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NRL Proficiency Study Report

NRL Proficiency Study Report

E F SM.2010-E-1

E F SM.2010-E-1 SM.2010-E-2 SM.2010-E-3 SM.2010-E-4 SM.2010-E-5 SM.2010-F-1 SM.2010-F-2 SM.2010-F-3 SM.2010-F-4 SM.2010-F-5 Suspect Suspect Compliant Suspect Suspect --- --- --- --- --- 14 --- No sulfonamides found No sulfonamides found No sulfonamides found 356.5 355.9 No sulfonamides No sulfonamides No sulfonamides Containing sulfonamides (sulfadiazine) Containing sulfonamides (sulfadiazine) No sulfonamides No sulfonamides No sulfonamides Containing sulfonamides (sulfadiazine) Containing sulfonamides (sulfadiazine)

The calculation of the Z-scores for the different laboratories was used to assess the accuracy of the results. x − X Z − score = σ x = Result of each participant X = Assigned value (median value or spiked value) σ = Target standard deviation = Evaluation of the Z-score can be summarized as followed Labo B C IPH |Z| ≤ 2 → satisfactory 2 < |Z| < 3 → questionable |Z| ≥ 3 = → unsatisfactory 15 0.02 × assigned value Table 9. Results and Z-scores for the sulfadiazine analysis Assigned Value (Median of the results) = 353.5 µg kg -1 σ = 66.13 Result (µg kg -1 ) 353.5 330.0 356.2 10 -9 0.8495 Z-score 0 0.36 0.04

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