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<strong>Electromagnetic</strong> Testing<br />

MFLT/ ECT/ Microwave/RFT<br />

Chapter 9B – 漏 磁 检 测<br />

More Reading on Magnetic Field Leakage Testing MFLT<br />

1st Feb 2015<br />

My ASNT Level III Pre-Exam Preparatory<br />

Self Study Notes<br />

Charlie Chong/ Fion Zhang


Refinery & Appurtenances<br />

Charlie Chong/ Fion Zhang


Ship building<br />

Charlie Chong/ Fion Zhang


Offshore Structures & Appurtenances<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/CANDU_reactor


Offshore Structures & Appurtenances<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/CANDU_reactor


Offshore Structures & Appurtenances<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/CANDU_reactor


Offshore Structures & Appurtenances<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/CANDU_reactor


Offshore Structures & Appurtenances<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/CANDU_reactor


Offshore Structures & Appurtenances<br />

Charlie Chong/ Fion Zhang


Nuclear Power Station<br />

Charlie Chong/ Fion Zhang


Offshore Structures & Appurtenances<br />

Charlie Chong/ Fion Zhang


Power Piping<br />

Charlie Chong/ Fion Zhang


Power Piping<br />

Charlie Chong/ Fion Zhang


Offshore Structures & Appurtenances<br />

Charlie Chong/ Fion Zhang


Charlie Chong/ Fion Zhang


NDT Level III Examinations<br />

Basic and Method Exams<br />

ASNT NDT Level III certification candidates are required to pass both the NDT Basic and a<br />

method examination in order to receive the ASNT NDT Level III certificate.<br />

Exam Specifications<br />

The table below lists the number of questions and time allowed for each exam. Clicking on an<br />

exam will take you to an abbreviated topical outline and reference page for that exam. For the full<br />

topical outlines and complete list of references, see the topical outlines listed in the American<br />

National Standard ANSI/ASNT CP-105, Standard Topical Outlines for Qualification of<br />

Nondestructive Testing Personnel.<br />

MFL<br />

Magnetic Flux Leakage Testing<br />

90 Questions Time: 2 hrs Certification: NDT only<br />

Charlie Chong/ Fion Zhang


Fion Zhang at Shanghai<br />

2015 February<br />

Charlie Chong/ Fion Zhang<br />

Shanghai 上 海


Charlie Chong/ Fion Zhang


Chapter 9B:<br />

Magnetic Field Testing<br />

Charlie Chong/ Fion Zhang<br />

ASM Metal Handbook Vol.17 Nondestructive evaluation and Quality control


PART 1. Magnetic Field Testing<br />

1.0 Introduction<br />

MAGNETIC FIELD TESTING includes some of the older and more widely<br />

used methods for the nondestructive evaluation of materials. Historically,<br />

such methods have been in use for more than 50 years in the examination of<br />

magnetic materials for defects such as cracks, voids, or inclusions of foreign<br />

material. More recently, magnetic methods for assessing other material<br />

properties, such as grain size, texture, or hardness, have received increasing<br />

attention.<br />

Because of this diversion of applications, it is natural to divide the field of<br />

magnetic materials <strong>testing</strong> into two parts, one directed toward defect<br />

detection and characterization and the other aimed at material properties<br />

measurements. This article is primarily concerned with the first class of<br />

applications, namely, the detection, classification, and sizing of material flaws.<br />

However, an attempt has also been made to provide at least an introductory<br />

description of materials characterization principles, along with a few examples<br />

of applications. This is supplemented by references to other review articles.<br />

Charlie Chong/ Fion Zhang<br />

ASM Metal Handbook Vol.17 Nondestructive evaluation and Quality control


Keywords:<br />

Field of magnetic materials <strong>testing</strong> into two parts,<br />

• one directed toward defect detection and characterization and<br />

• the other aimed at material properties measurements.<br />

Charlie Chong/ Fion Zhang<br />

ASM Metal Handbook Vol.17 Nondestructive evaluation and Quality control


All magnetic methods of flaw detection rely in some way on the detection and<br />

measurement of the magnetic flux leakage field near the surface of the<br />

material, which is caused by the presence of the flaw. For this reason,<br />

magnetic <strong>testing</strong> techniques are often described as flux leakage field or<br />

magnetic perturbation methods. The magnetic particle inspection method is<br />

one such flux leakage method that derives its name from the particular<br />

method used to detect the leakage field. Because the magnetic particle<br />

method is described in the article "Magnetic Particle Inspection" in this<br />

Volume, the techniques discussed in this article will be limited to other forms<br />

of leakage field measurement.<br />

Keywords:<br />

flux leakage field FLF or magnetic perturbation 扰 动 methods.<br />

Charlie Chong/ Fion Zhang


Although it is conceivable that leakage field fluctuations associated with<br />

metallurgical microstructure might be used in the analysis of material<br />

properties, the characterization methods now in use rely on bulk<br />

measurements of the hysteretic properties of material magnetization or of<br />

some related phenomenon, such as Barkhausen noise. The principles and<br />

applications of magnetic characterization presented in this article are not<br />

intended to be exhaustive, but rather to serve as illustrations of this type of<br />

magnetic <strong>testing</strong>.<br />

The principles and techniques of leakage field <strong>testing</strong> and magnetic<br />

characterization are described in the two sections that follow. These sections<br />

will discuss concepts and methods that are essential to an understanding of<br />

the applications described in later sections. The examples of applications<br />

presented in the third section will provide a brief overview of the variety of<br />

inspection methods that fall under the general heading of magnetic <strong>testing</strong>.<br />

Keywords:<br />

■ Barkhausen noise<br />

Charlie Chong/ Fion Zhang


Barkhausen Noise<br />

The Barkhausen effect is a name given to the noise in the magnetic output of a<br />

ferromagnet when the magnetizing force applied to it is changed. Discovered by<br />

German physicist Heinrich Barkhausen in 1919, it is caused by rapid changes of size<br />

of magnetic domains (similarly magnetically oriented atoms in ferromagnetic<br />

materials).<br />

Barkhausen's work in acoustics and magnetism led to the discovery, which provided<br />

evidence that magnetization affects whole domains of a ferromagnetic material, rather<br />

than individual atoms alone. The Barkhausen effect is a series of sudden changes in<br />

the size and orientation of ferromagnetic domains, or microscopic clusters of aligned<br />

atomic magnets (spins), that occurs during a continuous process of magnetization or<br />

demagnetization. The Barkhausen effect offered direct evidence for the existence of<br />

ferromagnetic domains, which previously had been postulated theoretically. Heinrich<br />

Barkhausen discovered that a slow, smooth increase of a magnetic field applied to a<br />

piece of ferromagnetic material, such as iron, causes it to become magnetized, not<br />

continuously but in minute steps.<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Barkhausen_effect


Barkhausen noise: Magnetization (J) or flux density (B) curve as a function<br />

of magnetic field intensity (H) in ferromagnetic material. The inset shows<br />

Barkhausen jumps.<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Barkhausen_effect


Barkhausen noise: Domain wall motion with a Barkhausen jump<br />

Charlie Chong/ Fion Zhang<br />

http://upload.wikimedia.org/wikipedia/commons/7/79/Barkhausensprung.gif


Barkhausen noise<br />

A coil of wire wound on the ferromagnetic material can demonstrate the sudden,<br />

discontinuous jumps in magnetization. The sudden transitions in the magnetization of<br />

the material produce current pulses in the coil. These can be amplified to produce a<br />

series of clicks in a loudspeaker. This sounds as crackle, complete with skewed<br />

pulses which sounds like candy being unwrapped, Rice crispier, or a pine log fire.<br />

Hence the name Barkhausen noise. Similar effects can be observed by applying only<br />

mechanical stresses (e.g. bending) to the material placed in the detecting coil.<br />

These magnetization jumps are interpreted as discrete changes in the size or rotation<br />

of ferromagnetic domains. Some microscopic clusters of atomic spins aligned with the<br />

external magnetizing field increase in size by a sudden reversal of neighbouring spins;<br />

and, especially as the magnetizing field becomes relatively strong, other whole<br />

domains suddenly turn into the direction of the external field. Simultaneously, due to<br />

exchange interactions the spins tend to align themselves with their neighbours. The<br />

tension between the various pulls creates avalanching, where a group of neighbouring<br />

domains will flip in quick succession to align with the external field. So the material<br />

magnetizes neither gradually nor all at once, but in fits and starts.<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Barkhausen_effect


Practical use<br />

A set-up for non-destructive <strong>testing</strong> of ferromagnetic materials: green – magnetising<br />

yoke, red – inductive sensor, grey – sample under test. The amount of Barkhausen<br />

noise for a given material is linked with the amount of impurities, crystal dislocations,<br />

etc. and can be a good indication of mechanical properties of such a material.<br />

Therefore, the Barkhausen noise can be used as a method of non-destructive<br />

evaluation of the degradation of mechanical properties in magnetic materials<br />

subjected to cyclic mechanical stresses (e.g. in pipeline transport) or high-energy<br />

particles (e.g. nuclear reactor) or materials such as high-strength steels which may be<br />

subjected to damage from grinding. Schematic diagram of a simple non-destructive<br />

set-up for such a purpose is shown on the right.<br />

Barkhausen noise can also indicate physical damage in a thin film structure due to<br />

various nanofabrication processes such as reactive ion etching or using an ion milling<br />

machine<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Barkhausen_effect


A set-up for non-destructive <strong>testing</strong> of ferromagnetic materials:<br />

• green – magnetizing yoke,<br />

• red – inductive sensor,<br />

• grey – sample under test.<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Barkhausen_effect


Magnetic Dipole<br />

Charlie Chong/ Fion Zhang


Magnetic Dipole<br />

Charlie Chong/ Fion Zhang


2.0 Principles of Magnetic Leakage Field Testing MLFT<br />

2.1 Origin of Defect Leakage Fields.<br />

The origin of the flaw leakage field is illustrated in Fig. 1. Figure 1(a) shows a<br />

uniformly magnetized rod, which consists of a large number of elementary<br />

magnets aligned with the direction of magnetization. Inside the material, each<br />

magnetic pole is exactly compensated by the presence of an adjacent pole of<br />

opposite polarity, and the net result is that interior poles do not contribute to<br />

the magnetic field outside the material. At the surfaces, however, magnetic<br />

poles are uncompensated and therefore produce a magnetic field in the<br />

region surrounding the specimen. This is illustrated in Fig. 1(a) by flux lines<br />

connecting uncompensated elementary poles.<br />

Charlie Chong/ Fion Zhang


If a slot is cut in the rod, as illustrated in Fig. 1(b), the poles on the surface of<br />

this slot are now also uncompensated and therefore produce a localized<br />

magnetic field near the slot. This additional magnetic field, which is<br />

represented by the extra flux lines in Fig. 1(b), is the leakage field associated<br />

with the slot. Figure 1, although adequate for a qualitative understanding of<br />

the origin of leakage fields, does not provide an exact quantitative description.<br />

The difficulty is the assumption that the magnetization remains uniform when<br />

the flaw is introduced. In general, this does not happen, because the<br />

presence of the flaw changes the magnetic field in the vicinity of the flaw, and<br />

this in turn leads to a change in magnetization near the flaw. With regard to<br />

Fig. 1, this means that the strengths and orientations of the elementary<br />

dipoles (magnets) actually vary from point to point in the vicinity of the flaw,<br />

and this variation also contributes to the flaw leakage field. The end result is<br />

that the accurate description of a flaw leakage field poses a difficult<br />

mathematical problem that usually requires a special-purpose computer code<br />

for its solution.<br />

Charlie Chong/ Fion Zhang


Fig. 1 Origin of defect leakage fields. (a) Magnetic flux lines of a magnet<br />

without a defect. (b) Magnetic flux lines of a magnet with a surface defect.<br />

Source: Ref 1<br />

Charlie Chong/ Fion Zhang


2.2 Experimental Techniques.<br />

One of the first considerations in the experimental application of magnetic<br />

leakage field methods is the generation of a suitable magnetic field within the<br />

material. In some ferromagnetic materials, the residual field (the field that<br />

remains after removal of an external magnetizing field) is often adequate for<br />

surface flaw detection. In practice, however, residual magnetization is rarely<br />

used because use of an applied magnetizing field ensures that the material is<br />

in a desired magnetic state (which should be known and well characterized)<br />

and because applied fields provide more flexibility (that is, one can produce a<br />

high or low flux density in the specimen as desired. Experience has shown<br />

that control of the strength and direction of the magnetization can be useful in<br />

improving flaw detectability and in discriminating among different types of<br />

flaws. In general, the magnitude of the magnetization should be chosen to<br />

maximize the flaw leakage field with respect to other field sources that might<br />

interfere with flaw detection; the optimum magnetization is usually difficult to<br />

determine in advance of a test and is often approached by trial-and-error<br />

experimentation. The direction of the field should be perpendicular to the<br />

largest flaw dimension to maximize the effect of the flaw on the leakage field.<br />

Charlie Chong/ Fion Zhang


Keywords:<br />

The direction of the field should be perpendicular to the largest flaw<br />

dimension to maximize the effect of the flaw on the leakage field.<br />

Charlie Chong/ Fion Zhang


It is possible to generate a magnetic field in a specimen either directly or<br />

indirectly. In direct magnetization, current is passed directly through the part.<br />

With the indirect approach, magnetization is induced by placing the part in a<br />

magnetic field that is generated by an adjacent current conductor or<br />

permanent magnet. This can be done, for example, by threading a conductor<br />

through a hollow part such as a tube or by passing an electric current through<br />

a cable wound around the part. Methods of magnetizing a part both directly<br />

and indirectly are illustrated schematically in Fig. 2.<br />

Charlie Chong/ Fion Zhang


Fig. 2 Methods of magnetization. (1) Head-shot method. (b) Magnetization<br />

with prods. (c) Magnetization with a central conductor. (d) Longitudinal<br />

magnetization. (e) Yoke magnetization<br />

Charlie Chong/ Fion Zhang


The flaw leakage field can be detected with one of several types of magnetic<br />

field sensors. Aside from the use of magnetic particles, the sensors most<br />

often used are the inductive coil and the Hall effect device. The inductive coil<br />

sensor is based on Faraday's law of induction, which states that the voltage<br />

induced in the coil is proportional to the number of turns in the coil multiplied<br />

by the time rate of change of the flux Ф threading the coil. It follows that<br />

detection of a magnetostatic field requires that the coil be in motion so that<br />

the flux through the coil changes with time. The principle is illustrated in Fig. 3,<br />

in which the coil is oriented so as to sense the change in flux parallel to the<br />

surface of the specimen. If the direction of coil motion is taken as x, then the<br />

induced electromotive force, E, in volts is given by:<br />

for Ф = B∙A<br />

Charlie Chong/ Fion Zhang


where N is the number of turns in the coil, A is its cross-sectional area, and B<br />

is the flux density, in Gauss, parallel to the surface of the part. Thus, the<br />

voltage induced in the coil is proportional to the gradient of the flux density<br />

along the direction of coil motion multiplied by the coil velocity. Figure 4<br />

shows the flux density typical of the leakage field from a slot, along with the<br />

corresponding signal from a search coil oriented as in Fig. 3.<br />

Charlie Chong/ Fion Zhang


Fig. 3 Flux leakage measurement using a search coil. Source:<br />

Charlie Chong/ Fion Zhang


Fig. 4 Leakage flux and search coil signal as a function of position.<br />

Charlie Chong/ Fion Zhang


Unlike the inductive coil, which provides a measure of the flux gradient, a Hall<br />

effect sensor directly measures the component of the flux itself in the direction<br />

perpendicular to the sensitive area of the device. Because the response of a<br />

Hall effect sensor does not depend on the motion of the probe, it can be<br />

scanned over the surface to be inspected at any rate that is mechanically<br />

convenient. In this respect, the Hall device has an advantage over the coil<br />

sensor because there is no need to maintain a constant scanning speed<br />

during the inspection. On the other hand, Hall effect sensors are more difficult<br />

to fabricate, are somewhat delicate compared to inductive coil sensors, and<br />

require more complex electronics. Other magnetic field sensors that are used<br />

less often in leakage field applications include the flux gate magnetometer,<br />

magnetoresistive sensors, magnetic resonance sensors, and magnetographic<br />

sensors, in which the magnetic field at the surface of a part is registered on a<br />

magnetic tape pressed onto the surface.<br />

Keywords:<br />

Hall device has an advantage over the coil sensor because there is no need<br />

to maintain a constant scanning speed during the inspection.<br />

Charlie Chong/ Fion Zhang


2.3 Analysis of Leakage Field Data.<br />

In most applications of the leakage field method, there is a need not only to<br />

detect the presence of a flaw but also to estimate its severity. This leads to<br />

the problem of flaw characterization, that is, the determination of flaw<br />

dimensions from an analysis of leakage field data. The most widely used<br />

method of flaw characterization is based on the assumptions that the leakage<br />

field signal amplitude is proportional to the size of the flaw (which usually<br />

means its depth into the material) and that the signal amplitude can therefore<br />

be taken as a direct measure of flaw severity. In situations where all flaws<br />

have approximately the same shape and where calibration experiments show<br />

that the signal amplitude is indeed proportional to the size parameter of<br />

concern, this empirical method of sizing works quite well.<br />

Keywords:<br />

The most widely used method of flaw characterization is based on the<br />

assumptions that the leakage field signal amplitude is proportional to the size<br />

of the flaw (which usually means its depth into the material) ()<br />

Charlie Chong/ Fion Zhang


There are, however, many situations of interest where flaw shapes vary<br />

considerably and where signal amplitude is not uniquely related to flaw depth,<br />

as is the case for corrosion pits in steel tubing. In addition, different types of<br />

flaws, such as cracks and pits, can occur in the same part, in which case it<br />

becomes necessary to determine the flaw types present as well as their<br />

severity.<br />

In such cases, a more careful analysis of the relationship between signal and<br />

flaw characteristics is required if serious errors in flaw characterization are to<br />

be avoided. One of the earliest attempts to use a theoretical model in the<br />

analysis of leakage field data was based on the analytic solution for the field<br />

perturbed by a spherical inclusion. Two conclusions were drawn from this<br />

analysis. First, when one measures the leakage flux component normal to the<br />

surface of the part, the center of the flaw is located below the scan plane at a<br />

distance equal to the peak-to-peak separation distance in the flaw signal (Fig.<br />

5), and second, the peak-to-peak signal amplitude is proportional to the flaw<br />

volume. A number of experimental tests of these sizing rules have confirmed<br />

the predicted relationships for nonmagnetic inclusions in steel parts<br />

Charlie Chong/ Fion Zhang


Keywords:<br />

Two conclusions were drawn from this analysis.:<br />

• First, when one measures the leakage flux component normal to the<br />

surface of the part, the center of the flaw is located below the scan plane<br />

at a distance equal to the peak-to-peak separation distance in the flaw<br />

signal (Fig. 5), and<br />

• Second, the peak-to-peak signal amplitude is proportional to the flaw<br />

volume. A number of experimental tests of these sizing rules have<br />

confirmed the predicted relationships for nonmagnetic inclusions in steel<br />

parts<br />

peak-to-peak signal amplitude is<br />

proportional to the flaw volume.<br />

Lateral<br />

dimension<br />

Charlie Chong/ Fion Zhang


Fig. 5 Dependence of magnetic signal peak separation (a) on the depth of a<br />

spherical inclusion (b)<br />

Charlie Chong/ Fion Zhang


Further theoretical and experimental data for spheroidal inclusions and<br />

surface pits have shown, however, that the simple characterization rules for<br />

spherical inclusions do not apply when the flaw shape differs significantly<br />

from the ideal sphere. In such cases, the signal amplitude depends on the<br />

lateral extent of the flaw and on its volume, and characterization on the basis<br />

of leakage field analysis becomes much more complicated.<br />

Finally, there has been at least one attempt to apply finite-element<br />

calculations of flaw leakage fields to the development of characterization<br />

rules for a more general class of flaws. Hwang and Lord performed most of<br />

their computations for simple flaw shapes, such as rectangular and triangular<br />

slots and inclusions, and from the results devised a set of rules for estimating<br />

the depth, width, and angle of inclination of a flaw with respect to the surface<br />

of the part. One of their applications to a flaw of complex shape is shown in<br />

Fig. 6.<br />

Charlie Chong/ Fion Zhang


Fig. 6 Characterization of a ferrite-tail type of defect. The dashed line shows<br />

the flaw configuration estimated from the leakage field data.<br />

Charlie Chong/ Fion Zhang


The promising results obtained from the finite-element work of Hwang and<br />

Lord, as well as the analytically based work on spheroidal flaws, suggest that<br />

the estimation of flaw size and shape from leakage field data is feasible.<br />

Another numerical method potentially applicable to flux leakage problems is<br />

the boundary integral method, which may prove useful in flaw<br />

characterization. Unfortunately, much more work must be done on both the<br />

theoretical basis and on experimental <strong>testing</strong> before it will be possible to<br />

analyze experimental leakage field data with confidence in terms of flaw<br />

characteristics.<br />

Charlie Chong/ Fion Zhang


PART 2. Principles of Magnetic Characterization of Materials<br />

1.0 Metallurgical and Magnetic Properties.<br />

The use of magnetic measurements to monitor the metallurgical properties<br />

of ferromagnetic materials is based on the fact that variables such as<br />

crystallographic phase, chemical composition, and microstructure, which<br />

determine the physical properties of materials, also affect their magnetic<br />

characteristics. Some parameters, such as grain size and orientation,<br />

dislocation density, and the existence of precipitates, are closely related to<br />

measurable characteristics of magnetic hysteresis, that is, to the behavior of<br />

the flux density, B, induced in a material as a function of the magnetic field<br />

strength, H. This relationship can be understood in principle from the physical<br />

theory of magnetic domains. Magnetization in a particular direction increases<br />

as the domains aligned in that direction grow at the expense of domains<br />

aligned in other directions. Factors that impede domain growth also impede<br />

dislocation motion; hence the connection, at a very fundamental level,<br />

between magnetic and mechanical properties.<br />

Charlie Chong/ Fion Zhang


Keywords:<br />

Metallurgical properties:<br />

• Crystallographic phase,<br />

• Chemical composition,<br />

• Grain size and orientation,<br />

• Dislocation density, and<br />

• Existence of precipitates,<br />

are closely related to measurable characteristics of magnetic hysteresis, that<br />

is, to the behavior of the flux density, B, induced in a material as a function of<br />

the magnetic field strength, H.<br />

Charlie Chong/ Fion Zhang


Hysteresis Curves<br />

Charlie Chong/ Fion Zhang


Other magnetic properties, such as the saturation magnetization, which is the<br />

maximum value B can achieve, or the Curie temperature at which there is a<br />

transition to a nonmagnetic state, are less dependent on microstructure, but<br />

are sensitive to such factors as crystal structure and chemical composition.<br />

Interest in the magnetic characterization of materials, principally steels,<br />

derives from many such relationships between measurable magnetic<br />

parameters and metallurgical properties. These relationships are, however,<br />

quite complicated in general, and it is often difficult to determine how or if a<br />

particular measurement or combination of measurements can be used to<br />

determine a property of interest.<br />

Charlie Chong/ Fion Zhang


Nevertheless, the prospect of nondestructive monitoring and quality control is<br />

an attractive one, and for this reason research on magnetic materials<br />

characterization continues to be an active field. It is not the purpose of this<br />

article to explore such magnetic methods in depth, but simply to point out that<br />

it is an active branch of nondestructive magnetic <strong>testing</strong>. The more<br />

fundamental aspects of the relationship between magnetism and metallurgy<br />

are discussed in Ref 26 and 28. Engineering considerations are reviewed in<br />

Ref 24. The proceedings of various symposia also contain several papers<br />

that provide a good overview of the current status of magnetic materials<br />

characterization.<br />

Charlie Chong/ Fion Zhang


Curie temperature<br />

In physics and materials science, the Curie temperature (Tc), or Curie point, is the temperature<br />

where a material's permanent magnetism changes to induced magnetism. The force of<br />

magnetism is determined by magnetic moments. The Curie temperature is the critical point<br />

where a material's intrinsic magnetic moments change direction. Magnetic moments are<br />

permanent dipole moments within the atom which originate from electrons' angular momentum<br />

and spin. Materials have different structures of intrinsic magnetic moments that depend on<br />

temperature. At a material's Curie Temperature those intrinsic magnetic moments change<br />

direction.<br />

Permanent magnetism is caused by the alignment of magnetic moments and induced magnetism<br />

is created when disordered magnetic moments are forced to align in an applied magnetic field.<br />

For example, the ordered magnetic moments (ferromagnetic, figure 1) change and become<br />

disordered (paramagnetic, figure 2) at the Curie Temperature. Higher temperatures make<br />

magnets weaker as spontaneous magnetism only occurs below the Curie Temperature. Magnetic<br />

susceptibility only occurs above the Curie Temperature and can be calculated from the Curie-<br />

Weiss Law which is derived from Curie's Law. In analogy to ferromagnetic and paramagnetic<br />

materials, the Curie temperature can also be used to describe the temperature where a<br />

material's spontaneous electric polarisation changes to induced electric polarisation or the<br />

reverse upon reduction of the temperature below the Curie temperature.<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Curie_temperature


Curie temperature<br />

Below T c<br />

Ferromagnetic<br />

Ferrimagnetic<br />

Antiferromagnetic<br />

Above T c<br />

↔ Paramagnetic<br />

↔ Paramagnetic<br />

↔ Paramagnetic<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Curie_temperature


Ferromagnetism The magnetic moments in a ferromagnetic material. The<br />

moments are ordered and of the same magnitude in the absence of an<br />

applied magnetic field.<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Curie_temperature


Paramagnetism The magnetic moments in a paramagnetic material. The<br />

moments are disordered in the absence of an applied magnetic field and<br />

ordered in the presence of an applied magnetic field.<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Curie_temperature


Ferrimagnetism The magnetic moments in a ferrimagnetic material. The<br />

moments are aligned oppositely and have different magnitudes due to being<br />

made up of two different ions. This is in the absence of an applied magnetic<br />

field.<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Curie_temperature


Antiferromagnetism The magnetic moments in an antiferromagnetic<br />

material. The moments are aligned oppositely and have the same<br />

magnitudes. This is in the absence of an applied magnetic field.<br />

Charlie Chong/ Fion Zhang<br />

http://en.wikipedia.org/wiki/Curie_temperature


2.0 Experimental Techniques.<br />

A typical setup for measuring the B-H characteristic of a rod specimen is<br />

shown in Fig. 7. The essential elements are an electromagnet for generating<br />

the magnetizing field, a coil wound around the specimen for measuring the<br />

time rate of change of the magnetic flux, B, in the material, and a magnetic<br />

field sensor, in this case a Hall effect probe, for measuring the magnetic field<br />

strength, H, parallel to the surface of the part. The signal generator provides a<br />

low-frequency magnetizing field, typically of the order of a few Hertz, and the<br />

output of the flux measuring coil is integrated over time to give the flux density<br />

in the material. In the arrangement shown in Fig. 7, an additional feature is<br />

the provision for applying a tensile load to the specimen for studies of the<br />

effects of stress on the hysteresis data. When using a rod specimen such as<br />

this, it is important that the length-to-diameter ratio of the specimen be large<br />

so as to minimize the effects of stray fields from the ends of the rod on the<br />

measurements of B and H.<br />

Charlie Chong/ Fion Zhang


Fig. 7 Experimental arrangement for hysteresis loop measurements.<br />

Charlie Chong/ Fion Zhang


Another magnetic method that uses a similar arrangement is the<br />

measurement of Barkhausen noise. As the magnetic field strength, H, is<br />

varied at a very slow rate, discontinuous jumps in the magnetization of the<br />

material can be observed during certain portions of the hysteresis cycle.<br />

These jumps are associated with the sudden growth of a series of magnetic<br />

domains that have been temporarily stopped from further growth by such<br />

obstacles as grain boundaries, precipitates, or dislocations. Barkhausen<br />

noise is therefore dependent on microstructure and can be used<br />

independently of hysteresis measurements, or in conjunction with such<br />

measurements, as another method of magnetic <strong>testing</strong>. The experimental<br />

arrangement differs from that shown in Fig. 7 in that a single sensor coil,<br />

oriented to measure the flux normal to the surface of the specimen, is used<br />

instead of the Hall probe and the flux winding.<br />

Charlie Chong/ Fion Zhang


The review articles and conference proceedings cited above contain<br />

additional detail on experimental technique and a wealth of information on the<br />

interpretation of hysteresis and Barkhausen data. However, it should be noted<br />

that test methods and data interpretation are often very specific to a particular<br />

class of alloy, and techniques that seem to work well for one type of material<br />

may be totally inappropriate for another. The analysis of magnetic<br />

characterization data is still largely empirical in nature, and controlled <strong>testing</strong><br />

of a candidate technique with the specific alloy system of interest is advisable.<br />

Charlie Chong/ Fion Zhang


PART 3. Application<br />

1.0 Flaw Detection by the Flux Leakage Method.<br />

Perhaps the most prevalent use of the flux leakage method is the<br />

inspection of ferromagnetic tubular goods, such as gas pipelines, down hole<br />

casing, and a variety of other forms of steel piping. In applications in the<br />

petroleum industry, the technique is highly developed, but details on<br />

inspection devices and methods of data analysis are, for the most part,<br />

considered proprietary by the companies that provide inspection services.<br />

Still, the techniques currently in use have certain features in common, and<br />

these are exemplified by the typical system described below. The device<br />

shown in Fig. 8 is an inspection tool for large-diameter pipelines.<br />

Magnetization is provided by a large electromagnet fitted with wire brushes to<br />

direct magnetic flux from the electromagnet into the pipe wall. To avoid<br />

spurious signals from hard spots in the material, the magnetization circuit is<br />

designed for maximum flux density in the pipe wall in an attempt to<br />

magnetically saturate the material.<br />

Charlie Chong/ Fion Zhang


Leakage field sensors are mounted between the pole pieces of the magnet in<br />

a circle around the axis of the device to provide, as nearly as possible, full<br />

coverage of the pipe wall. In most such tools, the sensors are the inductive<br />

coil type, oriented to measure the axial component of the leakage field<br />

gradient. Data are usually recorded on magnetic tape as the system is<br />

propelled down a section of pipe. After the inspection, the recorded signals<br />

are compared with those from calibration standards in an attempt to interpret<br />

flaw indications in terms of flaw type and size.<br />

Charlie Chong/ Fion Zhang


Fig. 8 Typical gas pipeline inspection pig. The tool consists of a drive unit, an<br />

instrumentation unit, and a center section with an electromagnetic and flux<br />

leakage sensors.<br />

Sensor<br />

Pipe<br />

Pole<br />

Pole<br />

Coil<br />

Sensor<br />

Charlie Chong/ Fion Zhang


In addition to systems for inspecting rotationally symmetric cylindrical parts,<br />

flux leakage inspection has been applied to very irregular components, such<br />

as helicopter rotor blade D-spars, gear teeth, and artillery projectiles. Several<br />

of these special-purpose applications have involved only laboratory<br />

investigations, but in some cases specialized instrumentation systems have<br />

been developed and fabricated for factory use. These systems are uniquely<br />

adapted to the particular application involved, and in most cases only one or<br />

at most several instrumentation systems have been built. Even in the case of<br />

laboratory investigations, special-purpose detection probe and magnetizing<br />

arrangements have been developed for specific applications.<br />

Charlie Chong/ Fion Zhang


One such system for automated thread inspection on drill pipe and collars is<br />

described: The device consists of an electromagnet and an array of sensors<br />

mounted outside a nonmagnetic cone that threads onto the tool joint. The<br />

assembly is driven in a helical path along the threads by a motor/clutch<br />

assembly. To minimize the leakage flux signal variations caused by the<br />

threads, signals from the sensor array are compared differentially. The<br />

system is capable of operating in a high field strength mode for the detection<br />

of cracks and corrosion pits and also in a residual field mode for the detection<br />

of other forms of damage. At last report, the system was undergoing field<br />

tests and was found to offer advantages, in terms of ease of application and<br />

defect detection, over the magnetic particle technique normally used for<br />

thread inspection.<br />

Charlie Chong/ Fion Zhang


The flux leakage method is also finding application in the inspection of ropes<br />

and cables made of strands of ferromagnetic material. One approach is to<br />

induce magnetization in the piece by means of an encircling coil energized by<br />

a direct current (dc). With this method, one measures the leakage field<br />

associated with broken strands using a Hall effect probe or an auxiliary<br />

sensor coil. A complementary method with alternating current (ac), which is<br />

actually an eddy current test rather than flux leakage, is to measure the ac<br />

impedance variations in an encircling coil caused by irregularities in the<br />

cross-sectional area of the specimen. Haynes and Underbakke describe<br />

practical field tests of an instrumentation system that utilizes both the ac and<br />

dc methods. They conclude that instrumentation capable of a combination of<br />

inspection techniques offers the best possibility of detecting both localized<br />

flaws and overall loss of cross section caused by generalized corrosion and<br />

wear. They also present detailed information on the practical characteristics<br />

of a commercially available device that makes use of both the ac and dc<br />

methods.<br />

Charlie Chong/ Fion Zhang


Charlie Chong/ Fion Zhang<br />

The flux leakage method is also finding application in<br />

the inspection of ropes and cables


Another area in which the flux leakage method has been successfully<br />

implemented is the inspection of rolling-element antifriction bearings. A<br />

schematic illustration of the method as applied to an inner bearing race is<br />

shown in Fig. 9. In this application, the part is magnetized by an<br />

electromagnet, as indicated in Fig. 9(a). The race is then rotated by a spindle,<br />

and the surface is scanned with an induction coil sensor. Typically, the race is<br />

rotated at a surface speed of about 2.3 m/s (7.5 ft/s), and the active portion of<br />

the raceway is inspected by incrementally indexing the sensor across the<br />

raceway. Magnetizing fields are applied in the radial and circumferential<br />

orientations. It has been shown that radial field inspection works best for<br />

surface flaws, while circumferential field inspection shows greater sensitivity<br />

to subsurface flaws. Data have been collected on a large number of bearing<br />

races to establish the correlation between leakage field signals and inclusion<br />

depths and dimensions determined by metallurgical sectioning.<br />

Charlie Chong/ Fion Zhang


Fig. 9 Flux leakage inspection of a bearing race. (a) Magnetization of inner<br />

race. (b) Perturbation in the magnetic flux at the surface of the inner race. (c)<br />

Probe scanning the surface<br />

Charlie Chong/ Fion Zhang


Finally, the flux leakage method has also been adapted to the inspection of<br />

steel reinforcement in concrete beams. The basic function of the magnetic<br />

field disturbance (MFD) inspection equipment is to provide maps of the<br />

magnetic field across the bottom and sides of the beam. An electromagnet on<br />

an inspection cart, which is suspended on tracks below the beam, provides a<br />

magnetic field that induces magnetization in permeable structures in its<br />

vicinity, such as steel rebars, cables, and stirrups. An array of Hall effect<br />

sensors distributed across the bottom and sides of the beam measures the<br />

field produced by magnetized structures within the beam. If a flaw is present<br />

in one of these magnetized structures, it will produce a disturbance of the<br />

normal magnetic field pattern associated with the unflawed beam. Thus, the<br />

idea behind the MFD system is to search the surface of the beam for field<br />

anomalies that indicate the presence of flaws in reinforcing steel within the<br />

structure.<br />

Keywords:<br />

magnetic field disturbance (MFD)<br />

Charlie Chong/ Fion Zhang


A flaw, such as a broken wire in a cable or a fractured rebar, produces a<br />

distinctive magnetic field anomaly that depends on the size of the<br />

discontinuity and its distance from the sensor. Because the signal shape that<br />

results from such an anomaly is known, flaw detection is enhanced by<br />

searching magnetic field records for specific signal shapes, that is, those that<br />

are characteristic of discontinuities in magnetic materials. In the MFD system,<br />

this is accomplished by a computer program that compares signal shapes<br />

with typical flaw signal shapes. The program produces a correlation<br />

coefficient that serves as a measure of similarity of the observed signal shape<br />

to a typical flaw signal shape. Flaw detection is therefore not only enhanced<br />

by signal shape discrimination but also automated by computer processing of<br />

the magnetic field data. Laboratory tests have demonstrated the ability of the<br />

system to detect fracture in steel rebars and cables in a large pre-stressed<br />

concrete structure. Also planned are field tests of the equipment in the<br />

inspection of bridge decks for reinforcement corrosion damage.<br />

Charlie Chong/ Fion Zhang


Steel rebars and cables in a large pre-stressed concrete structure.<br />

Charlie Chong/ Fion Zhang


2.0 Nondestructive Characterization of Materials.<br />

Only two examples of magnetic methods for monitoring material<br />

properties are given because the examples chosen should suffice to illustrate<br />

the types of tests that might be employed. Measurements of magnetic<br />

characteristics can, however, provide a wealth of data, and various features<br />

of such data can yield information on different material properties. For<br />

example, it has been demonstrated that different features of magnetic<br />

hysteresis data can be interpreted in terms of heat treatment and<br />

microstructure, plastic deformation, residual stress, and mechanical hardness.<br />

An example of the effects of mechanical hardness on hysteresis data is<br />

shown in Fig. 10. These data were obtained in the absence of applied tensile<br />

stress with the experimental arrangement shown in Fig. 7. Specimens of<br />

different hardness were prepared by tempering at different temperatures. The<br />

grain size (ASTM No. 7) was the same for all four specimens used in these<br />

tests. Other data showed, however, that grain size has little effect on<br />

hysteretic behavior for the classes of alloys studied.<br />

Charlie Chong/ Fion Zhang


Fig. 10 Effect of mechanical hardness on hysteresis loop data. (a) AISI 410<br />

stainless steel. (b) SAE 4340 steel.<br />

Charlie Chong/ Fion Zhang


The main point illustrated in Fig. 10 is that the mechanically harder<br />

specimens of the same alloy are also harder to magnetize; that is, the flux<br />

density, B, obtained at a large value of H is smaller for mechanically harder<br />

specimens than for softer specimens. For one alloy, AISI 410 stainless steel,<br />

the hysteresis loop intersects the B = 0 axis at larger values of H for the<br />

harder specimen than for the softer specimen; that is, the coercive force is<br />

greater for the harder material. However, for the other material, SAE 4340<br />

steel, the coercive force does not change with hardness. This suggests that,<br />

for the two alloys considered here, the saturation flux density provides a more<br />

reliable measure of hardness than the coercive force. Mayos et al. used two<br />

quite different techniques to measure the depth of surface decarburization of<br />

steels. One method was a variation of a standard eddy current test, with the<br />

difference from standard practice being that eddy current probe response was<br />

measured in the presence of a low-frequency (~0.1 Hz) magnetic field. This<br />

arrangement provides a measure of incremental permeability, that is, the<br />

magnetic permeability corresponding to changes in the applied field about<br />

some quasistatic value. The second method employed was Barkhausen<br />

noise analysis.<br />

Charlie Chong/ Fion Zhang


Keywords:<br />

• For one alloy, AISI 410 stainless steel, the hysteresis loop intersects the B<br />

= 0 axis at larger values of H for the harder specimen than for the softer<br />

specimen; that is, the coercive force is greater for the harder material.<br />

However, for the other material, SAE 4340 steel, the coercive force does<br />

not change with hardness.<br />

• This suggests that, for the two alloys considered here, the saturation flux<br />

density provides a more reliable measure of hardness than the coercive<br />

force.<br />

Charlie Chong/ Fion Zhang


Depth of decarburization was analyzed by varying the frequency of the<br />

excitation field, thus changing the skin depth in the material. Experiments<br />

were performed with both artificial samples containing two layers of different<br />

carbon content and industrial samples in which carbon concentration varied<br />

smoothly with distance from the surface. It was shown that certain features of<br />

both Barkhausen noise and incremental permeability data can be correlated<br />

with depth of decarburization. The Barkhausen noise method showed a<br />

somewhat stronger sensitivity to depth, but was useful over a smaller range of<br />

depths than the incremental permeability method. It can be concluded that<br />

both methods are useful, with the optimum choice depending on accuracy<br />

requirements and the expected depth of decarburization.<br />

Charlie Chong/ Fion Zhang


Offshore Structures<br />

Charlie Chong/ Fion Zhang


Offshore Structures<br />

Charlie Chong/ Fion Zhang


VLCC<br />

Charlie Chong/ Fion Zhang


Offshore Structures<br />

Charlie Chong/ Fion Zhang


Offshore Structures<br />

Charlie Chong/ Fion Zhang


Offshore Structures<br />

Charlie Chong/ Fion Zhang


Pipeline & Piping<br />

Charlie Chong/ Fion Zhang


Pipeline & Piping<br />

Charlie Chong/ Fion Zhang


Charlie Chong/ Fion Zhang


ass<br />

Charlie Chong/ Fion Zhang

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