Electromagnetic testing emt-mft chapter 9b
Electromagnetic testing emt-mft chapter 9b
Electromagnetic testing emt-mft chapter 9b
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<strong>Electromagnetic</strong> Testing<br />
MFLT/ ECT/ Microwave/RFT<br />
Chapter 9B – 漏 磁 检 测<br />
More Reading on Magnetic Field Leakage Testing MFLT<br />
1st Feb 2015<br />
My ASNT Level III Pre-Exam Preparatory<br />
Self Study Notes<br />
Charlie Chong/ Fion Zhang
Refinery & Appurtenances<br />
Charlie Chong/ Fion Zhang
Ship building<br />
Charlie Chong/ Fion Zhang
Offshore Structures & Appurtenances<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/CANDU_reactor
Offshore Structures & Appurtenances<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/CANDU_reactor
Offshore Structures & Appurtenances<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/CANDU_reactor
Offshore Structures & Appurtenances<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/CANDU_reactor
Offshore Structures & Appurtenances<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/CANDU_reactor
Offshore Structures & Appurtenances<br />
Charlie Chong/ Fion Zhang
Nuclear Power Station<br />
Charlie Chong/ Fion Zhang
Offshore Structures & Appurtenances<br />
Charlie Chong/ Fion Zhang
Power Piping<br />
Charlie Chong/ Fion Zhang
Power Piping<br />
Charlie Chong/ Fion Zhang
Offshore Structures & Appurtenances<br />
Charlie Chong/ Fion Zhang
Charlie Chong/ Fion Zhang
NDT Level III Examinations<br />
Basic and Method Exams<br />
ASNT NDT Level III certification candidates are required to pass both the NDT Basic and a<br />
method examination in order to receive the ASNT NDT Level III certificate.<br />
Exam Specifications<br />
The table below lists the number of questions and time allowed for each exam. Clicking on an<br />
exam will take you to an abbreviated topical outline and reference page for that exam. For the full<br />
topical outlines and complete list of references, see the topical outlines listed in the American<br />
National Standard ANSI/ASNT CP-105, Standard Topical Outlines for Qualification of<br />
Nondestructive Testing Personnel.<br />
MFL<br />
Magnetic Flux Leakage Testing<br />
90 Questions Time: 2 hrs Certification: NDT only<br />
Charlie Chong/ Fion Zhang
Fion Zhang at Shanghai<br />
2015 February<br />
Charlie Chong/ Fion Zhang<br />
Shanghai 上 海
Charlie Chong/ Fion Zhang
Chapter 9B:<br />
Magnetic Field Testing<br />
Charlie Chong/ Fion Zhang<br />
ASM Metal Handbook Vol.17 Nondestructive evaluation and Quality control
PART 1. Magnetic Field Testing<br />
1.0 Introduction<br />
MAGNETIC FIELD TESTING includes some of the older and more widely<br />
used methods for the nondestructive evaluation of materials. Historically,<br />
such methods have been in use for more than 50 years in the examination of<br />
magnetic materials for defects such as cracks, voids, or inclusions of foreign<br />
material. More recently, magnetic methods for assessing other material<br />
properties, such as grain size, texture, or hardness, have received increasing<br />
attention.<br />
Because of this diversion of applications, it is natural to divide the field of<br />
magnetic materials <strong>testing</strong> into two parts, one directed toward defect<br />
detection and characterization and the other aimed at material properties<br />
measurements. This article is primarily concerned with the first class of<br />
applications, namely, the detection, classification, and sizing of material flaws.<br />
However, an attempt has also been made to provide at least an introductory<br />
description of materials characterization principles, along with a few examples<br />
of applications. This is supplemented by references to other review articles.<br />
Charlie Chong/ Fion Zhang<br />
ASM Metal Handbook Vol.17 Nondestructive evaluation and Quality control
Keywords:<br />
Field of magnetic materials <strong>testing</strong> into two parts,<br />
• one directed toward defect detection and characterization and<br />
• the other aimed at material properties measurements.<br />
Charlie Chong/ Fion Zhang<br />
ASM Metal Handbook Vol.17 Nondestructive evaluation and Quality control
All magnetic methods of flaw detection rely in some way on the detection and<br />
measurement of the magnetic flux leakage field near the surface of the<br />
material, which is caused by the presence of the flaw. For this reason,<br />
magnetic <strong>testing</strong> techniques are often described as flux leakage field or<br />
magnetic perturbation methods. The magnetic particle inspection method is<br />
one such flux leakage method that derives its name from the particular<br />
method used to detect the leakage field. Because the magnetic particle<br />
method is described in the article "Magnetic Particle Inspection" in this<br />
Volume, the techniques discussed in this article will be limited to other forms<br />
of leakage field measurement.<br />
Keywords:<br />
flux leakage field FLF or magnetic perturbation 扰 动 methods.<br />
Charlie Chong/ Fion Zhang
Although it is conceivable that leakage field fluctuations associated with<br />
metallurgical microstructure might be used in the analysis of material<br />
properties, the characterization methods now in use rely on bulk<br />
measurements of the hysteretic properties of material magnetization or of<br />
some related phenomenon, such as Barkhausen noise. The principles and<br />
applications of magnetic characterization presented in this article are not<br />
intended to be exhaustive, but rather to serve as illustrations of this type of<br />
magnetic <strong>testing</strong>.<br />
The principles and techniques of leakage field <strong>testing</strong> and magnetic<br />
characterization are described in the two sections that follow. These sections<br />
will discuss concepts and methods that are essential to an understanding of<br />
the applications described in later sections. The examples of applications<br />
presented in the third section will provide a brief overview of the variety of<br />
inspection methods that fall under the general heading of magnetic <strong>testing</strong>.<br />
Keywords:<br />
■ Barkhausen noise<br />
Charlie Chong/ Fion Zhang
Barkhausen Noise<br />
The Barkhausen effect is a name given to the noise in the magnetic output of a<br />
ferromagnet when the magnetizing force applied to it is changed. Discovered by<br />
German physicist Heinrich Barkhausen in 1919, it is caused by rapid changes of size<br />
of magnetic domains (similarly magnetically oriented atoms in ferromagnetic<br />
materials).<br />
Barkhausen's work in acoustics and magnetism led to the discovery, which provided<br />
evidence that magnetization affects whole domains of a ferromagnetic material, rather<br />
than individual atoms alone. The Barkhausen effect is a series of sudden changes in<br />
the size and orientation of ferromagnetic domains, or microscopic clusters of aligned<br />
atomic magnets (spins), that occurs during a continuous process of magnetization or<br />
demagnetization. The Barkhausen effect offered direct evidence for the existence of<br />
ferromagnetic domains, which previously had been postulated theoretically. Heinrich<br />
Barkhausen discovered that a slow, smooth increase of a magnetic field applied to a<br />
piece of ferromagnetic material, such as iron, causes it to become magnetized, not<br />
continuously but in minute steps.<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Barkhausen_effect
Barkhausen noise: Magnetization (J) or flux density (B) curve as a function<br />
of magnetic field intensity (H) in ferromagnetic material. The inset shows<br />
Barkhausen jumps.<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Barkhausen_effect
Barkhausen noise: Domain wall motion with a Barkhausen jump<br />
Charlie Chong/ Fion Zhang<br />
http://upload.wikimedia.org/wikipedia/commons/7/79/Barkhausensprung.gif
Barkhausen noise<br />
A coil of wire wound on the ferromagnetic material can demonstrate the sudden,<br />
discontinuous jumps in magnetization. The sudden transitions in the magnetization of<br />
the material produce current pulses in the coil. These can be amplified to produce a<br />
series of clicks in a loudspeaker. This sounds as crackle, complete with skewed<br />
pulses which sounds like candy being unwrapped, Rice crispier, or a pine log fire.<br />
Hence the name Barkhausen noise. Similar effects can be observed by applying only<br />
mechanical stresses (e.g. bending) to the material placed in the detecting coil.<br />
These magnetization jumps are interpreted as discrete changes in the size or rotation<br />
of ferromagnetic domains. Some microscopic clusters of atomic spins aligned with the<br />
external magnetizing field increase in size by a sudden reversal of neighbouring spins;<br />
and, especially as the magnetizing field becomes relatively strong, other whole<br />
domains suddenly turn into the direction of the external field. Simultaneously, due to<br />
exchange interactions the spins tend to align themselves with their neighbours. The<br />
tension between the various pulls creates avalanching, where a group of neighbouring<br />
domains will flip in quick succession to align with the external field. So the material<br />
magnetizes neither gradually nor all at once, but in fits and starts.<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Barkhausen_effect
Practical use<br />
A set-up for non-destructive <strong>testing</strong> of ferromagnetic materials: green – magnetising<br />
yoke, red – inductive sensor, grey – sample under test. The amount of Barkhausen<br />
noise for a given material is linked with the amount of impurities, crystal dislocations,<br />
etc. and can be a good indication of mechanical properties of such a material.<br />
Therefore, the Barkhausen noise can be used as a method of non-destructive<br />
evaluation of the degradation of mechanical properties in magnetic materials<br />
subjected to cyclic mechanical stresses (e.g. in pipeline transport) or high-energy<br />
particles (e.g. nuclear reactor) or materials such as high-strength steels which may be<br />
subjected to damage from grinding. Schematic diagram of a simple non-destructive<br />
set-up for such a purpose is shown on the right.<br />
Barkhausen noise can also indicate physical damage in a thin film structure due to<br />
various nanofabrication processes such as reactive ion etching or using an ion milling<br />
machine<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Barkhausen_effect
A set-up for non-destructive <strong>testing</strong> of ferromagnetic materials:<br />
• green – magnetizing yoke,<br />
• red – inductive sensor,<br />
• grey – sample under test.<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Barkhausen_effect
Magnetic Dipole<br />
Charlie Chong/ Fion Zhang
Magnetic Dipole<br />
Charlie Chong/ Fion Zhang
2.0 Principles of Magnetic Leakage Field Testing MLFT<br />
2.1 Origin of Defect Leakage Fields.<br />
The origin of the flaw leakage field is illustrated in Fig. 1. Figure 1(a) shows a<br />
uniformly magnetized rod, which consists of a large number of elementary<br />
magnets aligned with the direction of magnetization. Inside the material, each<br />
magnetic pole is exactly compensated by the presence of an adjacent pole of<br />
opposite polarity, and the net result is that interior poles do not contribute to<br />
the magnetic field outside the material. At the surfaces, however, magnetic<br />
poles are uncompensated and therefore produce a magnetic field in the<br />
region surrounding the specimen. This is illustrated in Fig. 1(a) by flux lines<br />
connecting uncompensated elementary poles.<br />
Charlie Chong/ Fion Zhang
If a slot is cut in the rod, as illustrated in Fig. 1(b), the poles on the surface of<br />
this slot are now also uncompensated and therefore produce a localized<br />
magnetic field near the slot. This additional magnetic field, which is<br />
represented by the extra flux lines in Fig. 1(b), is the leakage field associated<br />
with the slot. Figure 1, although adequate for a qualitative understanding of<br />
the origin of leakage fields, does not provide an exact quantitative description.<br />
The difficulty is the assumption that the magnetization remains uniform when<br />
the flaw is introduced. In general, this does not happen, because the<br />
presence of the flaw changes the magnetic field in the vicinity of the flaw, and<br />
this in turn leads to a change in magnetization near the flaw. With regard to<br />
Fig. 1, this means that the strengths and orientations of the elementary<br />
dipoles (magnets) actually vary from point to point in the vicinity of the flaw,<br />
and this variation also contributes to the flaw leakage field. The end result is<br />
that the accurate description of a flaw leakage field poses a difficult<br />
mathematical problem that usually requires a special-purpose computer code<br />
for its solution.<br />
Charlie Chong/ Fion Zhang
Fig. 1 Origin of defect leakage fields. (a) Magnetic flux lines of a magnet<br />
without a defect. (b) Magnetic flux lines of a magnet with a surface defect.<br />
Source: Ref 1<br />
Charlie Chong/ Fion Zhang
2.2 Experimental Techniques.<br />
One of the first considerations in the experimental application of magnetic<br />
leakage field methods is the generation of a suitable magnetic field within the<br />
material. In some ferromagnetic materials, the residual field (the field that<br />
remains after removal of an external magnetizing field) is often adequate for<br />
surface flaw detection. In practice, however, residual magnetization is rarely<br />
used because use of an applied magnetizing field ensures that the material is<br />
in a desired magnetic state (which should be known and well characterized)<br />
and because applied fields provide more flexibility (that is, one can produce a<br />
high or low flux density in the specimen as desired. Experience has shown<br />
that control of the strength and direction of the magnetization can be useful in<br />
improving flaw detectability and in discriminating among different types of<br />
flaws. In general, the magnitude of the magnetization should be chosen to<br />
maximize the flaw leakage field with respect to other field sources that might<br />
interfere with flaw detection; the optimum magnetization is usually difficult to<br />
determine in advance of a test and is often approached by trial-and-error<br />
experimentation. The direction of the field should be perpendicular to the<br />
largest flaw dimension to maximize the effect of the flaw on the leakage field.<br />
Charlie Chong/ Fion Zhang
Keywords:<br />
The direction of the field should be perpendicular to the largest flaw<br />
dimension to maximize the effect of the flaw on the leakage field.<br />
Charlie Chong/ Fion Zhang
It is possible to generate a magnetic field in a specimen either directly or<br />
indirectly. In direct magnetization, current is passed directly through the part.<br />
With the indirect approach, magnetization is induced by placing the part in a<br />
magnetic field that is generated by an adjacent current conductor or<br />
permanent magnet. This can be done, for example, by threading a conductor<br />
through a hollow part such as a tube or by passing an electric current through<br />
a cable wound around the part. Methods of magnetizing a part both directly<br />
and indirectly are illustrated schematically in Fig. 2.<br />
Charlie Chong/ Fion Zhang
Fig. 2 Methods of magnetization. (1) Head-shot method. (b) Magnetization<br />
with prods. (c) Magnetization with a central conductor. (d) Longitudinal<br />
magnetization. (e) Yoke magnetization<br />
Charlie Chong/ Fion Zhang
The flaw leakage field can be detected with one of several types of magnetic<br />
field sensors. Aside from the use of magnetic particles, the sensors most<br />
often used are the inductive coil and the Hall effect device. The inductive coil<br />
sensor is based on Faraday's law of induction, which states that the voltage<br />
induced in the coil is proportional to the number of turns in the coil multiplied<br />
by the time rate of change of the flux Ф threading the coil. It follows that<br />
detection of a magnetostatic field requires that the coil be in motion so that<br />
the flux through the coil changes with time. The principle is illustrated in Fig. 3,<br />
in which the coil is oriented so as to sense the change in flux parallel to the<br />
surface of the specimen. If the direction of coil motion is taken as x, then the<br />
induced electromotive force, E, in volts is given by:<br />
for Ф = B∙A<br />
Charlie Chong/ Fion Zhang
where N is the number of turns in the coil, A is its cross-sectional area, and B<br />
is the flux density, in Gauss, parallel to the surface of the part. Thus, the<br />
voltage induced in the coil is proportional to the gradient of the flux density<br />
along the direction of coil motion multiplied by the coil velocity. Figure 4<br />
shows the flux density typical of the leakage field from a slot, along with the<br />
corresponding signal from a search coil oriented as in Fig. 3.<br />
Charlie Chong/ Fion Zhang
Fig. 3 Flux leakage measurement using a search coil. Source:<br />
Charlie Chong/ Fion Zhang
Fig. 4 Leakage flux and search coil signal as a function of position.<br />
Charlie Chong/ Fion Zhang
Unlike the inductive coil, which provides a measure of the flux gradient, a Hall<br />
effect sensor directly measures the component of the flux itself in the direction<br />
perpendicular to the sensitive area of the device. Because the response of a<br />
Hall effect sensor does not depend on the motion of the probe, it can be<br />
scanned over the surface to be inspected at any rate that is mechanically<br />
convenient. In this respect, the Hall device has an advantage over the coil<br />
sensor because there is no need to maintain a constant scanning speed<br />
during the inspection. On the other hand, Hall effect sensors are more difficult<br />
to fabricate, are somewhat delicate compared to inductive coil sensors, and<br />
require more complex electronics. Other magnetic field sensors that are used<br />
less often in leakage field applications include the flux gate magnetometer,<br />
magnetoresistive sensors, magnetic resonance sensors, and magnetographic<br />
sensors, in which the magnetic field at the surface of a part is registered on a<br />
magnetic tape pressed onto the surface.<br />
Keywords:<br />
Hall device has an advantage over the coil sensor because there is no need<br />
to maintain a constant scanning speed during the inspection.<br />
Charlie Chong/ Fion Zhang
2.3 Analysis of Leakage Field Data.<br />
In most applications of the leakage field method, there is a need not only to<br />
detect the presence of a flaw but also to estimate its severity. This leads to<br />
the problem of flaw characterization, that is, the determination of flaw<br />
dimensions from an analysis of leakage field data. The most widely used<br />
method of flaw characterization is based on the assumptions that the leakage<br />
field signal amplitude is proportional to the size of the flaw (which usually<br />
means its depth into the material) and that the signal amplitude can therefore<br />
be taken as a direct measure of flaw severity. In situations where all flaws<br />
have approximately the same shape and where calibration experiments show<br />
that the signal amplitude is indeed proportional to the size parameter of<br />
concern, this empirical method of sizing works quite well.<br />
Keywords:<br />
The most widely used method of flaw characterization is based on the<br />
assumptions that the leakage field signal amplitude is proportional to the size<br />
of the flaw (which usually means its depth into the material) ()<br />
Charlie Chong/ Fion Zhang
There are, however, many situations of interest where flaw shapes vary<br />
considerably and where signal amplitude is not uniquely related to flaw depth,<br />
as is the case for corrosion pits in steel tubing. In addition, different types of<br />
flaws, such as cracks and pits, can occur in the same part, in which case it<br />
becomes necessary to determine the flaw types present as well as their<br />
severity.<br />
In such cases, a more careful analysis of the relationship between signal and<br />
flaw characteristics is required if serious errors in flaw characterization are to<br />
be avoided. One of the earliest attempts to use a theoretical model in the<br />
analysis of leakage field data was based on the analytic solution for the field<br />
perturbed by a spherical inclusion. Two conclusions were drawn from this<br />
analysis. First, when one measures the leakage flux component normal to the<br />
surface of the part, the center of the flaw is located below the scan plane at a<br />
distance equal to the peak-to-peak separation distance in the flaw signal (Fig.<br />
5), and second, the peak-to-peak signal amplitude is proportional to the flaw<br />
volume. A number of experimental tests of these sizing rules have confirmed<br />
the predicted relationships for nonmagnetic inclusions in steel parts<br />
Charlie Chong/ Fion Zhang
Keywords:<br />
Two conclusions were drawn from this analysis.:<br />
• First, when one measures the leakage flux component normal to the<br />
surface of the part, the center of the flaw is located below the scan plane<br />
at a distance equal to the peak-to-peak separation distance in the flaw<br />
signal (Fig. 5), and<br />
• Second, the peak-to-peak signal amplitude is proportional to the flaw<br />
volume. A number of experimental tests of these sizing rules have<br />
confirmed the predicted relationships for nonmagnetic inclusions in steel<br />
parts<br />
peak-to-peak signal amplitude is<br />
proportional to the flaw volume.<br />
Lateral<br />
dimension<br />
Charlie Chong/ Fion Zhang
Fig. 5 Dependence of magnetic signal peak separation (a) on the depth of a<br />
spherical inclusion (b)<br />
Charlie Chong/ Fion Zhang
Further theoretical and experimental data for spheroidal inclusions and<br />
surface pits have shown, however, that the simple characterization rules for<br />
spherical inclusions do not apply when the flaw shape differs significantly<br />
from the ideal sphere. In such cases, the signal amplitude depends on the<br />
lateral extent of the flaw and on its volume, and characterization on the basis<br />
of leakage field analysis becomes much more complicated.<br />
Finally, there has been at least one attempt to apply finite-element<br />
calculations of flaw leakage fields to the development of characterization<br />
rules for a more general class of flaws. Hwang and Lord performed most of<br />
their computations for simple flaw shapes, such as rectangular and triangular<br />
slots and inclusions, and from the results devised a set of rules for estimating<br />
the depth, width, and angle of inclination of a flaw with respect to the surface<br />
of the part. One of their applications to a flaw of complex shape is shown in<br />
Fig. 6.<br />
Charlie Chong/ Fion Zhang
Fig. 6 Characterization of a ferrite-tail type of defect. The dashed line shows<br />
the flaw configuration estimated from the leakage field data.<br />
Charlie Chong/ Fion Zhang
The promising results obtained from the finite-element work of Hwang and<br />
Lord, as well as the analytically based work on spheroidal flaws, suggest that<br />
the estimation of flaw size and shape from leakage field data is feasible.<br />
Another numerical method potentially applicable to flux leakage problems is<br />
the boundary integral method, which may prove useful in flaw<br />
characterization. Unfortunately, much more work must be done on both the<br />
theoretical basis and on experimental <strong>testing</strong> before it will be possible to<br />
analyze experimental leakage field data with confidence in terms of flaw<br />
characteristics.<br />
Charlie Chong/ Fion Zhang
PART 2. Principles of Magnetic Characterization of Materials<br />
1.0 Metallurgical and Magnetic Properties.<br />
The use of magnetic measurements to monitor the metallurgical properties<br />
of ferromagnetic materials is based on the fact that variables such as<br />
crystallographic phase, chemical composition, and microstructure, which<br />
determine the physical properties of materials, also affect their magnetic<br />
characteristics. Some parameters, such as grain size and orientation,<br />
dislocation density, and the existence of precipitates, are closely related to<br />
measurable characteristics of magnetic hysteresis, that is, to the behavior of<br />
the flux density, B, induced in a material as a function of the magnetic field<br />
strength, H. This relationship can be understood in principle from the physical<br />
theory of magnetic domains. Magnetization in a particular direction increases<br />
as the domains aligned in that direction grow at the expense of domains<br />
aligned in other directions. Factors that impede domain growth also impede<br />
dislocation motion; hence the connection, at a very fundamental level,<br />
between magnetic and mechanical properties.<br />
Charlie Chong/ Fion Zhang
Keywords:<br />
Metallurgical properties:<br />
• Crystallographic phase,<br />
• Chemical composition,<br />
• Grain size and orientation,<br />
• Dislocation density, and<br />
• Existence of precipitates,<br />
are closely related to measurable characteristics of magnetic hysteresis, that<br />
is, to the behavior of the flux density, B, induced in a material as a function of<br />
the magnetic field strength, H.<br />
Charlie Chong/ Fion Zhang
Hysteresis Curves<br />
Charlie Chong/ Fion Zhang
Other magnetic properties, such as the saturation magnetization, which is the<br />
maximum value B can achieve, or the Curie temperature at which there is a<br />
transition to a nonmagnetic state, are less dependent on microstructure, but<br />
are sensitive to such factors as crystal structure and chemical composition.<br />
Interest in the magnetic characterization of materials, principally steels,<br />
derives from many such relationships between measurable magnetic<br />
parameters and metallurgical properties. These relationships are, however,<br />
quite complicated in general, and it is often difficult to determine how or if a<br />
particular measurement or combination of measurements can be used to<br />
determine a property of interest.<br />
Charlie Chong/ Fion Zhang
Nevertheless, the prospect of nondestructive monitoring and quality control is<br />
an attractive one, and for this reason research on magnetic materials<br />
characterization continues to be an active field. It is not the purpose of this<br />
article to explore such magnetic methods in depth, but simply to point out that<br />
it is an active branch of nondestructive magnetic <strong>testing</strong>. The more<br />
fundamental aspects of the relationship between magnetism and metallurgy<br />
are discussed in Ref 26 and 28. Engineering considerations are reviewed in<br />
Ref 24. The proceedings of various symposia also contain several papers<br />
that provide a good overview of the current status of magnetic materials<br />
characterization.<br />
Charlie Chong/ Fion Zhang
Curie temperature<br />
In physics and materials science, the Curie temperature (Tc), or Curie point, is the temperature<br />
where a material's permanent magnetism changes to induced magnetism. The force of<br />
magnetism is determined by magnetic moments. The Curie temperature is the critical point<br />
where a material's intrinsic magnetic moments change direction. Magnetic moments are<br />
permanent dipole moments within the atom which originate from electrons' angular momentum<br />
and spin. Materials have different structures of intrinsic magnetic moments that depend on<br />
temperature. At a material's Curie Temperature those intrinsic magnetic moments change<br />
direction.<br />
Permanent magnetism is caused by the alignment of magnetic moments and induced magnetism<br />
is created when disordered magnetic moments are forced to align in an applied magnetic field.<br />
For example, the ordered magnetic moments (ferromagnetic, figure 1) change and become<br />
disordered (paramagnetic, figure 2) at the Curie Temperature. Higher temperatures make<br />
magnets weaker as spontaneous magnetism only occurs below the Curie Temperature. Magnetic<br />
susceptibility only occurs above the Curie Temperature and can be calculated from the Curie-<br />
Weiss Law which is derived from Curie's Law. In analogy to ferromagnetic and paramagnetic<br />
materials, the Curie temperature can also be used to describe the temperature where a<br />
material's spontaneous electric polarisation changes to induced electric polarisation or the<br />
reverse upon reduction of the temperature below the Curie temperature.<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Curie_temperature
Curie temperature<br />
Below T c<br />
Ferromagnetic<br />
Ferrimagnetic<br />
Antiferromagnetic<br />
Above T c<br />
↔ Paramagnetic<br />
↔ Paramagnetic<br />
↔ Paramagnetic<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Curie_temperature
Ferromagnetism The magnetic moments in a ferromagnetic material. The<br />
moments are ordered and of the same magnitude in the absence of an<br />
applied magnetic field.<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Curie_temperature
Paramagnetism The magnetic moments in a paramagnetic material. The<br />
moments are disordered in the absence of an applied magnetic field and<br />
ordered in the presence of an applied magnetic field.<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Curie_temperature
Ferrimagnetism The magnetic moments in a ferrimagnetic material. The<br />
moments are aligned oppositely and have different magnitudes due to being<br />
made up of two different ions. This is in the absence of an applied magnetic<br />
field.<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Curie_temperature
Antiferromagnetism The magnetic moments in an antiferromagnetic<br />
material. The moments are aligned oppositely and have the same<br />
magnitudes. This is in the absence of an applied magnetic field.<br />
Charlie Chong/ Fion Zhang<br />
http://en.wikipedia.org/wiki/Curie_temperature
2.0 Experimental Techniques.<br />
A typical setup for measuring the B-H characteristic of a rod specimen is<br />
shown in Fig. 7. The essential elements are an electromagnet for generating<br />
the magnetizing field, a coil wound around the specimen for measuring the<br />
time rate of change of the magnetic flux, B, in the material, and a magnetic<br />
field sensor, in this case a Hall effect probe, for measuring the magnetic field<br />
strength, H, parallel to the surface of the part. The signal generator provides a<br />
low-frequency magnetizing field, typically of the order of a few Hertz, and the<br />
output of the flux measuring coil is integrated over time to give the flux density<br />
in the material. In the arrangement shown in Fig. 7, an additional feature is<br />
the provision for applying a tensile load to the specimen for studies of the<br />
effects of stress on the hysteresis data. When using a rod specimen such as<br />
this, it is important that the length-to-diameter ratio of the specimen be large<br />
so as to minimize the effects of stray fields from the ends of the rod on the<br />
measurements of B and H.<br />
Charlie Chong/ Fion Zhang
Fig. 7 Experimental arrangement for hysteresis loop measurements.<br />
Charlie Chong/ Fion Zhang
Another magnetic method that uses a similar arrangement is the<br />
measurement of Barkhausen noise. As the magnetic field strength, H, is<br />
varied at a very slow rate, discontinuous jumps in the magnetization of the<br />
material can be observed during certain portions of the hysteresis cycle.<br />
These jumps are associated with the sudden growth of a series of magnetic<br />
domains that have been temporarily stopped from further growth by such<br />
obstacles as grain boundaries, precipitates, or dislocations. Barkhausen<br />
noise is therefore dependent on microstructure and can be used<br />
independently of hysteresis measurements, or in conjunction with such<br />
measurements, as another method of magnetic <strong>testing</strong>. The experimental<br />
arrangement differs from that shown in Fig. 7 in that a single sensor coil,<br />
oriented to measure the flux normal to the surface of the specimen, is used<br />
instead of the Hall probe and the flux winding.<br />
Charlie Chong/ Fion Zhang
The review articles and conference proceedings cited above contain<br />
additional detail on experimental technique and a wealth of information on the<br />
interpretation of hysteresis and Barkhausen data. However, it should be noted<br />
that test methods and data interpretation are often very specific to a particular<br />
class of alloy, and techniques that seem to work well for one type of material<br />
may be totally inappropriate for another. The analysis of magnetic<br />
characterization data is still largely empirical in nature, and controlled <strong>testing</strong><br />
of a candidate technique with the specific alloy system of interest is advisable.<br />
Charlie Chong/ Fion Zhang
PART 3. Application<br />
1.0 Flaw Detection by the Flux Leakage Method.<br />
Perhaps the most prevalent use of the flux leakage method is the<br />
inspection of ferromagnetic tubular goods, such as gas pipelines, down hole<br />
casing, and a variety of other forms of steel piping. In applications in the<br />
petroleum industry, the technique is highly developed, but details on<br />
inspection devices and methods of data analysis are, for the most part,<br />
considered proprietary by the companies that provide inspection services.<br />
Still, the techniques currently in use have certain features in common, and<br />
these are exemplified by the typical system described below. The device<br />
shown in Fig. 8 is an inspection tool for large-diameter pipelines.<br />
Magnetization is provided by a large electromagnet fitted with wire brushes to<br />
direct magnetic flux from the electromagnet into the pipe wall. To avoid<br />
spurious signals from hard spots in the material, the magnetization circuit is<br />
designed for maximum flux density in the pipe wall in an attempt to<br />
magnetically saturate the material.<br />
Charlie Chong/ Fion Zhang
Leakage field sensors are mounted between the pole pieces of the magnet in<br />
a circle around the axis of the device to provide, as nearly as possible, full<br />
coverage of the pipe wall. In most such tools, the sensors are the inductive<br />
coil type, oriented to measure the axial component of the leakage field<br />
gradient. Data are usually recorded on magnetic tape as the system is<br />
propelled down a section of pipe. After the inspection, the recorded signals<br />
are compared with those from calibration standards in an attempt to interpret<br />
flaw indications in terms of flaw type and size.<br />
Charlie Chong/ Fion Zhang
Fig. 8 Typical gas pipeline inspection pig. The tool consists of a drive unit, an<br />
instrumentation unit, and a center section with an electromagnetic and flux<br />
leakage sensors.<br />
Sensor<br />
Pipe<br />
Pole<br />
Pole<br />
Coil<br />
Sensor<br />
Charlie Chong/ Fion Zhang
In addition to systems for inspecting rotationally symmetric cylindrical parts,<br />
flux leakage inspection has been applied to very irregular components, such<br />
as helicopter rotor blade D-spars, gear teeth, and artillery projectiles. Several<br />
of these special-purpose applications have involved only laboratory<br />
investigations, but in some cases specialized instrumentation systems have<br />
been developed and fabricated for factory use. These systems are uniquely<br />
adapted to the particular application involved, and in most cases only one or<br />
at most several instrumentation systems have been built. Even in the case of<br />
laboratory investigations, special-purpose detection probe and magnetizing<br />
arrangements have been developed for specific applications.<br />
Charlie Chong/ Fion Zhang
One such system for automated thread inspection on drill pipe and collars is<br />
described: The device consists of an electromagnet and an array of sensors<br />
mounted outside a nonmagnetic cone that threads onto the tool joint. The<br />
assembly is driven in a helical path along the threads by a motor/clutch<br />
assembly. To minimize the leakage flux signal variations caused by the<br />
threads, signals from the sensor array are compared differentially. The<br />
system is capable of operating in a high field strength mode for the detection<br />
of cracks and corrosion pits and also in a residual field mode for the detection<br />
of other forms of damage. At last report, the system was undergoing field<br />
tests and was found to offer advantages, in terms of ease of application and<br />
defect detection, over the magnetic particle technique normally used for<br />
thread inspection.<br />
Charlie Chong/ Fion Zhang
The flux leakage method is also finding application in the inspection of ropes<br />
and cables made of strands of ferromagnetic material. One approach is to<br />
induce magnetization in the piece by means of an encircling coil energized by<br />
a direct current (dc). With this method, one measures the leakage field<br />
associated with broken strands using a Hall effect probe or an auxiliary<br />
sensor coil. A complementary method with alternating current (ac), which is<br />
actually an eddy current test rather than flux leakage, is to measure the ac<br />
impedance variations in an encircling coil caused by irregularities in the<br />
cross-sectional area of the specimen. Haynes and Underbakke describe<br />
practical field tests of an instrumentation system that utilizes both the ac and<br />
dc methods. They conclude that instrumentation capable of a combination of<br />
inspection techniques offers the best possibility of detecting both localized<br />
flaws and overall loss of cross section caused by generalized corrosion and<br />
wear. They also present detailed information on the practical characteristics<br />
of a commercially available device that makes use of both the ac and dc<br />
methods.<br />
Charlie Chong/ Fion Zhang
Charlie Chong/ Fion Zhang<br />
The flux leakage method is also finding application in<br />
the inspection of ropes and cables
Another area in which the flux leakage method has been successfully<br />
implemented is the inspection of rolling-element antifriction bearings. A<br />
schematic illustration of the method as applied to an inner bearing race is<br />
shown in Fig. 9. In this application, the part is magnetized by an<br />
electromagnet, as indicated in Fig. 9(a). The race is then rotated by a spindle,<br />
and the surface is scanned with an induction coil sensor. Typically, the race is<br />
rotated at a surface speed of about 2.3 m/s (7.5 ft/s), and the active portion of<br />
the raceway is inspected by incrementally indexing the sensor across the<br />
raceway. Magnetizing fields are applied in the radial and circumferential<br />
orientations. It has been shown that radial field inspection works best for<br />
surface flaws, while circumferential field inspection shows greater sensitivity<br />
to subsurface flaws. Data have been collected on a large number of bearing<br />
races to establish the correlation between leakage field signals and inclusion<br />
depths and dimensions determined by metallurgical sectioning.<br />
Charlie Chong/ Fion Zhang
Fig. 9 Flux leakage inspection of a bearing race. (a) Magnetization of inner<br />
race. (b) Perturbation in the magnetic flux at the surface of the inner race. (c)<br />
Probe scanning the surface<br />
Charlie Chong/ Fion Zhang
Finally, the flux leakage method has also been adapted to the inspection of<br />
steel reinforcement in concrete beams. The basic function of the magnetic<br />
field disturbance (MFD) inspection equipment is to provide maps of the<br />
magnetic field across the bottom and sides of the beam. An electromagnet on<br />
an inspection cart, which is suspended on tracks below the beam, provides a<br />
magnetic field that induces magnetization in permeable structures in its<br />
vicinity, such as steel rebars, cables, and stirrups. An array of Hall effect<br />
sensors distributed across the bottom and sides of the beam measures the<br />
field produced by magnetized structures within the beam. If a flaw is present<br />
in one of these magnetized structures, it will produce a disturbance of the<br />
normal magnetic field pattern associated with the unflawed beam. Thus, the<br />
idea behind the MFD system is to search the surface of the beam for field<br />
anomalies that indicate the presence of flaws in reinforcing steel within the<br />
structure.<br />
Keywords:<br />
magnetic field disturbance (MFD)<br />
Charlie Chong/ Fion Zhang
A flaw, such as a broken wire in a cable or a fractured rebar, produces a<br />
distinctive magnetic field anomaly that depends on the size of the<br />
discontinuity and its distance from the sensor. Because the signal shape that<br />
results from such an anomaly is known, flaw detection is enhanced by<br />
searching magnetic field records for specific signal shapes, that is, those that<br />
are characteristic of discontinuities in magnetic materials. In the MFD system,<br />
this is accomplished by a computer program that compares signal shapes<br />
with typical flaw signal shapes. The program produces a correlation<br />
coefficient that serves as a measure of similarity of the observed signal shape<br />
to a typical flaw signal shape. Flaw detection is therefore not only enhanced<br />
by signal shape discrimination but also automated by computer processing of<br />
the magnetic field data. Laboratory tests have demonstrated the ability of the<br />
system to detect fracture in steel rebars and cables in a large pre-stressed<br />
concrete structure. Also planned are field tests of the equipment in the<br />
inspection of bridge decks for reinforcement corrosion damage.<br />
Charlie Chong/ Fion Zhang
Steel rebars and cables in a large pre-stressed concrete structure.<br />
Charlie Chong/ Fion Zhang
2.0 Nondestructive Characterization of Materials.<br />
Only two examples of magnetic methods for monitoring material<br />
properties are given because the examples chosen should suffice to illustrate<br />
the types of tests that might be employed. Measurements of magnetic<br />
characteristics can, however, provide a wealth of data, and various features<br />
of such data can yield information on different material properties. For<br />
example, it has been demonstrated that different features of magnetic<br />
hysteresis data can be interpreted in terms of heat treatment and<br />
microstructure, plastic deformation, residual stress, and mechanical hardness.<br />
An example of the effects of mechanical hardness on hysteresis data is<br />
shown in Fig. 10. These data were obtained in the absence of applied tensile<br />
stress with the experimental arrangement shown in Fig. 7. Specimens of<br />
different hardness were prepared by tempering at different temperatures. The<br />
grain size (ASTM No. 7) was the same for all four specimens used in these<br />
tests. Other data showed, however, that grain size has little effect on<br />
hysteretic behavior for the classes of alloys studied.<br />
Charlie Chong/ Fion Zhang
Fig. 10 Effect of mechanical hardness on hysteresis loop data. (a) AISI 410<br />
stainless steel. (b) SAE 4340 steel.<br />
Charlie Chong/ Fion Zhang
The main point illustrated in Fig. 10 is that the mechanically harder<br />
specimens of the same alloy are also harder to magnetize; that is, the flux<br />
density, B, obtained at a large value of H is smaller for mechanically harder<br />
specimens than for softer specimens. For one alloy, AISI 410 stainless steel,<br />
the hysteresis loop intersects the B = 0 axis at larger values of H for the<br />
harder specimen than for the softer specimen; that is, the coercive force is<br />
greater for the harder material. However, for the other material, SAE 4340<br />
steel, the coercive force does not change with hardness. This suggests that,<br />
for the two alloys considered here, the saturation flux density provides a more<br />
reliable measure of hardness than the coercive force. Mayos et al. used two<br />
quite different techniques to measure the depth of surface decarburization of<br />
steels. One method was a variation of a standard eddy current test, with the<br />
difference from standard practice being that eddy current probe response was<br />
measured in the presence of a low-frequency (~0.1 Hz) magnetic field. This<br />
arrangement provides a measure of incremental permeability, that is, the<br />
magnetic permeability corresponding to changes in the applied field about<br />
some quasistatic value. The second method employed was Barkhausen<br />
noise analysis.<br />
Charlie Chong/ Fion Zhang
Keywords:<br />
• For one alloy, AISI 410 stainless steel, the hysteresis loop intersects the B<br />
= 0 axis at larger values of H for the harder specimen than for the softer<br />
specimen; that is, the coercive force is greater for the harder material.<br />
However, for the other material, SAE 4340 steel, the coercive force does<br />
not change with hardness.<br />
• This suggests that, for the two alloys considered here, the saturation flux<br />
density provides a more reliable measure of hardness than the coercive<br />
force.<br />
Charlie Chong/ Fion Zhang
Depth of decarburization was analyzed by varying the frequency of the<br />
excitation field, thus changing the skin depth in the material. Experiments<br />
were performed with both artificial samples containing two layers of different<br />
carbon content and industrial samples in which carbon concentration varied<br />
smoothly with distance from the surface. It was shown that certain features of<br />
both Barkhausen noise and incremental permeability data can be correlated<br />
with depth of decarburization. The Barkhausen noise method showed a<br />
somewhat stronger sensitivity to depth, but was useful over a smaller range of<br />
depths than the incremental permeability method. It can be concluded that<br />
both methods are useful, with the optimum choice depending on accuracy<br />
requirements and the expected depth of decarburization.<br />
Charlie Chong/ Fion Zhang
Offshore Structures<br />
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Offshore Structures<br />
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VLCC<br />
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Offshore Structures<br />
Charlie Chong/ Fion Zhang
Offshore Structures<br />
Charlie Chong/ Fion Zhang
Offshore Structures<br />
Charlie Chong/ Fion Zhang
Pipeline & Piping<br />
Charlie Chong/ Fion Zhang
Pipeline & Piping<br />
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Charlie Chong/ Fion Zhang
ass<br />
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