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4.1. Carbide

4.1. Carbide characterization………………………...… …..…24 4.1.1. XRD characterization…………………………… ………24 4.1.2. SEM characterization……………………………… …....34 4.1.3. Nano-diffraction characterization………………….……….34 4.2. XRD & SEM Tableau…………………………..…………34 4.2.1. XRD phase analysis.35 4.2.2. SEM……………………………………………….....…..38 4.2.3. Nano-diffraction….……………………….……....………41 5. Conclusion.…………………………………...……..…..44 6. Outlook……………………………………………45 References……………………………………………………..…..48 vi

Abbreviations a-C:W Amorphous tungsten doped carbon films. BSE: Backscattered Electrons CFC: Carbon Fibre Reinforced Carbon DC: Differentiating Current EDX: Energy Dispersive X-Ray EXAFS: Extended X-ray Absorption Fine Structure FIB: Focused Ion Beam FWHM: Full Width Half Maximum GID: Grazing Incidence Diffraction IBA: Ionic Beam Analysis ICDD: International Centre for Diffraction Data IPP: Institut für Plasmaphysik ITER: International Thermonuclear Energy Reactor JET: Joint European Torus LMIS: Liquid Metal Ion Source NEXAFS: Near-Edge X-ray Absorption Fine Structure PDF: Windows Powder Diffraction File PFM: Plasma Facing Material PVD: Physical Vapour Deposition RBS: Rutherford Backscattering RF: Radio Frequency SE: Secondary Electrons SEM: Scanning Electron Microscope SIMNRA: Simulated Nuclear Reaction Analysis STEM: Scanning Transmission Electron Microscope WC: Tungsten Carbide W2C: Tungsten Carbide WC1-x: Tungsten Carbide PDF: Windows Powder Diffraction File XPS: X-Ray Photoelectron Spectroscopy XRD: X-Ray Diffraction vii

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