AC SIMDIS Solutions - ROFA Praha sro

AC SIMDIS SolutionsTrue Boiling Point Distributionup to C120• Compliance with Global Standard Test Methods• Unique Solutions include AC 8634 & Crude Oil Analyzer• Dedicated Correlations & CalculationsONE WORLD…ONE COMPANY…ONE TEAMwww.paclp.com

www.simdis.com2Complete Range of ApplicationsAC Analytical Controls (AC), the global SIMDIS market leader,provides solutions that accurately determine true boiling pointdata – from naphtha up to crude oil samples.• Full range of SIMDIS applicationsdetermine boiling points up to C120• Product range includes several uniquesolutions:- AC 8634 analyzer for acceleratedD 86 data of jet fuel and diesel- Crude Oil analyzer Merges DHA FrontEnd with High Temp SIMDIS Technique- Sulfur and Nitrogen SIMDIS solutionsto determine Hydrocarbon, Sulfur andNitrogen BP distributions in a singlerun- Wax ASTM D 5442 application• Dedicated correlations and calculationsare available for:- Correlation to Physical DistillationD 86 & D 1160 (ASTM D 2887; IP 406;ISO 3924)- NOACK - DIN 51.581-2- MOV - ASTM D 6417- Conversion to volume % for crude oil- Cutpoints & fractions- Flashpoint (ASTM D 7215)• Excellent LIMS connectivity: upload theresults directly to your LIMS or manuallyafter approval• Solutions comply with ASTM, CEN, DIN,IP and ISO SIMDIS methods• A broad set of calibration, reference andquality control samples completes eachSIMDIS application• User group meetings allows users toimprove analyzer performance• SIMDIS software is compatible withmajor chromatographic data systems• AC software puts the instrument instandby mode after analysis, to savegas and keep the instrument in optimalcondition• Several features contribute to theanalysis precision:- Use of pre-programmed sample types- Automatic blank subtraction,calibration and system validation- Customer selective start and endalgorithmVersion 6,1,0,0simdi s IP PM-CF-98 2Sample name : REFAcquired on : 3/9/01 4:05:16 PM Vial : 103Processed on : 6/11/01 7:52:35 AM Injection : 1Data File : HT750A\103F0401.DGeneral VariablesUsed BlankHT750A\101F0201.DUsed BP calibrant HT750A\102F0301.DUsed ReferenceUsed Start elution (min) 5.005Used End elution (min) 30.452Total area 173938New Response factor 5.7492e-006SignalReference CheckRecovered Target Values Determined Valuesmass % BP °C dBP °C BP °C dBP °C10.0 421.0 3.5 420.8 0.020.0 437.0 3.5 436.6 0.530.0 448.0 3.5 447.0 1.040.0 457.0 3.5 456.0 1.050.0 464.0 3.5 464.5 -0.560.0 473.0 3.5 472.5 0.570.0 481.0 3.5 480.7 0.580.0 489.0 3.5 489.6 -0.590.0 501.0 3.5 501.4 -0.5Maximum Squared Deviation = 43FoundMaximumSquaredSquaredDeviationDeviation= 434Squared Found Squared test passed Deviation = 4Squared test passedRetention Time (min)AC High Temp SIMDIS analysis of a reference sample

Compliance with GlobalStandard Test MethodsBoiling point data is a major specification in characterizing petroleumstreams. SIMDIS uses a gas chromatographic technique to determine the trueboiling point (TBP) distribution. By automating the analysis the AC SIMDISapplications provide fast and accurate boiling point results.Our active involvement in worldwide standardization committees resulted in a compliance with allASTM, CEN, DIN, IP and ISO methods and a listing of these methods in current jet fuel and dieselspecifications. The AC SIMDIS application meets and exceeds the reproducibility of the worldwidestandard test methods.www.simdis.com3Method NumberASTMD 3710ASTMD 7096ASTMD 2887*ASTMD 5307ASTMD 7213ASTMD 6352ASTMD 7169ASTMD 7398ASTMD 7500Maximum CarbonNumber reportedC 15C 16C 44C 44C 60C 90C 100C 60C 110SampleRange• Gasoline• Naphtha• Gasoline• Naphtha• Jet Fuel• Diesel• Crude Oil• Lube Oil BaseStocks• Lube Oil BaseStocks• Residue• Crude Oil• FAMES(biodiesel, B100)Blends of Dieseland Biodiesel(B1 throughB100)• Distillates,• Base Oils• Lubricating• Base StocksBoilingRangeSampleFBP < 260°C(500°F)FBP < 280°C(536°F)FBP < 538°C(1000°F)IBP > 100°C(212°F)FBP < 615°C(1138°F)IBP > 174°C(345°F)FBP < 700°C(1292°F)FBP > 720° C(1328°F)FBP < 538°C(1000°F)IBP > 100°C(212°F)FBP < 735°C(1355°F)Overview of SIMDIS ASTM methods*includes Accelerated SIMDIS/8634 TMMethod NumberISO 3924IP 406IP 480EN 15199-1DIN 51.435IP 507EN 15199-2prEN 15199-3IP 545Maximum CarbonNumber reportedC 44C 120C 120C 120SampleRange• Jet Fuel• Diesel• Lube Oil Base Stocks(totally eluting)• Residue• Crude OilBoilingRangeSampleFBP < 538°C(1000°F)IBP > 100°C (212°F) FBP< 750°C (1382°F)IBP > 100°C (212°F)FBP > 750°C (1382°F)FBP > 750°C (1382°F)Overview of SIMDIS CEN, DIN, IP, ISO methodsSignalBP° FRecovery MassRetention Time (min)Accelerated SIMDIS analysis of a reference sample

www.simdis.com4Flexible ConfigurationThe AC SIMDIS solutions are based on the new Agilent Technologies7890 Series or the 6850 gas chromatograph equipped with:• Single or dual channel, packed or capillary column(s)for boiling point separation• AC proprietary Temperature ProgrammableInlet to simplify system maintenance, improve peakidentification and prevent column contamination• Flame Ionization Detector• A 16-shot automatic liquid sampler (150 tray optional)• A set of calibration, reference, and quality controlssamples dedicated to the methodData System CompatibilityThe AC SIMDIS application offers you achoice in selecting a chromatographicdata system. The AC software allowsfully automated analysis processing andoperates on the following chromatographicdata systems:• ChemStation - Agilent Technologies• EZChrom Elite - Agilent Technologies• Atlas - Thermo ElectronSIMDIS report menu offers severalplot options for the chromatogramExtensive Report OptionsThe AC SIMDIS applications offer severaloptions to report the true boiling pointdistribution & analysis parametersand include dedicated correlations& calculations. Reports are fullyconfigurable per sample type.Report Options• Chromatogram and boiling pointdistribution plot• List of calculation parameters• Quality control report check• Report of peak skew and columnresolution parameters• Tables and graphs of boiling pointversus retention time or versus mass%• Several correlation reports such as D86and D1160, Flashpoint (D7215)• Output of report to several formats,such as CSV, PDF file, for reviewing theresults outside the SIMDIS software,direct import to excel, or direct uploadto a LIMS system.

Accurate Crude Oil AnalysisOne unique AC solution is the Crude Oil Analyzer, whichcombines detailed hydrocarbon analysis (DHA) front endtechnique with high temperature simulation distillation.Merging the DHA and SIMDIS data of the crude oil analysisimproves accuracy. This merging technique is an ACinnovation and is standardized as IP 545, ASTM D 7169and prEN 15199-3.The dedicated system design of the Crude Oil Analyzer consists of thefollowing:• The AC High Temp SIMDIS application that incorporates all ASTM, DIN, IPand CEN methods for high temperature simulated distillation• The AC DHA Front End application which uses a single capillary columnconform IP PM-DL to characterize the C1-nC9 fraction in crude oilMerging principle for DHA& SIMDISwww.simdis.com5High Temp SIMDIS analysis of a crude oilConversion to Volume%The AC High Temp SIMDIS Analyzer includes a special reportoption to convert data from mass% to volume % for crudeoils that comply with:• FBP > 538 ºC (1000°F)• T (50wt%)< 538 ºC (1000°F)Converting Mass % to Volume %

www.simdis.com6Jet Fuel and Diesel AnalysisASTM D 2887, IP 406 & ISO 3924To determine the true boiling point (TBP) distribution for jet fuel and diesel AC Analytical Controls offersthe SIMDIS ASTM D 2887, IP 406 & ISO 3924 application. Jet fuel specifications ASTM D 1655 and DEFSTAN 91-91 list ASTM D 2887 as an alternative to physical distillation ASTM D 86 in determining distillationproperties for Jet A & A-1. The AC application reports both the TBP and correlated ASTM D 86 data.D 86 Boiling PointTo assist refiners in determining D 86 boiling range data, AC developed the AC 8634 application. TheAC8634 TM principle is now accepted within several standard methods, such as ASTM D 2887.HydrocarbonAC 8634 analysis of a gasoilSulfur and NitrogenBoiling PointAC enhanced the SIMDIS applicationwith a dedicated Sulfur and NitrogenChemiluminescence Detector to characterizethe sulfur and nitrogen specifications. TheAC CNS SIMDIS applications report theHydrocarbon, Nitrogen and Sulfur boilingpoint distributions.Nitrogen199 ppm NCarbazoleAnilines, Indoles, QuinolinesC1-CAC2-CAC3+-CASulfur325 ppm SC1-BDTHC2-BDTHC3-BDTHDiBenzoThiopheneBenzoThiophene C1-BDTHC2-BDTHAC Sulfur SIMDIS analysis of a NIST standardExample of a diesel sample on CNS - A single analysis run yields three chromatograms

AMERICASUNITED STATESPAC Corporate Headquarter8824 Fallbrook DriveHouston, TX 77064USAPhone: 800.444.TESTor +1 281 940 1803Fax: +1 281 580 0719EMEAIGERMANYBadstrasse 3-5, P.O. Box 1241DE-97912 Lauda-KönigshofenGermanyPhone: +49 (0) 9343 6400Fax: +49 (0) 9343 640 101FRANCEBP 70285 - VERSON14653 CARPIQUET CedexFrancePhone: +33 (0) 231 264 300Fax: +33 (0) 231 266 293THE NETHERLANDSInnsbruckweg 353047 AG RotterdamThe NetherlandsPhone: +31 (0) 10 462 4811Fax: +31 (0) 10 462 6330RUSSIA & CISShabolovka street, 34, Bldg. 2115419, Moscow, RussiaPhone: +7-495-617-10-86Fax: +7-495-913-97-65UAEVilla#8/1, Street#9Al Karama DistrictP.O.Box 10917Abu Dhabi, United Arab EmiratesPhone: +971 2 446 9671Fax: +971 2 446 9672ASIASINGAPORE61, Science Park Road#03-09/10 The GalenSingapore Science Park IIISingapore 117525Phone: + 65 6412 0890Fax: + 65 6412 0899CHINARm.1003, Sunjoy MansionNo.6 RiTan Rd.ChaoYang District, BeijingP.R. China 100020Phone: +86-10-65072236 ext370/371/372/373/375Fax: +86-10-65072454Features and Benefits• Full range of SIMDIS applications determines boiling points up to C120• Product range includes several unique solutions:- AC 8634 analyzer for accelerated D 86 data of jet fuel and diesel- Crude Oil analyzer merges DHA Front End with High Temp SIMDISTechnique- Sulfur and Nitrogen SIMDIS solutions to determine sulfur and nitrogendistributions- Wax ASTM D 5442 application• Solutions comply with ASTM, CEN, DIN, IP and ISO SIMDIS methods• A broad set of calibration, reference and quality control samples completeseach SIMDIS application• User group meetings help users network and improve analyzer performance• SIMDIS software is compatible with major chromatographic data systems• Dedicated correlations and calculations are included for:- Correlation to Physical Distillation D 86 & D 1160(ASTM D 2887; IP 406; ISO 3924)- NOACK - DIN 51.581-2- MOV - ASTM D 6417- Conversion to volume % for crude oils- Cutpoints & fractions- Flashpoint (ASTM D 7215)• Excellent LIMS connectivity: upload the results directly to your LIMS ormanually after approval• Several features contribute to the analysis precision:- Use of pre-programmed sample types- Automatic blank subtraction, calibration and system validation- Customer selective start and end algorithmThe AC SIMDIS is a complete, turnkey system that’s completely assembledwith all necessary valves, connections, and analyzer columns. It’s ready to go,calibrated, tested to certified calibration blends, fine-tuned and delivered tothe customer’s facility in ‘plug and play’ condition. A qualified and dedicatedService Engineer will visit at the customer’s convenience after delivery toperform installation and training, so that the customer can begin getting themost benefit out of their SIMDIS right away. Plus, PAC’s solid guarantee coversall parts and analytical performance during the first year.THAILAND25 Floor, M. Thai Tower, All seasonsplace’ 87 Wireless Road, LumpiniPhatumwanBangkok 10330 ThailandPhone : +66 2 627 9410Fax : +66 2 627 9401SOUTH KOREAWorld Vision Building #62124-2 Youido-dong,Youngdeungpoku 150-877 SeoulKoreaPhone: +82-2-785 3900Fax: +82-2-785 397700.00.006Copyright 2010 PAC L.P. All rights reserved