Waste<br />

Management<br />

Total 9 - 22 20 190 310 500<br />

Semester I<br />

ENGINEERING MATHEMATICS-I<br />

Course Code: EAS101 L T P C<br />

Page 6


B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

3 1 0 4<br />

Objective:<br />

• To familiarize the basics of matrices, differential calculus, multiple integrals and vector calculus.<br />

• To solve all problems related to matrices, calculus and vectors.<br />

Course Contents<br />

Unit I (Lectures 08)<br />

Matrices: Elementary row and column transformation; Rank of matrix; Linear dependence; Consistency<br />

of linear system of equations; Characteristic equation; Cayley-Hamilton Theorem; Eigen values and<br />

Eigen vectors; Diagonalization; Complex and unitary matrices.<br />

Unit II (Lectures 08)<br />

Differential Calculus-I: Successive differentiation; Leibnitz theorem; Partial differentiation; Euler’s<br />

theorem; Curve tracing; Change of variables; Expansion of function of several variables<br />

Unit III (Lectures 08)<br />

Differential Calculus–II: Jacobian; Approximation of errors; Extrema of functions of several variables;<br />

Lagrange’s method of multipliers (Simple applications).<br />

Unit IV (Lectures 08)<br />

Multiple Integrals: Double and triple integral; Change of order & Change of variables; Beta and Gamma<br />

functions; Applications to area, volume; Dirichlet integral and applications.<br />

Unit V (Lectures 08)<br />

Vector Calculus: Point functions; Gradient, Divergence and Curl of a vector and their physical<br />

interpretations; Line, Surface and Volume integrals; Green’s & Stokes’ theorem; Gauss’ divergence<br />

theorem.<br />

Text Books<br />

1. Grewal B.S., Higher <strong>Engineering</strong> Mathematics, Khanna Publishers.<br />

2. Prasad C., <strong>Engineering</strong> Mathematics for Engineers, Prasad Mudralaya.<br />

3. Dass H.K., <strong>Engineering</strong> Mathematics Vol-I, S. Chand.<br />

Reference Books<br />

1. Kreyszig E., Advanced <strong>Engineering</strong> Mathematics, Wiley Eastern.<br />

2. Piskunov N, Differential & Integral Calculus, Moscow Peace Publishers.<br />

3. Narayan Shanti, A Text book of Matrices, S. Chand.<br />

Page 7


Semester I/II<br />

PHYSICS-I<br />

Course Code: EAS102/EAS 202 L T P C<br />

3 0 0 3<br />

Objective:<br />

• To understand the fundamentals of physics like interference, diffraction, lasers etc.<br />

Course Contents<br />

Unit I (Lectures 08)<br />

Semiconductor Physics: Distinction among metal, insulator & semiconductor on the basis of band<br />

theory; Intrinsic and Extrinsic semiconductors; Basic concepts of Fermi level; Electron and hole<br />

mobilities; Electrical conductivity and Hall effect; Basics of p-n Junction.<br />

Unit II (Lectures 08)<br />

Interference: Basics of interference of light; coherent Sources, Conditions of Interference; Interference<br />

by division of wave front and amplitude (Fresnel’s bi-prism, Newton’s Rings).<br />

Diffraction: Single and multiple slit Diffraction; Diffraction Grating; Rayleigh’s criterion of resolution;<br />

Resolving Power of Telescope, Microscope and Grating.<br />

Unit III (Lectures 08)<br />

Polarization: Phenomenon of double refraction; Ordinary and extra-ordinary rays; Nicol Prism;<br />

Production and analysis of Plane, Circularly and Elliptically Polarized Light; Optical Activity; Specific<br />

Rotation, Polarimeter.<br />

Laser: Principle of Laser action; Einstein’s Coefficients; Construction and working of He-Ne and Ruby<br />

Laser.<br />

Unit IV (Lectures 08)<br />

Fiber Optics and Holography: Fundamentals of fiber optics; Types of fibers; Acceptance angle ;<br />

Numerical aperture; Attenuation, signal loss in optical fiber and dispersion; Propagation mechanism and<br />

communication in optical fiber.<br />

Basic principle of holography; Construction of a hologram and wave reconstruction; Applications of<br />

holography.<br />

Unit V (Lectures 08)<br />

Electromagnetics: Ampėre’s law and displacement current; Maxwell’s equations in Integral and<br />

Differential Forms; Equation of continuity; Electromagnetic Wave Propagation in Free Space and<br />

Conducting Media; Poynting Theorem.<br />

Text Books<br />

1. Malik K. H., <strong>Engineering</strong> Physics, Tata McGraw Hill.<br />

2. Subramanyam N, Optics, Tata McGraw Hill.<br />

Reference Book<br />

1. Yadav V. S., <strong>Engineering</strong> Physics, Tata McGraw Hill.<br />

2. Mehta Neeraj, <strong>Engineering</strong> Physics Vol. I & II, Prentice Hall of India Pvt. Ltd.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 8


Semester I/II<br />

CHEMISTRY<br />

Course Code: EAS103/EAS203 L T P C<br />

3 0 0 3<br />

Objective:<br />

• To understand the fundamentals of chemistry like Bonding, Pollution, Polymers, Water Chemistry, etc.<br />

Course Contents<br />

Unit I (Lectures 08)<br />

<strong>Chemical</strong> bonding & Solid State Chemistry:<br />

Molecular theory of diatomic hetero-molecules; Band theory of bonding in metals; Hydrogen bonding;<br />

Radius Ratio Rule; Space lattice (only cubes); Type of unit cell, Bragg’s Law, Calculation of Density of<br />

unit cell; One & Two Dimensional solids; graphite as two dimensional solid and its conducting<br />

properties; Fullerene & its applications.<br />

Unit II (Lectures 08)<br />

Polymers , Reaction Kinetics, Phase rule & Electrochemistry:<br />

Structures of the following polymers, viz, Natural and synthetic rubbers, Polyamide and Polyester fibres,<br />

polymethylmethacrylate, poly acrylonitrile and polystyrene; A brief account of conducting polymers<br />

(polypyrrole & polytriphene) & their applications.<br />

Order & Molecularity of reactions; First & Second order reactions; Energy of activation.<br />

Phase Rule: Its application to one component system (Water). Equilibrium Potential, Introduction of<br />

electrochemical cells & Types: Galvanic & Concentration cells, Electrochemical theory of corrosion &<br />

protection of corrosion.<br />

Unit III (Lectures 08)<br />

Water Chemistry & Fuels:<br />

Hardness of water; water softening by Lime Soda Process, Calgon process, Zeolites and ion-exchange<br />

resins; Reverse osmosis;<br />

Classification of fuels, Coal, Biomass & Biogas; Determination of gross and net calorific values using<br />

Bomb Calorimeter.<br />

Unit IV (Lectures 08)<br />

Glass & Ceramics:<br />

Concept of glass & its constituents; Classification & uses of different glasses; Elementary idea of<br />

manufacturing process of glass; Introduction to Ceramics materials & its constituents, Industrial<br />

application of glass & ceramics.<br />

Unit V (Lectures 08)<br />

Lubricants:<br />

Introduction to lubricants; Mechanism of lubrication; Classification of lubricants; Flash and fire points,<br />

Selection of lubricants.<br />

Text Books<br />

1. Agarwal R. K., <strong>Engineering</strong> Chemistry, Krishna Prakashan.<br />

2. Morrison & Boyd, Organic Chemistry, Prentice Hall<br />

3. Chawla Shashi, <strong>Engineering</strong> Chemistry, Dhanpat Rai Publication.<br />

Reference Books<br />

1. Barrow Gordon M., Physical Chemistry, McGraw-Hill.<br />

2. Manahan Stanley E., Environmental Chemistry, CRC Press.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 9


Semester I/II<br />

ENGINEERING MECHANICS<br />

Course Code: EME101/EME201 L T P C<br />

3 0 0 3<br />

Objective:<br />

To study about mechanics, force system, torsion, beams, trusses, frames etc.<br />

Course Contents<br />

Unit I (Lectures 08)<br />

Force systems and analysis: Basic concept; Newton’s laws of motion; Transfer of force to a parallel<br />

position; Determination of resultant of planer force system; Free body diagrams; Equilibrium of forces<br />

and its equations.<br />

Friction: Introduction; Coulomb’s law of friction; Equilibrium of bodies involving dry fiction; Belt<br />

Friction.<br />

Unit II (Lectures 08)<br />

Structural Analysis: Beams; Introduction; Shear force and Bending Moment; shear force and Bending<br />

Moment Diagram for statically determinate beams.<br />

Trusses: Introduction; Simple Trusses; Determination of Forces in simple trusses members; methods of<br />

joints and method of section.<br />

Unit III (Lectures 08)<br />

Centroid and Moment of Inertia: Centroid of plane; curve, area, volume and composite bodies;<br />

Moment of inertia of plane area; Parallel Axes Theorem; Perpendicular axes theorems; Principal Moment<br />

Inertia; Mass Moment of Inertia of Circular Ring, Disc, Cylinder, Sphere and Cone about their axis of<br />

symmetry<br />

Unit IV (Lectures 08)<br />

Simple stress and strain: Introduction; Normal shear stresses; stress-strain diagrams for ductile and<br />

brittle materials; Elastic constants; one dimensional loading of members of varying cross sections.<br />

Unit V (Lectures 08)<br />

Pure Bending of Beams: Introduction; Simple bending theory; Stress in Beams of different cross<br />

sections.<br />

Torsion: Introduction; Torsion of shafts of circular section; Torque and Twist; Shear stress due to<br />

Torque.<br />

Text Books<br />

1. Bansal R. K., <strong>Engineering</strong> Mechanics, Laxmi Publications.<br />

2. Kumar D. S., <strong>Engineering</strong> Mechanic, S. K. Kataria & Sons.<br />

3. Kumar K. L., Kumar V., <strong>Engineering</strong> Mechanics, Tata McGraw Hill Publication.<br />

4. Khurmi R. S., <strong>Engineering</strong> Mechanics, S. Chand Publications.<br />

Reference Books<br />

1. Shames, <strong>Engineering</strong> Mechanics, Prentice Hall of India Pvt. Ltd.<br />

2. Ryder G. H., Strength of Materials, Macmillan Publishers India Ltd.<br />

3. Ramamruthams, Strength of materials, Dhanpat Rai Publications.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 10


Semester I/II<br />

MANUFACTURING SCIENCE<br />

Course Code: EME102/EME202 L T P C<br />

3 0 0 3<br />

Objective: To expose the students about basics of manufacturing processes as applicable in Mechanical<br />

<strong>Engineering</strong>.<br />

Course Contents<br />

Unit I (Lectures 08)<br />

Basic Metals & Alloys: Properties and Applications; Properties of Materials: Strength, elasticity,<br />

stiffness, malleability, ductility, brittleness, toughness, and hardness; Elementary ideas of fracture fatigue<br />

& creep.<br />

Unit II (Lectures 10)<br />

Metal Forming: Basic metal forming operations & uses of such as: Forgoing, Rolling, Wire<br />

drawing/making and Extrusion, and its products/application; Press-work; die & punch assembly, cutting<br />

and forming, its application; Hot-working versus cold-working; Introduction to Plastics: Types,<br />

Machines: Injection Moulding.<br />

Casting: Pattern & allowance; Molding sands its desirable properties; Mould making with the use of<br />

core; Gating system, Casting defects & remedies; Cupola Furnace, Die-casting and its uses.<br />

Unit III (Lectures 10)<br />

Machining: Basic principles of Lathe-machine and operations performed on it; basic description of<br />

machines and operations of Shaper-Planner, Drilling, Milling & Grinding.<br />

Welding: Importance & basic concepts of welding; Classification of welding processes: Gas-welding,<br />

types of flames and principle; Electric-Arc welding; Resistance welding; Soldering, & Brazing and its<br />

uses.<br />

Unit IV (Lectures 8)<br />

Unconventional Manufacturing Process: Limitations of conventional manufacturing process; need of<br />

unconventional manufacturing processes; Basic Principles and working of unconventional manufacturing<br />

process and their applications; Electro-Discharge machining; Electro-chemical machining; Ultrasonic<br />

machining; Abrasive jet machining; Water jet machining;, Laser cutting and Laser beam welding.<br />

Unit V (Lectures 04)<br />

Super Finishing Processes: Introduction; Lapping; Honing; Buffing; Burnishing; Powder coating;<br />

Polishing<br />

Text Books<br />

1. Hajra & Bose, Workshop Technology, Vol 1 & 2, Roy Media Promoters.<br />

2. Pandey & Singh, Production <strong>Engineering</strong> Science, Standard Publishers.<br />

3. R.K. Jain, Production technology, Khanna publishers.<br />

Reference Books<br />

1. Raghuvanshi, B.S., Workshop Technology, Vol 1 & 2, Dhanpat Rai & Sons.<br />

2. Laxmi Narayan & Vaish W, A Text Book of Practical Geometrical Drawing, Pearson Education.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 11


Semester I/II<br />

COMPUTER BASICS & ‘C’ PROGRAMMING<br />

Course Code: ECS101/ECS201 L T P C<br />

3 0 0 3<br />

Objective:<br />

• To learn the basics of computers & C programming language.<br />

Course Contents:<br />

Unit I (Lectures 08)<br />

Concepts in Computer Application: Definition of Electronic Computer; History; Generations;<br />

Characteristics and Application of Computers; Classification of Computers; Functional Component of<br />

Computer: CPU, I/O devices, Type of Memory & Memory Hierarchy, Firmware and Human ware.<br />

Data and data types: Definitions, data, data types: Integer, Character, Float, String, etc.; Constants<br />

and Variable Declaration; Token; Keyboard; Identifier.<br />

Unit II (Lectures 08)<br />

Programming Language Classification & Computer Languages: Generation of Languages;<br />

Introduction to 4GLs; Translators; Assemblers; Compilers; Interpreters.<br />

Number System: Decimal, Octal, Binary and Hexadecimal & their Conversions; Various Code: BCD,<br />

ASCII and EBCDIC and Gray Code.<br />

Operators and Expressions: Numeric and relation operators; logical operator; bit operator; operator<br />

precedence and associativity.<br />

Unit III (Lectures 08)<br />

Internet and Web Technologies: Hypertext Markup Language; WWW; Gopher; FTP; Telnet; Web<br />

Browsers; Search Engines; Email.<br />

Control Structure: while statement, if, else, Nested if else statement. Nested logic: for loop, do- while<br />

loop, loop inside a loop structure, Switch Statement. Break and default with switch.<br />

Unit IV (Lectures 08)<br />

Concepts in Operating Systems: Elementary Concepts in Operating Systems; Textual Vs GUI Interface.<br />

Arrays: Notation and representation; Manipulation of array elements; Multidimensional arrays.<br />

Unit V (Lectures 08)<br />

Functions & Strings: Definition; Declaration; Call by Value; Call by Reference; Returns values and<br />

their types; Function calls<br />

Text Books<br />

1. Sinha P. K., Computer Fundamentals, BPB Publications.<br />

2. Yadav, DS, Foundations of IT, New Age.<br />

3. Curtin, Information Technology: Breaking News, Tata McGraw Hill.<br />

4. Rajaraman,R, Introduction to Computers, Prentice Hall of India.<br />

Reference Books<br />

1. Peter Nortans, Introduction to Computers, Tata McGraw Hill.<br />

2. Leon & Leon, Fundamental of Information Technology, Vikas Publishing.<br />

3. Kanter, Managing Information System, Prentice-Hall.<br />

4. CISTems, Internet: An Introduction, Tata McGraw Hill.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 12


Semester I/II<br />

ENVIRONMENTAL SCIENCE<br />

Course Code: EAS104/EAS204 L T P C<br />

3 0 0 3<br />

Objective: To create awareness among students about environment protection.<br />

Unit I (Lectures 08)<br />

Introduction: Definition, Scope, Segments of Environment and its Multidisciplinary Nature; Some Major<br />

Environmental Problems; Definition and Scope of Ecology.<br />

Unit II (Lectures 08)<br />

Ecology And Environment: Concept of an Ecosystem- its components and functions; Trophic Levels-<br />

Producer; Consumer and Decomposer; Energy Flow in an Ecosystem; Biogeochemical Cycles; Food<br />

Chain; Food Web and Ecological Pyramid.<br />

Unit III (Lectures 08)<br />

Air & water pollution: Various segments of Atmosphere and their Significance; Sources and Effects of<br />

Air Pollution; Sources of Air Pollution: Photochemical Smog, Acid Rain, Global Warming, Ozone Layer -<br />

Its Depletion and Control Measures; Sources of Water Pollution; Treatment of Water Pollution;<br />

Eutrophication.<br />

Unit IV (Lectures 08)<br />

Soil & Thermal pollution: Soil pollution: Sources and Consequences; Solid Wastes – Pollution;<br />

Treatment & Disposal.<br />

Thermal - sources and consequences; Sustainable Development; Dams and Reservoirs- Their Benefits and<br />

Problems.<br />

Unit V (Lectures 08)<br />

Biodiversity & its conservation<br />

Bio-Diversity Hot-spots of Biodiversity in India and World; Conservation; Importance and Factors<br />

Responsible for Loss of Biodiversity; Deforestation- causes and effects; Biogeographical Classification of<br />

India; Environment Conservation Movement in India (Chipko Movement, Appiko Movement),<br />

Bioremediation; Biological Magnification.<br />

Text Books<br />

1. De A.K., Environmental Chemistry, New Age Publishers Pvt. Ltd.<br />

2. Masters, G.M., Introduction to Environmental <strong>Engineering</strong> and Science, Prentice Hall India Pvt. Ltd.<br />

3. Odum, E.P., Fundamentals of Ecology, W. B. Sannders Co.<br />

Reference Books<br />

1. Bryant,P.J., Biodiversity and Conservation, Hypertext Book.<br />

2. Tewari, Khulbe & Tewari, Textbook of Environment Studies, I.K. Publication.<br />

3. Trivedi, R.K., Handbook of Environmental Laws, Rules, Guidelines, Compliances and Standards, Vol<br />

I and II, Environment Media.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 13


Semester I/II<br />

BASIC ELECTRICAL ENGINEERING<br />

Course Code: EEE101/EEE201 L T P C<br />

3 0 0 3<br />

Objective<br />

• To understand the fundamental concept of Electrical <strong>Engineering</strong> like DC Network, AC Network,<br />

Measuring Instruments, Energy Conversion Devices etc.<br />

Course Contents<br />

Unit I (Lectures 08)<br />

D.C. Network Theory: Circuit theory concepts-Mesh and node analysis; Network Theorems-<br />

Superposition theorem, Thevenin’s theorem, Norton’s theorem and Maximum Power Transfer theorem;<br />

Star Delta transformation.<br />

Unit II (Lectures 08)<br />

Steady State Analysis of A.C. Circuits: Sinusoidal and phasor representation of voltage and current;<br />

Single phase A.C. circuit behaviour of resistance, inductance and capacitance and their combination in<br />

series & parallel; Power factor; Series and parallel resonance; Band width and quality factor; magnetic<br />

circuit.<br />

Unit III (Lectures 08)<br />

Measuring Instruments: Construction and principles of operation of voltage and current measuring<br />

instruments; introduction to power and energy meters.<br />

Three Phase A.C. Circuits: Star-Delta connections; Line and phase voltage/current relations; Three<br />

phase power and its measurement.<br />

Unit IV (Lectures 08)<br />

Transformer: Principle of operation; Types of construction; Phasor diagram; Equivalent circuit;<br />

Efficiency and voltage regulation of single phase transformer; Open and short circuit tests.<br />

D.C. Machines: Principles of electromechanical energy conversion; Types of D.C. machines; E.M.F.<br />

equation; Magnetization and load characteristics; Losses and efficiency; Starter and speed control of D.C.<br />

Motors; Motor applications.<br />

Unit V (Lectures 08)<br />

Three phase induction Motor: Principle of operation; Types and methods of starting; slip-torque<br />

characteristics; Applications.<br />

Synchronous Machines: Principle of Operation of Alternator and synchronous motor<br />

Single phase Motors: Principle of operation and methods of starting of induction motor,<br />

Text Books<br />

1. V. Del Toro, Principles of Electrical <strong>Engineering</strong>, Prentice-Hall International.<br />

2. W.H. Hayt & J.E. Kemmerly, <strong>Engineering</strong> Circuit Analysis, McGraw Hill.<br />

Reference Books<br />

1. Nagrath I.J., Basic Electrical <strong>Engineering</strong>, Tata McGraw Hill.<br />

2. Fitzgerald A.E & Higginbotham ., D.E., Basic Electrical <strong>Engineering</strong>, McGraw Hill.<br />

3. A Grabel, Basic Electrical <strong>Engineering</strong>, McGraw Hill.<br />

4. Cotton H., Advanced Electrical Technology, Wheeler Publishing.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 14


Semester I/II<br />

BASIC ELECTRONICS ENGINEERING<br />

Course Code: EEC101/EEC201 L T P C<br />

3 0 0 3<br />

Objective<br />

• To understand the basic concept of Electronics <strong>Engineering</strong> like p-n Junction, Bipolar Junction<br />

Transistor, Field Effect Transistor, Operational Amplifier etc.<br />

Course Contents<br />

Unit I (Lectures 08)<br />

p-n Junction: Properties of Elements; Crystal Structure; Energy band diagram; Introduction to PN-<br />

Junction; Depletion layer; V-I characteristics Diode Ratings (average current, peak-inverse voltage); p-n<br />

junction as rectifiers (half wave and full wave) & filter; calculation of ripple factor and load regulation;<br />

clipping and clamping circuits; Zener diode and its application as shunt regulator.<br />

Unit II (Lectures 08)<br />

Bipolar Junction Transistor (BJT): Basic construction; transistor action; CB, CE and CC<br />

configurations; input/output characteristics; Biasing of transistors: Fixed bias, emitter bias, potential<br />

divider bias; Graphical analysis of CE amplifier; concept of Voltage gain current gain; λ-parameter model<br />

(low frequency); Computation of Ai, Av, Ri & Ro of single transistor CE amplifier configuration.<br />

Unit III (Lectures 08)<br />

Field Effect Transistor (FET): Basic construction of JFET; Principle of working; concept of pinch-off<br />

maximum drain saturation current; input and transfer characteristics; Characteristics equation; CG, CS<br />

and CD Configuration; fixed and self biasing of JFET amplifier Introduction of MOSFET; Depletion and<br />

Enhancement type MOSFET- Construction; Operation and Characteristics.<br />

Unit IV (Lectures 08)<br />

Operational Amplifier (Op-Amp): Concept of ideal operational amplifier; ideal and practical Op-Amp<br />

parameters; inverting, non-inverting and unity gain configurations; Applications of Op-Amp as adders,<br />

difference amplifiers, integrators and differentiator.<br />

Unit V (Lectures 08)<br />

Switching Theory: Number system; conversion of bases (decimal, binary, octal and hexadecimal<br />

numbers); Adder & Subtraction; BCD numbers; Seven Segment Display; Boolean Algebra; Logic gates;<br />

Concept of universal gates; Canonical forms; minimization using K-Map<br />

Text Books<br />

1. Robert Boylestad & Louis Nashelsky, Electronic Circuit and Devices, Pearson India.<br />

2. Millman & Halkias, Integrated Electronics, McGraw Hill.<br />

3. Millman & Halkias, Electronics Devices and Circuits, McGraw Hill.<br />

4. Morris Mano M., Digital Design, Prentice Hall.<br />

Reference Books<br />

1. Sedra and Smith, Microelectronic Circuits, Oxford <strong>University</strong> Press .<br />

2. Gayakwad, R A, Operational Amplifiers and Linear Integrated circuits, Prentice Hall of India Pvt.<br />

Ltd.<br />

3. Chattopadhyay D and P C Rakshit, Electronics Fundamentals and Applications, New Age<br />

International.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 15


Semester-I<br />

FOUNDATION ENGLISH - I<br />

Course code: EHM101 L T P C<br />

2 0 2 3<br />

(Common with BPH105/BED105/BAL101/AR107/BHM101/BFS106/BCA106/BBA106/ BCH106/<br />

BFA103)<br />

Course Contents:<br />

Unit I (Lectures 10)<br />

Functional Grammar: Patterns & Parts of speech Subject, Predicate, Noun, Pronoun, Adjective,<br />

Adverb, Verb, Verb phrases, Conjunction, Interjection.<br />

Unit II (Lectures 10)<br />

Vocabulary: Word formation, Prefix, Suffix, Compound words, Conversion, Synonyms, Antonyms,<br />

Homophones and Homonyms, How to look up a dictionary.<br />

Unit III (Lectures 10)<br />

Communication: Meaning & importance of communication, Barriers to effective communication,<br />

Channels of communication, Language as a tool of communication<br />

Unit IV (Lectures 10)<br />

Requisites of Sentence writing: Fragmented sentences, A good sentence, expletives, Garbled sentences,<br />

Rambling sentences, Loaded sentences, Parallel Comparison, Squinting construction, Loose & periodic<br />

sentences.<br />

Text Books:<br />

1. Martin & Wren - High School English Grammar & Composition, S.Chand & Co.<br />

2. Lewis Norman - Word Power made easy, W.R.Goyal Publication & Distributors.<br />

3. Better Your English: A Workbook for 1 st year Students, Macmillan India.<br />

Reference Books:<br />

1. Raman Meenakshi & Sharma Sangeeta, Technical Communication: Principles & Practices, Oxford<br />

<strong>University</strong> Press, New Delhi.<br />

2. Mohan Krishna & Banerji Meera, Developing Communication Skills, Macmillan India Ltd.<br />

3. Rosen Blum M., How to Build Better Vocabulary, Bloomsbury Publication. London.<br />

NOTE:<br />

This syllabus has been designed to improve the oral and written communication skills of students.<br />

The faculty members should put emphasis on practical (oral) activities for generating students’<br />

interest in language learning.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 16


Semester I/II<br />

PHYSICS (LAB)<br />

Course Code: EAS151/EAS251 L T P C<br />

0 0 3 1.5<br />

LIST OF EXPERIMENTS<br />

1. To determine the wavelength of Sodium light by Newton’s rings.<br />

2. To determine the wavelength of Sodium light by Fresnel’s Biprism.<br />

3. To determine the Specific Rotation of the Cane sugar solution with the help of Polari meter.<br />

4. To determine the wavelength of the sodium light by Michelson’s interferometer.<br />

5. To study the PN junction characteristics.<br />

6. To determine the high resistance by Leakage method.<br />

7. To study the energy band gap by four probe method.<br />

8. To study the variation of magnetic field using Stewart and Gee’s apparatus.<br />

9. To determine the frequency of A.C. mains by means of a Sonometer.<br />

10. To study the Hall Effect.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 17


Semester I/II<br />

CHEMISTRY (LAB)<br />

Course Code: EAS152/EAS252 L T P C<br />

0 0 3 1.5<br />

LIST OF EXPERIMENTS<br />

1. To determine total alkalinity in the given water sample.<br />

2. To determine the temporary and permanent hardness in water sample using EDTA as standard<br />

solution.<br />

3. To determine the available chlorine in bleaching powder solution.<br />

4. To determine the chloride content in the given water sample by Mohr’s method.<br />

5. To determine the pH of the given solution using pH meter and pH-metric titration.<br />

6. To determine the Equivalent weight of Iron by the chemical displacement method.<br />

7. To determine the Viscosity of an addition polymer like polyester by Viscometer.<br />

8. To determine the dissolved oxygen present in a water sample.<br />

9. To prepare the Bakelite resin polymer.<br />

10. To determine the viscosity of a given sample of a lubricating oil using Redwood Viscometer.<br />

11. To determine the carbon dioxide content in polluted water sample.<br />

12. To find chemical oxygen demand of waste water sample by potassium dichromate.<br />

13. To determine the total hardness in water sample using complexometric method.<br />

14. To determine the iron content in the given sample using external indicator.<br />

15. To determine the strength of given HCL solution by titrating against N/10 Standard Sodium<br />

hydroxide solution.<br />

Note: Minimum of 10 experiments has to be completed for completion of curriculum.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 18


Semester I/II<br />

ENGINEERING MECHANICS (LAB)<br />

Course Code: EME151/EME251 L T P C<br />

0 0 3 1.5<br />

(Any 10 experiments of the following or such experiments suitably designed)<br />

LIST OF EXPERIMENTS<br />

1. To conduct the tensile test and determine the ultimate tensile strength, percentage elongation for a steel<br />

specimen.<br />

2. To conduct the compression test and determine the ultimate compressive strength for a specimen.<br />

3. To conduct the Impact test on Impact-testing machine to find the toughness by Charpy impact test.<br />

4. To conduct the Impact-test on Impact-testing machine to find the toughness by Izod impact Test.<br />

5. To determine the hardness of the given specimen using Rockwell hardness testing machine.<br />

6. To determine the hardness of the given specimen using Brinell hardness testing machine.<br />

7. To determine gear ratio of simple and compound gear train.<br />

8. To determine the mechanical advantage of worm and worm wheel for load lifting.<br />

9. To find the coefficient of friction on inclined plane.<br />

10. To perform torsion test for rod on torsion testing machine.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva voce taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 19


Semester I/II<br />

COMPUTER BASICS & C PROGRAMMING (LAB)<br />

Course Code: ECS 151/ 251 L T P C<br />

0 0 3 1.5<br />

Perform any ten experiments.<br />

Course Contents<br />

1. To write a program to calculate Sum & average of N numbers.<br />

2. To write a program to convert integer arithmetic to a given number of day and month.<br />

3. To write a program to find maximum and minimum out of 3 numbers a, b & c.<br />

4. To write a program to find factorial of positive integer.<br />

5. To write a program to find sum of series up to n number, 2+5+8+…………………+n.<br />

6. To write a program to print all the number between 1 to 100 which are dividing by 7.<br />

7. To write a program to generate Fibonacci series up to n.<br />

8. To write a program to implement a function to calculate area of a circle.<br />

9. To write a program to implement a recursive function to calculate factorial of given number.<br />

10. To write a program to find whether number is prime or not.<br />

11. To write a program to find that the enter character is a letter or digit.<br />

12. To write a program to find addition of two matrix of n*n order.<br />

13. To write a program to find multiplication of two matrix of n*n order.<br />

14. To write a program to add 6 digit numbers in even case & multiple 6 digit number in odd case.<br />

15. To write a program to find even or odd up to a given limit n.<br />

16. To write a program to find whether a given no is palindrome or not.<br />

17. To write a program to joining & Comparing the 2 string.<br />

Evaluation of Practical Examination:<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 20


Semester I/II<br />

ENGINEERING DRAWING (LAB)<br />

Course Code: EME152/EME252 L T P C<br />

0 0 4 2<br />

1. To write all Numbers (0 to 9) and alphabetical Letters (A to Z) as per the standard dimensions.<br />

2. To draw the types of lines and conventions of different materials.<br />

3. To draw and study dimensioning and Tolerance.<br />

4. To construction geometrical figures of Pentagon and Hexagon<br />

5. To draw the projection of points and lines<br />

6. To draw the Orthographic Projection of given object in First Angle<br />

7. To draw the Orthographic Projection of given object in Third Angle<br />

8. To draw the sectional view of a given object<br />

9. To draw the development of the lateral surface of given object<br />

10. To draw the isometric projection of the given orthographic projection.<br />

Reference Books<br />

1. Bhatt. N.D., Elementary <strong>Engineering</strong> Drawing, Charothar Publishing.<br />

2. Narayana K.L. & Vaish W., A Text Book of Practical Geometry on Geometrical Drawing, Pearson<br />

Education.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each sheet prepared would be evaluated by the faculty concerned on the date of preparing the sheet on a<br />

5 point scale which would include the sheet drawn by the students and a Viva voce taken by the faculty<br />

concerned. The marks shall be entered on the index sheet.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 21


Semester I/II<br />

WORKSHOP PRACTICE (LAB)<br />

Course Code: EME153/EME253 L T P C<br />

0 0 4 2<br />

List of Experiments<br />

Perform any ten experiments selecting at least one from each shop.<br />

Carpentry Shop:<br />

1. To prepare half-lap corner joint.<br />

2. To prepare mortise & tenon joint.<br />

3. To prepare a cylindrical pattern on woodworking lathe.<br />

Fitting Bench Working Shop:<br />

1. To prepare a V-joint fitting<br />

2. To prepare a U-joint fitting<br />

3. To prepare a internal thread in a plate with the help of tapping process<br />

Black Smithy Shop:<br />

1. To prepare a square rod from given circular rod<br />

2. To prepare a square U- shape from given circular rod<br />

Welding Shop:<br />

1. To prepare a butt and Lap welded joints using arc welding machine.<br />

2. To prepare a Lap welded joint Gas welding equipment.<br />

3. To prepare a Lap welded joint using spot welding machine.<br />

Sheet-metal Shop:<br />

1. To make round duct of GI sheet using ‘soldering’ process.<br />

2. To prepare a tray of GI by fabrication<br />

Machine Shop:<br />

1. To prepare a bolt on the lathe machine as per given. diagram<br />

2. To prepare a job on the lathe machine as per given diagram.<br />

Foundry Shop:<br />

1. To prepare core as per given size.<br />

2. To prepare a mould for given casting.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

Page 22


EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

Semester I/II<br />

BASIC ELECTRICAL ENGINEERING (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

TOTAL EXTERNAL<br />

(50 MARKS)<br />

Course Code: EEE151/EEE251 L T P C<br />

0 0 3 1.5<br />

LIST OF EXPERIMENTS<br />

1. To verify the Kirchhoff’s current and voltage laws.<br />

2. To verify the Superposition theorem.<br />

3. To verify the Thevenin’s theorem.<br />

4. To verify the Norton’s theorem.<br />

5. To verify the maximum power transfer theorem.<br />

6. To determine the efficiency of single-phase transformer by load test.<br />

7. To determine the external characteristics of DC Shunt generator.<br />

8. To measure current and speed for speed control of D.C. Shunt Motor.<br />

9. To measure the power in a 3-phase system by two-wattmeter method<br />

10. To measure the power factor in an RLC by varying the capacitance.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 23


Semester I/II<br />

BASICS ELECTRONICS ENGINEERING (LAB)<br />

Course Code: EEC151/EEC251 L T P C<br />

0 0 3 1.5<br />

LIST OF EXPERIMENTS<br />

1. To study the V-I characteristics of p-n junction diode.<br />

2. To study the diode as clipper and clamper.<br />

3. To study the half-wave & full-wave rectifier using silicon diode.<br />

4. To study transistor in Common Base configuration & plot its input/output characteristics.<br />

5. To study transistor in Common Emitter configuration & plot its input/output characteristics. .<br />

6. To study the operational amplifier in inverting & non inverting modes using IC 741.<br />

7. To study the operational amplifier as differentiator & integrator.<br />

8. To study the Zener diode as a shunt regulator.<br />

9. To study various logic gates & verify their truth tables.<br />

10. To study half adder/full adder & verify their truth tables.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 24


Semester II<br />

ENGINEERING MATHEMATICS- II<br />

Course Code: EAS201 L T P C<br />

3 1 0 4<br />

Objective: To familiarize the basic concept of Differential Equations, Laplace Transform, Fourier series<br />

and Partial Differential Equations etc.<br />

Course Contents<br />

Unit I (Lectures 08)<br />

Differential Equations: Ordinary differential equations of first order; Exact differential equations;<br />

Linear differential equations of first order, Linear differential equations of nth order with constant<br />

coefficients; Complementary functions and particular integrals; Simultaneous linear differential<br />

equations; Solutions of second order differential equations by changing dependent and independent<br />

variables; Method of variation of parameters; Applications to engineering problems (without derivation).<br />

Unit II (Lectures 08)<br />

Series Solutions and Special Functions: Series solutions of ODE of 2nd order with variable coefficients<br />

with special emphasis to differential equations of Legendre and Bessel; Legendre polynomials; Bessel’s<br />

functions and their properties.<br />

Unit III (Lectures 10)<br />

Partial Differential Equations and applications: Introduction of partial differential equations; Linear<br />

partial differential equations with constant coefficients of 2nd order and their classifications – parabolic;<br />

elliptic and hyperbolic with illustrative examples.<br />

Method of separation of variables for solving partial differential equations; Wave equation up to two<br />

dimensions; Laplace equation in two-dimensions; Heat conduction equations up to two-dimensions;<br />

Equations of transmission Lines.<br />

Unit IV (Lectures 06)<br />

Fourier Series: Periodic functions, Trigonometric series; Fourier series; Euler’s formulae; Even and odd<br />

functions, Half range sine and cosine series.<br />

Unit V (Lectures 08)<br />

Laplace Transform: Laplace transform; Existence theorem; Laplace transform of derivatives and<br />

integrals; Inverse Laplace transform; Unit step function; Diracth delta function; Laplace transform of<br />

periodic functions; Convolution theorem; Application to solve simple linear and simultaneous differential<br />

equations.<br />

Text Books<br />

1. Grewal B.S., Higher <strong>Engineering</strong> Mathematics, Khanna Publishers.<br />

2. Prasad C., <strong>Engineering</strong> Mathematics for Engineers, Prasad Mudralaya.<br />

3. Das H.K., <strong>Engineering</strong> Mathematics Vol-II, S. Chand.<br />

Reference Books<br />

1. Kreyszig E., Advanced <strong>Engineering</strong> Mathematics, Wiley Eastern.<br />

2. Piskunov N, Differential & Integral Calculus, Moscow Peace Publishers.<br />

3. Narayan Shanti, A Text book of Matrices, S. Chand<br />

4. Bali N.P., <strong>Engineering</strong> Mathematics-II, Laxmi Publications.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 25


Semester-II<br />

FOUNDATION ENGLISH - II<br />

Course code: EHM 201 L T P C<br />

2 0 2 3<br />

(Common with BPH206/BBA206/BCA206/BHM201/AR207/BCH206/BFA203)<br />

Unit I (Lectures 10)<br />

Functional Grammar: Articles, Preposition, Tenses: Functions, Synthesis, Transformation, Spotting<br />

errors and correction of sentences.<br />

Unit II (Lectures 10)<br />

Pre- Requisites of Technical written Communication: One word substitution, Spelling rules, Words<br />

often confused & misused, Phrases.<br />

Unit III (Lectures 10)<br />

The Structure of sentences/ clauses: Adverb clause, Adjective clause, Noun clause. Sentences: Simple,<br />

Double, Multiple and complex, Transformation of sentences: simple to complex & vice versa, simple to<br />

compound & vice-versa, Interrogative to assertive & negative & vice-versa.<br />

Unit IV (Lectures 10)<br />

Technical Communication: Nature, Origin and Development, Salient features, Scope & Significance,<br />

Forms of Technical Communication, Difference between Technical Communication & General writing,<br />

Objective Style vs. Literary Composition<br />

Text-Books:<br />

1. Wren & Martin, High School English Grammar & Composition – S. Chand & Co.<br />

2. Raman Meenakshi & Sharma Sangeeta, Technical Communication-Principles & Practice, Oxford<br />

<strong>University</strong> Press, New Delhi, 2007.<br />

3. Mitra Barum K., Effective Technical Communication, Oxford <strong>University</strong> Press, New Delhi.<br />

4. Better Your English- A Workbook for 1 st year Students- Macmillan India.<br />

Reference Books:<br />

1. Horn A.S., Guide to Patterns & Usage in English, Oxford <strong>University</strong> Press, New Delhi.<br />

NOTE:<br />

This syllabus has been designed to improve the oral and written communication skills of students.<br />

The faculty members should put emphasis on practical (oral) activities for generating students’<br />

interest in language learning.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 26


Course Code: ECH-301<br />

Semester-III<br />

CHEMICAL ENGINEERING THERMODYNAMICS-I<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I (Lectures 08)<br />

Introduction; Definitions and Concepts - System, Surroundings, Property, Intensive and Extensive<br />

Energy, Work, Thermodynamic equilibrium, stability of equilibrium states; Zeroth Law of<br />

Thermodynamics; Perfect Gas scale.<br />

Unit – II (Lectures 08)<br />

First law of Thermodynamics and Its Applications; First law analysis of processes; Control mass and<br />

control volume analysis; Steady state and Transient state flow processes.<br />

Thermodynamic properties of fluids - pure substance, Concept of Phase, Ideal gas equation of state, Van<br />

der Waals’ equation of state, two parameter corresponding states principle, Compressibility charts; Steam<br />

Tables and applications.<br />

Unit – III (Lectures 08)<br />

Second law of Thermodynamics - Limitation of First Law, Kelvin-Planck and Clausius Statements,<br />

Reversible and Irreversible Processes, Carnot cycle, Entropy; Second Law analysis of a control volume;<br />

Heat Engine and Heat Pump; Fundamental Thermodynamic Relations; Maxwell Relations; Clapeyron’s<br />

Equation; Kirchoff’s equation; Phase Rule.<br />

Unit – IV (Lectures 08)<br />

Ideal gas mixture ; Air-Water mixture; Humidity; Psychrometric chart and its applications.<br />

Power Cycles - Rankine cycle and its modifications, Otto cycle, Diesel cycle; Refrigeration Cycles -<br />

Vapor Compression Refrigeration cycle, Absorption Refrigeration cycle<br />

Unit – V (Lectures 08)<br />

Statistical Thermodynamics - Postulates, Macrostates and microstates, Partition Function, Maxwell-<br />

Boltzmann, Bose-Einstein and Fermi-Dirac statistics; Applications of Statistical Thermodynamics - Ideal<br />

gas, Maxwell speed distribution, Einstein & Debye Models of a solid.<br />

Text Books:<br />

1. Rao, Y. V. C., “An Introduction to Thermodynamics,” John Wiley, 1993.<br />

2. Van Wylen, G. J. and Sonntag, R. E., “Fundamentals of Classical Thermodynamics,” 2nd ed., John<br />

Wiley, New Delhi.<br />

Reference Books:<br />

1. Yannes & Smith. John , <strong>Chemical</strong> Engg. Thermdynamics Wiley, New Delhi.<br />

2. Yunus A. Cengel Michael A. Boles, An-thermodyanamic Engg, John Wiley, New Delhi.<br />

3. Gordon Rogers Yon Mayhew. Engg- thermodyanamic , John Wiley, New Delhi.<br />

Page 27


Semester-III<br />

PHYSICAL CHEMICAL TECHNOLOGY<br />

Course Code: ECH-302<br />

L T P C<br />

3 0 0 3<br />

Unit I (Lectures 08)<br />

Liquid State: Liquefaction of Gases; Critical constants; Classius-Clayperon Equation; Vapor pressure of<br />

Liquids.<br />

Unit II (Lectures 08)<br />

Physical Properties of Liquids: Surface tension - Explanation, Measurement, Effect of temperature on<br />

surface tension, Applications; Viscosity - Definition, Measurement, Applications; Intermolecular forces<br />

in liquids; Hydrogen Bond.<br />

Unit III (Lectures 08)<br />

Thermodynamics and Thermochemistry: First law - Internal Energy, Work and Heat changes,<br />

Enthalpy, reversible changes, maximum work; Heat capacities at constant pressure and volume;<br />

Adiabatic changes; Heat of Reaction; Heat of Formation; Heat of Combustion; Second law - Entropy and<br />

Entropy change for an ideal gas, Gibb’s Free Energy and applications.<br />

Unit IV (Lectures 08)<br />

Phase Rule: Definition and explanation of terms involved in Phase Rule; Derivation of the Phase Rule;<br />

One component systems (water system) and two component system (Ag-Pb and KI-H2O) - Eutectic point<br />

and its significance.<br />

Unit V (Lectures 08)<br />

<strong>Chemical</strong> Kinetics and Catalysis: Order and molecularity of a reaction; Specific reaction rate and its<br />

determination; First Order and Second Order reactions - Half-Life period. Effect of temperature on<br />

reaction rate; Energy of Activation - Elementary treatment of collision theory and activated complex<br />

theory.<br />

Text Books:<br />

1. Samuel Glasstone and David Lewis, Elements of Physical Chemistry, Macmillan & Co.Ltd.,<br />

London.<br />

2. P.W.Atkins, Physical Chemistry (3 rd. Edition), Oxford <strong>University</strong> Press, New Delhi.<br />

Reference Books:<br />

1. Bahl & Tuli, Text Book of Physical Chemistry, S. Chand and Co, New Delhi.<br />

2. Puri, Sharma and Pathania, Principles of Physical Chemistry, VISHAL PUBLISHING Company,<br />

Delhi.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 28


Course Code: ECH-303<br />

Semester-III<br />

APPLIED CHEMISTRY<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

UNIT-I (Lectures 08)<br />

Electrochemistry: Specific, equivalent and molecular conductance and their determination; Debye-<br />

Huckel theory of strong electrolytes; Galvanic cells; Standard cell; Standard electrode potential;<br />

Determination of dissociation constants of acids and bases - Solubility product, Hydrolysis constant,<br />

Hydrogen ion concentration, Complex formation.<br />

UNIT –II (Lectures 08)<br />

Photochemistry: Photochemical Reactions; Laws of Photochemistry.<br />

Reactions and their Mechanism: Types of mechanism; Types of reactions and method of determination<br />

of mechanism.<br />

UNIT-III (Lectures 08)<br />

<strong>Chemical</strong> Bonding: Basic concepts of bonding; Types of bonding - covalent bonding, multiple bonding;<br />

Inductive and field effects and bond energy; Aromaticity and Huckle’s rule of electrons;<br />

Hyperconjugation and Tautomerism; Bonding weaker than covalent, resonance and field effects<br />

UNIT-IV (Lectures 08)<br />

Aromatic Chemistry: Structure of benzene resonance and orbital picture; Orientation and directive<br />

influence of substituents.<br />

Heterocyclic Compounds: Heterocyclic compounds containing one heteroatom - Pyrrole; Thiophene;<br />

Furan, Pyridine and their aromatic character.<br />

UNIT-V (Lectures 08)<br />

Carbohydrates: Introduction; Definition and classification; Structure of glucose and fructose.<br />

Stereochemistry: A brief account of stereochemistry - optical activity and chirality, configuration and<br />

strain.<br />

Text Book:<br />

1. Jerry March, “Organic Chemistry,” John Wiley, New York.<br />

2. Finar, I. L.,“Organic Chemistry,” ELBS, New Delhi.<br />

3. Morrison and Boyd, “Organic Chemistry,” MacMillan, New Delhi.<br />

Reference Books:<br />

1. Glasstone, S., “A Textbook of Physical Chemistry,” MacMillan, New Delhi.<br />

2. Bahl and Tuli, “Essentials of Physical Chemistry,” S. Chand and Co, New Delhi.<br />

Page 29


Course Code: ECH-305<br />

Semester-III<br />

CHEMICAL PROCESS CALCULATIONS<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

UNIT-I (Lectures 08)<br />

Introduction to <strong>Chemical</strong> <strong>Engineering</strong>: Calculations, Definition and Strichiometry - Units and<br />

dimensions, the mole unit, conventions in methods of analysis and measurement, basis, temperature,<br />

pressure, the chemical equation and chemical formulae.<br />

UNIT –II<br />

Gases, Vapours, Liquids and Solids: Ideal gas law and its related calculations; Real gas relationships;<br />

Vapour pressure and liquids;Saturation, partial saturation and humidity; Introduction to vapour-liquid<br />

equilibria for multicomponent systems; Material balances involving condensation and vaporization.<br />

UNIT-III (Lectures 08)<br />

Material Balances: Material balance of physical processes with and without chemical reaction, including<br />

recycle, purge and bypass.<br />

UNIT-IV (Lectures 08)<br />

Energy Balances: Concept and Units; Calculation of enthalpy changes; General balance with and<br />

without reactions; Heats of solution and mixing.<br />

UNIT-V (Lectures 08)<br />

Unsteady-state material and energy balances: Solids, liquids and gaseous fuels; Some industrial<br />

examples of the above; Simple estimation of physical properties (transport, thermodynamic) of fluids and<br />

mixtures.<br />

Text Book:<br />

1. Himmelblau, D. M., “Basic Principles and Calculations in <strong>Chemical</strong> <strong>Engineering</strong>,”<br />

6th ed., Prentice-Hall of India, New Delhi.<br />

2. Bhatt and Vora, “Stoichiometry,” 3rd ed., Tata McGraw-Hill, New Delhi.<br />

3. Hougen, Watson and Ragatz, “<strong>Chemical</strong> Process Principles,” Vol. 1, Asia Publishing House, New<br />

Delhi.<br />

Reference Books:<br />

1. Saha, S. N., “Fundamentals of <strong>Chemical</strong> <strong>Engineering</strong>,” Dhanpat Rai Publishing Co., New Delhi.<br />

Page 30


Semester-III<br />

INDUSTRIAL ENGINEERING<br />

Course Code: EME305 L T P C<br />

3 0 0 3<br />

Objective: To know about productivity, work study, production planning and control techniques in<br />

industry.<br />

Unit I (Lectures 8)<br />

Productivity: Introduction, Definition, Measurement, Productivity index, Productivity improvement;<br />

Types of Production Systems.<br />

Work study: Meaning and benefits of work study, Time & motion study; Micro-motion study Pre<br />

determine motion time study Man machine Diagram flow chart; Motion economy; Method study; Work<br />

measurement; Work sampling; Standard time.<br />

Unit II (Lectures 8)<br />

Plant layout and materials Handling: Plant location; Type of layout; Principles of facility layout;<br />

Principles of material handling; Material Handling equipments.<br />

Production planning and control: Objectives; Forecasting; Product design and development functions;<br />

steps in PPC; Planning routine, scheduling, Dispatching & follow-up; Effectiveness of PPC; Introduction<br />

of JIT.<br />

Unit III (Lectures 8)<br />

Managerial Economics : Introduction; Assumptions; Time Value of money; Step-in Break Even<br />

Analysis; Purpose; Costs: Overheads, Fixed & variable costs; Margin of safety; Angle of incidence;<br />

Profit volume graph.<br />

Depreciation Analysis: Causes; Obsolescence; Methods.<br />

Maintenance Management: Maintenance, Planning & Control; Maintenance Strategy.<br />

Unit IV (Lectures 8)<br />

Inventory Control: Inventory; Function; Cost; Deterministic models; Introduction to MRP; Supplychain<br />

Management<br />

Quality Control: Introduction; Process control; SQC control Charts; Single, double & sequential<br />

sampling; Introduction to TQM & bench marking.<br />

Unit V (Lectures 8)<br />

Industrial Ownership: Proprietorship; Partnership; Joint stock & co-operative stores.<br />

Manpower Planning: Process.<br />

Organization: Principles of organization; Development of Organizational charts like line, staff, line and<br />

staff & Functional types.<br />

Job Evaluation & Merit rating: Job analysis; Job description; Job simplification and job evaluation<br />

methods & description; Merit rating; Wage incentive plans.<br />

Text Books<br />

1. Koontz H. Donnel C.O., Principles of Management: An Analysis of Management Functions, Tata<br />

McGraw Hill.<br />

2. Moore J., Manufacturing Management”, Prentice Hall.<br />

3. Mahajan, Industrial <strong>Engineering</strong>, Dhanpat Rai & Sons.<br />

Reference Books<br />

1. Khanna O.P., Industrial <strong>Engineering</strong> & Management, Dhanpat Rai & Sons .<br />

2. Shanker. Ravi, Industrial <strong>Engineering</strong>, Galgotia Publications.<br />

3. Buffa E.S., Modern Production Operations Management, Wiley Eastern<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 31


Semester-III/IV<br />

MATHEMATICS-III<br />

Course Code: EAS301/EAS 401 L T P C<br />

3 1 0 4<br />

Unit I (Lectures 08)<br />

Integral Transforms: Fourier integral, Fourier complex transform, Fourier sine and cosine transforms and<br />

applications to simple heat transfer equations.<br />

Z – Transform and its application to solve difference equations.<br />

Unit II (Lectures 08)<br />

Functions of a Complex Variable: Analytic functions; C-R equations and harmonic functions; Line<br />

integral in the complex plane; Cauchy's integral theorem, Cauchy's integral formula for derivatives of<br />

analytic functions; Liouvilles theorem.<br />

Unit III (Lectures 08)<br />

Functions of a Complex Variable II: Representation of a function by power series; Taylor's and<br />

Laurent's series; Singularities, zeroes and poles; Residue theorem, evaluation of real integrals; conformal<br />

mapping and bilinear transformations.<br />

Unit IV (Lectures 08)<br />

Statistical Techniques: Moments, Moment generating functions, Skewness, Kurtosis, Curve Fitting and<br />

Solution of Equations: Method of least squares and curve fitting of straight line and parabola, Solution of<br />

cubic and bi-quadratic equations, Correlation and Regression, Binomial distribution, Poisson distribution,<br />

Normal distribution.<br />

Unit V (Lectures 08)<br />

Numerical Technique: Bisection method, Regula – Falsi method, Newton - Raphson method.<br />

Interpolation: Finite difference, Newton’s forward and backward interpolation, Lagrange’s and<br />

Newton’s divided difference formula for unequal intervals; Numerical Differentiation, Numerical<br />

Integration; Trapezoidal, Simpson’s 1/3 and 3/8 rule.<br />

Text Books<br />

1. Grewal B.S., Higher <strong>Engineering</strong> Mathematics, Khanna Publishers.<br />

2. Prasad C., <strong>Engineering</strong> Mathematics for Engineers, Prasad Mudralaya.<br />

3. Das H.K., <strong>Engineering</strong> Mathematics Vol-II, S. Chand.<br />

Reference Books<br />

1. Kreyszig E., Advanced <strong>Engineering</strong> Mathematics, Wiley Eastern.<br />

2. Piskunov N, Differential & Integral Calculus, Moscow Peace Publishers.<br />

3. Narayan Shanti, A Text book of Matrices, S. Chand.<br />

4. Bali N.P., <strong>Engineering</strong> Mathematics-III, Laxmi Publications.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 32


Semester-III/IV<br />

PHYSICS II<br />

Course Code: EAS302/EAS 402 L T P C<br />

3 1 0 4<br />

Objective: To understand modern physics like nanotechnology, cryogenics etc.<br />

Course Contents<br />

Unit I (Lectures 08)<br />

Relativistic Mechanics: Inertial and Non- inertial Frames; Michelson-Morley Experiment;<br />

Postulates of Special Theory of Relativity; Galilean and Lorentz Transformation; Length Contraction<br />

and Time Dilation; Addition of Velocities; Mass Energy Equivalence and Variation of Mass with<br />

Velocity.<br />

Unit II (Lectures 08)<br />

Modern Physics: Bragg’s Law; Compton Effect; Wave Particle Duality; De Broglie matter wave;<br />

Davisson and Germer's Experiment; Phase and Group velocities; Uncertainty Principle and<br />

application.<br />

Unit III (Lectures 08)<br />

Quantum Mechanics II : Physical Interpretation of Wave Function and its Normalization;<br />

Expectation Value; Schrodinger Equation in One Dimension; Solutions of Time-Independent<br />

Schrodinger Equation for Free Particle; Particle in an Infinite Square Well; Potential Barrier and<br />

Tunneling; Hydrogen atom (qualitative<br />

Unit IV (Lectures 08)<br />

Superconductivity: Temperature dependence of resistivity; Meissner effect; Penetration depth; Type<br />

I and Type II superconductors; Temperature dependence of critical filed; BCS theory of<br />

superconductors; applications of superconductors.<br />

Introduction to Nanomaterials: Basic principles of nanoscience and technology; creation and use of<br />

buckyballs; properties and use of carbon nanotubes; applications of nanomaterials.<br />

Unit V (Lectures 08)<br />

Vacuum Physics: Mean free path; rotary and diffusion pumps; Pirani and Penning Gauges.<br />

Nuclear Physics: Nuclear Forces; Binding Energy; Liquid Drop Model; Fission; Nuclear Reactors;<br />

Fusion and Energy Processes in Stars, Controlled Thermonuclear Reactions.<br />

Text Books:<br />

1. Robert Resmick, Introduction to Special Theory of Relativity, Wiley.<br />

2. A. Beiser, Perspectives of Modern Physics, McGraw Hill.<br />

3. R. Booker and E. Boysen, Nanotechnology, Wiley.<br />

4. G. G. Haselden, Cryogenic Fundamentals, Academic Press.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 33


Course Code: ECH-351<br />

Semester-III<br />

CHEMICAL ENGINEERING THERMODYNAMIC-I (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

1. To find indicated power of four stroke petrol engine by Morse Test.<br />

2. To prepare heat balance sheet of petrol engine test ring.<br />

3. To prepare the heat balance sheet for diesel engine test ring.<br />

4. To identify the differences between two stroke and four stroke S.I. engine.<br />

5. To determine the calorific value of a liquid fuel using Bomb Calorimeter.<br />

6. To determine the calorific value of a liquid fuel using Gas Calorimeter.<br />

7. To find out the COP (Coefficient of Performance) of a Vapour Compression Refrigeration<br />

system.<br />

8. To study the working of velocity compounded Steam Turbine.<br />

9. Study of steam Engine model.<br />

10. Study of Gas Turbine Model<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 34


Semester-III<br />

PHYSICAL CHEMICAL TECHNOLOGY (LAB)<br />

Course Code: ECH-352<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

1. To study the adsorption of acetic acid on dispersed charcoal.<br />

2. To determine pH of a solution using pH-meter and pH-metric titration.<br />

3. Determination of the strength of HCl solution using a standard solution of Sodium Hydroxide pH<br />

metrically.<br />

4. To find out the rate constant for the inversion of sugar cane in acid medium and to show that<br />

inversion follows the first order kinetics.<br />

5. To estimate Mohrs salt by titrating against a standard solution of potassium dichromate<br />

potentiometrically.<br />

6. To determine the partition coefficient of iodine between carbon tetrachloride and water.<br />

7. To determine the reaction rate constant of an acid catalyzed hydrolysis of an ester- titrimetry.<br />

8. To determine the coefficient of viscosity of the given liquid at room temperature by using<br />

Ostwald’s viscometer.<br />

9. To determine the surface tension of the given liquid by drop number method.<br />

10. To find out the molecular weight of a given substance by Rast’s camphor method.<br />

11. To determine the solubility of potassium nitrate at different temperatures.<br />

12. To determine the transition temperature of Glauber’s salt by thermometric method.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 35


Course Code: ECH-353<br />

Semester-III<br />

APPLIED CHEMISTRY (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

1. Estimation of Glucose.<br />

2. Freundlich adsorption isotherm verification.<br />

3. Conductivity: (i) Conductivity titration strength of strong acid vs. strong base, (ii) Dissociation<br />

constant of a weak acid (CH3COOH).<br />

4. Applications of TLC in the organic chemistry.<br />

5. Determination of dissolved oxygen percent in a given water sample (Winkler’s method)<br />

6. Determination of iron by spectrophotometric method.<br />

7. Determination of the strength of HCl solution using a standard solution of sodium hydroxide p H<br />

metrically.<br />

8. Estimation of mohrs salt by titrating against a standard solution of potassium dichromate<br />

potentiometrically.<br />

9. Determination of conductance of a given sample of water with a conductivity meter.<br />

10. Determination of partition coefficient of iodine between carbon tetrachloride and water.<br />

11. Determination of reaction rate constant of an acid catalyzed hydrolysis of an ester.<br />

12. Determination of the coefficient of viscosity of the given liquid by Ostwald viscometer.<br />

13. Identification of organic compounds in the mixture.<br />

14. Functional group test of organic compounds.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 36


Course Code: ECH-401<br />

Semester-IV<br />

HEAT TRANSFER<br />

L T P C<br />

3 0 0 3<br />

Unit – I (Lectures 08)<br />

Introduction: Modes of heat transfer - Conduction, convection, radiation.<br />

Steady-State Conduction in One Dimension: Fourier’s Law; Thermal conductivity; Steady-state<br />

conduction of heat through a single and composite solid - cylinder and sphere; Steady-state heat<br />

conduction in bodies with heat sources - plane wall, cylinder and sphere.<br />

Heat Transfer Coefficient: Convective heat transfer and the concept of heat transfer coefficient; Overall<br />

heat transfer coefficient; Heat transfer from extended surfaces; Thermal contact resistance; Critical and<br />

optimum insulation thickness.<br />

Unit – II (Lectures 08)<br />

Forced Convection: Flow over a flat plate; Thermal boundary layer; Flow across a cylinder;<br />

Dimensional analysis - Buckingham Pi theorem, Dimensionless groups in heat transfer; Correlations for<br />

the heat transfer coefficient - Laminar flow through a circular pipe, turbulent flow through a non-circular<br />

duct, flow over flat plate, flow across a cylinder, flow past a sphere, flow across a bank of tubes, heat<br />

transfer coefficient in a packed and fluidized bed; Double-pipe heat exchanger in parallel and countercurrent<br />

flow.<br />

Free Convection: Introduction; Heat transfer correlations for free convection - flat surface, cylinder,<br />

sphere, enclosure; Combined free and forced convection.<br />

Unit – III (Lectures 08)<br />

Boiling and Condensation: Boiling phenomenon; Nucleate boiling; Correlations for pool boiling heat<br />

transfer - Nucleate boiling, critical heat flux, stable film boiling; Forced convection boiling;<br />

Condensation phenomena - Film condensation on a vertical surface, turbulent film condensation,<br />

condensation outside a horizontal tube and tube bank, Condensation inside a horizontal tube, effect of<br />

non-condensable gases, Dropwise condensation.<br />

Unit – IV (Lectures 08)<br />

Radiation Heat Transfer: Basic concepts of radiation from a surface - Black body radiation, Planck’s<br />

Law, Wien’s Displacement Law, Stefan-Boltzmann Law, Kirchoff’s Law, Gray body; Radiation intensity<br />

of a black body; Spectral emissive power of a black body over a hemisphere; Radiation heat exchange<br />

between surfaces – the view factor; Radiation exchange between black bodies and between diffuse gray<br />

surfaces.<br />

Unit – V (Lectures 08)<br />

Heat Exchangers: Construction of a shell and tube heat exchanger; Fouling of a heat exchanger; LMTD;<br />

Temperature distribution in multi-pass heat exchangers; Individual heat transfer coefficients and their<br />

relations with overall H.T. coefficients; Types of shell and tube heat exchanger.<br />

Evaporators: Types of evaporators – Natural circulation evaporators, forced circulation evaporators,<br />

falling film evaporators, climbing film evaporators, agitated thin film evaporators and plate evaporators;<br />

Principles of evaporation and evaporators; Single and multiple effect evaporators; Capacity and<br />

economy; Boiling point rise; Enthalpy balance of a solution; Calculations of single effect and multieffect<br />

evaporators; Methods of feeding to multieffect evaporators.<br />

Unsteady-State Heat Conduction: Mathematical formulations and initial and boundary conditions;<br />

Analytical solution; Numerical solution.<br />

Text Books:<br />

1. Dutta, B. K., “Heat Transfer: Principles and Applications,” PHI, New Delhi,<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 37


2001.<br />

2. Holman, J. P., “Heat Tansfer,” 8th ed., McGraw-Hill,New Delhi<br />

3. A.J. Chapman, “Heat Transfer,” Maxwell Macmillan, 1984. New Delhi<br />

4. Kern D.Q., “Process Heat Transfer”, Tata McGraw Hill, 1950. New Delhi<br />

Reference Books:<br />

1. Hewitt, G. F., Shires, G.L. and Bott, T. R., “Process Heat Transfer”, CRC Press,1994, New Delhi<br />

2. Rao, Y. V. C., “Heat Transfer”. New Age International, Delhi<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 38


Course Code: ECH-402<br />

Semester-IV<br />

INORGANIC CHEMICAL TECHNOLOGY<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I (Lectures 08)<br />

Water: Sources of water; Hardness; Treatment for different end-uses; Municipal water conditioning;<br />

Industrial waste and water treatment.<br />

Unit – II (Lectures 08)<br />

Sulphur and sulphuric acid: Sources of sulphur; Sulphuric acid; Different processes of manufacturing -<br />

Contact process, DCDA process.<br />

Nitrogen based compounds: Manufacture of ammonia; Nitric acid; Urea and ammonium nitrate.<br />

Unit – III (Lectures 08)<br />

Phosphorous and phosphoric acid: Methods for production of phosphorous and phosphoric acid;<br />

Manufacture of super phosphate and triple super phosphate.<br />

Chloro-alkali : - Manufacture of soda ash; Caustic soda and chlorine.<br />

Unit – IV (Lectures 08)<br />

Cement: Types of cement; Manufacture of ordinary Portland cement; Slag cement.<br />

Fuel and industrial gases: Production of water gas; producer gas and coke oven gas; Production of<br />

acetylene, oxygen and nitrogen.<br />

Unit – V (Lectures 08)<br />

Metallurgy: Manufacture of pig iron; Cast iron; Methods of making steel - open hearth process;<br />

Production of aluminium by electrolytic process.<br />

Textbooks:<br />

1. Gopala Rao, M & Marshall Sitting, “Dryden’s Outlines of <strong>Chemical</strong> Technology” .Affiliated East<br />

West Press Pvt. Ltd. New Delhi<br />

2. Austin, G.T., “Shreve’s <strong>Chemical</strong> Process Industries” McGraw Hill Book. New Delhi<br />

Reference Books:<br />

1. Kirk, R.E. & Othmer, D.F.“ Encyclopedia of <strong>Chemical</strong> Technology” John Wiley. New Delhi.<br />

Page 39


Semester-IV<br />

MATERIAL SCIENCE AND TECHNOLOGY<br />

Course Code: ECH-403<br />

L T P C<br />

3 0 0 3<br />

Unit- I (Lectures 08)<br />

Introduction to Materials<br />

<strong>Engineering</strong> materials - Classification, Characteristics and basic principles for their selection; Structure of<br />

atom; Types of bonds; Crystal structure - Defects in crystal structure and their influence on properties of<br />

a material.<br />

Unit- II (Lectures 08)<br />

Metals and Their Alloys<br />

Phase equilibrium diagram for Iron-carbon and Copper-zinc system; Ferrous and nonferrous alloys; Mild<br />

steels; Special steels; Stainless steels; Brasses; Bronzes; Aluminum alloys; Titanium alloys; Methods for<br />

fabrications - Rolling, Forging, Extrusion and Joining.<br />

Unit- III (Lectures 08)<br />

Polymers<br />

Types of plastics; Structure; Properties; Correlations of important plastics; Polymerization processes and<br />

additives; Fibre-reinforced plastics; Rubbers & elastomers and Applications.<br />

Unit- IV (Lectures 08)<br />

Ceramics and Glass<br />

Structure – Properties, Correlations, Oxide and non-oxide ceramics, Vitreous and borosilicate glasses,<br />

glass-ceramics and enamels; Major electrical, optical and mechanical properties of ceramics and glasses;<br />

Enameling and glass lining.<br />

Unit- V (Lectures 08)<br />

Corrosion and its Control<br />

Types of corrosion; <strong>Chemical</strong> and electrochemical reactions; Methods of corrosion prevention;<br />

Corrosion-resistant materials.<br />

Text Books:<br />

1. James, F. Shackelford, “Introduction to Materials Science”, Macmillan Pub. Co., NY, 1990<br />

2. Jestrazebaski, D.Z., “ Properties of <strong>Engineering</strong> Materials”, 3rd ed., Toppen Co. Ltd.<br />

3. Smith, W. F., “Foundations of Materials Science and <strong>Engineering</strong>,” 2nd ed., McGraw-Hill, 1993.<br />

Reference Books:<br />

1. Raghavan, V., “Materials Science and <strong>Engineering</strong>,” PHI, New Delhi.<br />

2. Van Vlack, L. H., “Materials Science and <strong>Engineering</strong>,” Addison Wesley. New Delhi.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 40


Semester-IV<br />

CHEMICAL ENGINEERING THERMODYNAMICS-II<br />

Course Code: ECH-404<br />

L T P C<br />

3 0 0 3<br />

Unit – I (Lectures 08)<br />

Review: First and second laws of thermodynamics<br />

Volumetric Properties of Pure Fluids: PVT behavior of pure substances; Virial equation and its<br />

applications; Cubic equations of state; Generalized correlations for gases and liquids.<br />

Heat Effects: Sensible heat effect; Heat effects accompanying phase changes of pure substances;<br />

Standard heats of reaction, formation and combustion; Effect of temperature on the standard heat of<br />

reaction.<br />

Unit – II (Lectures 08)<br />

Thermodynamic Properties of Fluids: Fundamental relations; Maxwell’s equations; Residual<br />

properties; Clapeyron’s Equation; Generalized correlations for thermodynamic properties of gases.<br />

Unit – III (Lectures 08)<br />

Multicomponent Systems: <strong>Chemical</strong> potential; Ideal-gas mixture; Ideal solution; Raoult’s Law; Partial<br />

properties; Fugacity and fugacity coefficient; Generalized correlations for the fugacity coefficient; Excess<br />

Gibbs’ energy; Activity coefficient.<br />

Unit – IV (Lectures 08)<br />

Phase Equilibria at low to moderate pressures - Phase rule, Phase behavior for vapor liquid systems;<br />

Margules equation; Van laar equation; Wilson equation; NRTL equation; Dew point; Bubble point and<br />

flash calculations.<br />

Solution Thermodymics: Ideal solution; Fundamental residual – property relation; Fundamental excess<br />

– property relation; Evaluation of partial properties; Heat effects of mixing processes; Partially miscible<br />

systems.<br />

Unit – V (Lectures 08)<br />

<strong>Chemical</strong> Reaction Equilibria: Reaction coordinate; Equilibrium criteria to chemical reactions;<br />

Standard Gibbs’ energy change and the equilibrium constant; Effect of temperature on the equilibrium<br />

constant; Evaluation of equilibrium constants; Relations between equilibrium constants and compositions<br />

- gas-phase reactions, liquid- phase reactions; Calculation of equilibrium compositions for single-phase<br />

reactions; Multireaction equilibria.<br />

Text Books:<br />

1. McCabe, W.L., Smith, J.C., and Harriott, P., “Unit Operations of <strong>Chemical</strong> <strong>Engineering</strong>”, 6th ed.,<br />

McGraw Hill. New Delhi<br />

2. Brown, G. G., et al, “Unit Operations,” CBS Publications, Delhi.<br />

3. Coulson, J. H. and Richardson, J. F., “<strong>Chemical</strong> <strong>Engineering</strong>,” Vol. 2, Asian Books<br />

Private Ltd., New Delhi.<br />

Reference Books:<br />

1. Perry, R. H., et al, “<strong>Chemical</strong> Engineers’ Handbook,” 7th ed., McGraw-Hill. New Delhi.<br />

2. Foust, A.S., et al., “Unit Operations”, 2nd ed., John Wiley. New Delhi.<br />

3. Bhattacharya, “Unit Operations”, Vol. 1., Khanna Publishers. New Delhi.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 41


Semester-IV<br />

NUMERICAL METHODS IN CHEMICAL ENGINEERING<br />

Course Code: ECH-405<br />

L T P C<br />

3 1 0 4<br />

Unit – I (Lectures 08)<br />

Linear Algebraic Equations: Introduction; Gauss-Elimination; Gauss-Siedel and LU Decomposition<br />

Methods; Thomas’ algorithm.<br />

Eigen Values and Eigen Vectors of Matrices: Introduction; Fadeev Leverrier’s method; Power method;<br />

Householder’s and Givens’ method.<br />

Unit – II (Lectures 08)<br />

Nonlinear, Algebraic Equations: Single variable and multivariable successive substitution method;<br />

Single variable and multivariable Newton-Raphson technique; Polynomial root finding methods.<br />

Unit – III (Lectures 08)<br />

Ordinary Differential Equations: Initial Value Problems; Explicit Adams–Bashforth technique;<br />

Implicit Adams-Moulton technique; Predictor-corrector technique; Runge-Kutta method; Stability of<br />

algorithms.<br />

Unit – IV (Lectures 08)<br />

Ordinary Differential equations: Boundary Value Problems; Finite difference technique; Orthogonal<br />

collocation (OC); Orthogonal collocation on finite Elements (OCFE); Galerkin Finite Element (GFE)<br />

technique; Shooting techniques.<br />

Unit – V (Lectures 08)<br />

Partial differential Equations: Partial Differential Equations (PDE); Classification of PDE; Finite<br />

difference technique (Method of lines); Orthogonal collocation; Case Studies; Use of spreadsheets in<br />

<strong>Chemical</strong> <strong>Engineering</strong>.<br />

Text Books:<br />

1. Gupta, S.K., “Numerical Methods for Engineers”, New Age International Ltd. New Delhi,1995.<br />

Reference Books:<br />

1. Hanna, O.T. and Sandall, O.C., “Computational Methods in <strong>Chemical</strong> <strong>Engineering</strong>” Prentice-Hall,<br />

New Delhi 1975.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 42


Course Code: ECH-451<br />

Semester-IV<br />

HEAT TRANSFER (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

1. To determine total thermal resistance and thermal conductivity of composite wall.<br />

2. To determine the thermal conductivity of a metal rod.<br />

3. To determine the natural convective heat transfer coefficient for a vertical tube.<br />

4. To determine critical heat flux point for pool boiling of water.<br />

5. To determine forced convective heat transfer coefficient for air flowing through a pipe.<br />

6. To determine over-all heat transfer coefficient in double pipe heat exchanger.<br />

7. To study temperature distribution along the length of a pin fin under natural and forced<br />

convection conditions.<br />

8. To determine Stefan-Boltzmann constant.<br />

9. To determine emissivity of a given plate at various temperatures.<br />

10. To determine radiation constant of a given surface.<br />

11. To study shell and tube heat exchanger.<br />

12. Estimation of unsteady state film heat transfer coefficient between the medium in which the body<br />

is cooled.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 43


Course Code: ECH-452<br />

Semester-IV<br />

INORGANIC CHEMICAL TECHNOLOGY (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

1. To analyze the given inorganic mixture containing five radicals by semi micro technique.<br />

2. To find out the chemical oxygen demand of a waste water sample using potassium dichromate.<br />

3. To determine the chlorine concentration in a supplied water sample using silver nitrate method.<br />

4. To find out the strength of the supplied magnesium salt solution using EDTA as an intermediate<br />

solution.<br />

5. To find out the strength of the supplied calcium salt solution using EDTA as an intermediate<br />

solution by substitution method.<br />

6. To determine the carbon dioxide content in polluted water.<br />

7. To estimate barium as barium sulphate from the solution of barium chloride.<br />

8. To prepare the micro-cosmic salt.<br />

9. To prepare sodium thiosulphate by using sodium sulphate with powdered roll sulphur.<br />

10. To prepare tetra ammine copper (II) sulphate.<br />

11. To determine the percentage of available chlorine in a given sample of bleaching powder.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 44


Course Code: ECH-501<br />

Semester-V<br />

PROCESS INSTRUMENTATION<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Introduction, general principles of measurement, its classification by physical characteristics, direct and<br />

inferential measurement.<br />

(Lectures 08)<br />

Unit – II<br />

Static and dynamic characteristics of instruments. Measurement of temperature, pH, pressure, vacuum,<br />

flow rate, liquid level, differential pressure<br />

(Lectures 08)<br />

Unit – III<br />

Viscosity, conductivity, nuclear radiation, humidity and gas composition, spectroscopy.<br />

(Lectures 08)<br />

Unit – IV<br />

Classification of sensors and transducers. Building blocks of an instrument, transducer, amplifier signal<br />

conditioner, signal isolation, transmission, display, data acquisition modules, interfaces, recording.<br />

(Lectures 08)<br />

Unit – V<br />

Control centre, instrumentation diagram, On line instrumentation in modern plants.<br />

Text Books:<br />

1. Nakra, “Instrumentation, Measurement and Analysis”; Tata McGraw Hill,<br />

New Delhi.<br />

2. Patranabis, D., “Principles of Industrial Instrumentation” 2nd ed. Tata McGraw<br />

Hill, New Delhi.<br />

3. Eckman, D.P., “Industrial Instrumentation” Wiley Eastern, 1978.<br />

4. Liptak, B.G., “Industrial Engineers’ Handbook” Vol.1 and 2, CRC Press,<br />

1994.<br />

Reference Books:<br />

1. Andrew, W.G., et al., “Applied Instrumentation in the Process Industries,”<br />

Gulf Pub.1993.<br />

2. Wightman, E.J., “Instrumentation in Process Control,” Butterworth, 1972.<br />

3. Doebelin, E., “Measurement Systems: Applications and Design,” 4th ed.,<br />

McGraw Hill, 1990<br />

(Lectures 08)<br />

Page 45


Course Code: ECH-502<br />

Semester-V<br />

ORGANIC CHEMICAL TECHNOLOGY<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit I<br />

Coal and Coal chemicals: Types of coal, different uses, distillation of coal, treatment of products, low<br />

and high temperature carbonization of coal, coal tar distillation,<br />

Petroleum: Origin, classification, composition of crude oil, production of crude oil, distillation of crude<br />

petroleum, refining-methods, uses of products, (Lectures 08)<br />

Unit II<br />

Extraction of vegetable oils: Purification, acid value, hydrogenation of oils,<br />

Iodine value: Manufacture of fatty acids and soaps, saponification value, detergents- classification and<br />

manufacture. (Lectures 08)<br />

Unit III<br />

Paints and varnishes: Constituents of paints, functions of paint, manufacturing procedures, Pigmentsmanufacture<br />

of lithophone, varnishes, (Lectures 08)<br />

Unit IV<br />

Manufacture of pulp: Kraft process and sulphite process, production of paper.<br />

Manufacture of cane sugar: Refining, manufacture of starch, dextrin and dextrose, production of<br />

ethanol by fermentation, manufacture of pencillin, (Lectures 08)<br />

Unit V<br />

Polymerisation: Different methods, manufacture of polyethylene, phenol formaldehyde, SBR, synthetic<br />

fibres, rayon, 6-nylon, 6,6-nylon, polyesters. (Lectures 08)<br />

Text books:<br />

1.`Dryden’s out lines of chemical Technology’ by Gopala Rao, M. & Marshall Sitting, .Affilated East<br />

West Press Pvt.Ltd.<br />

2.`Shreve’s <strong>Chemical</strong> Process Industries’ Austin,G.T,,. Mcgraw Hill Publishers<br />

Reference book:<br />

1.`Encyclopedia of <strong>Chemical</strong> Technology’ by Kirk.R.E & othmer,D.F., Inter Science.<br />

Page 46


Course Code: ECH-503<br />

Semester-V<br />

MASS TRANSFER – I<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Diffusion phenomenon: Molecular and eddy diffusion in gases, liquids and solids, interface mass<br />

transfer Mass transfer theories: Film theory penetration theory and surface renewal theory.<br />

(Lectures 08)<br />

Unit – II<br />

Concept of Mass transfer coefficient: Individual and film coefficients, overall mass transfer co-efficient<br />

and their inter relationships. Continuous contact and differential contact, mass transfer concepts of NTU<br />

and HTU, their inter relationship.<br />

Interphase Mass Transfer: Equilibrium, diffusion between phases, material balances, stages and<br />

concept of operating line and tie line.<br />

(Lectures 08)<br />

Unit – III<br />

Equipment for gas liquid contact: Sparged vessel, mechanically agitated vessel, tray towers, venture<br />

scrubber, wetted wall towers, spray towers and packed towers, tray tower vs packed tower.<br />

Absorption: Absorption in continuous contact columns, Co-current, Counter current and cross current<br />

contacting of fluids, calculation of NTU and HTU, concept of HETP.<br />

(Lectures 08)<br />

Unit – IV<br />

Adsorption: Adsorption theories, types of adsorbent, activated carbon silica, silica and molecular sieves,<br />

Batch and column adsorption. Break through curves, gas adsorption, BDST models for adsorption<br />

calculation.<br />

(Lectures 08)<br />

Unit – V<br />

Drying: Equilibrium mechanism theory of drying, drying rate curve, Batch and continuous drying,<br />

working principle of different types of dryers such as tray driers, Drum dryers, spray and tunnel dryers.<br />

(Lectures 08)<br />

Text Books:<br />

1. Treybal, R.E.; “Mass Transfer Operation”, McGraw-Hill, 1980.<br />

2 King, C.J. “Separation Processes”, McGraw – Hill, NY.<br />

3 Smith, B.D., “Design of Equilibrium stage Processes”, McGraw-Hill, NY<br />

Reference Books:<br />

1. McCabe, W.L. Smith, J.C. and Harriot, P., “Unit Operations of <strong>Chemical</strong> <strong>Engineering</strong>”, 6th ed,<br />

McGraw-Hill, NY.<br />

2. Coulson, J.M. and Richardson, J.F., “<strong>Chemical</strong> <strong>Engineering</strong>”, Vol. I and II, Asian<br />

Books Pvt., New Delhi..<br />

Page 47


Course Code: ECH-504<br />

Semester-V<br />

SPECTROSCOPY TECHNIQUES<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Components of instruments for optical spectroscopy : Components and configuration of instruments<br />

for optical spectroscopy, radiation sources, sample contains, radiation detection, signal processor and<br />

vadouts.<br />

An Introduction to absorption Spectroscopy : Terms employed in absorption spectroscopy,<br />

quantitative aspects of absorption measurements (Lectures 08)<br />

Unit – II<br />

Application of Ultraviolet and visible Spectroscopy: Absorption species, typical instruments,<br />

application of absorption measurements to qualitative and quantitative Measurement.<br />

Infra Red Absorption Spectroscopy : Theory of infrared absorption, infrared instruments qualitative<br />

and quantitative application. (Lectures 08)<br />

Unit – III<br />

Raman Spectroscopy: Theory of Raman spectroscopy, instrumentation application of Raman<br />

spectroscopy<br />

Nuclear Magnetic Resonance Spectroscopy : Theory of instrumentation of NMR, application of protein<br />

NMR to analysis of compounds. (Lectures 08)<br />

Unit – IV<br />

Mass Spectroscopy : Theory of Flame Spectroscopy, flame characteristics, atomizer for<br />

atomic spectroscopy atomic absorption spectroscopy. (Lectures 08)<br />

Unit – V<br />

Atomic Spectroscopy : Theory of Flame Spectroscopy, flame characteristics, atomizer for<br />

atomic spectroscopy, atomic absorption spectroscopy. (Lectures 08)<br />

Text Books:<br />

1. D. Holen and H.Peck, “Analytical Biochemistry” Longman, 1983.<br />

Reference Books:<br />

1. Wilson and J. Walker, “Practical Biochemistry” <strong>University</strong> Press, 2000<br />

Page 48


Course Code: ECH-505<br />

Semester-V<br />

ENVIRONMENTAL ENGINEERING<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Atmosphere- Introduction, structure of the atmosphere, chemical and photochemical reaction in the<br />

atmosphere, primary air pollutants-sources. Carbon, Nitrogen & Sulfur Cycle. (Lectures 08)<br />

Unit – II<br />

Wastewater Treatment: Characterization of industrial wastewater, primary, secondary and tertiary<br />

treatment. Segregation, screening, equalization, coagulation, flocculation, precipitation, flotation,<br />

sedimentation, aerobic treatment, anaerobic treatment, absorption, ion exchange, membrane filtration,<br />

electrodialysis, sludge dewatering and disposal methods. (Lectures 08)<br />

Unit – III<br />

Air Pollution Control: Sources and classification of air pollutants, nature and characteristics of gaseous<br />

and particulate pollutants, from automobiles. Air pollution meteorology, plume and its behavior and<br />

atmospheric dispersion, control of particulate emission by gravity settling chamber, cyclones , wet<br />

scrubbers, bag filters and electrostatic precipitators (General Explanation). Control of gaseous<br />

emission by absorption, adsorption, chemical transformation and combustion.<br />

(Lectures 08)<br />

Unit – IV<br />

Solid Waste Management: solid waste, waste disposal methods, recycling of solid waste and its<br />

management. Hazardous and non-hazardous waste, methods of treatment and disposal, land filling,<br />

leachate treatment and incineration of solid wastes. (Lectures 08)<br />

Unit – V<br />

Environmentally Pollution Monitoring Legislation, standards for water and air, Effects of air pollutants<br />

on human health, vegetation and materials, Air pollution monitoring instruments COx, NOx, SOx,<br />

Hydrocarbon and Ozone. Hydrocarbons particulates, sampling techniques. Global warming, Green house<br />

effect, depletion of ozone layer, human activity and meteorology.<br />

(Lectures 08)<br />

Text Books:<br />

1. Dhameja, S.K., “Environmental <strong>Engineering</strong> and Management”, S.K. Kataria & Sons,<br />

Delhi, 2002.<br />

2. Masters, G.M., “Introduction to Environmental <strong>Engineering</strong> and Science”, Prentice Hall of<br />

India, New Delhi, 2001.<br />

3. Bhatia, S.C., “Environmental Pollution and Control in <strong>Chemical</strong> Process Industries”,<br />

Khanna Publishers, Delhi, 2001.<br />

Reference Books:<br />

1. Pandey G.N. and Karney, “Environmental <strong>Engineering</strong>” Tata McGraw Hill, Delhi.<br />

2. Instrumentation by Khandpur. Metcalf & Eddy, Inc., “Wastewater <strong>Engineering</strong>: Treatment and<br />

Reuse”, 4th ed., Tata McGraw Hill, New Delhi, 2003.<br />

3. Modi, P.N. “Sewage Treatment and disposal and Waste Water <strong>Engineering</strong>,” Vol.II, Standard<br />

book house, Delhi, 2001.<br />

Page 49


Semester V<br />

<strong>Engineering</strong> and Managerial Economics<br />

Course Code: EHM503<br />

L T P C<br />

3 0 0 3<br />

Objective:<br />

• To understand the Scope of Economics, Demand Forecasting and Market Study.<br />

Unit-I<br />

Introduction: Meaning, Nature and Scope of Economics, Meaning of Science, <strong>Engineering</strong> and<br />

Technology; Managerial Economics and its scope in engineering perspective.<br />

Unit-II<br />

Demand: Basic Concepts Demand Analysis, Law of Demand, Determinates of Demand; Elasticity of<br />

Demand-Price; Income and cross Elasticity; Uses of concept of elasticity of demand in managerial<br />

decision.<br />

Unit-III<br />

Forecasting: Demand forecasting Meaning, significance and methods of demand forecasting; production<br />

function; Laws of returns to scale & Law of Diminishing returns scale.<br />

Short and Long run Cost curves: fixed cost, variable cost, average cost, marginal cost, Opportunity<br />

cost.<br />

Unit-IV<br />

Market Study: Market Structure Perfect Competition; Imperfect competition: Monopolistic, Oligopoly,<br />

Duopoly sorbent features of price determination and various market conditions.<br />

Unit-V<br />

Inflation: National Income; Inflation and Business Cycles Concept of N.I. and Measurement; Meaning<br />

of Inflation; Type causes & prevention methods; Phases of business cycle.<br />

Text Books:<br />

1. Koutsoyiannis, A : Modern Microeconomics, ELBS.<br />

2. Kakkar, D.N., Managerial Economics for <strong>Engineering</strong>, New Age International Publication.<br />

Reference Books:<br />

1. Dwivedi, D.N., Managerial Economics, Vikas Publishing.<br />

2. Maheshwari, Y., Managerial Economics, Prentice Hall of India.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 50


Course Code: ECH-551<br />

Semester-V<br />

PROCESS INSTRUMENTATION (LAB)<br />

1. Calibration of thermocouple.<br />

2. Calibration of Bimetallic thermocouple.<br />

3. Calibration of Resistance thermocouple.<br />

4. Calibration of Pressure gauge.<br />

5. Calibration of Pnuematic pressure recorder.<br />

6. Calibration of Differential pressure recorder.<br />

7. Calibration of Orificemeter<br />

8. Calibration of Venturimeter / Rotameter/ Gas flow meter.<br />

9. Estimation of viscosity by Redwood/ Saybolt/<br />

10. Estimation of viscosity by Ostwald viscometer.<br />

11. Calibration of pH meter.<br />

12. Calibration of Conductivity meter.<br />

13. Calibration of Turbidity meter.<br />

14. Estimation of surface tension by Tensiometer.<br />

Evaluation of Practical Examination:<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 51


Course Code: ECH-552<br />

Semester-V<br />

ORGANIC CHEMICAL TECHNOLOGY (LAB)<br />

A. Analysis of water:<br />

1. Total solids, dissolved solids,pH<br />

2. Chlorides and sulphates<br />

3. Temporary, permanent and total hardness.<br />

B. Analysis of oils:<br />

4. Acid value<br />

5. Iodine value<br />

6. Saponification value<br />

C. Miscellaneous analysis:<br />

7. Analysis of coal: Proximate analysis and ultimate analysis.<br />

8. Analysis of lime: Estimation of acid insolubles, available lime and<br />

calcium carbonate<br />

9. Analysis of bleaching powder: Estimation of chlorine content.<br />

10. Analysis of starch/glucose: Estimation of total reducing sugars<br />

11. Analysis of saw dust: Estimation of total cellulose and –cellulose<br />

E. Miscellaneous preparations:<br />

12. Preparation of soap<br />

13. Preparation of copper pigment<br />

14. Preparation of chrome yellow pigment<br />

15. Preparation of phenol formaldehyde resin<br />

16. Prepare nitrobenzene from benzene<br />

17. Prepare m-dinitro benzene from nitro benzene<br />

18. Prepare p-nitro acetanilide from acetanilide<br />

Evaluation of Practical Examination:<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE & VIVA<br />

DURING THE SEMESTER (40 MARKS)<br />

EXPERIMENT FILE WORK VIVA<br />

(10 MARKS) (10 MARKS) (10 MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5 MARKS)<br />

VIVA<br />

(10 MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50 MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

Page 52


Course Code: ECH-553<br />

Semester-V<br />

MASS TRANSFER-I (LAB)<br />

1. To study the steam distillation.<br />

2. To study differential distillation.<br />

3. To estimate the height equivalent to a theoretical plate .<br />

4. To study vapor-liquid equilibria.<br />

5. To determine the liquid diffusion coefficient.<br />

6. To determine the vapor diffusion coefficient.<br />

7. To study the surface evaporation.<br />

8. To estimate the height of a transfer unit.<br />

9. To study the absorption unit.<br />

10. To study the evaporator (Feed forward and Feed backward).<br />

11. To study the drying unit.<br />

Evaluation of Practical Examination:<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 53


Semester V<br />

INDUSTRIAL TRAINING<br />

(PRESENTATION BASED ON INDUSTRIAL TRANING DONE AFTER THE IV<br />

SEMESTER EXAMINATION IN SUMMER)<br />

Course Code: ECH-591<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 0 2<br />

Students will attend Industrial training of four weeks in any industry or reputed organization after the IV<br />

semester examination in summer vacation. The evaluation of this training shall be included in the V<br />

semester evaluation.<br />

The student will be assigned a faculty guide who would be the supervisor of the student. The faculty<br />

would be identified before the end of the IV semester and shall be the nodal officer for coordination of<br />

the training.<br />

Students will also be required to prepare an exhaustive technical report of the training undertaken during<br />

the V semester which will be duly signed by the officer under whom training was taken in the industry/<br />

organization. The covering format shall be signed by the concerned office in-charge of the training in the<br />

industry. The officer-in-charge of the trainee would also give his rating of the student in the standard<br />

<strong>University</strong> format in a sealed envelope to the Director of the college.<br />

The student at the end of the V semester will present his report about the training before a committee<br />

constituted by the Director of the College which would be comprised of at least three members<br />

comprising of the Department Coordinator, Class Coordinator and a nominee of the Director. The<br />

students guide would be a special invitee to the presentation. The seminar session shall be an open house<br />

session. The internal marks would be the average of the marks given by each member of the committee<br />

separately in a sealed envelope to the Director.<br />

The marks by the external examiner would be based on the report submitted by the student which shall be<br />

evaluated by the external examiner and cross examination done of the student concerned.<br />

Not more than three students would form a group for such industrial training/ project submission.<br />

The marking shall be as follows.<br />

Internal: 50 marks<br />

By the Faculty Guide - 25 marks<br />

By Committee appointed by the Director – 25 marks<br />

External: 50 marks<br />

By Officer-in-charge trainee in industry – 25 marks<br />

By External examiner appointed by the <strong>University</strong> – 25 marks<br />

Page 54


Course Code: ECH-601<br />

Unit – I<br />

Semester-VI<br />

CHEMICAL REACTION ENGINEERING – I<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Introduction: Definition of reaction rates, variable affecting reaction rates, classification of reactions,<br />

order, molecularity.<br />

(Lectures 08)<br />

Unit – II<br />

Kinetics of Homogenous Reactions: Concentration dependent term of a rate equation, temperature<br />

dependent term of a rate equation, searching for a mechanism.<br />

Interpretation of Batch Reactor Data: Constant volume batch reactor, variable volume batch reactor,<br />

temperature and reaction rate.<br />

(Lectures 08)<br />

Unit – III<br />

Introduction to Reactor Design: Ideal reactors for single reaction: Ideal batch reactor, steady state<br />

mixed flow Reactor, steady state PFR, Holding time and space time for flow systems.<br />

Design for single reactions: Size comparison, multiple reactor systems, recycle reactor, auto catalytic<br />

reactions.<br />

Design for multiple reactions: Reactions in parallel, reactions in series, series – parallel reactions.<br />

(Lectures 08)<br />

Unit – IV<br />

Temperature and Pressure Effects on Reactions: Single reactions: Heat of reaction, equilibrium<br />

constants, graphical design procedure, optimum temperature progression, adiabatic operations. Multiple<br />

reactions: Product distribution and temperature.<br />

(Lectures 08)<br />

Unit – V<br />

Stability of Multiple Steady – States: Multiple steady-states of a CSTR with a first order reaction,<br />

Ignition – extinction curve.<br />

(Lectures 08)<br />

Texts Books:<br />

1. Levenspiel, O., “<strong>Chemical</strong> Reaction <strong>Engineering</strong>” 3rd ed., John Wiley & Sons,<br />

Singapore 1999.<br />

2. Fogler, H.S., “Elements of <strong>Chemical</strong> Reaction <strong>Engineering</strong>” 3rd ed., Prentice Hall of<br />

India, 2003.<br />

3. Smith, J.M. “<strong>Chemical</strong> <strong>Engineering</strong> Kinetics”, 3rd McGraw-Hill, 1981.<br />

Reference Books:<br />

1. Dawande S.D. “Principles of <strong>Chemical</strong> Reaction <strong>Engineering</strong>,” 2nd ed., Central Techno<br />

Publications, Nagpur, 2003.<br />

2. Richardson, J.F. and peacock D.G., “Coulson and Richardson’s <strong>Chemical</strong><br />

<strong>Engineering</strong>,” Vol.3, 3rd ed. Asian Books Pvt. Ltd. New Delhi 1998.<br />

Page 55


Course Code: ECH-602<br />

Semester-VI<br />

MASS TRANSFER–II<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Distillation : Vapor liquid Equilibria, Boiling point diagram, Relative volatility, flash and differential<br />

distillation for two component mixture, steam distillation, azeotropic distillation, extractive distillation.<br />

Continuous and differential contact distillation: Rectification, reflux ratio and its importance,<br />

Minimum reflux, total and optimum reflux ration, material balance and Q-line equation, open steam,<br />

multiple feed and multiple product calculations, Enthalpy concentration diagram, panchon-Savarit and<br />

McCabe Theile method for calculation of number of plates. Approximate wquation; Fensky and<br />

underwood equation for minimum reflux and minimum number of plate calculation, Batch distillation.<br />

(Lectures 08)<br />

Unit – II<br />

Liquid – Liquid extraction : Liquid-Liquid equilibrium, packed and spray column, conjugate curve and<br />

tie line data, plait-point, ternary liquid-liquid extraction, co-current, counter current and parallel current<br />

system, selection of solvent for extraction.<br />

(Lectures 08)<br />

Unit – III<br />

Leaching : Solid-liquid equilibrium, Equipment, principles of leaching, co-current and counter current<br />

systems and calculation of number of stage required.<br />

Unit – IV<br />

Humidification : General theory, psychometric chart, fundamental concepts in humidification and<br />

dehumidification, drybulb and wet bulb temperature, adiabatic saturation temperature, measurement of<br />

humidity calculation of humidification operation, cooling towers and related equipments.<br />

(Lectures 08)<br />

Unit – V<br />

Crystallization : Supersaturation, methods to achieve supersaturation, Factors governing nucleation and<br />

crystal growth rates, controlled-growth of crystals, super saturation curve, principle and design of batch<br />

and continuous type crystallizers, Inverted soliability, fractional crystallization.<br />

(Lectures 08)<br />

Text Books:<br />

1. Treybal, R.E; “Mass Transfer Operation”, McGraw-Hill,1980.<br />

2. King, C.J. “Separation Process”, McGraw-Hill, NY.<br />

3. Smith, B.D., “Design of Equilibrium stage Processes”, McGraw-Hill, NY.<br />

References Books:<br />

1. McCabe, W.L., Smith, J.C. and Harriot, P., “Unit Operation of <strong>Chemical</strong> <strong>Engineering</strong>”, 6th<br />

ed, McGraw-Hill, NY.<br />

2. Coulson, J.M. and Richardson, J.F., “<strong>Chemical</strong> <strong>Engineering</strong>”, Vol. I and II, Asian Books<br />

Pvt., New Delhi.<br />

Page 56


Course Code: ECH-603<br />

Semester-VI<br />

PETROLEUM REFINING<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Introduction: World Petroleum resources, petroleum industry in India, origin, exploration, drilling,<br />

composition and classification of petroleum crude, ASTM, TBP and FEV and production of petroleum<br />

crude, transportation and pretreatment of crude oil. (Lectures 08)<br />

Unit – II<br />

Distillation of crude oil Atmospheric and Vacuum distillation. Properties and specification of petroleum<br />

products-LPG, Gasoline, naphtha, kerosene, diesel oil, lubricating oil, wax etc Testing and uses of<br />

petroleum products. Safety and pollution considerations in refineries. (Lectures 08)<br />

Unit – III<br />

Conversion process: Thermal and catalytic in vapor, liquid and mixed phases, Hydro cracking, Thermal<br />

reforming, Polyforming and plat forming, Catalytic reforming. (Lectures 08)<br />

Unit – IV<br />

Conversion of petroleum gases into motor fuel with reference to Alkylation, Polymerization,<br />

Isomerisation, Hydrogenation, Production of aviation gasoline, motor fuel, kerosene, diesel oil and jet<br />

fuel. (Lectures 08)<br />

Unit – V<br />

Vacuum distillation: Design and operation of topping and vacuum distillation units. Tube still furnaces<br />

solvent extraction, uses of lubricating oils & waxes, <strong>Chemical</strong> & clay treatment of petroleum products,<br />

Desulphurization. (Lectures 08)<br />

Text Books:<br />

1. Nelson, W.L., “Petroleum Refinery <strong>Engineering</strong>,” 4th Ed., McGraw Hill,<br />

1987<br />

2. Garry, J.H. and Handwrek, G.E. “Petroleum Refining, Technology and Economics” 2nd Ed.,<br />

Marcel-Dekker<br />

3. Prasad, R., “Petroleum Refining Technology” Khanna Publishers, Delhi, 2000<br />

4. Kobe, K.A., and Mcketta, J.J. “Advances in Petroleum Chemistry and Refining”, Wiley<br />

Interscience<br />

Reference Books:<br />

1. Gruse, W.A. and Steven, D.R. “<strong>Chemical</strong> Technology of Petreleum” McGraw Hill<br />

2. Rao, M.G. and sitting, M. “Dryden’s Outlines of <strong>Chemical</strong> Technology”, East West Press,<br />

1997<br />

Page 57


Course Code: ECH-604<br />

Semester-VI<br />

BIOCHEMICAL TECHNOLOGY<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Biochemical : Introduction, Biochemical <strong>Engineering</strong>, Biological Process, Definition of Fermentation,<br />

Overview of industrial bioprocesses with emphasis on new material.<br />

(Lectures 08)<br />

Unit – II<br />

Enzyme Kinetics: Introduction, Simple Enzyme Kinetics, Evaluation of Kinetic Parameters, Enzyme<br />

Reactor with Simple Kinetics, Inhibition of Enzyme Reactions, Influences on Enzyme Activity, Industrial<br />

Applications of Enzymes.<br />

(Lectures 08)<br />

Unit – III<br />

Downstream Processing, Solid-Liquid Separation, Cell Rupture, Recovery, Purification, Sterilization,<br />

Sterilization Methods, Batch Sterilization, Air Sterilization, Continuous Sterilization, Design Criterion.<br />

(Lectures 08)<br />

Unit – IV<br />

Sulfa drugs, antibiotic and vitamins-introduction, use- vitamins C, vitamins K. Side effect of sulfa drugs<br />

antibiotic and vitamins. (Lectures 08)<br />

Unit – V<br />

Pharmaceutical products- introduction, preparation, uses, environmental impact Effect of Pharmaceutical<br />

products on human health. (Lectures 08)<br />

Text Books:<br />

1. Atkinson, B. andMavituna, F., “Biochemical <strong>Engineering</strong> and Biotechnology<br />

Handbook,” Nature Press, Macmillan, 1983<br />

2. Glazer, A.N. and Nikaido, H., “Microbial Biotechnology: Fundamentals of Applied<br />

Microbiology,” WH Freeman & Co., New York, 1995<br />

References Books:<br />

1.Reed, G. (Ed.), “Prescott & Dunn’s Industrial Microbiology” 4th Ed., CBS Publishers &<br />

Distributors, New Delhi, 1999.<br />

Semester VI<br />

Page 58


Technical Writing<br />

Course code: EHM601 L T P C<br />

2 0 2 3<br />

Course Contents:<br />

Unit I<br />

Forms of Technical Communication: Report writing, Definition and characteristics, Steps towards<br />

report writing, Structure, style of Report writing, Types & forms of Reports, Presentation of Reports,<br />

importance of Report writing.<br />

Unit II<br />

Technical Paper writing: Definition and purpose, essentials of a good technical paper/Article,<br />

Scientific Article writing, Difference between Technical paper/Article and scientific article,<br />

elements/steps in writing Technical paper & Scientific Article, Methods of writing technical paper &<br />

Scientific article.<br />

Unit III<br />

Technical Proposal: Definition and meaning of Technical Proposal, Significance of Proposal, Kinds,<br />

Types of proposal, Characteristics of a good Proposal, Structure, Parts, Format of Proposal,<br />

Supplementary parts, Uses of Proposals.<br />

Unit IV<br />

Writing Skills: Reporting events, Writing News paper, Reports, Essentials of essay writing –writing an<br />

essay of about 300 words on a given topic. Bio-Data Making, Writing of CV & Resumes, Difference<br />

between CV and Resume, Writing Job application etc.<br />

Unit V<br />

Value-based Text Reading: R.K. Narayan- A Bookish Topic.<br />

1. Francis Bacon- of studies.<br />

2. CEM Joad – The Civilization of Today.<br />

(Note: The two periods per week may be utilized in Language Lab covering the above syllabus.)<br />

Text Books:<br />

1. Singh R.P., An Anthology of English Easy O.U.P. New Delhi.<br />

2. Raman Meenakshi & Sharma Sangeeta, Technical Communication-Principles & Practice O.U.P.<br />

New Delhi. 2007.<br />

Reference Books:<br />

1. Monippally Matthukutty M., Business Communication Strategies Tata- Mc Graw Hill Publications<br />

Company, New Delhi.<br />

2. Mohan K. & Sharma R.C., Business Correspondence of Report Writing,TMH, New Delhi.<br />

Semester VI<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 59


Industrial Psychology<br />

Course code: EHM602 L T P C<br />

3 0 0 3<br />

Unit I<br />

Sociology in the industrial Perspective: Concept of Sociology, Sociology as a Science, Sociology of<br />

work & industry, Perspectives for sociological analysis of work, Class- Conflict in Industry, Social<br />

impact of industrialization, Corporate skills in the fast growing multinational set up.<br />

(Lectures 08)<br />

Unit II<br />

Work and Social change: Nature of modern societies, emergence of industrial capitalism, Technology &<br />

Social change, the information society after the industrial society, post-modernity, globalization &<br />

Convergence, Significance of the service sector today, work restructuring and corporate management.<br />

(Lectures 08)<br />

Unit III<br />

Work experience in Industry: The concept of alienation, Work satisfaction, Technology & work<br />

experience, and Social background of workers, Work orientations, Stress & anxiety of the worker, Work<br />

& Leisure, Unemployment, Conflicts in the work place. (Lectures 08)<br />

Unit IV<br />

General and Applied Ethics- Ethics and the professions – Standard of right and wrong, problems of<br />

Ethical Certainty, Significance of professional Ethics for Engineers, New Technology and Ethics,<br />

Applied Ethics - Cases in professional <strong>Engineering</strong> Practice, Principles of business ethics, Individual in<br />

the organization. (Lectures 08)<br />

Unit V<br />

Ethical Leadership: Decision making, corporate culture and reputation management, corporate social<br />

responsibility and social reporting. (Lectures 08)<br />

Text Books:<br />

1. Sheth N.R., Social Frame Work of Indian Factory, O.U.P. Bombay.<br />

2. Gisbert P., Fundamentals of Industrial Sociology, O.U.P. New Delhi.<br />

3. Watson Tony J., Sociology: Work & Industry, New York. Routledge.<br />

4. Schinzinger, Roland & Mike W. Martin, Introduction to <strong>Engineering</strong> Ethics- Boston, McGraw<br />

Hill.<br />

Reference Books:<br />

1. Fleddermann Charles, <strong>Engineering</strong> Ethics, Upper Saddle River- N.J. Prentice Hall.<br />

2. Miller & Form, Industrial Sociology, London Harper & Row.<br />

3. Parsons Richard D., The Ethics of Professional Practice- Allyn & Bacon, London.<br />

4. Govindarajan - <strong>Engineering</strong> Ethics- Prentice Hall (India) New Delhi.<br />

Bhatia S.K. - Business Ethics & Management Values- Deep & Deep Publication. N. Delhi<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 60


Course Code: ECH-651<br />

Semester-VI<br />

CHEMICAL REACTION ENGINEERING-I (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

1. To determine the relative rates of reaction of iodide ion with hydrogen peroxide at room temperature<br />

using different concentrations of the iodide ion.<br />

2. To separate Organic Compounds by Paper Chromatography.<br />

3. To study the effect of temperature, concentration of the reactants and a catalyst on the rate of chemical<br />

reaction.<br />

4. To study the activity results or oxidation-reduction replacement reaction.<br />

5. To purify water by ion -exchange.<br />

6. To determine the order and rate constant of esterification reaction at room temperature.<br />

7. To determine the order and rate constant of saponification reaction at room temperature.<br />

8. To study the residence time distribution (R.T.D.) in a stirred tank reactor.<br />

9. To study the residence time distribution (R.T.D.) in a plug flow reactor.<br />

10. To study the decomposition of calcium carbonate<br />

11. To determine the energy of activation of a given chemical reaction.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

Semester-VI<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 61


Course Code: ECH-652<br />

MASS TRASNFER-II (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

1. To determine the ternary liquid equillibria (Binodal curve).<br />

2. To study the liquid-liquid equilibria.<br />

3. To determine the limiting flow rates in spray tower.<br />

4. To determine the hydrodynamics of perforated plate tower.<br />

5. To determine the volumetric mass transfer coefficients in perforated plate tower.<br />

6. To determine the dynamics of liquid drops (Single drop extraction tower).<br />

7. To studies of axial mixing characteristics in a packed bed.<br />

8. To determine the gas-liquid mass transfer in packed tower.<br />

9. To determine the drying characteristics of a given material.<br />

10. To determine the Mass balance and Energy balance in Feed forward and Feed backward Evaporator.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

Semester-VI<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 62


CHEMICAL PLANT SAFETY & OCCUPATIONAL HAZARD (ELECTIVE)<br />

Course Code: ECH-605<br />

Unit-I<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

INDUSTRIAL SAFETY<br />

<strong>Chemical</strong> process Industries - First degree and second-degree hazards. Lines of defense-first, second and<br />

third line defense-chemical and physical job safety analysis-high pressure - high temperature operationdangerous<br />

and toxic chemicals-highly radio active materials-Safe handling and operation of materials and<br />

machineriesplanning layout-safety slogans. (Lectures 08)<br />

Unit-II<br />

SAFETY PROGRAMS IN INDUSTRIES<br />

Effective steps to implement safety procedures-Periodic Advice and checking to follow safety procedures<br />

and rules-proper selection and replacement of handling equipment-personnel safety and protective<br />

equipment. (Lectures 08)<br />

Unit-III<br />

ACCIDENTS<br />

Industrial accident costs-Identification of accident spots, Remedial measures, Identification and analysis<br />

of causes of injury to men and machineries- Accident prevention -accident proneness-vocational<br />

guidance, fire prevention and fire protection. (Lectures 08)<br />

Unit-IV<br />

HEALTH HAZARD Hazard identification and Assessment-involvement of human factors and errorsoccupational<br />

and industrial health hazards. (Lectures 08)<br />

Unit-V<br />

Role of Government, Safety Organization, Management and trade unions in promoting industrial safety-<br />

On-site and Off-site safety provisions. (Lectures 08)<br />

Text Book:<br />

1. Krishnan, Safety Management in Industry, Jaico Publishers, New Delhi, 1997<br />

2. Fawcett H.H. and Wood W.S., Safety and Accident Prevention in <strong>Chemical</strong> Operations, John<br />

Wiley & sons, U.S.A.,1965<br />

3. Anton, Occupational Safety and Health Management, McGraw Hill Book Co., New York, 1998<br />

References Books:<br />

1. William, Industrial Safety Handbook, McGraw Hill, 2001<br />

Page 63


Course Code: ECH-606<br />

Semester-VI<br />

FERTILISER TECHNOLOGY (ELECTIVE)<br />

Unit – I<br />

Introduction: Plant nutrients, different types of fertilizers and their production in India.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

(Lectures 08)<br />

Unit – II<br />

Nitrogenous Fertilizers: Different feed stocks, synthesis gas production by steamnaptha reforming and<br />

gas purification. Ammonia synthesis, Urea manufacturing processes. Manufacture of sulphuric acid and<br />

ammonium sulphate. Nitric acid and ammonium nitrate manufacture.<br />

(Lectures 08)<br />

Unit – III<br />

Phosphatic Fertilizers : Availability and grinding of rock phosphate, manufacturing processes for single<br />

and triple super-phosphate and phosphoric acid. (Lectures 08)<br />

Unit – IV<br />

Mixed fertilizers: Availability and manufacture of muriate of potash.<br />

Mixed Fertilizers: Mono and di-ammonium phosphate, ure ammonium phosphates, NPK complex<br />

fertilizers, granulation techniques. (Lectures 08)<br />

Unit – V<br />

<strong>Engineering</strong> Problems: Fertilizers Storage and handling. Corrosion problems in fertilizers industries.<br />

Fertilizer plant effluent treatment and disposal. (Lectures 08)<br />

Text Books:<br />

1. Slack A.V. “Chemistry and Technology of Fertilizers”, Wiley linter science Publishers.<br />

2. Waggaman W.H., “Phosphoric Acid, Phosphates and Phosphatic Fertilizers”<br />

Hafner Pub.<br />

3. Austin G.T., “Shreve’s <strong>Chemical</strong> Processes Industries”, 5th Ed. McGraw Hill.<br />

Reference Books:<br />

1.Rao M.G. and Sittig M., “Dryden’s Outlines of <strong>Chemical</strong> Technology”,<br />

Affiliated East West Press, Delhi.<br />

Page 64


Course Code: ECH-607<br />

Semester-VI<br />

RUBBER SCIENCE AND TECHNOLOGY (ELECTIVE)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Rubber Science : Classification of polymers – Thermoplastic, elastomers (rubber), thermosets,<br />

Description of elastomers- rubber vulcanizates, classification of rubbers, glass rubber transition behavior,<br />

Rubber physics-elastic behaviour. (Lectures 08)<br />

Unit – II<br />

Rubber Rheology: Flow behaviour of unvulcanized rubber compounds, measurement of plasticity,<br />

viscoelasticity and relaxation properties, Rheological models. (Lectures 08)<br />

Unit – III<br />

Natural Rubber : Hevea Brasiliensis, Preservation and concentration of NR latex, Comparison of<br />

natural rubber and synthesis CIS 1,4 polyisoprene, Special features and uses of natural rubber<br />

Synthetic Rubber: Polymerization methods, addition polymerization and condensation polymerization.<br />

(Lectures 08)<br />

Unit – IV<br />

Rubber Compounding : Introduction to rubber compounding bulcanization and its effects, vulcanization<br />

systems, vulcanizate physical properties and their significance, properties desired for different rubber<br />

compounds, compounding ingredients and formulations.<br />

(Lectures 08)<br />

Unit – V<br />

Rubber Processing : Mixing, extrusion, and molding techniques.<br />

Manufacture of Rubber Products : Pneumatic tyres, lates products, rubber footwear and rubber<br />

moulded products<br />

Rubber Characterization : Rubber Compound analysis and identification of rubber.Behavior in service.<br />

(Lectures 08)<br />

Text Book:<br />

1. Blow, C.M. and Hepburn, “Rubber Technology and Manufacture” 2nd ed.<br />

Butterworth, London, 1982.<br />

2. Evans, C.M. “Practical Rubber Compounding and processing” Elsevier<br />

Applied Science Publisher, 1981.<br />

Reference Books:<br />

1. “Rubber <strong>Engineering</strong>” by Indian Rubber Institute published by Tata McGraw-<br />

Hill, 1998<br />

Page 65


Course Code: ECH-701<br />

Semester-VII<br />

CHEMICAL REACTION ENGINEERING – II<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 2 0 3<br />

Unit – I<br />

Catalysts : Description, method of preparation and manufacture; catalyst characterization – BET surface<br />

area, pore volume, pore size distribution.<br />

Catalyst Reaction Kinetic Models : Physical and chemical absorption; determination of rate expressions<br />

using absorption, surface reaction and desorption as rate-controlling steps. (Lectures 08)<br />

Unit – II<br />

Determination of Global Rate of Reaction : Heterogeneous laboratory reactors; Determination of rate<br />

expressions from experimental data. (Lectures 08)<br />

Unit – III<br />

Effect of Intrapellet Diffusion on Reaction Rates in Isothermal Pellets : Concept of effectiveness<br />

factor, Thiele modulus, experimental determination of effectiveness factor- wesiz-Prater criteria, Non-<br />

Isothermal effectiveness factor; Prater number, maximum temperature rise in a pellet, multiple steady<br />

states in heterogeneous reactors. (Lectures 08)<br />

Unit – IV<br />

Non-catalytic Gas-Solid Reactions : Progressive conversion model, Shrinking core model; various<br />

controlling regimes, design of gas-solid reactors.<br />

(Lectures 08)<br />

Unit – V<br />

Gas-Liquid Reactions : Effect of diffusion on rate of reaction, enhancement factor.<br />

Introduction to Design of Heterogeneous Reactors : One dimensional model for fixed-bed reactors,<br />

parametric sensitivity; design of fluidized bed reactors.<br />

(Lectures 08)<br />

Text Book:<br />

1. Levenspiel, O., “<strong>Chemical</strong> Reaction <strong>Engineering</strong>” 3rd Ed., John Wiley, 1999.<br />

2. Smith, J.M., “<strong>Chemical</strong> <strong>Engineering</strong> Kinetics” 3rd Ed., Mc Graw-Hill, 1981.<br />

3. Fogler, H.S., “Elements of <strong>Chemical</strong> Reaction <strong>Engineering</strong>” 3rd Ed.,<br />

Prentice-Hall of India, Delhi, 2003.<br />

4. Carberry, J.J., “Catalytic Reaction <strong>Engineering</strong>” Mc Graw-Hill, 1976.<br />

Reference Books:<br />

1. Dawande, S.D., “Principles of Reaction <strong>Engineering</strong>” Central Techno Pub.,<br />

Nagpur, 2001.<br />

6. Levenspiel, O., “The <strong>Chemical</strong> Reactor Omnibook” OSU Bookstores,<br />

Corvallis Oregon, 1996.<br />

Page 66


Course Code: ECH-702<br />

Semester-VII<br />

INTRODUCTION TO OIL/FAT TECHNOLOGY<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 2 0 3<br />

Unit – I<br />

Fats and Oils: An Overview, Properties of Fats and Oils, Sources of Fats and Oils, Characteristics of<br />

Oilseed, Oils and fats Oil Milling and Solvent Extraction, Nutritional and Health Aspects of Dietary<br />

Lipids, Oil Trading. (Lectures 08)<br />

Unit – II<br />

Fats and Oils Processing, Recovery of Fats and Oils from Plant and Animal Sources, Refining of Fats and<br />

Oils, Bleaching, Hydrogenation, Fractionation, Processes and Products of Interesterification,<br />

Deodorization Specialty Fats and Oils. (Lectures 08)<br />

Unit – III<br />

Packaging and Bulk Handling of Edible Fats and Oils, , Regulatory Considerations for Oilseed<br />

Processors and Oil Refiners, Economics of Fats and Oils Plants, Flavor Quality of Fats and Oils, Oil<br />

Quality Improvement through Processing.<br />

(Lectures 08)<br />

Unit – IV<br />

Managing Oil Quality, Utilization of Fats and Oils, Shortening Technology, Margarine Types and<br />

Preparation Technology, Oil and Fats Derivatives, Liquid Oils Technology.<br />

(Lectures 08)<br />

Unit – V<br />

Environmental Considerations in Fats and Oils Technologies, Design and Application of Fat-Based<br />

Surfactants, By-Product Utilization, Strategies for Replacement of Fat in Food Products, Genetically<br />

Engineered and Identity Preserved Oils, Health and Nutrition. (Lectures 08)<br />

Text Books:<br />

1. Swern, D. (ed.) “Bailey’s Industrial Oil and Fat Products,” 4th Ed. John Wiley and Sons, NY 1982<br />

2. Hilditch, T.P., “The Industrial Chemistry of Fats and Waxes,” 3rd ed. Bailliere,<br />

Tindall and Cox, London, 1949<br />

References Books:<br />

1. Patterson, H.B.W. “Handling and storage of Oilseeds, Oils Fats and Meat”<br />

Elsevier Applied Science, Landon 1989<br />

2. O'Brien, Richard D.; Farr, Walter E.; Wan, Peter J. ‘Introduction to Fats and Oils Technology (2nd<br />

Edition)’ AOCS Press, New Delhi.<br />

Page 67


Course Code: ECH-703<br />

Semester-VII<br />

BIOPROCESS ENGINEERING<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Introduction to Bioprocesses<br />

Historical development of bioprocess technology, an overview of traditional and modern applications of<br />

biotechnology industry, outline of an integrated bioprocess and the various (upstream and down stream)<br />

unit operations involved in bioprocess, generalized process flow sheets.<br />

(Lectures 08)<br />

Unit – II<br />

Fermentation Process-I : General requirements of fermentation processes, Basic design and<br />

construction of fermentor and ancillaries, Main parameters to be monitored and controlled in<br />

fermentation process;<br />

Fermentation Process-II : An overview of aerobic and anaerobic fermentation processes and their<br />

application in the biotechnology industry, solid-substrate, slurry fermentation and its applications, whole<br />

cell immobilization, behaviour of microbes in different reactors (air lift, fluidized, batch, continuous fed<br />

batch condition). (Lectures 08)<br />

Unit – III<br />

Media Design : Medium requirements for fermentation process, Carbon, nitrogen, minerals, vitamins<br />

and other complex nutrients, oxygen requirements, medium formulation for optimal growth and product<br />

formation, examples of simple and complex media, design and usage of various commercial media for<br />

industrial fermentations.<br />

Sterilization : Thermal death kinetics of microorganisms, batch and continuous heat. Sterilization of<br />

liquid media, filter sterilization of liquid media, Air, Design of sterilization equipment.<br />

(Lectures 08)<br />

Unit – IV<br />

Metabolic Stoichiometry : Stoichiometry of Cell growth and product formation, elemental balances,<br />

degrees of reduction of substrate and biomass, available electron balances, yield coefficients of biomass<br />

and product formation, maintenance coefficients.<br />

Energetics : Energetic analysis of microbial growth and product formation, oxygen consumption and<br />

heat evolution in aerobic cultures thermodynamic efficiency of growth.<br />

(Lectures 08)<br />

Unit – V<br />

Kinetics of Microbial Growth and Product Formation : Phases of cell growth in batch cultures.<br />

Simple unstructured kinetic models for microbial growth, Monod Model, Growth of Filamentous<br />

organisms, Growth associated (Primary) and non growth associated (secondary) product formation<br />

Kinteics. Leudeking-Piret models, substrate and product inhibition on cell growth and product formation,<br />

introduction to Structured Models for growth and product formation.<br />

(Lectures 08)<br />

Text Books:<br />

1. Biochemical <strong>Engineering</strong> Fundamentals Balley and Ollis, McGraw Hill (2nd<br />

Ed.), 1986.<br />

2. Bioprocess <strong>Engineering</strong>, Shule and Kargi, Prentice Hall, 1992.<br />

References Books:<br />

1. Stanbury, P.F., Whitaker, A., & Hall, S.J., (1998), Principles of fermentation Technology,<br />

2nd ed., Elsevier Science Publishers, BV, Amsterdam.<br />

Page 68


Course Code: ECH-704<br />

Semester-VII<br />

SUGAR TECHNOLOGY<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Sugar Industry and sugar scenario in India and world. Raw materials such as Sugar cane and beet root<br />

and their availability. Raw materials and their preparation, continuous operations, cane processing,<br />

weighment, chopping, grading crushing, milling and imbibition. Seeparation of bagase and bagacillo.<br />

(Lectures 08)<br />

Unit – II<br />

Juice purification – screening filtration, chemical treatment, sulfitation, carbonization, precipitation and<br />

clarification. Working of filter press, vacuum filtration and dorrclarifier settler.<br />

(Lectures 08)<br />

Unit – III<br />

Concentration of clarified juice in multi effect evaporation, triple and quadruple effect, and capacity,<br />

stream economy, Co-current and countercurrent flow of juice in the evaporators.<br />

(Lectures 08)<br />

Unit – IV<br />

Operations of vacuum pan. Theory of sugar crystallization, strike- pans sugar crystallizers. Crystal<br />

drying, screening and grading. (Lectures 08)<br />

Unit – V<br />

Sugar Industry bye products – bagasse, press mud, molasses; mud wax captive power and their<br />

utilization. (Lectures 08)<br />

Text Books:<br />

1. Birch and Parket, “Sugar Sciences and Technology” App. Sci Pub.<br />

2. Hong. P. “Principles of Sugar Technology” 3rd ed., Elsevier New York<br />

3. Gopal Rao and Marshal Sitting, “Dryden Outlines of <strong>Chemical</strong> Technology,” East-West<br />

Press, 3rd ed., New Delhi 1977<br />

Reference Books:<br />

1. Austin, G.T., “Shreve’s <strong>Chemical</strong> Process Industries,” 5th Ed. McGraw Hill Book Co. Singapore.<br />

Page 69


Course Code: ECH-751<br />

1. Preparation of Aspirin.<br />

2. Preparation of Benzanilide.<br />

3. Preparation of m-dinitrobenzene.<br />

4. Preparation of Benzoic acid.<br />

5. Preparation of Phthalimide.<br />

6. Preparation of Methyl Orange.<br />

7. Preparation of Parabenzoquinone.<br />

8. Preparation of nerolin.<br />

9. Detection of Extra elements.<br />

10. Analysis of Compound -1<br />

11. Analysis of Compound -2<br />

12. Analysis of Compound -3<br />

13. Analysis of Compound -4<br />

14. Analysis of Compound -5<br />

15. Analysis of Compound -6<br />

Evaluation of Practical Examination:<br />

Semester VII<br />

CHEMICAL REACTION ENGINEERING-II (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 70


Course Code: ECH-752<br />

Semester VII<br />

INTRODUCTION TO OIL/FAT TECHNOLOGY (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

a) Determine various properties of fuels (diesel, petrol and kerosene) by measuring:<br />

Flash point and fire point, carbon residue, viscosity test, ASTM distillation, corrosion test (copper strip<br />

and silver strip), Annealing point, specific gravity, pore point and cloud pont.<br />

b) Analysis of oilseeds and oil bearing materials for following:<br />

Moisture content, oil content, protein content, fiber content, ash content etc.<br />

c) Determination of physical characteristics of oils and fats derived from oilseeds and cake:<br />

Refractive index, color, specific gravity, titre, melting point, gel test, cloud point, carbon residue,<br />

viscosity test.<br />

d) Determination of chemical characteristics of oils and fats derived from oilseeds and cake: Acid<br />

value, saponification value, Iodine value, hydroxyl value, Acetyl value, peroxide value, Anisidine<br />

value, R.M., P and K value, Diene value, thicocynagen value etc.<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 71


Course Code: ECH-705<br />

Semester-VII<br />

PROCESS EQUIPMENT DESIGN (ELECTIVE)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Heat Exchangers: Auxiliary calculations; Review of Kern method; Bell’s method and HTRI method of<br />

Shell-and-tube heat exchanger design; Plate heat exchanger design; finned tube heat exchanger;<br />

Optimization of shell-and-tube exchanger. (Lectures 08)<br />

Unit – II<br />

Reboliers: Design of Kettle and thermosyphon reboilers.<br />

Evaporators : Sizing of drum; central core pipe size and number of tubes for short and long tube<br />

evaporators. (Lectures 08)<br />

Unit – III<br />

Agitated Vessels: Design of mixing vessels, gas-spraying systems; impellers, propellers, anchors and<br />

helical ribbon-type agitators. (Lectures 08)<br />

Unit – IV<br />

Gas Liquid Contact Systems: Distillation column, Absorption tower, tray hydraulics of sieve and valve<br />

trays; Design of packed bed columns. (Lectures 08)<br />

Unit – V<br />

Design of Reactors: CSTR, Batch and packed bed. (Lectures 08)<br />

Text Books:<br />

1. Sinnott, R.K., “Coulson and Richardson’s <strong>Chemical</strong> <strong>Engineering</strong>” Vol. 6, 3rd<br />

Ed., Butterworth Heinmann, New Delhi, 2002.<br />

2. Kern, D.Q., “Process Heat Transfer” McGraw-Hill, 1950.<br />

3. Evans, F.I., “Equipment Design Handbook” 2nd Ed., Vol.2, Gulf Publishing, 1980.<br />

Reference Books:<br />

1. Smith,B.D., “Design of Equilibrium Stage Process” Mc Graw-Hill, 1963.<br />

2.. Dawande, S.D., “Process Design of Equipments,” 2nd Ed., Central Techno Publications,<br />

Nagpur, 2000.<br />

Page 72


Course Code: ECH-706<br />

Semester-VII<br />

AIR POLLUTION AND CONTROL EQUIPMENTS (ELECTIVE)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit I<br />

Air Pollutant Sources, Effects and Clean Air Acts: Pollution of air: Sources and effects of air pollutants<br />

on physical environment and living systems, Monitoring of air pollution, Air pollution Laws and national<br />

standards. (Lectures 08)<br />

Unit II<br />

Air Pollutant Formation, Dipersion, Analysis: Formation of pollutants through large-scale combustion of<br />

fossil fuels, mineral processing, automobiles in urban areas and at source minimisation of release -<br />

Meteorological aspects of air pollutant dispersion. <strong>Chemical</strong> reactions in a contaminated atmosphere,<br />

urban air pollution, acid rain, Air sampling and measurement, Analysis of air pollutants.<br />

(Lectures 08)<br />

Unit III<br />

Air Pollution Control Methods for Particulates Removal: Control Methods – Source Correction methods -<br />

Particulate emission control: Dry techniques: Design of industrial dust collectors, gravity settling<br />

chambers, cyclone and multiclone separators, fabric & Fibrous filters, electrostatic precipitators, relative<br />

merits and demerits, overall selection of gas cleaning equipment, economics. Wet techniques: Design of<br />

wet dust collection, wet cyclone, empty scrubber, column (packed) scrubber, ventury scrubber,<br />

suitability, merits and demerits, economics. (Lectures 08)<br />

Unit IV<br />

Control of Specific Gaseous Pollutants: Cleaning of Gaseous effluents - Control of sulphur dioxide<br />

emission by various methods - Control of nitrogen oxides in combustion products - Control of release of<br />

carbon monoxide and hydrocarbons to the atmosphere; Case studies: Role of APC techniques in coal<br />

fired thermal power plants,cement plant and petroleum refinery. (Lectures 08)<br />

Unit V<br />

Noise Pollution and Control: Sound pressure, Power and Intensity - Measures of Noise-Outdoor noise<br />

propagation- Indoor Noise propagation- Noise Control.<br />

(Lectures 08)<br />

Texts Books:<br />

1. B.G. Verma, H. Brauer," Air Pollution Control Equipments", Springer, Verlag Berlin, 1981<br />

2. M.N. Rao and H.V.N. Rao, "Air Pollution", Tata McGraw Hill, New Delhi, 1993<br />

3. Rao C .S. "Environmental Pollution Control <strong>Engineering</strong>,” 2nd Edition, New Age International<br />

Publishers, 2006<br />

References Books:<br />

1.A. P. Sincero and G.A. Sincero Environmental <strong>Engineering</strong>: A Design Approach, Prentice Hall of India<br />

Pvt Ltd, N.Delhi, 1996<br />

2. Air Pollution Control Equipment: Selection, Design, Operation and Maintenance, Louis Theodore<br />

(Editor), Anthony J. Buonicore (Editor), Springer-Verlag Telos, 1994.<br />

Page 73


Course Code: ECH-707<br />

Semester VII<br />

INDUSTRIAL POLLUTION CONTROL (ELECTIVE)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit-I<br />

INTRODUCTION Definition of pollutant, types of pollution; Air, Water, Land, noise- adverse effects of<br />

pollutants eco system and human health - need for effluent treatment and toxicity, control. Water<br />

standards for portable, agricultural and left-off streams- air standards for cities, industrial areas, resorts.<br />

(Lectures 08)<br />

Unit-II<br />

AIR POLLUTION CONTROL METHODS Particulate emission control- gravitational settling chambers-<br />

cyclone separators, fabric filters, electrostatic precipitators, wet scrubbers, absorbers. Control of sulphur<br />

di oxide, oxides of nitrogen, carbon monoxide and hydrocarbons. Noise pollution measurements and its<br />

control. (Lectures 08)<br />

Unit-III<br />

WASTE WATER Origin of waste water, types of water pollutants and their effects, waste water sampling<br />

and analysis, determination of organic and inorganic matters, physical characteristics, bacteriological<br />

measurements. (Lectures 08)<br />

Unit-IV<br />

BASIC PROCESS OF WATER TREATMENT Primary , secondary and tertiary treatments - advanced<br />

waste water treatments; recovery of metals from process effluents. (Lectures 08)<br />

Unit-V<br />

POLLUTION CONTROL ASPECTS IN TYPICAL CHEMICAL PROCESS INDUSTRIES Fertilizer,<br />

petroleum refinery, petrochemical, pulp and paper, tanning, sugar, distilleries, textile industries.<br />

Text Book:<br />

1. Rao C.S., Environmental Pollution Control <strong>Engineering</strong>, Wiley Eastern Limited, 1991<br />

(Lectures 08)<br />

Reference Book:<br />

1.Rose G.R.D., Air pollution and Industry, Van Nostrand Reinhold Co., New York 1972.<br />

2. Pandey G.N. and Carney G.C., Environmental <strong>Engineering</strong>, Tata McGraw Hill, New Delhi,1989<br />

3.Kapoor B.S., Environmental <strong>Engineering</strong>, 3rd Edn., Khanna publishers,1997<br />

4.Mahajan S.P., Pollution Control in Process Industries, 1st Edn., Tata McGraw Hill Publishing<br />

Company Ltd., New Delhi, 1995<br />

Page 74


Semester VII<br />

INDUSTRIAL TRAINING PRESENTATION<br />

(BASED ON INDUSTRIAL TRAINING DONE AFTER THE VI SEMESTER<br />

EXAMINATION IN SUMMER)<br />

Course Code: ECH-791<br />

L T P C<br />

0 0 0 3<br />

Students will have to undergo industrial training of six weeks in any industry or reputed organization<br />

after the VI semester examination in summer. The evaluation of this training shall be included in the VII<br />

semester evaluation.<br />

The student will be assigned a faculty guide who would be the supervisor of the student. The faculty<br />

would be identified before the end of the VI semester and shall be the nodal officer for coordination of<br />

the training.<br />

Students will prepare an exhaustive technical report of the training during the VII semester which will be<br />

duly signed by the officer under whom training was undertaken in the industry/ organization. The<br />

covering format shall be signed by the concerned office in-charge of the training in the industry. The<br />

officer-in-charge of the trainee would also give his rating of the student in the standard <strong>University</strong> format<br />

in a sealed envelope to the Director of the college.<br />

The student at the end of the VII semester will present his report about the training before a committee<br />

constituted by the Director of the College which would comprise of at least three members comprising of<br />

the Department Coordinator, Class Coordinator and a nominee of the Director. The students guide would<br />

be a special invitee to the presentation. The seminar session shall be an open house session. The internal<br />

marks would be the average of the marks given by each member of the committee separately in a sealed<br />

envelope to the Director.<br />

The marks by the external examiner would be based on the report submitted by the student which shall be<br />

evaluated by the external examiner and cross examination done of the student concerned.<br />

Not more than three students would form a group for such industrial training/ project submission.<br />

The marking shall be as follows.<br />

Internal: 50 Marks<br />

By the faculty guide - 25 marks<br />

By committee appointed by the director – 25 marks<br />

External: 50 Marks<br />

By officer-in-charge trainee in industry – 25 marks<br />

By external examiner appointed by the university – 25 marks<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 75


Semester VII<br />

PROJECT WORK PHASE- 1<br />

(Synopsis, Literature Survey & Presentation)<br />

Course Code: ECH-799 L T P C<br />

0 0 6 3<br />

A group of students, not more than three, will be assigned a faculty guide who would be the supervisor of<br />

the student. The faculty would be identified in the starting of the VII semester.<br />

The group will carry out the literature search and collect required material for carrying out the project.<br />

The group will prepare a report not exceeding 15 pages at the end of semester.<br />

The assessment of performance of students should be made at least twice in each semester i.e. VII and<br />

VIII. In this semester the student shall present the progress of project live as also using overheads project<br />

or power point presentation on LCD to the internal committee as also the external examiner.<br />

The evaluation committee shall consist of faculty members constituted by the college which would<br />

comprise of at-least three members comprising of the Department Coordinator, Class Coordinator and a<br />

nominee of the Director. The students guide would be a special invitee to the presentation. The seminar<br />

session shall be an open house session. The internal marks would be the average of the marks given by<br />

each member of the committee separately in a sealed envelope to the Director.<br />

The marking shall be as follows.<br />

Internal: 100 Marks<br />

By The Faculty Guide - 50 Marks<br />

By Committee Appointed By the Director – 50 Marks<br />

Semester VIII<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 76


Course Code: ECH-801<br />

POLYMER SCIENCE AND TECHNOLOGY<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Chemistry of Polymerization Reactions : Functionality, polymerization reactions, polycondensation,<br />

addition free radical and chain polymerization. Copolymerization, block and graft polymerizations,<br />

stereospecific polymerization. (Lectures 08)<br />

Unit – II<br />

Polymerization Kinetics : Kinetics of radical, chain and ionic polymerization and copolymerization<br />

systems. (Lectures 08)<br />

Unit – III<br />

Molecular Weight Estimation : Average molecular weight: number average and weight average.<br />

Theoretical distributions, methods for the estimation of molecular weight. (Lectures 08)<br />

Unit – IV<br />

Polymerization Processes : Bulk, solution, emulsion and suspension polymerization. Thermoplastic<br />

composites, fibre reinforcement fillers, surface treatment reinforced thermoset composites – Resins,<br />

Fibres, additives, fabrication methods. (Lectures 08)<br />

Unit – V<br />

Rheology : Simple Rheological response, simple linear viscoelastic models – Maxwell,, Voigt, material<br />

response time, temperature dependence of viscosity, Rheological studies. (Lectures 08)<br />

Text Books:<br />

1. Rodringuez, “Principles of Polymer Systems”, Tata McGraw Hill, 1960<br />

2. Billmayer Jr. and Fred. W., “Textbook of Polymer Science”, Wiley Tappers, 1965<br />

3. David, J.W., “Polymer Science and <strong>Engineering</strong>”, Prentice Hall, 1971<br />

4. Schmidt, A.K. and Marlies, G.A., “High Polymers – Theory and Practice”, McGraw<br />

Hill, 1948.<br />

Reference Book:<br />

1. McKelvey, J.M., “Polymer Processing, “John Wiley, 1962<br />

2. Manoriffs, R.W., “Man-made Fibres,” Wiley Inter Science.<br />

Semester VIII<br />

Page 77


Course Code: ECH-802<br />

PULP AND PAPER TECHNOLOGY<br />

Unit – I<br />

Introduction: Present status of pulp industries: Fivrous raw materials, Fibre Chemistry.<br />

Raw Material Preparation: Debarking, chipping, chip screening, storage.<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

(Lectures 08)<br />

Unit – II<br />

Pulping : <strong>Chemical</strong>, semi chemical, mechanical, chemimechanical and nonconventional.<br />

Secondary fibre pulping. Advances and recent trends in pulping.<br />

Pulp Manufacture: Stock preparation, beating and refining, functional and control additives for<br />

papermaking, wet-end chemistry, polymer chemistry, retention sizing.<br />

(Lectures 08)<br />

Unit – III<br />

Bleaching : Objective of bleaching, bleachability measurement, bio-bleaching<br />

<strong>Chemical</strong> Recovery: Composition and properties of black liquor, oxidation and desilication,<br />

concentration of black liquor and its incineration, causticizing and clarification sludge washing and<br />

burning. (Lectures 08)<br />

Unit – IV<br />

Paper Manufacture: Approach flow system, wire part, sheet forming process, sheet transfer mechanism,<br />

press part, theory of pressing, dryer part, paper drying process, calendering, cylinder mould machine,<br />

finishing, fibre recovery systems, recent developments in paper making. Coating and lamination.<br />

(Lectures 08)<br />

Unit – V<br />

Paper Properties: Physical (Optical, strength and resistance) <strong>Chemical</strong> and electrical properties, paper<br />

defects<br />

Paper Grades: Types, composition, manufacturing techniques, properties and uses<br />

(Lectures 08)<br />

Text Books:<br />

1. Britt, K.W. (Ed.) “Handbook of Pulp and paper Technology” 2nd ed., CBS<br />

Publishers & Distributors, Delhi, 1984.<br />

2. Casey, J.P. “Pulp and paper Chemistry and <strong>Chemical</strong> Technology” Vol.1, 3rd ed. Wiley<br />

Interscience.<br />

3. Rydholm. S.A. “Pulping Processes” Wiley Interscience.<br />

4. Libby, C.E. “Pulp and paper Science and Technology” Vol.1, McGraw-Hill.<br />

5. Clark, JDA, “Pulp Technology and Treatment for Paper” 2nd ed. Miller Freeman.<br />

Reference Books:<br />

1. McDonald, R.G., “Pulp and Paper Manufacture,” Vol.1, 2nd ed. McGraw-Hill.<br />

2. Biermann, C.J. “Essentials of Pulpingand Paper Making,” Academic Press.<br />

3. Saltman, D., “Paper Basics” Van Nostrand, 1978.<br />

Semester VIII<br />

Page 78


Course Code: ECH-851<br />

POLYMER SCIENCE & TECHNOLOGY (LAB)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

0 0 4 2<br />

a) Identification of following polymers<br />

Polyethylene, Polypropylene, Polystyrene, Polyamide, Polyvinyl chloride, PMMA, PE, UF, MF<br />

Analysis of following polymers PVA, Alkyd resin, PVAc, Epoxy resin<br />

b) Synthesis of following polymers (at least five)<br />

1. Polyvinyl acetate by bulk polymerization, 2. Polyvinyl chloride by emulsion polymerization,<br />

3. Polystyrene by solution polymerization, 4.PMMA by Suspension polymerization, 5. Epoxy resin by<br />

condensation polymerization, 6. UF by condensation polymerization,7 PF by condensation<br />

polymerization, 8. MF by condensation polymerization<br />

c) Determine CAC and CMC of polymer-surfactant mixture by conductivity test using conductivity<br />

meter and surface tension test by using Tensiometer.<br />

d) Characterization (at least Five)<br />

1. Acid value, 2.Hydroxyl value, 3. Iodine value 5. Epoxy value and epoxy content, 6. Amine value,<br />

7. K-value, 8. Chlorine content<br />

Evaluation of Practical Examination:<br />

Internal Evaluation (50 marks)<br />

Each experiment would be evaluated by the faculty concerned on the date of the experiment on a 5 point<br />

scale which would include the practical conducted by the students and a Viva taken by the faculty<br />

concerned. The marks shall be entered on the index sheet of the practical file.<br />

Evaluation scheme:<br />

PRACTICAL PERFORMANCE &<br />

VIVA DURING THE SEMESTER (30<br />

EXPERIMENT<br />

(10 MARKS)<br />

MARKS)<br />

FILE<br />

WORK<br />

(10<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

ATTENDANCE<br />

(5 MARKS)<br />

QUIZ<br />

(5<br />

MARKS)<br />

VIVA<br />

(10<br />

MARKS)<br />

TOTAL<br />

INTERNAL<br />

(50<br />

MARKS)<br />

External Evaluation (50 marks)<br />

The external evaluation would also be done by the external Examiner based on the experiment conducted<br />

during the examination.<br />

EXPERIMENT<br />

(20 MARKS)<br />

FILE WORK<br />

(10 MARKS)<br />

VIVA<br />

(20 MARKS)<br />

TOTAL<br />

EXTERNAL<br />

(50 MARKS)<br />

Page 79


Semester VIII<br />

PROJECT WORK PHASE-2<br />

(Report, Analysis, Implementation/Simulation and Presentation)<br />

Course Code: ECH-899 L T P C<br />

0 0 18 9<br />

Students should devote themselves to prepare something tangible, which could be a working model of<br />

their thoughts based on their subject of choice.<br />

The project shall be finalized by the students based on the VII semester project work report and shall be<br />

completed and submitted at least one month before the last teaching day of the VIII semester, date of<br />

which shall be notified in the academic calendar.<br />

The assessment of performance of students should be made at least twice in each semester i.e. VII and<br />

VIII. In this semester student shall present the final project live as also using overheads project or power<br />

point presentation on LCD to the internal committee as also the external examiner.<br />

The evaluation committee shall consist of faculty members constituted by the college which would<br />

comprise of at-least three members comprising of the Department Coordinator, Class Coordinator and a<br />

nominee of the Director. The students guide would be a special invitee to the presentation. The seminar<br />

session shall be an open house session. The internal marks would be the average of the marks given by<br />

each member of the committee separately in a sealed envelope to the Director.<br />

The marking shall be as follows.<br />

Internal: 50 Marks<br />

By The Faculty Guide - 25 Marks<br />

By Committee Appointed By the Director – 25 Marks<br />

External: 50 Marks<br />

By External Examiner Appointed By the <strong>University</strong> – 50 Marks<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

Page 80


Course Code: ECH-803<br />

Semester VIII<br />

INDUSTRIAL SAFETY & HAZARD MANAGEMENT (ELECTIVE)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit I<br />

Industrial safety, Industrial hygiene and safety aspects related to toxicity, noise, pressure, temperature,<br />

vibrations, radiation etc. Explosions including dust, vapor, cloud and mist explosion.<br />

(Lectures 08)<br />

Unit II<br />

Elements of safety, safety aspects related to site, plant layout, process development and design stages,<br />

identification of hazards and its estimation, risk, risk analysis and assessment methods; fault free method,<br />

event free method, scope of risk assessment, controlling toxic chemicals and flammable materials.<br />

(Lectures 08)<br />

Unit III<br />

Toxic substances and degree of toxicity, its estimation, their entry routes into human system, their doses<br />

and responses, control techniques for toxic substances exposure, use of respirators, ventilation systems<br />

(Lectures 08)<br />

Unit IV<br />

Prevention of losses, pressure relief, provision for fire fighting, release of hazardous materials from tanks,<br />

pipes through holes and cracks , relief systems : types and location of reliefs.<br />

(Lectures 08)<br />

Unit V<br />

Handling, transportation and storage of of flammable liquids, gases, and toxic materials and wastes,<br />

regulation and legislation, government role, risk management routines, emergency preparedness, disaster<br />

planning and management.<br />

(Lectures 08)<br />

Text Books:<br />

1. D. A. Crowl and J.F. Louvar – <strong>Chemical</strong> Process Safety (Fundamentals with Applications), Prentice<br />

Hall (1990)<br />

2. H.H. Fawcett and W.S. Wood – Safety and Accident prevention in <strong>Chemical</strong> Operations, 2 nd Edition,<br />

John Wiley &Sons,New York, 1982.<br />

3. Coulson & Richardson’s <strong>Chemical</strong> <strong>Engineering</strong> – Vol. 6 – R.K. Sinnott, Butterworth – Heinmann Ltd.,<br />

1996.<br />

Reference Books:<br />

1. Sanjoy Banerjee, Industrial Hazards & Plant Safety, Taylor & Francis Group<br />

Page 81


Course Code: ECH-804<br />

Semester VIII<br />

ENERGY MANAGEMENT (ELECTIVE)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit I<br />

Energy Scenario : Commercial & Non commercial energy, primary energy resources, commercial<br />

energy production, final energy consumption, energy need of growing economy, long term energy<br />

scenario, energy pricing, energy sector reform, energy & environment, energy conservation and its<br />

importance, re- structuring of the energy supply sector, energy strategy for future, energy conservation<br />

act. (Lectures 08)<br />

Unit II<br />

Energy Management & Energy Planing : Definition & significance, energy strategy, energy policy &<br />

energy planning, two sides of energy management, sectors of supply side energy management, objective<br />

of energy management, hierarchical levels of supply side energy management, trade off b/w energy<br />

management, energy strategies & energy planning, energy & economy, essential imperatives & steps in<br />

supply side energy planning, energy planning flow for supply side, essential data for supply side energy<br />

planing, infrastructure planning, transportation of energy, per capita energy consumption, imperatives &<br />

steps in user side energy planning, energy management & control system for demand side, seven<br />

principal of energy management, energy policy of a supply organization & demand side organization,<br />

organization for energy management, training & human resource development, motivation.<br />

(Lectures 08)<br />

Unit III<br />

Energy Audit & Energy Monitoring, Targeting and Conservation: Introduction, need, types &<br />

procedure of energy audits, modern techniques and instruments for energy audit. Defining monitoring &<br />

targeting, element of monitoring & targeting, data & information analysis, techniques- energy<br />

consumption, production & cumulative sum of differences (CUSUM). Energy conservation opportunity,<br />

electrical & thermodynamic ECOs, ECOs in chemical process industries, waste management & recycling<br />

of discard material and energy. (Lectures 08)<br />

Unit IV<br />

Advancement In Technologies & Future Energy Alternatives: Recent advancement in energy<br />

technology towards 21st century, transport of energy, ethanol as a fuel. Fusion – introduction potential,<br />

condition for fusion, magnetic confinement fusion reactor, cold fusion laser induced fusion. Biomass –<br />

introduction, municipal waste, biomass conversion, wood combustion Geothermal energy – introduction,<br />

origin, nature, resources and exploration, environment impact, low temperature geothermal resources.<br />

(Lectures 08)<br />

Unit V<br />

Case Studies: Energy conservation in alcohol industry. Energy conservation in fertilizer industry and<br />

pulps & paper industry. Energy conservation in different units of refinery likes FCCU, HCU & ADU.<br />

(Lectures 08)<br />

Text Books:<br />

1. Murphy W.R. and Mckay G., Energy Management(BH)<br />

2. Hinrich & Kleinbach “Energy : its use and the environment” III ed. Harcourt.<br />

3. Boyle “Renewable Energy : Power for a sustainable future” Oxford.<br />

Reference Books:<br />

1. Rao S. & Parulckar B.B. ”Energy technology” khhanna publisher<br />

2. Capenart & Turner “ Guide to energy management ” 6 ed. Keinnedu fairmant press.<br />

Page 82


Course Code: ECH-805<br />

Semester VIII<br />

CATALYTIC PROCESSES (ELECTIVE)<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit – I<br />

Review of Heterogeneous Catalysis. (Lectures 08)<br />

Unit – II<br />

Transport Processes : Analysis of external transport processes in heterogeneous reactions in fixed ed,<br />

fluidized bed and slurry reactors, Intrapellet mass transfer, heat transfer, mass transfer with chemical<br />

reaction and simultaneous mass and heat transfer with chemical reaction. (Lectures 08)<br />

Unit – III<br />

Catalyst Selectivity: Effect of intrapellet diffusionon on selectivities in complex reactions, effect of<br />

external mass transfer on selectivities. (Lectures 08)<br />

Unit – IV<br />

Catalyst Deactivation: Modes of deactivation – poisoning, fouling and sintering. Determination of<br />

deactivation routes, combined effect of deactivation and diffusion on reaction rates, effect of deactivation<br />

on selectivity. (Lectures 08)<br />

Unit – V<br />

Reactor Design: Design calculation for ideal catalytic reactor operating at isothermal, adiabatic and nonadiabatic<br />

conditions. Deviations from ideal reactor performance. Design of industrial fixed-bed, fluidized<br />

bed and slurry reactors, Thermal stability of packed bed and fluidized bed reactors. (Lectures 08)<br />

Text Books:<br />

1. Smith, J.M., “<strong>Chemical</strong> <strong>Engineering</strong> Kinetics,” 3rd ed., McGraw-Hill, 1981<br />

2. Carberry, J.J., “Catalytic Reaction <strong>Engineering</strong>,” McGraw-Hill, 1977.<br />

3. Lee, H.H., “Heterogeneous Catalytic Reactors,” Butterworth<br />

4. Tarhan, M.O., “Catalytic Reactor Design,” McGraw-Hill, NY 1983<br />

Reference Book:<br />

1. Anderson, J.R. and Boudart, M., “Catalysis, Science and Technology,” Vol.7., Springer Verlag. N.Y.<br />

2 . Thomas, J.M. and Thomas, W.J., “Introduction to the Principles of Heterogeneous Catalysis,”<br />

Academic Press, 1967.<br />

Page 83


Semester VIII<br />

INDUSTRIAL POLLUTION ABATEMENT & WASTE MANAGEMENT (ELECTIVE)<br />

Course Code: ECH-806<br />

B.Tech (CHE) Syllabus Applicable w.e.f. Academic Session 2012-13[01112012]<br />

L T P C<br />

3 0 0 3<br />

Unit I<br />

Introduction: Environment and environmental pollution from chemical process industries,<br />

characterization of emission and effluents, environmental Laws and rules, standards for ambient air, noise<br />

emission and effluents.<br />

(Lectures 08)<br />

Unit II<br />

Pollution Prevention: Process modification, alternative raw material, recovery of by co-product from<br />

industrial emission effluents, recycle and reuse of waste, energy recovery and waste utilization. Material<br />

and energy balance for pollution minimization. Water use minimization, Fugitive emission/effluents and<br />

leakages and their control-housekeeping and maintenance.<br />

(Lectures 08)<br />

Unit III<br />

Air Pollution Control: Particulate emission control by mechanical separation and electrostatic<br />

precipitation, wet gas scrubbing, gaseous emission control by adsorption and adsorption, Design of<br />

cyclones, ESP, fabric filters and absorbers.<br />

Water Pollution Control: Physical treatment, pre-treatment, solids removal by setting and<br />

sedimentation, filtration centrifugation, coagulation and flocculation.<br />

(Lectures 08)<br />

Unit IV<br />

<strong>Chemical</strong> Treatment: Anaerobic and aerobic treatment biochemical kinetics, trickling filter, activated<br />

sludge and lagoons, aeration systems, sludge separation and drying.<br />

(Lectures 08)<br />

Unit V<br />

Waste management: Characterization of wastes-hazardous and non-hazardous wastes. Waste disposal<br />

and management laws and guidelines. Non-hazardous industrial wastes-treatment, disposal, utilization<br />

and management. Value-extraction from the wastes. Handling, storage and disposal of hazardous wastes.<br />

Case studies of a few real scenarios of waste management – sugar, pulp and paper, and fertilizer units<br />

(Lectures 08)<br />

Text Books:<br />

1. Pollution Control Acts, Rules and Notifications, CPCB, Delhi. 1995<br />

2. Vallero D., “Fundamentals of Air Pollution”, 4th Ed., Academic Press, 2007<br />

3. Eckenfelder W. W., “Industrial Water Pollution Control”, 2nd Ed., Mc Graw Hill, 1999<br />

4. Kreith F. and Tchobanoglous G., “Handbook of Solid Waste Management”, 2nd Ed., Mc Graw Hill,<br />

2002<br />

Reference Books:<br />

1. Pichtel J., “Waste Management Practices: Municipal, Hazardous and Industrial”, CRC, 2005<br />

2. Conway R.A. & Ross R.D., “Handbook of Industrial Waste Disposal”, Van-Nostrand Reinhold, 1980<br />

3. Tchobanoglous G., Theisen H. & Vigil S.A., “Integrated Solid Waste Management : <strong>Engineering</strong><br />

Principles and Management Issues”, McGraw Hill, 1993.<br />

Page 84

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