ASTM Standards

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ASTM Standards

Quality Control StandardsReal WorldGasolineD-02.03QCD-02.04AccuPetroCheck and AccuPetroTest Real World Gasoline QC StandardsIn cooperation with ASTM D-02 subcommittee 3 and 4, AccuStandard ampulled 21 Real World gasoline reference fuels. Consensus Values havebeen determined for these reference fuels by various ASTM Round Robins to provide Petrochemical Laboratories with a source of wellcharacterized gasoline standards for use in QA/QC applications and as Single Blind test samples over an extended period of time. As new ASTMD-02.03 and D-02.04 Test methods are promulgated they require mandatory Quality Control testing of real world samples. AccuStandard’sPetroTest & PetroCheck standards are being successfully used to achieve these new Quality Control requirements.QCAccuPetroCheckCARB Low Sulfur RFG QCStandardASTM-FUEL-QCS-01-PAKConsensus Value QC Standards$ 60 / 5 x 15 mLParameter Method Value Conc.Total Aromatics D-1319 24.5 Vol.%Total Olefins D-1319 5.3 Vol.%Total Saturates D-1319 58.3 Vol.%Sulfur D-2622 0.0057 Wt.%Sulfur D-4294 0.0078 Wt.%Sulfur D-5453 55.76 µg/gSulfur D-6344 59.31 µg/gBenzene D-5769 0.80 Vol.%Toluene D-5769 4.92 Vol.%Total Aromatics D-5769 23.42 Vol.%Benzene D-6277 0.78 Vol.%Total Olefins D-6550 5.3 Vol.%Conventional Gasoline QCStandardASTM-FUEL-QCS-02-PAK$ 60 / 5 x 15 mLParameter Method Value Conc.Total Aromatics D-1319 34.6 Vol.%Total Olefins D-1319 12.4 Vol.%Total Saturates D-1319 62.8 Vol.%Sulfur D-2622 0.0338 Wt.%Sulfur D-4294 0.0368 Wt.%Sulfur D-5453 317.36 µg/gSulfur D-6344 338.78 µg/gBenzene D-5769 0.55 Vol.%Toluene D-5769 5.53 Vol.%Total Aromatics D-5769 32.51 Vol.%Benzene D-6277 0.52 Vol.%Total Olefins D-6550 12.4 Vol.%AccuPetroCheck QC StandardsTwo of the fuels are available asAccuPetroCheck Consensus Value QCStandards. The AccuPetroCheck CARB andConventional gasoline reference materials haveall parameters listed on the certificate with theConsensus Values and the regression equationsfor reproducability. Use of these ReferenceMaterials improve the quality of laboratoryresults. The Consensus Values listed reflectinitial statistical treatment of the data at the timethe catalog was published. The actual certificateprovided with the AccuPetroCheck QC standardwill have the accepted Consensus Value based onstatistical treatment of the data.AccuPetroTestSulfur in Diesel Fuel QC StandardSBPT-SDF$ 25 / 2 x 15 mLParameterApprox. RangeSulfur20 - 11000 µg/gSee ASTM Methods D-2622, D-3120, D-3246-92,D-4294, D-5453 for Sulfur Calibration StandardsAccuPetroTest GasolineLow Sulfur QC SampleSBPT-LSGAS$ 25 / 2 x 15 mLParameter Method Approx. RangeSulfur D-5453 0 - 50 µg/gSulfur in White Mineral Oil QCStandardSBPT-SWMOOlefin QC SampleSBPT-OLEFINSFC$ 25 / 2 x 15 mLParameterApprox. RangeSulfur20 - 11000 µg/gSee ASTM Methods D-2622, D-3120,D-3246-92, D-4294, D-5453 for SulfurCalibration Standards$ 25 / 2 x 15 mLParameter Method Approx. RangeTotal Olefins D-6550 1 - 40 Vol.%Sulfur Single Blind AccuPetroTestAlternative Matrices StandardsAccuStandard has manufactured a number ofDiesel and White Mineral Oil QC productscontaining a gravimetrically prepared amount ofSulfur. Use of these alternative matrix materialscan provide further evaluation of the QA/QCprocess in the laboratory. Two samples will besent for the test parameter and a separate sealedenvelope containing the gravimetrically preparedsulfur values is also provided. The secondsample is for repeatability testing or for use as afuture QA/QC reference.AccuPetroTest GasolineComprehensive Single Blind Gasoline QC SampleSBPT-COMP$ 50 / 2 x 15 mLParameter Method Approx. Range Conc.Total Aromatics D-1319 8 - 60 Vol.%Total Olefins D-1319 1 - 40 Vol.%Total Saturates D-1319 30 - 80 Vol.%Sulfur D-2622 0.0001 - 0.0930 Wt.%Sulfur D-4294 0.0016 - 0.0930 Wt.%Sulfur D-5453 0.5 -500 µg/gSulfur D-6344 1.0 - 1000 µg/gBenzene D-5769 0.1 - 2.0 Vol.%Toluene D-5769 1.0 - 15 Vol.%Total Aromatics D-5769 8 - 60 Vol.%Benzene D-6277 0.1 - 2.0 Vol.%Total Olefins D-6550 1 - 40 Vol.%Technical NoteThis comprehensivesingle blind gasoline QCsample tests for moreparameters from a singlesample. The actualgasoline sample will haveconsensus values listedon the datasheet that fallwithin the range listed foreach parameter.Quality Control Standardscontinue on next pageTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 1


ASTM Round Robin&PTQCSamplesQuality Control StandardsQCAccuPetroTest Gasoline QCOlefins QC SampleSBPT-OLEFIN$ 25 / 2 x 15 mLParameter Method Approx. RangeTotal Aromatics D-1319 8-60 Vol.%Total Olefins D-1319 1 - 40 Vol.%Total Saturates D-1319 30-80 Vol. %See ASTM Method D-1319 for Sulfur CalibrationStandardsAromatics QC SampleSBPT-AROM$ 25 / 2 x 15 mLParameter Method Approx. RangeTotal Aromatics D-5769 8 - 60 Vol.%See ASTM Methods, D-3606, D-5580-95, D-5769-95for Benzene Calibration StandardsSulfur QC SampleSBPT-SGAS$ 25 / 2 x 15 mLParameter Method Approx. RangeSulfur D-2622 0.0001 - 0.0930 Wt.%Sulfur D-4294 0.0016 - 0.0930 Wt.%Sulfur D-5453 4.0 - 500 µg/gSulfur D-6344 1.0 - 1000 µg/gSee ASTM Methods D-2622, D-3120, D-3246-92,D-4294, D-5453 for Sulfur Calibration StandardsBenzene/Toluene QC SampleSBPT-BENZ$ 25 / 2 x 15 mLParameter Method Approx. RangeBenzene D-5769 0.1 - 2.0 Vol.%Toluene D-5769 1.0 - 15 Vol.%See ASTM Methods, D-3606, D-5580-95, D-5769-95for Benzene Calibration StandardsAccuPetroTest Single BlindStandardsPetrochemical laboratories looking to testthe performance of the laboratory for aspecific parameter can order the SingleBlind AccuPetroTest sample for theparameter of interest. Two real worldgasoline samples will be sent for the testparameter requested and a separate sealedenvelope containing the determinedConsensus Value is also provided. Thesecond sample is for repeatability testingor as a future QA/QC reference.Conducting a Petrochemical Round Robin for a new ASTM method?Select AccuStandard to prepare the necessary samples for the Round Robin studyAccuStandard has packaged for ASTM committee D-02 various select groups of gasoline fuels and hydrocarbon products for use in variousRound Robin studies.Large Sample OfferingAccuStandard was selected by ASTM committee D-02 to fill, seal and package an initial set of 21 different types of Round Robin Gasolines.Each gasoline was selected due to its unique properties. These unique properties will be determined by various ASTM methods under evaluationthrough ASTM subcommittees. AccuStandard has expanded this offering with additional materials blended for other ASTM Round Robins.FlexibilityUse the original 21 gasoline samples to conduct a Round Robin and we can label the samples appropriately to protect the integrity of the RoundRobin. In addition, we can easily add additional samples to your specific Round Robin study to expand the scope of the method for differentmatrices, concentrations or instrument types.Petro PT SamplesNEWOxygenate PT SampleWith MtBE contamination problems in drinking water, numerous states arenow requiring certification for Oxygenate monitoring. Join AccuStandard’snext study for Oxygenate analysis. Our timely PT schedule easily allowsyour lab to be proactive in new regulatory requirements. The analytes inthe standard and the PT sample have been drawn from the California listof known prevalent oxygenates in gasoline. These new Oxygenate PTsamples and standards allow your Lab to:• Expand testing capabilities• Generate new testing revenueWS-PT OxygenatesOPE-OXY-001-AS*OPE-OXY-001-ATOPE-OXY-001-AV*Sample conc. after prep 5.0-50 µg/LContains 4 analytes listed belowETBEDiisopropylether• Eliminate standard preparation• Easily combine with otherAccuStandard Volatile standardsMTBETAMESuggested Calibration StandardOxygenate Gasoline Additive StandardOGAD-001OGAD-001-PAKAt stated conc. in MeOHMtBE(2000 µg/mL)ETBE(2000 µg/mL)Isopropyl ether (2000 µg/mL)NEWTAMEt-Butanol$ 47 / 2 mL$ 47 / 2 mL$ 47 / 2 mL$ 30 / 1 x 1 mLSAVE 20% $ 120 / 5 x 1 mL5 comps.(2000 µg/mL)(10000 µg/mL)WP-PT Oil, Grease & TPHIPE-OILG-001-AS*IPE-OILG-001-ATIPE-OILG-001-AV *Sample conc. after prepContains 2 analytes listed belowAnalyte ListTotal Oil & Grease †TPHOil and GreaseSample range5-100 mg/L5-100 mg/LSuggested Calibration StandardWC-OILG-10X-11000 µg/mL Total Oil and Grease in n-Propanol$ 32 / 5 mL$ 32 / 5 mL$ 32 / 5 mLThis PT sample can be used by gravimetric oil and greasemethods. In addition, it can also be used for TPH analysis bygravimetric methods including the EPA method 1664. Thesample contains real world material commonly found atpetroleum containment sites.$ 45 / 100 mLContains 500 µg/mL vegetable oil and 500 µg/mL of petroleum oil.Shake well before use.SUFFIX KEY"AS" = Formal PT Study"AT" = Pre-Test"AV" = Values IncludedTechnical Note*Designed for NELAC/CA† Indicates that theses analytes areincluded in the NVLAP Scope ofAccreditation, Lab Code 200389-0Lab Code 200389-02 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Physical PropertiesMethod 56, 92, 9386445MemberASTM D-56, D-92, D-93Flash Point StandardsQCVerified by consensus analysis using ASTM Method # referencedCat. No. ASTM # Nominal Flash Point Price / UnitASTM-P-132-01 PMCC D93 65°C $ 110 / 250 mLASTM-P-132-02 PMCC D93 93°C 110 / 250 mLASTM-P-132-03 COC D92 200°C 110 / 250 mLASTM-P-132-04 COC D92 230°C 110 / 250 mLOriginally designed forASTM D-56-98a,D-92-98a, D-93-99bASTMCertified Flash Point StandardsThe reference material is a stable, pure hydrocarbon with a method specific flash pointdetermined by an inter-laboratory study using the ASTM Method # referenced.Cat. No. ASTM # Nominal Flash Point Price / UnitASTM-P-133-01 PMCC D93 65°C $ 175 / 250 mLASTM-P-133-02 PMCC D93 134°C 130 / 250 mLASTM-P-133-03 COC D92 138°C 130 / 250 mLASTM-P-133-04 TCC D56 67°C 175 / 250 mLASTM D-86Synthetic Distillation StandardThe automatic distillation apparatus duplicates the distillation conditions of the manual method. Theincreased reliance on electronic control requires an independent standard to verify that the apparatus isperforming correctly. This synthetic blend of hydrocarbons boil in the temperature range specified inASTM D-86 distillation groups 1 and 2, and a fuel oil that meets the group 4 criteria.The group 1 and 2 standards cover the boiling range 129 - 368 °F (54 - 187 °C) and are verified byconsensus analysis with twelve refinery laboratories. The group 4 standard covers the range from 410 -670 °F (210 - 355 °C). Products are packaged in convenient sizes to meet your laboratory sampleanalysis demands.Cat. No. Group Description Price / UnitASTM-P-126-01 1, 2 Synthetic Distillation Standard $ 160 / 500 mLASTM-P-126-SET 1, 2 Synthetic Distillation Standard 290 / 2 x 500 mLASTM-P-127-01 4 Distillation Standard 160 / 250 mLASTM-P-127-02 4 Distillation Standard 290 / 500 mLOriginally designed forASTM D-86-99aASTM D-92 & Flash & Fire Points by Cleveland Open Cup (COC) &ASTM D-93 Flash Point by Pensky Martin Closed Cup (PMCC)See Method D-56 on this page for the comprehensive line of flash point standardsASTM D-445Viscosity Calibration StandardsCat. No. Viscosity @ 40 °C Price / UnitASTM-P-128-01 4 Cst $ 60 / 500 mLASTM-P-128-02 7 Cst 60 / 500 mLASTM-P-128-03 19 Cst 60 / 500 mLASTM-P-128-04 61 Cst 60 / 500 mLASTM-P-128-05 180 Cst 60 / 500 mLASTM-P-128-06 520 Cst 60 / 500 mLOriginally designed forASTM D-445-97Technical NoteOils are tested inaccordance withASTM D-445Standards of InterestAlso see Cloud Point Standardsused for ASTM Method D-2500on page 5TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 3


Physical PropertiesMethod 1744-63042386Member 2500ASTM D-1744, E-1064, D-4377D-4928, D-6304Water in Liquid Petroleum Products byKarl FischerStandards are available for coulometric Karl Fischer titrations and are packaged in 2 mL, 5 mL, and 20 mL ampules insets of 5 and 10. The following concentrations are available:Cat. No. Description Price / UnitKF-0.6X-5ML-VAP Water content 60 µg/g $ 65 / 10 x 5 mLKF-1X-2ML-VAP Water content 100 µg/g 40 / 10 x 2 mLKF-1X-5ML-VAP Water content 100 µg/g 45 / 10 x 5 mLKF-1X-20ML-PAK Water content 100 µg/g 50 / 5 x 20 mLKF-10X-2ML-VAP Water content 1000 µg/g 40 / 10 x 2 mLKF-10X-5ML-VAP Water content 1000 µg/g 45 / 10 x 5 mLKF-10X-20ML-PAK Water content 1000 µg/g 50 / 5 x 20 mLKF-50X-2ML-VAP Water content 5000 µg/g 40 / 10 x 2 mLKF-50X-5ML-VAP Water content 5000 µg/g 45 / 10 x 5 mLKF-50X-20ML-PAK Water content 5000 µg/g 50 / 5 x 20 mLValue Added Paks (Cat. No.’sending in -VAP) providemultiple single units packagedtogether for both greaterstability and cost savings.Technical NoteMany ASTM Petrochemicalmethods and specificationsreference using QA/QCstandards for water contentmeasurements. AccuStandardhas formulated a comprehensiverange of water standardspackaged in convenient sizes tomeet the various referencedmethods.ASTMASTM D-2386ASTM D-2500Freezing Point Calibration StandardsCat. No. Nominal Freezing Point Price / UnitASTM-P-129-01 - 50 °C $ 110 / 250 mLASTM-P-129-02 - 45 °C 110 / 250 mLCloud Point Calibration StandardsCat. No. Cloud Point, Approx. Value Price / UnitASTM-P-131-01 + 5 °C $ 110 / 250 mLASTM-P-131-02 - 2 °C 110 / 250 mLASTM-P-131-03 - 10 °C 110 / 250 mLASTM-P-131-04 - 15 °C 110 / 250 mLASTM-P-131-05 - 20 °C 110 / 250 mLOriginally designed forD-2386-97Originally designed forD-2500-00Technical NoteVerified by consensus analysis byASTM Method D-2386Technical NoteVerified by consensus analysis byASTM Method D-2500TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 5


ASTM Methods forSulfurAnalysisSulfur StandardsD-2622-98, D-3120-96, D-3246-96, D-4294-98, D-5453-00, D-6334-98, D-6445-99 & Proposed ASTM Sulfur MethodsAccuStandard offers the Petroleum Industry the most complete line of calibration standards designed for today’s Proposed &Promulgated test methods for Sulfur analysis. These calibration standards are designed specifically for the analysis of Sulfur in awide variety of matrices such as #2 diesel fuel, white mineral oil, kerosene, gasoline, crude oil & residual oil.ASTMSULFURTraceability, Quality and CertificationAll Sulfur standards are manufactured from the highest quality raw materials, including well characterized starting materials & thelowest sulfur matrices available from the Petrochemical market. All standards are manufactured on a weight/weight basis usingbalances that are calibrated and verified daily against reference mass standards directly traceable to NIST under test No.822/254480. The concentration of these working level Sulfur standards have established traceability links to NIST SRM’s whereavailable.Convenient PackagingSince applicable concentration ranges will vary based on the instrumentation used & the nature of the sample the standards can beordered as complete sets, individual bottles, or Ready-to-Aspirate AccuShots.AccuShots... Packaged to improve analytical standard integrityAccuStandard is the first standard manufacturer to provide sulfur standards in convenient and Ready-to-Aspirate AccuShot 20 mLsealed ampules. Each 20 mL AccuShot provides the necessary material for calibration curve development or daily QA/QC. Bypurchasing AccuShots the analytical chemist can open a fresh shot for each analysis which eliminates opening and pipettingrepeatedly from a stock bottle. This minimizes contamination and evaporation. These ship with no haz fee for additional savings.ASTM D-5453Test to Low ppbSulfurContact us for a copy of theSouthwest Research InstituteD-5453 Fitness for Use ReportLow Sulfur Standards on following pages6 Quality System is Certified to comply with the International ISO 9001 Quality Standard


Analytical CapabilitiesMWD XRF Sulfur Analyzerin Diesel and Gasoline FuelsLimits of Detection < 1 ppmFast and easy sample preparation.Typical measurement time: 300 sec.Dynamic range: 0-1000 ppm in onecalibration.SULFURNo sample conversion or reagentsrequired.X-Ray Optical Systems, Inc.15 Tech Valley DriveEast Greenbush, NY 12061Tel. 518-880-1500website: www.xos.comXOS SINDIE AnalyzerX-Ray optics enable detection capability wellbeyond traditional XRF techniques. Thesame Monochromatic WD XRF technologyof the SINDIE bench-top sulfur analyzer isavailable in an on-line sulfur analyzer.Exceptional signal-to-backgroundprovides high sensitivity forlow-level sulfur fuelsSULFUR ANALYSIS INULTRA LOW SULFUR FUELSRepeatability:1 ppm 0.5 ppm10 ppm 1.7 ppm100 ppm 5.3 ppm500 ppm 11.7 ppmMonochromatic WDXRF Technology7


MethodSulfur StandardsASTM MethodsSulfur Standards for ASTM D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 &Proposed ASTM Sulfur MethodsASTM SulfurMethods for inKerosene SulfurASTM MethodsSulfur in KeroseneSulfur in Light Distillate KeroseneSulfur in Light Ready-to-UseConcentration Distillate Kerosene Sulfur AccuShotsµg/g Wt. % Cat. No. Cat. No.Blank 0.000 SK-BL-4 SK-BL-SHOT100 0.010 SK-1X-4 SK-1X-SHOT200 0.020 ---------------300 0.030 SK-3X-4 SK-3X-SHOT400 0.040 ---------------500 0.050 SK-5X-4 SK-5X-SHOT750 0.075 SK-7.5X-4 SK-7.5X-SHOT1,000 0.10 SK-10X-4 SK-10X-SHOT1,500 0.15 ---------------2,000 0.20 SK-20X-4 SK-20X-SHOT3,000 0.30 SK-30X-4 SK-30X-SHOT4,000 0.40 SK-40X-4 SK-40X-SHOT5,000 0.50 SK-50X-4 SK-50X-SHOT7,000 0.70 ---------------10,000 1.00 SK-100X-4 SK-100X-SHOT15,000 1.50 ---------------20,000 2.00 SK-200X-4 SK-200X-SHOT30,000 3.00 ---------------40,000 4.00 ---------------50,000 5.00 ---------------60,000 6.00 ---------------Sulfur in Heavy Distillate KeroseneConcentrationSulfur in HeavyDistillate Keroseneµg/g Wt. % Cat. No.Blank 0.000 SK-HD-BL-4100 0.010 SK-HD-1X-4200 0.020 SK-HD-2X-4300 0.030 SK-HD-3X-4400 0.040 SK-HD-4X-4500 0.050 SK-HD-5X-4750 0.075 SK-HD-7.5X-41,000 0.10 SK-HD-10X-41,500 0.15 SK-HD-15X-42,000 0.20 SK-HD-20X-43,000 0.30 SK-HD-30X-44,000 0.40 SK-HD-40X-45,000 0.50 SK-HD-50X-47,000 0.70 SK-HD-70X-410,000 1.00 SK-HD-100X-415,000 1.50 SK-HD-150X-420,000 2.00 SK-HD-200X-430,000 3.00 SK-HD-300X-440,000 4.00 SK-HD-400X-450,000 5.00 SK-HD-500X-460,000 6.00 SK-HD-600X-4Technical NoteSulfur concentrationcalculated from % sulfurin di-n-butyl sulfide.Standards of InterestFor the mandatory realworld QC samplesstipulated in the Method,see pages 1- 2.ASTM SULFURSet of above SK-CAL-SET-4 Each AccuShot productCat. No.’s 12 x 4 oz. $ 500 contains 5 x 20 mLIndividual Sulfur 1 -10 units 10 +unitsStandards 4 oz Bottle $ 55 ea $ 50 eaampules at the statedconc. for $ 60Set of above SK-HD-CAL-SET-4Cat. No.’s 21 x 4 oz. $ 950Individual Sulfur 1 -10 units 10 +unitsStandards 4 oz Bottle $ 55 ea $ 50 eaTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 9


ASTM 2622-6445Sulfur StandardsASTM MethodsASTMSULFURASTM D-2622, D-4294 Sulfur Calibration Standards ASTM D-2622, D-6334, Low Level SulfurD-6445 Calibration StandardsSulfur Calibration Standards in Isooctane forGasoline & Reformulated Gasoline AnalysisStandards can be mixed for quantity discounts1 to 4 units $ 60 each per Sulfur Standard5 to 10 units $ 55 each per Sulfur Standardmore than 10 units $ 50 each per Sulfur StandardCat. No. Sulfur Conc. Sulfur Wt. % UnitSTP-BL-4 Blank 0.0 4 oz.STP-1X-4 10 µg/g 0.001 4 oz.STP-2X-4 20 µg/g 0.002 4 oz.STP-3X-4 30 µg/g 0.003 4 oz.STP-5X-4 50 µg/g 0.005 4 oz.STP-10X-4 100 µg/g 0.010 4 oz.STP-20X-4 200 µg/g 0.020 4 oz.STP-30X-4 300 µg/g 0.030 4 oz.STP-40X-4 400 µg/g 0.040 4 oz.STP-60X-4 600 µg/g 0.060 4 oz.STP-100X-4 1000 µg/g 0.10 4 oz.STP-200X-4 2000 µg/g 0.20 4 oz.STP-300X-4 3000 µg/g 0.30 4 oz.STP-CAL-SETIn Isooctane$ 650 / set of 13 x 4 oz.Set contains the above 13 individual bottlesTechnical NoteOriginallydesigned forD-2622-98D-4294-98A well characterized di-n-butyl sulfide starting mat’l is used with alow sulfur Isooctane matrix for RFG/gasoline sulfur standards.Low Level Sulfur Calibration Standards for use on XRFEnergy Dispersive or Wavelength InstrumentsStandards can be mixed for quantity discounts1 to 4 units $ 60 each per Sulfur Standard5 to 10 units $ 55 each per Sulfur Standardmore than 10 units $ 50 each per Sulfur StandardOriginallydesigned forD-2622-98D-6334-98D-6445-99Cat. No. Sulfur Conc. Sulfur Wt. % UnitD-2622-LL-BL-4 Blank 0.0 4 oz.D-2622-LL-5X-4 5 µg/g 0.0005 4 oz.D-2622-LL-10X-4 10 µg/g 0.0010 4 oz.D-2622-LL-30X-4 30 µg/g 0.0030 4 oz.D-2622-LL-50X-4 50 µg/g 0.0050 4 oz.D-2622-LL-75X-4 75 µg/g 0.0075 4 oz.D-2622-LL-100X-4 100 µg/g 0.010 4 oz.D-2622-LL-300X-4 300 µg/g 0.030 4 oz.D-2622-LL-500X-4 500 µg/g 0.050 4 oz.D-2622-LL-1000X-4 1000 µg/g 0.100 4 oz.D-2622-LL-CAL-SET$ 450 / 10 x 4 oz.In Isooctane : Toluene (3:1)Set contains the above 10 individual bottlesTechnical NoteWell characterized Thiophene & 2-Methyl thiophene are usedin a low sulfur Isooctane/Toluene matrix for this calibration set.ASTM D-3120, D-3246Sulfur Calibration SetD-3120-92-CAL-SETIn IsooctaneSulfur Calibration Set$ 75 / set of 8 x 1 mLASTM D-2622, D-6334, Mid Level SulfurD-6445 Calibration StandardsNew Requested Additions for use on XRF EnergyDispersive or Wavelength InstrumentsCat. No. Sulfur Conc. Sulfur Wt. %D-3120-92-BL Blank ———D-3120-92-1X 1 µg/g 0.0001D-3120-92-3X 3 µg/g 0.0003D-3120-92-10X 10 µg/g 0.0010D-3120-92-30X 30 µg/g 0.0030D-3120-92-50X 50 µg/g 0.0050D-3120-92-75X 75 µg/g 0.0075D-3120-92-100X 100 µg/g 0.010Technical NoteWell characterized di-n-butyl sulfide is used in a low sulfurIsooctane matrix for this calibration set.Originallydesigned forD-3120-96D-3246-96Standards can be mixed for quantity discounts1 to 4 units $ 60 each per Sulfur Standard5 to 10 units $ 55 each per Sulfur Standardmore than 10 units $ 50 each per Sulfur StandardOriginallydesigned forD-2622-98D-6334-98D-6445-99Cat. No. Sulfur Conc. Sulfur Wt. % UnitD-2622-LL-200X-4 200 µg/g 0.020 4 ozD-2622-LL-400X-4 400 µg/g 0.040 4 ozD-2622-LL-600X-4 600 µg/g 0.060 4 ozD-2622-LL-700X-4 700 µg/g 0.070 4 ozD-2622-LL-800X-4 800 µg/g 0.080 4 ozD-2622-LL-900X-4 900 µg/g 0.090 4 ozD-2622-LL-1100X-4 1100 µg/g 0.110 4 ozD-2622-LL-1200X-4 1200 µg/g 0.120 4 ozStandards of InterestFor the mandatory real world QC samples stipulated in manyASTM Sulfur Methods, see page 1-2Technical NoteWell characterized Thiophene & 2-Methyl thiophene are usedin a low sulfur Isooctane/Toluene matrix for this calibration set.MemberAccuStandard is an active member in ASTM andstrives to keep abreast of ASTM method revisions. Ifour listed formulation does not meet the most recentmethod revision, please contact Technical Support,ext. 117 for an updated product.10 Quality System TECHLAB is Certified 4C La to Tannerie comply with - BP the 30055 International - 57072 - METZ ISO 9001 cedex Quality 3 Standard


Sulfur StandardsASTM MethodsSulfur Standards for ASTM D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 &Proposed ASTM Sulfur MethodsASTM 2789ASTM MethodsSulfur in Crude Oil StandardsConcentrationIndividual Sulfur 1 -10 units 10 +unitsStandards 4 oz Bottle $ 75 ea $ 65 eaSulfur Calibration StandardsSulfur in Crude Oilµg/g Wt. % Cat. No.1,000 0.10 SCO-10X-42,500 0.25 SCO-25X-45,000 0.50 SCO-50X-410,000 1.00 SCO-100X-420,000 2.00 SCO-200X-430,000 3.00 SCO-300X-440,000 4.00 SCO-400X-450,000 5.00 SCO-500X-4Set of aboveSCO-CAL-SET-4Cat. No.’s 8 x 4 oz. $ 500Sulfur in Residual Oil StandardsConcentrationSulfur in Crude Oilµg/g Wt. % Cat. No.3,500 0.35 SRO-35X-47,000 0.70 SRO-70X-410,000 1.00 SRO-100X-415,000 1.50 SRO-150X-420,000 2.00 SRO-200X-430,000 3.00 SRO-300X-440,000 4.00 SRO-400X-4Set of aboveSRO-CAL-SET-4Cat. No.’s 7 x 4 oz. $ 450Individual Sulfur 1 -10 units 10 +unitsStandards 4 oz Bottle $ 75 ea $ 65 eaTechnical NoteAccuStandard's TechnicalService Dept. can provideReady-to-Inject working levelcalibration standards to meetunique laboratory applications.Call or fax us your standardrequirements.ASTM SULFURASTM MethodsSulfur StandardsTotal Sulfur in Aromatic Compounds byHydrogenolysis & RateometricColorimetryASTM-P-0010-PAK1000 µg/mL in TolueneSulfur (as Thiophene)$ 75 / 5 x 1 mLTrace Quantities of Sulfur in LiquidAromatic Hydrocarbons by OxidativeMicrocoulometryASTM-P-0020-PAK1000 µg/mL in XylenesSulfur (as Dibenzothiophene)$ 75 / 5 x 1 mLASTM-SSTD-A/B-SET$ 100 / 10 x 2 mLThe set contains the following 10 standards in isooctaneCat. No. Description UnitASTM-SSTDA-BL Sulfur Blank 2 mLASTM-SSTDA-01 Sulfur @ 0.5 µg/g in Isooctane 2 mLASTM-SSTDA-02 Sulfur @ 1.0 µg/g in Isooctane 2 mLASTM-SSTDA-03 Sulfur @ 2.5 µg/g in Isooctane 2 mLASTM-SSTDA-04 Sulfur @ 5.0 µg/g in Isooctane 2 mLASTM-SSTDB-BL Sulfur Blank 2 mLASTM-SSTDB-04 Sulfur @ 5.0 µg/g in Isooctane 2 mLASTM-SSTDB-05 Sulfur @ 10.0 µg/g in Isooctane 2 mLASTM-SSTDB-06 Sulfur @ 25.0 µg/g in Isooctane 2 mLASTM-SSTDB-07 Sulfur @ 50.0 µg/g in Isooctane 2 mLASTM D-2789Composition Test MixD-2789-CTMD-2789-CTM-PAK(Vol. %)2-Methylpentane 7.22,4-Dimethylpentane 9.4n-Octane 16.6Methylcyclopentane 7.1Methylcyclohexane 10Hydrocarbon Types in Low Olefinic Gas by MS$ 40 / 1 x 1 mLSAVE 20% $ 160 / 5 x 1 mL9 comps.(Vol. %)cis-1,2-Dimethylcyclohexane 15.5Benzene 7.7Toluene 10p-Xylene 16.5Originallydesigned forD-2789-95Technical NoteBoth the actual volume %ratio and the final weightfractions for each analyte willbe listed on the certificate.TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 11


PIANOPIANOPONAPNAPIANO, PONA, PNAAccuStandard has introduced the PIANO line of quantitative and qualitative Petrochemical Standards for class type analysis of petrochemicalsamples or product streams. PIANO analysis involves the determination of the percentage of the following five fractions Paraffins, Isoparaffins,Aromatics, Naphthenes, and Olefins.PONA analysis involves analyzing the naphtha sample for Paraffins, Olefins, Naphthenes, and Aromatics. If the Isoparaffins and Olefins are notpresent, the analysis is just for PNA.The PIANO line of standards is used to determine quantitative and qualitative retention times and indices as well as to monitor response factorswithin the hydrocarbon blend. These complex mixes are prepared from materials of the highest available purity, accurate to four decimal places,and include a detailed data sheet on the formulation composition. The typical range for the analytes in each formulation has been provided foreach catalog item. The exact composition on a weight % basis for each analyte has been provided on the certificate, and a disk deliverablespreadsheet is available on request.Mini Inert Valves SealThe PIANO standards are supplied in convenient to use crimp top vials with Viton septa that resistmineral oil, aliphatic, aromatics hydrocarbons, and higher temperatures. Mini inert valve seals areavailable for an additional $ 25 vial. To order, add “-MIV” to any of the PIANO catalog numbers onthis page.PIANO, PONA, PNA AnalysisPIONAPIANO MixtureASTM-P-0030 $ 250 / 100 µL135 comps.The PIANO formulation contains the n-Paraffins,Isoparaffins,Aromatics, Naphthenes, and Olefins from thefive Cat. No.’s: ASTM-P-0031, ASTM-P-0032,ASTM-P-0033, ASTM-P-0034, ASTM-P-0035Approximate weight percentages for the total: n-Paraffins18.5%, Isoparaffins 17.9%, Aromatics 23.6%, Naphthenes20.9%, Olefins 19.0%.The actual certificate will list the weight % for all analytesin the formulation.High Aromatic PIAN BlendASTM-P-0037 $ 120 / 100 µL110 comps.High Aromatic blend contains the PIAN componentsblended to resemble a reformate. The actual certificatewill have the exact weight % for each analyte accurate tofour decimal places. Analyte list is drawn fromCat. No.’s: ASTM-P-0031, ASTM-P-0032,ASTM-P-0033, ASTM-P-0034Low Aromatic PIAN BlendASTM-P-0036 $ 120 / 100 µL110 comps.Low Aromatic blend contains the PIAN componentsblended to resemble a light naphtha. The actual certificatewill have the exact weight % for each analyte accurate tofour decimal places. Analyte list is drawn fromCat. No.’s: ASTM-P-0031, ASTM-P-0032,ASTM-P-0033, ASTM-P-0034Standards of InterestFor individual PIANO descriptions see next pageAccuStandard, Your Standards and Technical Information Source!Total PetroleumHydrocarbon PatternRecognition StandardsBOOK-TPH $ 35Analytical Standards andReference Material for all209 PCB CongenersS-3571 $ 2512 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


PIANO, PONA, PNAPIANOPIANOPONAPNAPIANO, PONA, PNA AnalysisPIANO Mix SetASTM-PIANO-SET $ 700 / 6 x 100 µLSet includes the following Cat. No.:ASTM-P-0030, ASTM-P-0031, ASTM-P-0032,ASTM-P-0033, ASTM-P-0034, ASTM-P-0035PIANO n-Paraffins MixASTM-P-0031 $ 80 / 100 µL11 paraffins listed below at varying Wt. %typically in the range from 7.0 to 11.0 Wt. %.The actual certificate will have the exact Wt.% for each analyte.Typ. Wt. %n-Pentane 9.4375n-Hexane 9.5661n-Heptanea 9.8048n-Octane 9.5518n-Nonane 9.0482n-Decane 9.2517n-Undecane 9.3172n-Dodecane 9.1855n-Tridecane 8.9332n-Tetradecane 8.7989n-Pentadecane 7.1057Special PackagingMini inert valve seals are available for an additional $ 25 / vial.To order, add “-MIV” to any of the PIANO cat.# on this page.PIANO Isoparaffins MixASTM-P-0032 $ 120 / 100 µL35 Isoparaffins listed below at varying Wt. % typically in the range from 0.5 to 6.0 Wt. %. The actualcertificate will have the exact Wt. % for each analyte.Typ. Wt. %Isopentane 2.19282,3-Dimethylbutane 0.44662-Methylpentane 3.28153-Methylpentane 5.38652,2-Dimethylpentane 1.77472,4-Dimethylpentane 3.69932,2,3-Trimethylbutane 3.92913,3-Dimethylpentane 1.18482-Methylhexane 2.23842,3-Dimethylpentane 1.78833-Methylhexane 1.67083-Ethylpentane 0.5080Typ. Wt. %2,2-Dimethylhexane 1.30612,5-Dimethyl hexane 3.69752,2,3-Trimethylpentane 1.73712,4-Dimethylhexane 1.62522,3-Dimethylhexane 1.62122-Methylheptane 4.40734-Methylheptane 3.20153-Methylheptane 5.51863-Ethylhexane 0.69993,3-Dimethylheptane 1.70112,5-Dimethylheptane 5.67313,5-Dimethylheptane 0.7565Typ. Wt. %2,3-Dimethylheptane 1.48703,4-Dimethylheptane 3.74502-Methyloctane 3.75763-Methyloctane 5.60203,3-Diethylpentane 1.57552,2-Dimethyloctane 3.41353,3-Dimethyloctane 3.25822,3-Dimethyloctane 3.88423-Ethyloctane 3.74822-Methylnonane 3.71443-Methylnonane 5.7687PIANO Aromatics MixASTM-P-0033 $ 120 / 100 µL38 Aromatics listed below at varying Wt. %typically in the range from 0.2 to 7.0 Wt. %.The actual certificate will have the exactWt. % for each analyte.Typ. Wt. %Benzene 7.1437Toluene 4.5738EthylBenzene 6.7670m-Xylene 2.2259p-Xylene 4.4815o-Xylene 2.2519Isopropylbenzene 2.2248n-Propylbenzene 4.49791-Methyl-3-ethylbenzene 2.22431-Methyl-4-ethylbenzene 2.22061,3,5-Trimethylbenzene 1.10761-Methyl-2-ethylbenzene 2.26111,2,4-Trimethylbenzene 2.2535tert-Butylbenzene 4.5310Isobutylbenzene 4.4216sec-Butylbenzene 2.23681-Methyl-3-isopropylbenzene 1.10661-Methyl-4-isopropylbenzene 1.06681-Methyl-2-isopropylbenzene 1.12411-Methyl-3-n-propylbenzene 2.11351-Methyl-4-n-propylbenzene 2.2336n-Butylbenzene 2.20871,2-Diethylbenzene 1.09471-Methyl-2-n-propylbenzene 2.26411,4-Dimethyl-2-ethylbenzene 2.28031,3-Dimethyl-5-ethylbenzene 2.28581,2-Dimethyl-4-ethylbenzene 2.25581,3-Dimethyl-2-ethylbenzene 1.14161,2-Dimethyl-3-ethylbenzene 2.18641,2,4,5-Tetramethylbenzene 0.23602-Methylbutylbenzene 1.1453trans-1-Butyl-2-methylbenzene 0.7641n-Pentylbenzene 4.4828t-1-Butyl,3,5-dimethylbenzene 2.1641t-1-butyl-ethylbenzene 2.23221,3,5-Triethylbenzene 4.56711,2,4-Triethylbenzene 1.1087n-Hexylbenzene 4.5029PIANO Naphthenes MixASTM-P-0034 $ 120 / 100 µL30 Napthenes listed below at varying Wt. %typically in the range from 0.5 to 8.0 Wt. %. Theactual certificate will have the exact Wt. % foreach analyte.Typ. Wt. %Cyclopentane 4.9143Methylcyclopentane 3.2829Cyclohexane 5.32681,1-Dimethylcyclopentane 3.4612cis-1,3-Dimethylcyclopentane 0.5963trans-1,2-Dimethylcyclopentane 1.4715trans-1,3-Dimethylcyclopentane 2.7531Methylcyclohexane 5.6091Ethylcyclopentane 3.5534ctc-1,2,3-Trimethylcyclopentane 1.5859cct-1,2,4-Trimethylcyclopentane 3.7208ctc-1,2,4-Trimethylcyclopentane 1.6467trans-1,4-Dimethylcyclohexane 3.64991-Ethyl-1-methylcyclopentane 1.0554trans-1,2-Dimethylcyclohexane 1.6537ccc-1,2,3-Trimethylcyclopentane 0.7971Isopropylcyclopentane 3.5042cis-1,2-Dimethylcyclohexane 3.7159n-Propylcyclopentane 3.6438ccc-1,3,5-Trimethylcyclohexane 3.52631,1,4-Trimethylcyclohexane 3.6791ctt-1,2,4-Trimethylcyclohexane 3.6107ctc-1,2,4-Trimethylcyclohexane 3.50691,1,2-Trimethylcyclohexane 3.3354Isobutylcyclopentane 3.7123Isopropylcyclohexane 5.7233n-Butylcyclopentane 3.6944Isobutylcyclohexane 5.6729t-1-Methyl-2-propylcyclohexane 3.8434t-1-Methyl-2-(4MP)cyclopentane 3.7534PIANO MixturePIANO Olefins MixASTM-P-0035 $ 120 / 100 µL25 Olefins listed below at varying Wt. %typically in the range from 1.2 to 9.0 Wt. %.The actual certificate will have the exact Wt. %for each analyte.Typ. Wt. %3-Methyl-1-butene 1.93961-Pentene 4.13552-Methyl-1-butene 1.44402-Methyl-1,3-butadiene 2.3889trans-2-Pentene 1.8034cis-2-Pentene 1.97924-Methylpentene-1 3.43721-Hexene 7.0484trans-2-Hexene 1.73022-Methylpentene-2 3.3901cis-2-Hexene 3.87651-Heptene 7.6134trans-3-Heptene 3.3469cis-3-Heptene 5.8657trans-2-Heptene 3.7217cis-2-Heptene 5.76791-Octene 7.6901trans-2-Octene 1.9432cis-2-Octene 3.95021-Nonene 7.6425trans-3-Nonene 1.9972cis-3-Nonene 4.0042trans-2-Nonene 1.9848cis-2-Nonene 2.79521-Decene 8.2053Production NoteAccuStandard may add and/or subtractPIANO Analytes and vary the weight %for each Analyte. The certificate willreflect the exact Analyte composition.ASTM-P-0030 $ 250 / 100 µL (135 comps.)The PIANO formulation contains the n-Paraffins, Isoparaffins,Aromatics, Naphthenes, and Olefins fromthe Five Cat. No.’s: ASTM-P-0031, ASTM-P-0032, ASTM-P-0033, ASTM-P-0034, ASTM-P-0035Approximate weight %’s for the total: n-Paraffins 18.5%, Isoparaffins 17.9%, Aromatics 23.6%,Naphthenes 20.9%, Olefins 19.0%. The certificate lists the weight % for all analytes in the formulation.PIONATECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 13


Method 2887DHADetailed Hydrocarbon AnalysisMemberDetailed Hydrocarbon AnalysisASTMProposed ASTM Method for Detailed Hydrocarbon Analysis (DHA)Determination of Individual Components and Groups of Components in Spark Ignition Engine fuels byHigh Efficiency Open Tubular Column Gas Chromatography (Detailed Hydrocarbon Analysis)Detailed Hydrocarbon Analysis (includes oxygenates)ASTM-P-0038 $ 120 / 100 µL30 Analytes listed below at varying targeted weight %. The actual certificate will has the exact Wt. % for each analyte.EthanolPentane2-Methyl-2-propanol2-Methylbutene2,3-DimethylbutaneMethyl-t-butyl etherHexaneMethylcyclopenteneBenzeneCyclohexane3-Ethylpentanet-1,2-DimethylcyclopentaneHeptane2,2,3-Trimethylpentane2,3,3-TrimethylpentaneToluenep-XyleneEthylbenzeneOctane2,3-DimethylheptaneNonane5-Methylnonane1-Ethyl-2-methylbenzeneDecaneUndecane1,2,3,5-TetramethylbenzeneNaphthaleneDodecane1-MethylnaphthaleneTridecaneDHA - PONA-VI (PONA 6) is aqualitative mixture of variousgasoline and refinery materialsprepared to provide nearly everycomponent that may be encounteredin feedstock and finished gasolines.Some oxygenates have been addedto allow this blend to be used forDHA method setup. This blendcontains approximately 450components (peaks).ASTM-P-0139 $ 120 / 100 µLASTM D-2887Calibration MixDRH-002NDRH-002N-10XWt. %n-Hexane 6n-Heptane 6n-Octane 8n-Nonane 8n-Decane 12n-Undecane 12n-Dodecane 12n-Tetradecane 12n-Hexadecane 10Column Test MixtureBoiling Range Distribution of Petroleum Fractions by GCWt. %n-Octadecane 5n-Eicosane 2n-Tetracosane 2n-Octacosane 1n-Dotriacontane 1n-Hexatriacontane 1n-Tetracontane 1n-Tetratetracontane 1ASTM-D2887$ 10 / 1 x 1 mL1% v/v in n-Octane 2 comps.n-Hexadecanen-Octadecane$ 10 / 100 mg$ 40 / 1 gm17 comps.Complete Hydrocarbon AnalysisHydrocarbon WindowDefining Standard*DRH-008S-R2$ 65 / 1 x 1 mLDRH-008S-R2-PAK SAVE 20% $ 260 / 5 x 1 mL500 µg/mL each in Chloroform 35 comps.OctaneNonaneDecaneUndecaneDodecaneTridecaneTetradecanePentadecaneHexadecaneHeptadecaneOctadecanePristaneNonadecanePhytaneEicosaneHeneicosaneDocosaneTricosaneTetracosanePentacosaneHexacosaneHeptacosaneOctacosaneNonacosaneTriacontanen-HentriacontaneDotriacontaneTritriacontaneTetratriacontanePentatriacontaneHexatriacontaneHeptatriacontaneOctatriacontaneNonatriacontaneTetracontaneOriginally designed for D-2887-99ASTM D-2887 Reference GasOil Sample Lot #2D-2887-REFOIL$ 35 / 1 x 1 mLTechnical NoteThis sample is a petroleum fractionhaving a boiling range from 250°F to850°F, evaluated in round robinstudies by the ASTM D-02committee. Use of this sample andthe supplied ASTM boiling rangeconsensus values helps to evaluatesystem performanceFuel Oil Degradation/RetentionTime Mix for Quantification ofC 17 /Pristane & C 18 /Phytane ratiosDRH-005S-10X$ 20 / 1 x 1 mL2.0 mg/mL each in CH 2 Cl 2 : CS 2 (1:1) 4 comps.HeptadecaneOctadecanePhytane (2,6,10,14-Tetramethylhexadecane)Pristane (2,6,10,14-Tetramethylpentadecane)Calibration Solution *DRH-002S-R1$ 50 / 1 x 1 mLDRH-002S-R1-PAK SAVE 20% $ 200 / 5 x 1 mLAt stated conc. in Chloroform17 comps.Technical NoteAccuStandard offers a hydrocarbon window defining standard with the C 8 to C 40 odd andeven Alkanes. As an added benefit, AccuStandard included pristane and phytane in theformulation. Use of this one standard measuring the C 17 / pristane and C 18 / phytane ratiocan be used to estimate degradation of fuel oil.If you prefer, AccuStandard has also developed a fuel oil degradation mixture containingjust the four required analytes to determine the C 17 /pristane and C 8 / phytane ratioCatalog Numbers DRH-005S-10X.NEWCalibration Solution *NEWDRH-002S-R2$ 50 / 1 x 1 gmDRH-002S-R2-PAKSAVE 20% $ 200 / 5 x 1 gm1 % Wt./Wt. each in Chloroform 20 comps.µg/mLn-Hexane 600n-Heptane 600n-Octane 800n-Nonane 800n-Decane 1200n-Undecane 1200n-Dodecane 1200n-Tetradecane 1200n-Hexadecane 1000µg/mLn-Octadecane 500n-Eicosane 200n-Tetracosane 200n-Octacosane 100n-Dotriacontane 100n-Hexatriacontane 100n-Tetracontane 100n-Tetratetracontane 100n-Tetratetracontanen-Tetracontanen-Hexatriacontanen-Dotriacontanen-Octacosanen-Tetracosanen-Eicosanen-Octadecanen-Hexadecanen-Tetradecanen-Dodecanen-Undecanen-Decanen-Nonanen-Octanen-Heptanen-Hexanen-Pentanen-Pentadecanen-Heptadecane* Can be shipped by Air and Sea14 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Petrochemical StandardsMethodSIM DISMemberSimulated Distillation (SIM DIS) and Proposed Motor Oil Volatility MethodAccuStandard has developed an extensive line of SIM DIS standards for normal and high temperature analytical requirements when generatingboiling point versus retention time calibration curves. Since normal paraffins above Alkane C60 are not readily available, Polywax 500, Polywax655, Polywax 850 and Polywax 1000 standards have been incorporated to perform SIM DIS analysis of heavy petroleum fractions with boilingpoints up to 1350 °F. If you require additional analytes added to the formulations for extended SIM DIS work, use our custom quotation requestform located in the back of the catalog.SIM DIS StandardsStock SIM DIS Paraffin SolutionASTM-P-0050Wt. %n-Pentane 6.66n-Hexane 6.66n-Heptane 6.66n-Octane 6.66n-Nonane 6.66n-Decane 6.66n-Undecane 6.66Polywax 500 ®ASTM-P-0051N-2GPolywax 500Polywax 655 ®ASTM-P-0053N-2GSimulated Distillation$ 85 / 1 x 5 mL14 comps.Wt. %n-Dodecane 13.33n-Tetradecane 6.66n-Pentadecane 6.66n-Hexadecane 6.66n-Heptadecane 6.66n-Octadecane 6.66n-Eicosane 6.66$ 20 / 2 grams$ 20 / 2 gramsWorking Level SIM DIS Paraffin Solutionwith Polywax 500ASTM-P-0052$ 40 / 1 x 1 mLASTM-P-0052-PAK SAVE 20% $ 160 / 5 x 1 mLAt stated conc. in Carbon disulfide15 comps.Wt. %n-Pentane 0.0333n-Hexane 0.0333n-Heptane 0.0333n-Octane 0.0333n-Nonane 0.0333n-Decane 0.0333n-Undecane 0.0333n-Dodecane 0.0666Polywax 850 ®ASTM-P-0137N-2GPolywax 850Polywax 1000 ®ASTM-P-0138N-2GWt. %n-Tetradecane 0.0333n-Pentadecane 0.0333n-Hexadecane 0.0333n-Heptadecane 0.0333n-Octadecane 0.0333n-Eicosane 0.0333Polywax 500 0.5$ 20 / 2 grams$ 20 / 2 gramsStandards of InterestSee ASTM Methods D-3710,D-5307, D-5442, D-6352 foradditional calibrationstandards for hydrocarbonanalysis.Technical NoteAccuStandard designed thefollowing formulations for aProposed ASTM Method underdevelopment for Motor OilVolatility analysis & SIM DISapplications.ASTMPolywax 655Polywax 1000For our complete line ofOrganic Standards,request a copy of ourOrganic CatalogFor our complete line ofInorganic Standards,request a copy of ourInorganics CatalogTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 15


Method 31203230,3231Member 3237ASTM StandardsASTM D-3120 & D-3246Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative MicrocoulometryASTMSulfur Calibration SetD-3120-92-CAL-SETIn Isooctane$ 75 / set of 8 x 1 mLCat. No. Sulfur Conc. Sulfur Wt.%D-3120-BL Blank BlankD-3120-92-1X 1 µg/g 0.0001D-3120-92-3X 3 µg/g 0.0003D-3120-92-10X 10 µg/g 0.0010D-3120-92-30X 30 µg/g 0.0030D-3120-92-50X 50 µg/g 0.0050D-3120-92-75X 75 µg/g 0.0075D-3120-92-100X 100 µg/g 0.010Originally designed forD-3120-96D-3246-96Technical NoteWell characterized di-n-butyl sulfide is usedin a low sulfur Isooctane matrix for thiscalibration set.Standards of InterestsSee page 1 for AccuStandard’scomprehensive line of CertifiedSulfur calibration standards,AccuPetroCheck, andAccuPetroTest quality controlproducts.ASTM D-3230Salts in Crude OilMixed Salt SolutionD-3230-89-1$ 75 / 100 mLD-3230-89-5$ 150 / 500 mLAt stated conc. in Alcohol Solution (1-butanol : MeOH) (ratio 63:37) tr. H 2 O 3 comps.Originally designed forD-3230-99Calcium chlorideMagnesium chloride10 µg/mL20 µg/mLSodium chloride70 µg/mLASTM D-3231 Phosphorus in GasolineOriginally designed for D-3231-99Element Quantity Cat. No. PriceMatrixConc.Phosphorus 100 mL ICP-41W-1 $ 34H 2 O1000 µg/mLPhosphorus 500 mL ICP-41W-5 $ 67H 2 O1000 µg/mLD-3231MeetsEPA Guidelinesfor RFGAnalysisASTM D-3237Lead in Gasoline by AA SpectroscopyLead Standard Calibration CurveD-3237-CAL-SETSet includes the following Catalog Numbers:$ 210 / 4 x 100 mLOriginally designed forD-3237-97Cat. No. Description Price / UnitD-3237-01 Blank 1% Aliquot 336/MIBK $ 20 / 100 mLD-3237-02 0.02 g Pb / gal ( 5.3 mg Pb/ L) in 1% Aliquat 336 / MIBK $ 80 / 100 mLD-3237-03 0.05 g Pb / gal ( 13.2 mg Pb/ L) in 1% Aliquat 336 / MIBK $ 80 / 100 mLD-3237-04 0.10 g Pb / gal ( 26.4 mg Pb/ L) in 1% Aliquat 336 / MIBK $ 80 / 100 mLD-3237MeetsEPA Guidelinesfor RFGAnalysisReady-to-Inject Petrochemical Standards and Calibration CurvesReduce CostsIncrease Time Spent for Sample AnalysisAre Validated Against Independent LotsInclude Internal Standards or SurrogatesFollow ASTM Method GuidelinesAllow Direct Transfer to Autosampler VialsReady-to-InjectWorking Level Standards &Continuing Calibration Check (CCC)16 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 324633403524Member 3605ASTM D-3246Sulfur in Petroleum Gas by Oxidative MicrocoulometrySee pages 6 - 11 for AccuStandards comprehensive line of certified sulfur calibration standardsASTM D-3340Lithium & Na in Lubricating Greases by Flame PhotometerASTMAccuStandard AccuTrace brand AA standards are produced under our rigorous ISO 9001 quality systemto exacting specifications. Each standard is prepared from high purity starting materials; deionized waterand high purity acids. Every standard is instrumentally assayed to verify 1000 ppm concentration ofspecified element; Actual Lot Analysis is provided on the label and a Certificate of Analysis is included forease of record keeping and availability at audits.Originally designed forD-3340-98Element Unit Cat. No. PriceMatrixASTM D-3524 (Reapproved 1999)D-3524 Calibration CurveD-3524-CAL-SET-5MLD-3524-CAL-SET-10ML1,000 µg/mLLithium * 100 mL AA30H-1 $ 12HCl 500 mL AA30H-5 30Sodium * 100 mL AA54H-1 13HCl 500 mL AA54H-5 33Technical Note* For your convenience these elements arealso available in HNO 3 . To order HNO 3change the H to N at the end of the Cat. No.Diesel Fuel Diluent in Used Diesel Engine Oils by GC$ 150 / set of 6 x 5 mL$ 250 / set of 6 x 10 mLOriginally designed forD-3524-90Analyte Standard 1 Standard 2 Standard 3 Standard 4 Standard 5 Standard 6Target Wt. % Target Wt. % Target Wt. % Target Wt. % Target Wt. % Target Wt. %# 2 Diesel 10 7.5 5 2.5 1 030 W Motor oil 90 92.5 95 97.5 99 100Test toLow ppbSulfurSee Pages 6-11WEAR METALSInternal Standard SolutionD-3524-IS-10ML$ 25 / 1 x 10 mLD-3524-IS-10ML-PAK SAVE 20% $ 100 / 5 x 10 mLAt stated conc. in n-Heptane2 comps.Wt. / Wt. %n-Decane 1.0n-Octadecane 0.2Mid Level Daily QC SolutionD-3524-QC-10ML$ 30 / 1 x 10 mL2 comps.Wt. / Wt. %# 2 Diesel 5.030 W Motor oil 95Column Resolution MixD-3524-CR$ 10 / 1 x 1 mLD-3524-CR-PAKSAVE 20% $ 40 / 5 x 1 mLAt stated conc. in n-Heptane2 comps.Wt. / Wt. %n-Hexadecane 1.0n-Octadecane 1.0ASTM D-3605(Reapproved 1995)D-3605-91 Trace Metals StandardTrace Metals in Gas Turbine Fuels by AA &Flame Emission SpectroscopyD-3605-91-1$ 165 / 1 x 100 mLAt stated conc. in 1,2,3,4-Tetrahydronaphthalene 4 comps.Originally designed forD-3605-91Standards of InterestsSee Table of Contents for theWear Metals Group pagesNa (Sodium)Pb (Lead)(250 µg/mL)(250 µg/mL)Ca (Calcium)V (Vanadium)(250 µg/mL)(250 µg/mL)TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 17


Method 36063610,ASTM StandardsMemberASTM D-3606Benzene & Toluene in Finished Motor & Aviation Gasoline by GCOriginally designed forD-3606-99ASTMAromatics Quantitative Calibration Standard (without Internal Standards)D-3606-SET-25ML$ 800 / set of 7 x 25 mLAnalyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7Calibr. range Target Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %Benzene 0.06 - 5.0 5.00 2.50 1.25 0.67 0.33 0.12 0.06Toluene 0.5 - 20 20.00 15.00 10.00 5.00 2.50 1.00 0.50Isooctane 75.00 82.50 88.75 94.33 97.17 98.88 99.44D-3606MeetsEPA Guidelinesfor RFGAnalysisAromatics Quantitative Calibration Standard (with Internal Standard: MEK)D-3606/IS-SETD-3606/IS-SET-2MLD-3606/IS-SET-2ML-PAK$ 115 / set of 7 x 1 mL$ 190 / set of 7 x 2 mL$ 760 / 5 x (7 x 2) mLAnalyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7Calibr. range Target Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %Benzene 0.06 - 5.0 4.8 2.4 1.2 0.6432 0.3168 0.1152 0.0576Toluene 0.5 - 20 19.2 14.4 9.6 4.8000 2.4000 0.9600 0.4800Isooctane 72.0 79.2 85.2 90.5568 93.2832 94.9248 95.4624Methyl ethyl ketone (Internal Std.) 4.0 4.0 4.0 4.0 4.0 4.0 4.0Gasoline Refinery Quality Control StandardsDaily Quality Control Standard(with Internal Standard: MEK)D-3606-QC/IS-10MLD-3606-QC/IS-10ML-PAKEach at stated quantitiesCompound Target Vol. %Benzene 0.6432Toluene 4.8000Isooctane 90.5568Methyl ethyl ketone (ISTD) 4.0$ 75 / 1 x 10 mL$ 300 / 5 x 10 mL4 comps.100Daily Quality Control Standard(without Internal Standard)D-3606-QC-25MLD-3606-QC-25ML-PAKEach at stated quantitiesCompound Target Vol. %Benzene 0.67Toluene 5.00Isooctane 94.33$ 125 / 1 x 25 mL$ 600 / 5 x 25 mL3 comps.100Aromatics Quantitative Calibration Standard (w/ Internal Standard: sec Butanol)D-3606/IS2-SETD-3606/IS2-SET-PAKGasoline Refinery Quality Control StandardsDaily Quality Control StandardDaily Quality Control Standard(with Internal Standard: sec Butanol) (without Internal Standard)D-3606-QC-IS2-25MLD-3606-QC-IS2-25ML-PAKEach at stated quantitiesCompound Target Vol. %Benzene 0.6432Toluene 4.8000Isooctane 90.5568sec-Butanol (ISTD) 4.0$ 125 / 1 x 25 mL$ 600 / 5 x 25 mL4 comps.100D-3606-QC-25MLD-3606-QC-25ML-PAKEach at stated quantities$ 115 / set of 7 x 1 mL$ 500 / 5 x (7 x 1) mLAnalyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7Calibr. range Target Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %Benzene 0.06 - 5.0 4.8 2.4 1.2 0.6432 0.3168 0.1152 0.0576Toluene 0.5 - 20 19.2 14.4 9.6 4.8000 2.4000 0.9600 0.4800Isooctane 72.0 79.2 85.2 90.5568 93.2832 94.9248 95.4624sec Butanol (Internal Standard) 4.0 4.0 4.0 4.0 4.0 4.0 4.0Compound Target Vol. %Benzene 0.67Toluene 5.00Isooctane 94.33$ 125 / 1 x 25 mL$ 600 / 5 x 25 mL3 comps.100Technical NoteDue to changes in the possibleuse of other oxygenates likeethanol added to gasoline,AccuStandard formulated anew calibration curve usingsec-butanol as an InternalStandard. The use of this newISTD minimizes coelutioncaused by the oxygenate(s)and pre column - standardcolumn configuration in the GCsystem.ASTM D-3610Total Cobalt in Alumina-Base Cobalt-Molybdenum Catalyst by Potentiometric TitrationCobalt Oxide StandardD-3610-93-1Cobalt oxide @ 1500 µg/mL in Water$ 50 / 1 x 100 mLOriginally designed forD-3610-88 (Re-Approved 1993)18 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


On-Line OrderingThere is an easier way to get Chemical Reference Standardse-Standards ®from AccuStandard.com5 Ways to Search“e-Standards” is the Fastest, Most Comprehensive Search Engineavailable and contains over 30,000 products.Search by:ASTMCatalog NumberSingle or Multiple Components,Method (EPA, ASTM, etc.)Chemical Category (Organic, Inorganic, Petroleum, etc.)Other Companies’ Part NumberLog on to www.accustandard.com and see how easy it is.Easy Ordering 24/7Find It Fast...simply search for a product, select it for purchase &click - it's that easy! Discounts may apply to online orders, seedetails on website.On-Line Custom ServicesAccuStandard specializes in synthesizing chemicals of high purityto be used as reference standards, and offers custom synthesiscapability for milligram to kilogram batches. If you can't find thespecific standard you need, we can prepare Custom Formulationsand Custom Packaging for both Organic and Inorganic needs.See our Website for more info.Over 30,000 Standardsjust a click awayCross Reference TableASTM IP ISO DIN JIS AFNOR sorted byASTM Method see beginning of CatalogTest toLow ppbSulfurSee Pages 6-11TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 19


Method 37103798, 3831ASTM StandardsMemberASTMASTM D-3710 (Reapproved 1999)Qualitative Calibration StandardD-3710-QUALD-3710-QUAL-PAKApprox.Wt./ Wt. %n-Butane 4.5n-Butylbenzene 3.2n-Decane 3.22,4-Dimethylpentane 5.4n-Dodecane 3.2n-Heptane 9.7n-Hexane 5.42-Methylbutane 9.72-Methylpentane 5.42-Methylpropane 1.5$ 30 / 1 x 1 mLSAVE 20% $ 120 / 5 x 1 mL19 comps.Approx.Wt./ Wt. %n-Octane 5.4n-Pentadecane 2.2n-Pentane 7.6n-Propane 1.5n-Propylbenzene 4.3n-Tetradecane 2.2Toluene 10.8n-Tridecane 2.2p-Xylene 13Boiling Range Distribution of Gasoline & Gasoline Fractions by GCThis SIM DIS (Simulated Distillation or GCD) Method is used to determine the boiling range distribution ofgasoline and gasoline components. ASTM Method D-3710 is used for petroleum products and fractionswith a final boiling point of 500°F (260°C) or lower. By having an insight into the composition of thegasoline blend, essential data for the calculation of vapor pressure and a prediction of the D-86 distillationcurve can be made.Quantitative Calibration StandardASTM-D3710ASTM-D3710-PAKVol./Vol. %n-Butylbenzene 3.5n-Decane 3.52,4-Dimethylpentane 5.8n-Dodecane 3.5n-Heptane 10.5n-Hexane 5.82-Methylbutane 10.52-Methylpentane 5.8$ 25 / 1 x 1 mLSAVE 36% $ 80 / 5 x 1 mL16 comps.Vol./Vol. %n-Octane 5.8n-Pentadecane 2.3n-Pentane 8.1n-Propylbenzene 4.7n-Tetradecane 2.3Toluene 11.6n-Tridecane 2.3p-Xylene 14.0NEWOriginally designed forD-3710-95Standards of InterestsSee page 3 for AccuStandard’snew D-86 QA/QC Standards.ASTM D-2887-99 Boiling Range Distribution of Petroleum Fractions by GCCalibration Solution *DRH-002S-R1$ 50 / 1 x 1 mLDRH-002S-R1-PAK SAVE 20% $ 200 / 5 x 1 mLAt stated conc. in Chloroform17 comps.µg/mLµg/mLµg/mLµg/mLn-Hexane 600 n-Undecane 1200 n-Octadecane 500 n-Dotriacontane 100n-Heptane 600 n-Dodecane 1200 n-Eicosane 200 n-Hexatriacontane 100n-Octane 800 n-Tetradecane 1200 n-Tetracosane 200 n-Tetracontane 100n-Nonane 800 n-Hexadecane 1000 n-Octacosane 100 n-Tetratetracontane100n-Decane 1200* Can be shipped by Air and SeaASTM D-3798p-Xylene Impurity Standardwith ISTDAnalysis of p-Xylene by GCAccuStandard’s R & D team has developed a special highly purified p-Xylene designed for ASTM MethodD-3798 specifications. The incorporation of this p-Xylene into the formulation allows the analytical chemistto qualitatively and quantitatively measure the impurities in the p-Xylene feedstock streams.D-3798-IS$ 30 / 1 x 1 mLD-3798-IS-PAK SAVE 33% $ 100 / 5 x 1 mLAt stated conc. by weight11 comps.Wt./Wt. %n-Pentane 0.15n-Octane 0.15Benzene 0.15Toluene 0.15Ethylbenzene 0.15p-Xylene 98.65m-Xylene 0.15Wt./Wt. %o-Xylene 0.15Cumene 0.15Propylbenzene 0.15Total Analytes 100plus n-Undecane* (ISTD)0.500gramsp-Xylene Impurity Standardwithout ISTDD-3798-10ML$ 65 / 1 x 10 mLD-3798-10ML-PAK SAVE 20% $ 260 / 5 x 10 mLAt stated conc. by weight10 comps.Wt./Wt. %n-Pentane 0.15n-Octane 0.15Benzene 0.15Toluene 0.15Ethylbenzene 0.15Wt./Wt. %p-Xylene 98.65m-Xylene 0.15o-Xylene 0.15Cumene 0.15Propylbenzene 0.15Technical NoteBulk Packaged p-Xylene withoutInternal StandardOther suggested internalstandards can be used inconjunction with the bulkpackaged D-3789 1 x 10 mLampule to meet your company’sapplication. If you prefer toeliminate making standards,contact AccuStandard’sTechnical Department with yourunique formulation for a customquotation. The customquotation request form islocated in the back of thiscatalog.ASTM D-3831Manganese in Gasoline by AA SpectroscopyManganese Stock SolutionD-3831 $ 65 / 1 x 100 mLOriginally designed forD-3831-98Manganese @ 1.0 g Mn / gal (264.2 mg Mn / L) in Methyl isobutyl ketone20 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 405942914294Member 4377ASTM D-4059Polychlorinated Biphenyls in Insulating Liquids by GCAroclors in PCB-Free Transformer Oil (At 2 concentrations in Transcrest W130)Aroclor #Conc.(ppm w/w)Cat. No.1 x 1 mLPricePAK Cat. No.5 x 1 mLPriceAroclor 1016 50 C-216-ST-1 $ 25 C-216-ST-1-PAK $ 90Aroclor 1016 500 C-216-ST-2 30 C-216-ST-2-PAK 120Aroclor 1221 50 C-221-ST-1 25 C-221-ST-1-PAK 90Aroclor 1221 500 C-221-ST-2 30 C-221-ST-2-PAK 120Aroclor 1232 50 C-232-ST-1 25 C-232-ST-1-PAK 90Aroclor 1232 500 C-232-ST-2 30 C-232-ST-2-PAK 120Aroclor 1242 50 C-242-ST-1 25 C-242-ST-1-PAK 90Aroclor 1242 500 C-242-ST-2 30 C-242-ST-2-PAK 120Aroclor 1248 50 C-248-ST-1 25 C-248-ST-1-PAK 90Aroclor 1248 500 C-248-ST-2 30 C-248-ST-2-PAK 120Aroclor 1254 50 C-254-ST-1 25 C-254-ST-1-PAK 90Aroclor 1254 500 C-254-ST-2 30 C-254-ST-2-PAK 120Aroclor 1260 50 C-260-ST-1 25 C-260-ST-1-PAK 90Aroclor 1260 500 C-260-ST-2 30 C-260-ST-2-PAK 120Aroclor 1262 50 C-262-ST-1 25 C-262-ST-1-PAK 90Aroclor 1262 500 C-262-ST-2 30 C-262-ST-2-PAK 120Aroclor 1268 50 C-268-ST-1 25 C-268-ST-1-PAK 90Aroclor 1268 500 C-268-ST-2 30 C-268-ST-2-PAK 120Originally designed forD-4059-96Additional Aroclors andPCB Congener Standardsavailable in our OrganicCatalogASTMNeat Individual AroclorsAroclor 1016 C-216N $ 25 / 100 mg 100 mgAroclor 1221 C-221N 25 / 100 mg 100 mgAroclor 1232 C-232N 25 / 10 mg 10 mgAroclor 1242 C-242N 25 / 100 mg 100 mgAroclor 1248 C-248N 25 / 10 mg 10 mgAroclor 1254 C-254N 25 / 100 mg 100 mgAroclor 1260 C-260N 25 / 100 mg 10 mgAroclor 1262 C-262N 25 / 100 mg 10 mgAroclor 1268 C-268N 25 / 10 mg 10 mgKit of above 9 Aroclors Z-008 $ 125 / 9 vialsZ-008Aroclor # Cat. No. Price / Unit (Kit)Aroclor-free transformer oilalso available as:T-W130$ 5 / 1 x 1 mLASTM D-4291 (Reapproved 1998)Trace Ethylene Glycol in Used Engine OilEthylene Glycol Stock StandardD-4291-93$ 20 / 1 x 1 mLD-4291-93-PAKSAVE 20% $ 80 / 5 x 1 mLOriginally designed forD-4291-93Ethylene glycol @ 2000 µg/mL in waterASTM D-4294Sulfur in Petroleum Products by ED-XRF SpectroscopySee page 8-11 for AccuStandard’s comprehensive line of Certified Sulfur Calibration Standardsdesigned for matrix specific applications as described in Method D-4294 in section 9.0(Calibration & Standardization).D-4294MeetsEPA Guidelinesfor RFGAnalysisASTM D-4377Water in Crude oils by Potentiometric Karl Fischer TitrationSee page 5 for AccuStandard’s comprehensive line of Certified Karl Fischer Water Standards.TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 21


Method 44204628,ASTM StandardsMemberASTM D-4420 Aromatics in Finished Gasolines by GCAromatics in Gasoline by GC/TCD-4420-CAL-SET$ 105 / set of 7 x 1 mLOriginally designed forD-4420-94ASTMAnalyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7Target Target Target Target Target Target TargetVol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %Benzene 0.05 0.10 0.25 0.75 1.25 2.50 5.00Toluene 0.5 1.00 2.50 5.00 10.00 15.00 25.00Total Xylenes (C 8 aromatics) 5 10.00 15.00 20.00 25.00 1.00 3.00n-Butylbenzene (C 9 + aromatics) 30.00 25.00 20.00 10.00 5.00 15.00 2.50Isooctane 64.45 63.90 62.25 64.25 58.75 66.50 64.50WEAR METALSAromatics in Gasoline by GC/TXD-4420-94D-4420-94-PAKVol. %Benzene 3.00Toluene 10.00Total Xylenes (C 8 aromatics) 15.00ASTM D-4628$ 20 / 1 x 1 mL$ 80 / 5 x 1 mL5 comps.Vol. %n-Butylbenzene(C 9 + aromatics) 15.00Isooctane 57.00Barium, Calcium, Magnesium & Zinc in Unused Lubricating OilLubricating Oil, Elements (Nominal Value) Wt.% listed belowASTM-P-0113-SET$ 2850 / 17 x 100 mLBa Ca Mg P S ZnCat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0113-01 0.025 0.600 0.100 0.005 0.175 0.060ASTM-P-0113-02 0.000 0.500 0.150 0.200 0.050 0.080ASTM-P-0113-03 0.100 0.400 0.350 0.150 0.300 0.180ASTM-P-0113-04 0.175 0.260 0.225 0.250 0.150 0.120ASTM-P-0113-05 0.150 0.005 0.450 0.005 0.450 0.070ASTM-P-0113-06 0.000 0.400 0.500 0.025 0.350 0.100ASTM-P-0113-07 0.100 0.300 0.325 0.060 0.250 0.120ASTM-P-0113-08 0.200 0.200 0.250 0.100 0.450 0.100ASTM-P-0113-09 0.050 0.060 0.100 0.080 0.300 0.130ASTM-P-0113-10 0.075 0.060 0.400 0.050 0.200 0.050ASTM-P-0113-11 0.010 0.050 0.300 0.120 0.100 0.075ASTM-P-0113-12 0.000 0.025 0.200 0.150 0.200 0.130ASTM-P-0113-13 0.175 0.005 0.375 0.200 0.400 0.150ASTM-P-0113-14 0.005 0.170 0.175 0.250 0.550 0.110ASTM-P-0113-15 0.000 0.100 0.425 0.100 0.200 0.200ASTM-P-0113-16 0.005 0.010 0.275 0.010 0.600 0.250ASTM-P-0113-17 0.000 0.000 0.000 0.000 0.000 0.000Originally designed forD-4628-97Standards of InterestsSee Table of Contents for theWear Metals Group pages.Ready-to-Inject Petrochemical Standardsand Calibration CurvesReduce CostsIncrease Time Spent for Sample AnalysisAre Validated Against Independent LotsInclude Internal Standards or SurrogatesFollow ASTM Method GuidelinesAllow Direct Transfer to Autosampler VialsCross Reference TableASTM IP ISO DIN JIS AFNOR sorted byASTM Method see beginning of Catalog22 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 4629MemberASTM D-4629Trace Nitrogen in Liquid Petroleum Hydrocarbons by Syringe/Inlet OxidativeCombustion and Chemiluminescence Detection. IP Designation 379/88Originally designed forD-4629-96Method D-4629 is used to determine trace total nitrogen naturally found in liquid hydrocarbons boiling from50 to 400°C with viscosities between 0.2 and 10 cSt. This method monitors feed stocks for nitrogen toprevent the poisoning of some process catalysts when trace nitrogenous materials are present.Nitrogen Calibration Set-Low Boiling SolventsD-4629-91-LB-CAL-SET$ 75 / set of 7 x 1 mLSet includes the following Cat. No.sTechnical NoteNitrogen introduced using PyridineCat. No. Description Price / UnitD-4629-91-LB-0.3X Nitrogen @ 0.3 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-1X Nitrogen @ 1 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-10X Nitrogen @ 10 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-25X Nitrogen @ 25 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-50X Nitrogen @ 50 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-75X Nitrogen @ 75 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-100X Nitrogen @ 100 µg/mL in Isooctane $ 20 / 1 x 1 mLASTMStock Nitrogen Solution for Low Boiling SolventsD-4629-91-LB-COND-4629-91-LB-CON-PAKNitrogen @ 1000 µg/mL in Isooctane(Pyridine @ 5.65 mg/mL in Isooctane)$ 20 / 1 x 1 mL$ 80 / 5 x 1 mLNitrogen Calibration Set-High Boiling SolventsD-4629-91-HB-CAL-SET$ 75 / set of 7 x 1 mLSet includes the following Cat. No.sTechnical NoteNitrogen introduced using CarbazoleCat. No. Description Price / UnitD-4629-91-HB-0.3X Nitrogen @ 0.3 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-1X Nitrogen @ 1 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-10X Nitrogen @ 10 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-25X Nitrogen @ 25 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-50X Nitrogen @ 50 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-75X Nitrogen @ 75 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-100X Nitrogen @ 100 µg/mL in Toluene $ 20 / 1 x 1 mLStock Nitrogen Solution for High Boiling SolventsD-4629-91-HB-COND-4629-91-HB-CON-PAK$ 20 / 1 x 1 mLSAVE 20% $ 80 / 5 x 1 mLNitrogen @ 1000 µg/mL in Toluene : Acetone (9:1)(Carbazole @ 11.95 mg/mL in Toluene : Acetone (9:1) )Low level Nitrogen Calibration SetASTM-P-0070-SET$ 75 / 6 x 1 mLSet includes the following Cat. No.sTechnical NoteNitrogen introduced using AnilineCat. No. Description UnitASTM-P-0070-BL Isooctane Blank 1 x 1 mLASTM-P-0070-1X Nitrogen @ 0.5 µg/g in Isooctane 1 x 1 mLASTM-P-0070-2X Nitrogen @ 1.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-4X Nitrogen @ 2.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-10X Nitrogen @ 5.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-20X Nitrogen @ 10.0 µg/g in Isooctane 1 x 1 mLLow level Nitrogen &Sulfur Calibration SetASTM-P-0071-SET$ 50 / 4 x 1 mLSet includes the following Cat. No.sTechnical NoteThe Nitrogen is introduced using Aniline and theSulfur is introduced using di-n-Butyl sulfideCat. No. Description UnitASTM-P-0071-BL Benzene Blank 1 x 1 mLASTM-P-0071-01 Nitrogen @ 0.25 µg/g & Sulfur @ 0.25 µg/g in Benzene 1 x 1 mLASTM-P-0071-02 Nitrogen @ 0.50 µg/g & Sulfur @ 0.50 µg/g in Benzene 1 x 1 mLASTM-P-0071-03 Nitrogen @ 1.00 µg/g & Sulfur @ 1.00 µg/g in Benzene 1 x 1 mLTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 23


Method 4815,ASTM StandardsMemberASTMASTM D-4815MtBE, EtBE, TAME, DIPE, Tertiary-amyl Alcohol andC 1 to C 4 Alcohols in Gasoline by GCOxygenate Quantitative Calibration Mixtures (without Internal Standard)D-4815-SET-10ML$ 300 / set of 5 x 10 mL of 5 component mixStd. 1 Std. 2 Std. 3 Std. 4 Std. 5Analyte Wt. % Wt. % Wt. % Wt. % Wt. %Ethanol 3.00 0.10 6.00 9.00 12.00t-Butanol 0.10 3.00 6.00 8.00 12.00Methyl t-butyl ether (MtBE) 20.0 15.00 10.00 5.00 0.10t-Pentanol 1.25 5.00 2.50 3.75 0.10Isooctane/xylene (65:35) 75.65 76.90 75.50 74.25 75.80Oxygenate Quantitative Calibration Mixtures (with Internal Standard)D-4815/IS-SET of 6 component mix $ 125 / set of 5 x 1 mLD-4815/IS-SET-PAK$ 500 / set of 5 x (5 x 1 mL)Originally designed forD-4815-99Calibration Std. 1 Std. 2 Std. 3 Std. 4 Std. 5Analyte Range Wt. % Wt. % Wt. % Wt. % Wt. %Ethanol 0.1 - 11.40 2.85 0.10 5.70 8.55 11.40t-Butanol 0.1 - 11.40 0.10 2.85 5.70 7.60 11.40Methyl t-butyl ether (MtBE) 0.1 - 19.0 19.00 14.25 9.50 4.75 0.10t-Pentanol 0.1 - 4.79 1.19 4.75 2.38 3.56 0.101,2-Dimethoxyethane (DME) (Internal Std.) 5.00 5.00 5.00 5.00 5.00Isooctane/xylene (65:35) 71.87 73.06 71.73 70.54 72.0Total Oxgenates & Internal Standard 28.14 26.95 28.28 29.46 28.00D-4815MeetsEPA Guidelinesfor RFGAnalysisTechnical NoteAdditional Oxygenatecalibration, check standards,and independent referencestandards can be found inASTM method D-5599 (pages34-36) or D-5622-94 (page 37)The required QA/QC proceduresin EPA methods stipulate acalibration check standard beused once per analytical batchor per 10 sample set.AccuStandard has bulkpackaged our check standardsto meet this increased usage.Quantitative Peak ID and RetentionTime MixtureD-4815-RTD-4815-RT-PAK$ 25 / 1 x 1 mLSAVE 20% $ 100 / 5 x 1 mLCompound Wt. %Methylcyclopentane 4.00Methanol 7.30Ethanol 7.30Isopropanol 7.30tert-Butanol 7.30n-Propanol 7.30Methyl tert-butyl ether (MtBE) 4.00sec-Butanol 7.30Diisopropyl ether (DIPE) 4.00Isobutanol 7.30Ethyl tert-butyl ether (EtBE) 4.00tert-Pentanol 7.301,2-Dimethoxyethane (ISTD) 6.00n-Butanol 7.30Benzene 5.00tert-Amyl methyl ether 7.3016 comp. core mix100Valve Timing MixtureD-4815-VT$ 25 / 1 x 1 mLD-4815-VT-PAK SAVE 20% $ 100 / 5 x 1 mL5 comps.Compound Wt. %Methylcyclopentane 10.00Diisopropyl ether (DIPE) 10.00Ethyl tert-butyl ether (EtBE) 10.00Methyl tert-butyl ether (MtBE) 10.00n-Hexane 60.00Oxygenate Internal Standard MixtureM-GRO-IS-5MLM-GRO-IS-5ML-PAK1,2-Dimethoxyethane (ISTD) (neat)Oxygenate Free Refinery GasolineBlankM-GRO-BLNK-10ML$ 10 / 1 x 10 mLM-GRO-BLNK-10ML-PAK SAVE 20% $ 40 / 5 x 10 mLRFA Gasoline (neat)$ 10 / 1 x 1 mLSAVE 20% $ 40 / 5 x 1 mLTest toLow ppbSulfurSee Pages 6-11Custom FormulationsAccuStandard offers over 30,000 different standards, and if you can't find the specific standard you need, we will prepare a custom formulation.Our custom organic and inorganic standards are a fast, economical way to address your unique requirements. To make an inquiry for CustomQuotes visit our website.You can also Email your requirements to techservice@accustandard.com or Fax us at 203-786-5287. Please include the following information:List of analytes and concentrations, Solvent or matrix, Quantity required (milliliters), Packaging unit size (milliliters per ampule, bottle, or vial).Quality Control Options1. Gravimetric/Volumetric Certification: Each standard is measured gravimetrically and then QC’ed instrumentally (where available). Everycomponent in the standard is guaranteed to be within ±0.5% of the requested value unless otherwise stated. The solutions are made up to volumeusing class A glassware. A certificate comes with each standard and documents the gravimetric values used.2. Quantitative Validation: Full QA/QC method includes extended GC analysis using both internal and calibration standards plus statisticalanalysis. A data package is provided containing analytical and gravimetric data (Organic customs only).Also available: OEM Standards - Privately labeled standards manufactured and tested to your specifications.24 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 492749284929MemberASTM D-4927 Elemental Analysis of Lubricant and Additive Components -Barium, Calcium,Phosphorus, Sulfur, and Zinc by WD-XRF SpectroscopyLubricating Oil, Elements (Nominal Value) Wt.% listed belowASTM-P-0110-SET$ 2300 / 17 x 100 mLBa Ca P S ZnCat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0110-01 0.100 0.600 0.005 0.175 0.060ASTM-P-0110-02 0.175 0.500 0.200 0.050 0.080ASTM-P-0110-03 0.000 0.400 0.150 0.300 0.180ASTM-P-0110-04 0.025 0.260 0.250 0.150 0.120ASTM-P-0110-05 0.150 0.005 0.005 0.450 0.070ASTM-P-0110-06 0.000 0.400 0.025 0.350 0.100ASTM-P-0110-07 0.200 0.300 0.060 0.250 0.120ASTM-P-0110-08 0.000 0.200 0.100 0.450 0.100ASTM-P-0110-09 0.100 0.060 0.080 0.300 0.130ASTM-P-0110-10 0.050 0.060 0.050 0.200 0.050ASTM-P-0110-11 0.075 0.050 0.120 0.100 0.075ASTM-P-0110-12 0.010 0.025 0.150 0.200 0.130ASTM-P-0110-13 0.005 0.005 0.200 0.400 0.150ASTM-P-0110-14 0.000 0.170 0.250 0.550 0.110ASTM-P-0110-15 0.000 0.100 0.100 0.200 0.200ASTM-P-0110-16 0.005 0.010 0.010 0.600 0.250ASTM-P-0110-17 0.000 0.000 0.000 0.000 0.000ASTM D-4928Originally designed forD-4927-96Water in Crude Oils by Potentiometric Karl Fischer TitrationSee page 5 for AccuStandard’s new line of Karl Fischer Water Standards.Standards of InterestsSee Table of Contents for theWear Metals Group pagesASTMWEAR METALSASTM D-4929Working Level Chlorine StandardD-4929-94D-4929-94-PAKChlorine @ 10 µg/mL in IsooctaneOrganic Chloride Content in Crude Oil - Test Method BCombustion and Microcoulometry$ 10 / 1 x 5 mLSAVE 20% $ 40 / 5 x 5 mLStock Chlorine StandardD-4929-94-100XD-4929-94-100X-PAK$ 15 / 1 x 5 mLSAVE 20% $ 60 / 5 x 5 mLChlorine @ 1000 µg/mL in IsooctaneOriginally designed forD-4929-99Standards of InterestsSee page 66 for additionalproposed and promulgatedChlorine in Lube Oil standardsCustom Ampulling for Bulk Quantity RequirementsAutomated ampule filling & sealing 0.2 mL up to 20 mLQuantities from 500 to over 500,000 ampulesHomogeneity testingAmber ampules for added product stabilityPrivate labeling and packagingWe can reduce your costs using the CozzoliAuto Filling/ Sealing Machine to package justthe right size product for your application.TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 25


Method 49515056,ASTM StandardsMemberASTMWEAR METALSASTM D-4951Additive Elements in Lubricating Oils byInductively Coupled Plasma Atomic Emission Spectrometry20 Wear Metal Multi-Element Standardcontaining no metallic sulfonatesConc. Cat. No. Price(µg/g)10 WM-20-NMS-1X-1 $ 15030 WM-20-NMS-3X-1 15050 WM-20-NMS-5X-1 150100 WM-20-NMS-10X-1 170300 WM-20-NMS-30X-1 230500 WM-20-NMS-50X-1 350900 WM-20-NMS-90X-1 500WM-20-NMS-SET-1 $ 1450set of above 7 x 100 mLRecommended Internal Standard (IS)Each Wear Metal Standard contains the belowlist of 20 elements in hydrocarbon oil at thestated concentrationAl (Aluminum)B (Boron)Ba (Barium)Ca (Calcium)Cd (Cadmium)Cr (Chromium)Cu (Copper)Fe (Iron)Mg (Magnesium)Mn (Manganese)Sulfur free Organometallic (IS) Sulfur free Organometallic (IS)Element @ 1000 µg/g Price @ 5000 µg/g PriceCat. No. 50 mL Cat. No. 50 mLCobalt WM-NMS-14 $ 75 WM-NMS-14-5X $ 110Mo (Molybdenum)Na (Sodium)Ni (Nickel)P (Phosphorus)Pb (Lead)Si (Silicon)Sn (Tin)Ti (Titanium)V (Vanadium)Zn (Zinc)Originally designed forD-4951-96Standards of InterestsSee Table of Contents for theWear Metals Group pages.Technical NotesThis calibration curve has beenformulated with startingmaterials containing no metalsulfonates. This way a sulfurcalibration curve can easily bedeveloped using a highconcentration sulfur standard.ASTM D-5056Trace Metals in Petroleum Coke by Atomic AbsorptionOriginally designed forD-5056-96Element @ 1000 µg/mL Unit Cat. No. PriceMatrix* Aluminum 100 mL AA01N-1 $ 13HNO 3 500 mL AA01N-5 33* Calcium 100 mL AA09N-1 12HNO 3 500 mL AA09N-5 30* Iron 100 mL AA27N-1 12HNO 3 500 mL AA27N-5 30Nickel 100 mL AA37N-1 12HNO 3 500 mL AA37N-5 30Element @ 1000 µg/mL Unit Cat. No. PriceMatrixSilicon 100 mL AA52W-1 $ 13H 2 O tr. NaOH 500 mL AA52W-5 33* Sodium 100 mL AA54N-1 13HNO 3 500 mL AA54N-5 33Vanadium 100 mL AA67N-1 13HNO 3 500 mL AA67N-5 33* For your convenience these elements are availablein HCl. To order, change the N to H at the end ofthe catalog numbers.Cross Reference TableASTM IP ISO DIN JIS AFNOR sorted byASTM Method see beginning of Catalog26 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 50595134MemberASTM D-5059 Lead in Gasoline by X-Ray Spectroscopy IP Designation 228/79Originally designed forD-5059-98Technical NotesAccuStandard has formulated the following standards to measure the lead content in gasoline for bothhigh and low concentrations using bismuth as an internal standard. For long term stability and ease ofuse AccuStandard provides the internal standard in two convenient packaging sizes. The bulk 4 oz.bottles are designed for laboratories analyzing many samples while the 10 mL ampules are forlaboratories that have limited requests for the test method. Should you require bulk quantities of theinternal standard conveniently packaged in single-use ampules, contact AccuStandard’s technicaldepartment for a quotation. Bulk volumes of 250 mL or more can be sealed into ampules (your choiceup to 20 mL size). Use of our ampulling services can provide substantial saving for the Laboratory.D-5059MeetsEPA Guidelinesfor RFGAnalysisASTMPart A - Lead in Gasoline StandardsD-5059-A-CAL-SET$ 450 / set of 7 x 4 ozThe Set contains the following 7 solutions in isooctaneCat. No. Lead Concentration Price /g Pb/US gal g Pb/ UK gal mg Pb/mL UnitD-5059-A-01 0.0000 0.000 0.000 $ 10 / 4 ozD-5059-A-02 0.1000 0.120 0.026 80 / 4 ozD-5059-A-03 1.0000 1.200 0.264 80 / 4 ozD-5059-A-04 2.0000 2.400 0.528 80 / 4 ozD-5059-A-05 3.0000 3.600 0.793 80 / 4 ozD-5059-A-06 4.0000 4.800 1.057 80 / 4 ozD-5059-A-07 5.0000 6.000 1.321 80 / 4 ozPart C - Lead in Gasoline StandardsD-5059-C-CAL-SET$ 450 / set of 7 x 4 ozThe Set contains the following 7 solutions in isooctaneInternal StandardD-5059-IS-4D-5059-IS-10ML-PAKTechnical Notes$ 80 / 1 x 4 oz bottle$ 60 / 5 x 10 mL ampsBismuth @ 0.793 mg/mL (3.00 g/US gal)(3.60 g/UK gal) in Mineral oilAll D-5059 Certificates have theconcentrations for the Standard listedin three convenient LeadConcentration units.Cat. No. Lead Concentration Price /g Pb/US gal g Pb/ UK gal µg Pb/mL UnitD-5059-C-01 0.0000 0.000 0.000 $ 10 / 4 ozD-5059-C-02 0.0010 0.001 0.264 80 / 4 ozD-5059-C-03 0.0050 0.006 1.321 80 / 4 ozD-5059-C-04 0.0100 0.012 2.642 80 / 4 ozD-5059-C-05 0.0500 0.060 13.209 80 / 4 ozD-5059-C-06 0.1000 0.120 26.417 80 / 4 ozD-5059-C-07 0.3000 0.360 79.252 80 / 4 ozASTM D-5134Petroleum Naphthas through n-Nonane by Capillary GCQualitative Reference Petroleum SetD-5134-92-SET$ 75 / 3 x 1 mLOriginally designed forD-5134-98Cat. No. Description Unit PriceD-5134-92-ALK Qualitative Reference Alkylate Standard neat fraction 1 x 1 mL $ 30approx. 30 components identifiedD-5134-92-NAP Qualitative Reference Naphtha Standard neat fraction 1 x 1 mL 30approx. 70 components identifiedD-5134-92-REF Qualitative Reference Reformate Standard neat fraction 1 x 1 mL 30approx. 100 components identifiedStandards of InterestsSee page 14 for additionalDetailed Hydrocarbon Analysis(DHA) blends.Column Evaluation MixD-5134-92-CEMWt. / Wt. %Toluene 0.5n-Heptane 1.02,3,3-Trimethylpentane 1.02-Methylheptane 1.0$ 35 / 1 x 1 mL7 comps.Wt. / Wt. %4-Methylheptane 1.0n-Octane 1.02-Methylpentane 94.5Linearity Check MixD-5134-92-LCM$ / 1 x 1 mL10% w/w each component 10 comps.Benzene2,4-Dimethylheptane2,4-Dimethylhexanen-Heptanen-Hexane2-Methylheptane2-Methylhexanen-Nonanen-OctaneTolueneTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 27


Method 51845185, 5186ASTM StandardsMemberASTM D-5184(Reapproved 1995)Aluminum and Silicon in Fuel Oils byAshing, Fusion, ICP-AES Spectrometry & AA SpectrometryOriginally designed forD-5184-91ASTMTartaric Acid / Hydrochloric AcidSolutionD-5184-91-TA-5Tartaric acid @ 0.5% w/v in 4% HCl$ 20 / 1 x 500 mLAluminum Standard SolutionD-5184-91-AL-1$ 34 / 1 x 100 mLD-5184-91-AL-5$ 67 / 1 x 500 mLAl @ 1000 µg/mL in 5 % HClSilicon Standard SolutionD-5184-91-SI-1$ 34 / 1 x 100 mLD-5184-91-SI-5$ 67 / 1 x 500 mLSilicon @ 1000 µg/mL in trace NaOHTechnical NoteContact the our Technical department for Ready-to-Aspirate working level calibration curves designed foryour laboratories' specific calibration ranges.WEAR METALSASTM D-5185Additive Elements, Wear Metals, & Contaminants in Used Lubricating Oils by ICP-AES21 Wear Metal Multi-Element StandardContaining No Metallic SulfonatesConc. Cat. No. Price(µg/g)10 WM-21-NMS-1X-1 $ 16030 WM-21-NMS-3X-1 16050 WM-21-NMS-5X-1 160100 WM-21-NMS-10X-1 180300 WM-21-NMS-30X-1 240500 WM-21-NMS-50X-1 350WM-21-NMS-SET-1 $ 1050set of above 6 x 100 mLRecommended Internal Standard (IS)Each Wear Metal Standard containsthe below list of 21 elements inhydrocarbon oil at the statedconcentrationAg (Silver)Al (Aluminum)B (Boron)Ba (Barium)Ca (Calcium)Cd (Cadmium)Cr (Chromium)Cu (Copper)Fe (Iron)Mg (Magnesium)Mn (Manganese)Sulfur free Organometallic (IS) Sulfur free Organometallic (IS)Element @ 1000 µg/g Price @ 5000 µg/g PriceCat. No. 50 mL Cat. No. 50 mLCobalt WM-NMS-14 $ 75 WM-NMS-14-5X $ 110Mo (Molybdenum)Na (Sodium)Ni (Nickel)P (Phosphorus)Pb (Lead)Si (Silicon)Sn (Tin)Ti (Titanium)V (Vanadium)Zn (Zinc)Originally designed forD-5185-97Standards of InterestsSee Table of Contents for theWear Metals Group pagesTechnical NotesThis calibration curve has beenformulated with startingmaterials containing no metalsulfonates. So a sulfurcalibration curve can easily bedeveloped using a highconcentration sulfur standard.ASTM D-5186Aromatic Content & Polynuclear Aromatic Content ofDiesel Fuels & Aviation Turbine Fuels by SFCOriginally designed forD-5186-99Performance SolutionD-5186-96-PMD-5186-96-PM-PAKWt. / Wt. %n-Hexadecane 75Naphthalene 2.0$ 25 / 1 x 1 mLSAVE 20% $ 100 / 5 x 1 mL4 comps.Wt. / Wt. %Tetralin 3.0Toluene 20Detector Linearity Check Solution SetD-5186-96-DLC-SET$ 30 / 2 x 1 mLSet includes the below two Cat. No.'sD-5186-96-DLC-25X 25% w/w #2 Diesel Fuel in n-HexadecaneD-5186-96-DLC-50X 50% w/w #2 Diesel Fuel in n-HexadecaneISO 9001:2000Certificate Number: 3169228 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 51885191 &5482Member 5307ASTM D-5188Vapor - Liquid Ratio Temperature StandardsPerformance Check Samples for daily monitoring of instrument performanceCat. No. V/L Temp Price / SetASTM-P-125-01-VAP 36.1˚C (96.9˚F) $ 45 / 5 x 20 mLASTM-P-125-02-VAP 68.0˚C (155.7˚F) 45 / 5 x 20 mLOriginally designed forD-5188-99ASTMASTM D-5191 & D-5482Vapor Pressure StandardsVapor Pressure Quality Control SamplesCat. No. Vapor Pressure Price / SetASTM-P-124-01-VAP 68.3kPa (9.91 psi) $ 65 / 10 x 10 mLASTM-P-124-02-VAP 68.0kPa (9.86 psi) 75 / 10 x 10 mLASTM-P-124-03-VAP 51.1kPa (7.41 psi) 70 / 10 x 10 mLASTM-P-124-04-VAP 46.7kPa (6.77 psi) 115 / 10 x 10 mLASTM-P-124-05-VAP 22.5kPa (3.26 psi) 50 / 10 x 10 mLASTM-P-124-06-VAP 7.1kPa (1.03 psi) 50 / 10 x 10 mLOriginally designed forD-5191-99 & D-5482-99Technical NoteConsists of puresolvents withknown vaporpressureValue Added Paks (Cat. No.’sending in -VAP) provide multiplesingle units packaged togetherfor both greater stability and costsavings.ASTM D-5307-97Boiling Range Distribution of Crude Petroleum by GCQuantitative Paraffins StandardD-5307-QUANTD-5307-QUANT-PAKEqual Wt. %n-Decanen-Undecanen-Dodecanen-Tridecanen-Tetradecanen-Pentadecanen-Hexadecanen-Heptadecane$ 60 / 1 x 2 mLSAVE 20% $ 240 / 5 x 2 mL16 comps.n-Octadecanen-Eicosanen-Tetracosanen-Octacosanen-Dotriacontanen-Hexatriacontanen-Tetracontanen-TetratetracontaneQualitative Paraffins StandardD-5307-QUALD-5307-QUAL-PAKAt stated approx. Wt. %Wt./Wt. %Propane 10Butane 15n-Pentane 15n-Hexane 15$ 40 / 1 x 1 mLSAVE 20% $ 160 / 5 x 1 mL7 comps.Wt./Wt. %n-Heptane 15n-Octane 15n-Nonane 15Column Resolution MixtureD-5307-CRD-5307-CR-PAKAt stated approx. Wt. %Wt./Wt. %n-Hexadecane 1.0n-Octadecane 1.0$ 15 / 1 x 1 mLSAVE 20% $ 60 / 5 x 1 mL3 comps.Wt./Wt. %n-Octane 98.0Internal StandardD-5307-IS-10MLD-5307-IS-10ML-PAKWt./Wt. %n-Tetradecane 25n-Pentadecane 25$ 30 / 1 x 10 mLSAVE 20% $ 120 / 5 x 10 mL4 comps.Wt./Wt. %n-Hexadecane 25n-Heptadecane 25MemberAccuStandard is an active member in ASTM andstrives to keep abreast of ASTM method revisions. Ifour listed formulation does not meet the most recentmethod revision, please contact Technical Support,ext. 117 for an updated product.TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 29


Method 5441ASTM StandardsMemberASTM D-5441Analysis of Methyl tert-butyl ether (MtBE) by GCOriginally designed forD-5441-98ASTMThe ASTM Committee D-02 on Petroleum Products and Lubricants has issued the Standard MethodD-5441-98 for the determination of the purity of methyl tert-butyl ether (MtBE) by Gas Chromatography.This method provides a procedure to measure impurities in MtBE such as C 4 to C 12 olefins, methyl,isopropyl and tert-butyl alcohols, methyl sec-butyl & methyl tert-amyl ethers, acetone, and methyl ethylketones. The presence of these impurities in MtBE can have a direct effect upon the value of the MtBE asa gasoline additive. AccuStandard has formulated the following reference standards to meet the methodspecifications. Different packaging sizes are available to meet various sample testing capacities .MtBE Contaminant StandardLow ConcentrationD-5441 $ 30 / 1 x 1 mLD-5441-PAKSAVE 20% $ 120 / 5 x 1 mLD-5441-5ML$ 100 / 1 x 5 mLD-5441-5ML-PAK SAVE 20% $ 400 / 5 x 5 mLEach comp. at 0.1% Wt./Wt. in MtBE 12 comps.tert-Amyl methyl ethertert-Butanoltert-Butyl ethyl ether4,4-Dimethyl-2-neopentyl-1-penteneMethanol2-Methylbutane2-Methyl-2-butene2,2',4,6,6'-Pentamethyl-3-heptenePentanecis-2-Pentenetrans-2-Pentene2,4,4-Trimethyl-1-penteneQualitative StandardD-5441-QUAL$ 145 / 1 x 1 mL0.1% Wt./Wt. in n-Dodecane 33 comps.MethanolIsobutylenen-Butanetrans-2-butenecis-2-butene3-Methyl-1-buteneAcetoneIsopentane2-Propanol1-Pentene2-Methyl-1-butenen-Pentanetrans-2-Pentenet-Butanolcis-2-Pentene2-Methyl-2-buteneCyclopenteneMtBE2,3-Dimethyl-1-butene4-Methyl-cis-2-pentene2-MethylpentaneMethylethyl ketone3-Methylpentanesec-Butyl methyl etherETBETAME3,5-Dimethyl-1-hexene2,4,4-Trimethyl-1-pentene2,4,4-Trimethyl-2-pentene3,4,4-Trimethyl-trans-2-pentene2,3,4-Trimethyl-2-pentene4,4-Dimethyl-2-neopentyl-1-pentene2,2’,4,6,6’-Pentamethyl-3-hepteneMtBE Resolution Test MixtureD-5441-RESD-5441-RES-PAK$ 20 / 1 x 1 mLSAVE 20% $ 80 / 5 x 1 mLD-5441-RES-5ML$ 60 / 1 x 5 mLD-5441-RES-5ML-PAK SAVE 20% $ 240 / 5 x 5 mLEach comp. at 1% Wt./Wt. in MtBE 3 comps.MtBE Contaminant StandardHigh ConcentrationD-5441-10XD-5441-10X-PAKtert-Amyl methyl ethertert-Butanoltert-Butyl ethyl ether4,4-Dimethyl-2-neopentyl-1-penteneMethanol2-Methylbutane2-Methyl-2-butene2,2',4,6,6'-Pentamethyl-3-heptenePentanecis-2-Pentenetrans-2-Pentene2,4,4-Trimethyl-1-pentene$ 30 / 1 x 1 mLSAVE 20% $ 120 / 5 x 1 mLD-5441-10X-5ML$ 100 / 1 x 5 mLD-5441-10X-5ML-PAK SAVE 20% $ 400 / 5 x 5 mLEach comp.at 1% Wt./Wt. in MtBE 12 comps.Quantitative StandardD-5441-QUANT$ 130 / 1 x 1 mL0.1% Wt./Wt. in n-Dodecane 29 comps.Methanol2-Methylpentane3-Methyl-1-butene Methyl ethyl ketoneAcetone3-MethylpentaneIsopentane sec-Butyl methyl ether2-Propanol Ethyl tert-butyl ether1-PenteneTAME2-Methyl-1-butene 3,5-Dimethyl-1-hexenen-Pentane2,4,4-Trimethyl-1-pentenetrans-2-Pentene 2,4,4-Trimethyl-2-pentenet-Butanol3,4,4-Trimethyl-trans-2-pentenecis-2-Pentene 2,3,4-Trimethyl-2-pentene2-Methyl-2-butene 4,4-Dimethyl-2-neopentyl-1-penteneCyclopentene 2,2’,4,6,6’-Pentamethyl-3-hepteneMtBE2,3-Dimethyl-1-butene4-Methyl-cis-2-penteneFor our complete line ofOrganic Standards andInorganic Standards, request acopy of the Catalog(s).trans-2-Pentenetert-Butanolcis-Pentene30 TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 544254435453MemberASTM D-5442 (Reapproved 1998)Quantitative Wax StandardD-5442-PAKAt stated Wt. % in CyclohexaneWt./Wt. %n-Dodecane 0.02n-Tetradecane 0.03n-Hexadecane 0.04n-Octadecane 0.05n-Eicosane 0.06n-Docosane 0.08Retention Time Standard Mix 1D-5442-RT1Equal parts by weightn-Hexadecane (c16)n-Octadecane (c18)n-Eicosane (c20)n-Docosane(c22)n-Tetracosane (c24)n-Hexacosane (c26)Wt./Wt. %n-Tetracosane 0.10n-Hexacosane 0.12n-Octacosane 0.12n-Triacontane 0.10n-Dotriacontane 0.08$ 50 / 500 mg12 comps.n-Octacosane (c28)n-Triacontane (c30)n-Dotriacontane (c32)n-Hexatriacontane (c36)n-Tetracontane (c40)n-Tetratetracontane (c44)Analysis of Petroleum Waxes by GC$ 95 / 5 x 1 mL16 comps.Wt./Wt. %n-Hexatriacontane 0.06n-Tetracontane 0.05n-Tetratetracontane 0.04n-Pentacontane 0.03n-Hexacontane 0.02NEWRetention Time Standard Mix 2D-5442-RT2Equal parts by weightn-Dodecane (c12)n-Tetradecane (c14)n-Hexadecane (c16)n-Octadecane (c18)n-Eicosane (c20)n-Docosane (c22)n-Tetracosane (c24)n-Hexacosane (c26)Column ResolutionStandardD-5442-CR-PAK $ 40 / 5 x 1 mLAt stated Wt. % in Cyclohexane2 comps.Wt./Wt. %n-Eicosane 0.05n-Tetracontane 0.05NEW$ 55 / 500 mg16 comps.n-Octacosane (c28)n-Triacontane (c30)n-Dotriacontane (c32)n-Hexatriacontane (c36)n-Tetracontane (c40)n-Tetratetracontane (c44)n-Pentacontane (c50)n-Hexacontane (c60)Originally designed forD-5442-93Standards of InterestSee ASTM Methods D-3710,D-5307, D-6352 for additionalcalibration standards for hydrocarbonanalysis or page 15 fornew proposed methods.ASTMASTM D-5443(Reapproved 1998)Paraffin, Naphthene, and Aromatic Hydrocarbon Type Analysis inPetroleum Distillates through 200°C by Multi-dimensional GCOriginally designed forD-5443-93Hydrocarbon Test MixtureD-5443-93-HTMAt stated Wt. %Wt./Wt. %Cyclopentane 1.00n-Pentane 1.00Cyclohexane 2.002,3-Dimethylbutane 2.00n-Hexane 2.00n-Hexene 1.50Methylcyclohexane 4.254-Methyl-1-hexene 1.50n-Heptane 3.50Wt./Wt. %1cis,2-Dimethylcyclohexane 5.00Isooctane 5.00n-Octane 5.001cis,2 cis,4-Trimethylcyclohexane 4.25n-Nonane 4.50n-Decane 4.25n-Undecane 3.50n-Dodecane 3.25Benzene 2.25Toluene 2.25$ 100 / 1 x 1 mL28 comps.Wt./Wt. %trans-Decahydronaphthelene 4.25n-Tetradecane 4.50Ethylbenzene 4.50o-Xylene 4.25n-Propylbenzene 5.001,2,4-Trimethylbenzene 4.501,2,3-Trimethylbenzene 5.001,2,4,5-Tetramethylbenzene 5.00Pentamethylbenzene 5.00Standards of InterestSee pages 6-11 for acomprehensive line of CertifiedSulfur Calibration Standards,Petrocheck, & Petrotest qualitycontrol products, pages 1-2.ASTM D-5453Low Level Sulfur SetMid Level Sulfur SetTotal Sulfur in Light Hydrocarbons,Motor Fuels and Oils by Ultraviolet FluorescenceD-5453-LL-SET$ 90 / 5 x 2 mLThe set contains the following 5 standards in IsooctaneCat. No. Description UnitD-5453-LL-BL Sulfur Blank 2 mLD-5453-LL-01 Sulfur @ 0.5 ng/µL 2 mLD-5453-LL-02 Sulfur @ 2.5 ng/µL 2 mLD-5453-LL-03 Sulfur @ 5.0 ng/µL 2 mLD-5453-LL-04 Sulfur @ 10.0 ng/µL 2 mLD-5453-ML-SET$ 90 / 6 x 2 mLThe set contains the following 5 standards in IsooctaneCat. No. Description UnitD-5453-ML-BL Sulfur Blank 2 mLD-5453-ML-01 Sulfur @ 5.0 ng/µL 2 mLD-5453-ML-02 Sulfur @ 25 ng/µL 2 mLD-5453-ML-03 Sulfur @ 50 ng/µL 2 mLD-5453-ML-04 Sulfur @ 100 ng/µL 2 mLD-5453-ML-05 Sulfur @ 200 ng/µL 2 mLReal World Sulfur in Various Gasoline& FuelsQC SamplesSBPT-LSGAS $ 25 / 2 x 15 mLParameter Method Approx .RangeSulfur D-5453-00 0 - 50 µg/gHigh Level Sulfur SetOriginally designed forD-5453-00D-5453-HL-SET$ 90 / 5 x 2 mLThe set contains the following 5 standards in IsooctaneCat. No. Description UnitD-5453-HL-BL Sulfur Blank 2 mLD-5453-HL-01 Sulfur @ 100 ng/µL 2 mLD-5453-HL-02 Sulfur @ 250 ng/µL 2 mLD-5453-HL-03 Sulfur @ 500 ng/µL 2 mLD-5453-HL-04 Sulfur @ 1000 ng/µL 2 mLD-5453MeetsEPA Guidelinesfor RFGAnalysisTechnical NoteDue to the wide variety ofrecommended solvents andstarting materials mentioned inthe preparation of the sulfurstandards, please review thecurrent product offering listedfor certified sulfur standards.Should AccuStandard’s currentsulfur standard line be missingthe necessary standards foryour application, please use ourcustom quotation request formto indicate your requiredformulation. For ppb Sulfurmeasurements, see page 6-11.Fax 203-786-5287 TECHLAB • Tél. Toll03 Free 87 75 800-442-5290 54 29 • Fax / 203-786-5290 87 36 23 90 • • Website www.techlab.fr www.accustandard.com31


Method 548054825501Member 5580ASTM StandardsASTM D-5480Engine Oil Volatility by GCOriginally designed forD-5480-95ASTMStock Column Resolution StandardD-5480-CR-PAKEach comp. at 10 µg/mL in CS 2D-5480-CR-100X-PAKEach comp. at 1000 µg/mL in CS 2n-Decanen-Dodecanen-Hexadecane$ 40 / 5 x 1 mL5 comps.$ 50 / 5 x 1 mL5 comps.n-Octadecanen-TetracosaneInternal Standard SolutionD-5480-IS-5ML$ 30 / 1 x 5 mLD-5480-IS-5ML-PAK SAVE 20% $ 120 / 5 x 5 mLEach comp. at equal weights3 comps.n-Decanen-Dodecanen-UndecaneTetracosane (Solution A)D-5480-C40-5MLD-5480-C40-5ML-PAK$ 15 / 1 x 5 mLSAVE 20% $ 60 / 5 x 5 mLStandards of InterestAlternative n-Paraffin standardsare available on page 15for further method developmentwork or more DetailedHydrocarbon Analysis (DHA).500 µg/mL in CS 2n-TetracosaneASTM D-5482 & D-5191Vapor Pressure StandardsVapor Pressure Quality Control SamplesCat. No. Vapor Pressure Price / Set of 10ASTM-P-124-01 68.3kPa (9.91 psi) $ 65 / 10 x 10 mLASTM-P-124-02 68.0kPa (9.86 psi) 75 / 10 x 10 mLASTM-P-124-03 51.1kPa (7.41 psi) 70 / 10 x 10 mLASTM-P-124-04 46.7kPa (6.77 psi) 125 / 10 x 10 mLASTM-P-124-05 22.5kPa (3.26 psi) 50 / 10 x 10 mLASTM-P-124-06 7.1kPa (1.03 psi) 50 / 10 x 10 mLTechnical NoteConsists ofpure solventswith knownvapor pressure.Originally designed forD-5482-99 & D-5191-99ASTM D-5501Ethanol Content of Denatured Fuel Ethanol by GCDenatured Fuel Ethanol Calibration SetD-5501-94-SET$ 75 / set of 7 x 1 mLCat. No. Comp.1 Wt./ Wt.% Comp.2 Wt./ Wt.% Comp.3 Wt./ Wt.% UnitD-5501-94-01 Ethanol 92 Methanol 0.6 Heptane 7.4 1 x 1 mLD-5501-94-02 Ethanol 93 Methanol 0.5 Heptane 6.5 1 x 1 mLD-5501-94-03 Ethanol 94 Methanol 0.4 Heptane 5.6 1 x 1 mLD-5501-94-04 Ethanol 95 Methanol 0.3 Heptane 4.7 1 x 1 mLD-5501-94-05 Ethanol 96 Methanol 0.2 Heptane 3.8 1 x 1 mLD-5501-94-06 Ethanol 97 Methanol 0.1 Heptane 2.9 1 x 1 mLD-5501-94-07 Ethanol 98 Methanol 0.05 Heptane 1.95 1 x 1 mLASTM D-5580 Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene, C 9 andHeavier Aromatics, & Total Aromatics in Finished Gasoline by GCAromatics Quantitative Calibration Mixes (without Internal Standard)D-5580-95-CAL-SET-10ML$ 300 / set of 5 x 10 mL of 6 component mixOriginally designed forD-5501-94Technical NoteAdditional Oxygenate calibration,check standards, andindependent referencestandards can be found inASTM method D-4815 (page24) or D-5622-94 (page 37).The required QA/QCprocedures in EPA methodsstipulate a calibration checkstandard be used once peranalytical batch or per 10sample set. AccuStandard hasbulk packaged check standardsto meet this increased usage.Originally designed forD-5580-00Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5Analyte Calibration range Wt. % Wt. % Wt. % Wt. % Wt. %Benzene 0.10 - 5.00 0.10 0.50 1.00 2.00 5.00Toluene 1.00 - 15.00 15.00 10.00 5.00 2.50 1.00Ethylbenzene 0.50 - 10.00 0.50 1.00 2.50 5.00 10.00o-Xylene 0.50 - 10.00 1.00 2.50 10.00 5.00 0.501,2,4-Trimethylbenzene 0.50 - 10.00 1.00 10.00 0.50 5.00 2.50Isooctane 82.40 76.00 81.00 80.50 81.00Aromatics Quantitative Calibration Mixes (with Internal Standard)D-5580-95-CAL-IS-SET$ 100 / set of 5 x 1 mL of 7 component mixAnalyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5Analyte Calibration range Wt. % Wt. % Wt. % Wt. % Wt. %Benzene 0.09 - 4.50 0.09 0.45 0.90 1.80 4.50Toluene 0.90 - 13.50 13.50 9.00 4.50 2.25 0.90Ethylbenzene 0.45 - 9.00 0.45 0.90 2.25 4.50 9.00o-Xylene 0.45 - 9.00 0.90 2.25 9.00 4.50 0.451,2,4-Trimethylbenzene 0.45 - 9.00 0.90 9.00 0.45 4.50 2.252-Hexanone (Internal Std.) 10.00 10.00 10.00 10.00 10.00Isooctane 74.16 68.40 72.90 72.45 72.90ASTM D-5580-00 Continuedon the Next Page32TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 5580MemberASTM D-5580-00 Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene, C9 &Continued Heavier Aromatics, and Total Aromatics in Finished Gasoline by GCValve Timing Calibration Mix(with Internal Standard)M-GRA-VT/IS-AS$ 25 / 1 x 1 mLM-GRA-VT/IS-AS-PAK SAVE 20% $ 100 / 5 x 1 mLEach at stated conc.6 comps.Wt./Wt. %Benzene 4.5Toluene 4.5Ethylbenzene 9.0o-Xylene 9.02-Hexanone (Internal Std.) 10.0Isooctane 63.0Internal StandardM-GRA-IS-AS-5MLM-GRA-IS-AS-5ML-PAK2-Hexanone (Neat)Wt./Wt. %n-Hexane 12n-Heptane 20n-Octane 15n-Decane 10n-Dodecane 1Isooctane 20Benzene 1$ 10 / 1 x 5 mLSAVE 20% $ 40 / 5 x 5 mLDaily Quality Control Standardwithout Internal StandardD-5580-QC-R1D-5580-QC-R1-PAK$ 125 / 1 x 10 mLSAVE 20% $ 500 / 5 x 10 mL14 comps.Wt./Wt. %Toluene 9Ethylbenzene 2p-Xylene 3o-Xylene 21,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 1Naphthalene 1Valve Timing Calibration Mix(without Internal Standard)M-GRA-VT-AS-10ML$ 100 / 1 x 10 mLM-GRA-VT-AS-10ML-PAK SAVE 20% $ 400 / 5 x 10 mLEach at stated conc.5 comps.Wt./Wt. %Benzene 5.0Toluene 5.0Ethylbenzene 10.0o-Xylene 10.0Isooctane 70.0Selectivity Check StandardM-GRA-SCS-AS$ 10 / 1 x 1 mLM-GRA-SCS-AS-PAK SAVE 20% $ 40 / 5 x 1 mLEach at stated conc.2 comps.Wt./Wt. %n-Dodecane 1.5Isooctane 98.5Daily Quality Control Standardwithout Internal StandardD-5580-QCD-5580-QC-PAKWt./Wt. %n-Hexane 12n-Heptane 20n-Octane 15n-Decane 10n-Triadecane 1Isooctane 20Benzene 1$ 125 / 1 x 10 mL$ 500 / 5 x 10 mL14 comps.Wt./Wt. %Toluene 9Ethylbenzene 2p-Xylene 3o-Xylene 21,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 1Naphthalene 1Originally designed forD-5580-00Technical NoteASTM D-5580 GasolineRefinery Quality ControlStandardAccuStandard was requested bythe Petrochemical Industry tomanufacture the following QA/QCstandards for ASTM MethodD-5580. The configuration of yourinstrument valve time switching andthe pre-column incorporateddetermines which QA/QC standardprovides optimum performancewhen analyzing gasolines samplesby Method D-5580. Use of theD-5580 standards in conjunctionwith the real world gasolineAccuPetroTest & AccuPetroCheckConsensus Value ReferenceMaterial (see pages 1-2) canprovide added assurance that theanalytical results being generatedby the laboratory are reproducibleand the analytical system isperforming to methodspecifications.ASTMExclusive Aromatic Chemical Reference MaterialBenefits from AccuStandardEvery analyte in each solution is individually weighedActual weights and weight percents are available with allASTM/EPA solutionsTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 33


Method 5599ASTMMemberASTM StandardsASTMASTM D-5599Oxygenates in Gas by GC & O-FIDOxygenates Calibration Curve with Internal StandardM-GRO-CAL/IS-SETM-GRO-CAL/IS-SET-PAK$ 250 / set of 8 x 1 mL$ 1,000 / 5 x (8 x 1) mLof 15 Comp. MixEvery analyte in each solutionis individually weighedAnalyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7 Std. 8Calibration range Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. %Methanol 0.1 - 5.0 --- 0.1 2.5 --- 5 0.5 1 ---Ethanol 1.0 - 12.0 12 --- 3 --- 8 5 1 ---Isopropanol 0.1 - 2.0 2 1 --- 0.1 0.3 --- 0.5 ---t-Butanol 0.1 - 2.0 0.5 0.1 1 --- 2 0.3 --- ---Propanol 0.2 - 2.0 2 --- 0.7 0.2 1 --- 0.4 ---MtBE 1.0 - 17.0 5 17 --- --- 1 2.5 10 ---sec-Butanol 0.1 - 2.5 1 --- 0.5 0.1 --- 2.5 0.7 ---Diisopropyl ether 0.1 - 2.0 --- 0.5 0.3 0.1 2 1 --- ---iso-Butanol 0.1 - 2.0 2 0.5 --- 1 0.1 0.3 --- ---EtBE 1.0 - 18.0 --- 3.5 18 7.5 --- 1 12 ---t-Pentanol 0.1 - 2.0 0.3 1 --- 0.5 0.1 2 --- ---Butanol 0.1 - 2.0 1 --- 0.3 --- 0.5 0.1 2 ---TAME 1.0 - 18.0 --- 3.5 1 18 7.5 12 --- ---1,2- Dimethoxyethane (ISTD) 4 4 4 4 4 4 4 ---RFA Gasoline 70.2 68.8 68.7 68.5 68.5 68.8 68.4 100Total oxygenates & ISTD 29.8 31.2 31.3 31.5 31.5 31.2 31.6 0Oxygenates Calibration Curve without Internal StandardM-GRO-CAL-SET$ 850 / set of 8 x 10 mLof 14 Comp. MixOriginally designed forD-5599-95Actual weights and weight percents areprovided with all ASTM/EPA SolutionsAnalyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7 Std. 8Calibration range Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. %Methanol 0.1 - 5.0 --- 0.1 2.5 --- 5 0.5 1 ---Ethanol 1.0 - 12.0 12 --- 3 --- 8 5 1 ---Isopropanol 0.1 - 2.0 2 1 --- 0.1 0.3 --- 0.5 ---t-Butanol 0.1 - 2.0 0.5 0.1 1 --- 2 0.3 --- ---Propanol 0.2 - 2.0 2 --- 0.7 0.2 1 --- 0.4 ---MtBE 1.0 - 17.0 5 17 --- --- 1 2.5 10 ---sec-Butanol 0.1 - 2.5 1 --- 0.5 0.1 --- 2.5 0.7 ---Diisopropyl ether 0.1 - 2.0 --- 0.5 0.3 0.1 2 1 --- ---iso-Butanol 0.1 - 2.0 2 0.5 --- 1 0.1 0.3 --- ---EtBE 1.0 - 18.0 --- 3.5 18 7.5 --- 1 12 ---t-Pentanol 0.1 - 2.0 0.3 1 --- 0.5 0.1 2 --- ---Butanol 0.1 - 2.0 1 --- 0.3 --- 0.5 0.1 2 ---TAME 1.0 - 18.0 --- 3.5 1 18 7.5 12 --- ---RFA Gasoline 74.2 64.8 64.7 64.5 64.5 64.8 64.4 100Total oxygenates 25.8 27.2 27.3 27.5 27.5 27.2 27.6 0Technical NoteOxygenate Calibration CurvesISTD-Free and LargerPackaging SizeAccuStandard has receivedrequests from the PetroleumIndustry to formulate our D-5599Oxygenate product without internalstandard (ISTD) and package it in alarger volume. We have met thoserequests by introducing the M-GRO-CAL-SET calibration curve.This curve is manufactured withoutincorporating an internal standardand is packaged in Ready-to-Use10 mL sample volume.The certified oxygenate calibrationcurve can be used in combinationwith other aromatic standards forcombined oxygenate/aromaticanalysis, to change the amount ofinternal standard added, or toincorporate alternative internalstandard analytes.D-5599MeetsEPA Guidelinesfor RFGAnalysisTechnical NoteAccuStandard’s M-GROoxygenate calibration curve hasbeen successfully used byPetroleum Refineries andsupporting laboratories for bothASTM Method D-5599 andASTM Method D-4815. Inaddition, AccuStandard’scertified oxygenate chemicalreference materials provide thefollowing features and benefitsfor superior performance andvalue.Benefits from AccuStandard’s OxygenatesFeatures:Benefits:Analytes checked for chemical purity & water content The use & validation of the highest purity neats enhance the integrity of the standard.Analyzed by Independent LaboratoriesCertified method specific calibration standardsElimination of standards preparationInternal Standards incorporatedWeights and weight percents providedAll necessary solutions includedVariations in Packaging sizeEconomicalIndependent product validation of certified values.Increased confidence in analytical results.Time is utilized quantifying samples.Ready-to-Inject Standards.Ease of use in performing back calculations.Provides single source for sample analysis.Meet laboratory sample volumes.Time is spent on analysis rather than preparing stds.7 stds. used to generate 5 point curve Generate a 5 point curve in 30% less time than competitors' 10 standard set.34TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 5599MemberASTM D-5599ContinuedDaily Quality Control Standard(without Internal Standard)M-GRO-QC-10MLM-GRO-QC-10ML-PAKOxygenates in Gasoline by GC & O-FIDASTM/EPA Oxygenate Quality Control StandardsCompound TargetOxygenate Wt. %Methanol 1Ethanol 1Isopropanol 1t-Butanol 1Propanol 1MtBE 3sec-Butanol 1Di-isopropyl ether 3$ 100 / 1 x 10 mLSAVE 20% $ 400 / 5 x 10 mLCompound TargetOxygenate Wt. %iso-Butanol 1EtBE 3t-Pentanol 1Butanol 1TAME 3RFA Gasoline 7914 comps. 100Revised Daily Quality Control Standard(without Internal Standard)M-GRO-QC-R-10MLM-GRO-QC-R-10ML-PAKCompound TargetOxygenate Wt. %Methanol 1Ethanol 1Isopropanol 1t-Butanol 1Propanol 1MtBE 3sec-Butanol 1Di-isopropyl ether 1Originally designed forD-5599-95$ 100 / 1 x 10 mLSAVE 20% $ 400 / 5 x 10 mLCompound TargetOxygenate Wt. %iso-Butanol 1EtBE 3t-Pentanol 1Butanol 1TAME 3RFA Gasoline 8114 comps. 100D-5599MeetsEPA Guidelinesfor RFGAnalysisTechnical NoteThe Daily Quality ControlStandard M-GRO-QC-R wasdeveloped in response to yourrequests for a QC mixbracketed by the CalibrationCurve.AccuStandard reduced thediisopropyl ether content from 3Wt. % to 1 Wt. % to meet themethod specifications.ASTMDaily Quality Control Standard(with Internal Standard)M-GRO-QC/IS-5ML$ 75 / 1 x 5 mLM-GRO-QC/IS-5ML-PAK SAVE 27% $ 275 / 5 x 5 mLCompound Target Compound TargetOxygenate Wt. % Oxygenate Wt. %Methanol 1 Di-isopropyl ether 3Ethanol 1 iso-Butanol 1Isopropanol 1 EtBE 3t-Butanol 1 t-Pentanol 1Propanol 1 Butanol 1MtBE 3 TAME 3sec-Butanol 1RFA Gasoline 791,2-Dimethoxyethane (ISTD) is combined withthe above 14 comps. in a 4 to 100 weight ratio15 comps.Gasoline Refinery Blank(with Internal Standard)100M-GRO-BLNK/IS-10ML$ 15 / 1 x 10mLM-GRO-BLNK/IS-10ML-PAK SAVE 20% $ 60 / 5 x 10mL2 comps.Wt. %1,2- Dimethoxyethane (ISTD) 4RFA Gasoline 96Revised Daily Quality Control Standard(with Internal Standard)M-GRO-QC-R/IS-5ML$ 75 / 1 x 5 mLM-GRO-QC-R/IS-5ML-PAK SAVE 27% $ 275 / 5 x 5 mLCompound Target Compound TargetOxygenate Wt. % Oxygenate Wt. %Methanol 1 Di-isopropyl ether 1Ethanol 1 iso-Butanol 1Isopropanol 1 EtBE 3t-Butanol 1 t-Pentanol 1Propanol 1 Butanol 1MtBE 3 TAME 3sec-Butanol 1RFA Gasoline 811,2-Dimethoxyethane (ISTD) is combined withthe above 14 comps. in a 4 to 100 weight ratio15 comps.O-FID/EPA Gasoline RefineryInternal StandardM-GRO-IS-5MLM-GRO-IS-5ML-PAK1,2- Dimethoxyethane (ISTD)100$ 10 / 1 x 5 mLSAVE 20% $ 40 / 5 x 5 mLTechnical NoteAdditional Oxygenatecalibration, check standards,and independent referencestandards can be found inASTM method D-4815 (page24) or D-5622 (page 37). Therequired QA/QC procedures inEPA methods stipulate acalibration check standard beused once per analytical batchor per 10 sample set.AccuStandard has bulkpackaged check standards tomeet this increased usage.O-FID Gasoline Refinery BlankM-GRO-BLNK-10ML$ 10 / 1 x 10mLM-GRO-BLNK-10ML-PAK SAVE 20% $ 40 / 5 x 10mLRFA Gasoline (neat)TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 35


Method 5599ASTMMemberOxygenates Using O-FIDEPA O-FID Oxygenate Petrochemical StandardsAccuStandard has formulated this second oxygenate version to meet the specific analyte requirements set forth in the EPA methodology.ASTMASTM D-5599EPA Gasoline Refinery Oxygenates Calibration CurvesEPA O-FID Quantitative Calibration Mixes (without Internal Standard)M-GRO-CAL-EPA-SET-10ML$ 350 / set of 5 x 10 mL5 comps.Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5Calibr. range Wt. % Wt. % Wt. % Wt. % Wt. %Methanol 0.30 - 12.00 6.00 12.00 3.00 0.30 9.00Ethanol 0.30 - 12.00 0.30 3.00 6.00 9.00 12.00t-Butanol 0.30 - 12.00 0.30 6.00 9.00 12.00 3.00MtBE 0.30 - 15.00 15.00 7.50 11.25 3.75 0.30RFA Gasoline 78.40 71.50 70.75 74.95 75.70Originally designed forD-5599-95For our complete line ofOrganic Standards,request a copy of ourCatalog.EPA O-FID Quantitative Calibration Mixes (with Internal Standard)M-GRO-CAL-IS/EPA-SET$ 175 / set of 5 x 1 mL6 comps.Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5Calibr. range Wt. % Wt. % Wt. % Wt. % Wt. %Methanol 0.29 - 11.40 5.70 11.40 2.85 0.29 8.55Ethanol 0.29 - 11.40 0.29 2.85 5.70 8.55 11.40t-Butanol 0.29 - 11.40 0.29 5.70 8.55 11.40 2.85MtBE 0.29 - 14.29 14.25 7.13 10.69 3.56 0.291,2-Dimethoxyethane (ISTD) 5.00 5.00 5.00 5.00 5.00RFA Gasoline 74.48 67.93 67.31 71.20 71.92EPA O-FID Quantitative CalibrationCheck Standard(without Internal Standard)M-GRO-EPA-CC-10ML$ 50 / 1 x 10 mLM-GRO-EPA-CC-10ML-PAK SAVE 20% $ 200 / 5 x 10 mL5 comps.Wt./Wt. %Methanol 4.0Ethanol 8.0tert-Butanol 5.0Wt./Wt. %Methyl tert-butyl ether 12.0RFA gasoline 71.0EPA O-FID Spiking SolutionM-GRO-EPA-SP-5MLM-GRO-EPA-SP-5ML-PAKWt./Wt. %Methanol 14.3Ethanol 28.6$ 50 / 1 x 5 mLSAVE 20% $ 200 / 5 x 5 mL4 comps.Wt./Wt. %tert-Butanol 14.3Methyl tert-butyl ether 42.8EPA O-FID Quantitative CalibrationCheck Standard(with Internal Standard)M-GRO-EPA-CC/IS-5ML$ 35 / 1 x 5 mLM-GRO-EPA-CC/IS-5MLPAK SAVE 20% $ 150 / 5 x 5 mL6 comps.Wt./Wt. %Methanol 3.80Ethanol 7.60tert-Butanol 4.75Wt./Wt. %Methyl tert-butyl ether 11.40RFA gasoline 67.45DME (internal standard) 5.0Oxygenate Free Gasoline RefineryBlankM-GRO-BLNK-10MLM-GRO-BLNK-10ML-PAKRFA Gasoline (neat)$ 10 / 1 x 10 mLSAVE 20% $ 40 / 5 x 10 mLTechnical NoteAdditional Oxygenatecalibration, check standards,and independent referencestandards can be found inASTM method D-4815 (page24) or D-5622 (page 37). Therequired QA/QC procedures inEPA methods stipulate acalibration check standard beused once per analytical batchor per 10 sample set.AccuStandard has bulkpackaged check standards tomeet this increased usage.Internal StandardM-GRO-IS-5MLM-GRO-IS-5ML-PAK$ 10 / 1 x 10 mLSAVE 20% $ 40 / 5 x 10 mL1,2-Dimethoxyethane (ISTD)Cross Reference TableASTM IP ISO DIN JIS AFNOR sorted byASTM Method see beginning of Catalog36TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 56005622MemberASTM D-5600AluminumBariumCalciumIronASTM D-5622MagnesiumManganeseNickelSiliconTrace Metals in Petroleum Coke by ICP-AESMulti-Element Calibration StandardD-5600-01-1$ 225 / 1 x 100 mL500 µg/mL each in 2-5% HNO 3 tr. HF 12 comps.SodiumTitaniumVanadiumZincHydrochloric Acid DiluentD-5600-BLH-5D-5600-BLH-L20% HCl in ASTM Type II waterLithium Borate DiluentD-5600-LIB-1D-5600-LIB-52.0% Lithium Borate in 10% HClTotal Oxygen in Gasoline & MeOH Fuels by Reductive Pyrolysis$ 50 / 1 x 500 mL$ 65 / 1 x 1 L$ 125 / 1 x 100 mL$ 180 / 1 x 500 mLOxygenate UnitCat. No. Description (2 x 10 mL, plus an RFA gasoline blank) Wt. % PriceASTM-P-0061-SET * Ethanol in Oxygenate free RFA gasoline 5.0 3 x 10 mL $ 50ASTM-P-0062-SET * Ethanol in Oxygenate free RFA gasoline 10.0 3 x 10 mL 50ASTM-P-0063-SET * t-Amyl methyl ether in Oxygenate free RFA gasoline 10.0 3 x 10 mL 50ASTM-P-0064-SET * t-Amyl methyl ether in Oxygenate free RFA gasoline 15.0 3 x 10 mL 50ASTM-P-0065-SET * Ethyl t-butyl ether in Oxygenate free RFA gasoline 10.0 3 x 10 mL 50ASTM-P-0066-SET * Ethyl t-butyl ether in Oxygenate free RFA gasoline 15.0 3 x 10 mL 50ASTM-P-0067-SET * Methyl t-butyl ether in Oxygenate free RFA gasoline 10.0 3 x 10 mL 50ASTM-P-0068-SET * Methyl t-butyl ether in Oxygenate free RFA gasoline 15.0 3 x 10 mL 50ASTM-P-0069-SET * Methanol & t-Butanol in Oxygenate free RFA gasoline 10.0 & 5.0 3 x 10 mL 50* Each Set includes M-GRO-BLNK-10MLOxygenate Free Gasoline Refinery BlankM-GRO-BLNK-10ML$ 10 / 1 x 10 mLRFA Gasoline (neat)Standards of InterestIndividual ICP Standards are on pages 67-72.Standards of InterestSee ASTM Methods D-4815 (page 24) and D-5599(pages 34-36) for additional oxygenate calibrationstandards.Technical NoteOriginally designed forD-5600-98Use M-GRO-BLNK-10ML as anoxygenate free RFA gasoline matrix tomake up your own oxygenatestandards or call our Technical Dept. tohave a Standard custom made for you.Technical NoteD-5600 Ready-to-AspirateStandardsAccuStandard has formulated thefollowing stock standards forASTM Method D-5600. We haveprepared numerous Ready-to-Aspirate ICP multi-elementsolutions. Should your companywant to eliminate the preparationprocess for Inorganic standardscontact our Technical Departmentfor a quote on a Ready-to-Aspirate working level Inorganicstandard.Originally designed forD-5622-95Technical NoteAccuStandard’s Oxygenatereference fuel line wasdesigned as a cost effectivealternative for PetrochemicalLaboratories. All oxygenateblends come with a certificateto maintain traceability links toNIST SRMs (when available).By packaging the standard in10 mL sealed ampules yourlaboratory will realize costsavings. The 10 mL size avoidshaving special packaging andhazardous material fees billedto your invoice.For our complete line ofInorganic Standards,request a copy of ourInorganics Catalog.ASTMTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 37


Method 5623ASTM StandardsMemberASTM D-5623Sulfur Compounds in Light Petroleum Liquids by GC andSulfur Selective DetectionOriginally designed forD-5623-94ASTMThis set of qualitative Sulfur Standards are formulated for research evaluation of the presence of the sulfuranalytes or their breakdown products.ASTM-P-0091-10X-SETApprox. 2.0 mg/mL each in Toluene$ 625 / set of 22 x 1 mLAnalyte Cat. No. Unit PriceHydrogen sulfide ASTM-P-0091-01-10X 1 x 1 mL $ 35Carbonyl sulfide (Carbon oxysulfide) ASTM-P-0091-02-10X 1 x 1 mL 35Methyl mercaptan (Methanethiol) ASTM-P-0091-03-10X 1 x 1 mL 35Ethyl mercaptan (Ethanethiol) ASTM-P-0091-04-10X 1 x 1 mL 35Methyl sulfide (Dimethyl sulfide) ASTM-P-0091-05-10X 1 x 1 mL 35Carbon disulfide ASTM-P-0091-06-10X 1 x 1 mL 352-Propanethiol (Isopropyl mercaptan ASTM-P-0091-07-10X 1 x 1 mL 352-Methyl-2-propanethiol (t-butyl mercaptan) ASTM-P-0091-08-10X 1 x 1 mL 351-Propanethiol (Propyl mercaptan) ASTM-P-0091-09-10X 1 x 1 mL 35Ethyl methyl sulfide ASTM-P-0091-10-10X 1 x 1 mL 351-Methyl-1-propanethiol (2-butanethiol) ASTM-P-0091-11-10X 1 x 1 mL 35Thiophene ASTM-P-0091-12-10X 1 x 1 mL 352-Methyl-1-propanethiol (Isobutyl mercaptan) ASTM-P-0091-13-10X 1 x 1 mL 35Diethyl sulfide ASTM-P-0091-14-10X 1 x 1 mL 351-Butanethiol (Butyl mercaptan) ASTM-P-0091-15-10X 1 x 1 mL 35Methyl disulfide (Dimethyl disulfide) ASTM-P-0091-16-10X 1 x 1 mL 352-Methylthiophene ASTM-P-0091-17-10X 1 x 1 mL 353-Methylthiophene ASTM-P-0091-18-10X 1 x 1 mL 35Diethyl disulfide (Ethyl disulfide) ASTM-P-0091-19-10X 1 x 1 mL 353-Methylbenzo[b]thiophene ASTM-P-0091-20-10X 1 x 1 mL 355-Methylbenzo[b]thiophene ASTM-P-0091-21-10X 1 x 1 mL 75Diphenyl sulfide ASTM-P-0091-22-10X 1 x 1 mL 35Custom Ampulling for Bulk Quantity RequirementsFill Volumes from 0.2 mL to 20 mL• FlammablesQC Services availableAccuStandard has the resources and equipment to meet yourcustom packaging requirements. Our full automated filler-sealercan accommodate a fill range from 0.2 to 20 mL, and ampulesizes from 1 mL to 20 mL.AccuStandard has extensive experience with Round Robinsamples for ASTM committees.Call our Technical Department for a quotation.We can reduce your costs by using the Cozzoli Auto Filling/Sealing Machine to packagejust the right size product for your application.38TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 5599MemberASTM D-5708Nickel, Vanadium, & Iron in Crude Oils & Residual Fuels by ICP-AESOriginally designed forD-5708-95aTest Method A - ICP with an Organic Solvent Specimen SolutionSulfur and Metals in Mineral OilASTM-P-0102-SET$ 1850 / 100 mLSulfur Iron Nickel VanadiumCat. No. Conc. Conc. Conc. Conc. Price(Wt. %) (µg/g) (µg/g) (µg/g) 100 mLASTM-P-0102-01 0.00 0 0 0 $ 200ASTM-P-0102-02 0.50 300 10 500 200ASTM-P-0102-03 1.00 500 100 25 200ASTM-P-0102-04 - 100 80 250 200ASTM-P-0102-05 2.00 200 40 100 200ASTM-P-0102-06 2.50 400 5 400 200ASTM-P-0102-07 3.00 0 60 300 200ASTM-P-0102-08 3.50 500 0 200 200ASTM-P-0102-09 - 100 100 0 200ASTM-P-0102-10 4.50 300 50 250 200ASTM-P-0102-11 5.00 200 20 500 200ASTM-P-0102-12 5.50 50 100 50 200Sulfur and Metals in Residual Fuel OilASTM-P-0103-SET$ 2100 / 100 mLSulfur Iron Nickel VanadiumCat. No. Conc. Conc. Conc. Conc. Price(Wt. %) (µg/g) (µg/g) (µg/g) 100 mLASTM-P-0103-01 0.00 0 0 0 $ 200ASTM-P-0103-02 0.50 300 10 500 200ASTM-P-0103-03 1.00 500 100 25 200ASTM-P-0103-04 - 100 80 250 200ASTM-P-0103-05 2.00 200 40 100 200ASTM-P-0103-06 2.50 400 5 400 200ASTM-P-0103-07 3.00 0 60 300 200ASTM-P-0103-08 3.50 500 0 200 200ASTM-P-0103-09 - 100 100 0 200ASTM-P-0103-10 4.50 300 50 250 200ASTM-P-0103-11 5.00 200 20 500 200ASTM-P-0103-12 5.50 50 100 50 200Stock Multi-Element inMineral OilD-5708-A-10X $ 150 / 4 oz.100 µg/g in 20 cSt mineral oil3 comps.IronNickelVanadiumStandards of InterestSee Table of Contents forthe Wear Metals Grouppages.For our complete line ofInorganic Standards,request a copy of ourInorganics CatalogASTMWEAR METALSStock Multi-ElementAqueous StandardD-5708-B-10X-1D-5708-B-10X-5Each at 100 µg/mL in 2-5% HNO 3IronNickelTest Method B - ICP after Acid Decomposition of Sample$ 60 / 100 mL$ 115 / 500 mL3 comps.VanadiumWorking Level Multi-ElementAqueous StandardD-5708-B-5Each at 10 µg/mL in 2-5% HNO 3IronNickel$ 105 / 500 mL3 comps.VanadiumNitric Acid BlankCLP-BLN-5CLP-BLN-L$ 30 / 500 mL$ 45 / L (2 x 500 mL)5% HNO 3 in ASTM Type I WaterMemberAccuStandard is an active member in ASTM andstrives to keep abreast of ASTM method revisions. Ifour listed formulation does not meet the most recentmethod revision, please contact Technical Support,ext. 117 for an updated product.TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 39


Method 5762ASTM StandardsMemberASTM D-5762Stock Nitrogen StandardD-5762-95-500X-PAKNitrogen in Petroleum & Petroleum Products by Boat-Inlet Chemiluminescence$ 45 / 5 x 1 mLOriginally designed forD-5762-98ASTMNitrogen @ 500 µg/mL in Xylene (Acridine @ 6397 µg/mL)Nitrogen Calibration SetD-5762-95-CAL-SET $ 75 / 6 x 1 mLCat. No. Description UnitD-5762-95-BL Xylene Blank 1 x 1 mLD-5762-95-1X Nitrogen @ 1.0 µg/mL in Xylene 1 x 1 mLD-5762-95-5X Nitrogen @ 5.0 µg/mL in Xylene 1 x 1 mLD-5762-95-10X Nitrogen @ 10 µg/mL in Xylene 1 x 1 mLD-5762-95-50X Nitrogen @ 50 µg/mL in Xylene 1 x 1 mLD-5762-95-100X Nitrogen @ 100 µg/mL in Xylene 1 x 1 mLTechnical NoteNitrogen introduced usingAcridine.Low level Nitrogen Calibration SetASTM-P-0070-SET $ 75 / 6 x 1 mLCat. No. Description UnitASTM-P-0070-BL Isooctane Blank 1 x 1 mLASTM-P-0070-1X Nitrogen @ 0.5 µg/g in Isooctane 1 x 1 mLASTM-P-0070-2X Nitrogen @ 1.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-4X Nitrogen @ 2.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-10X Nitrogen @ 5.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-20X Nitrogen @ 10.0 µg/g in Isooctane 1 x 1 mLTechnical NoteNitrogen introduced usingAcridine.Low level Nitrogen & Sulfur Calibration SetASTM-P-0071-SET $ 50 / 4 x 1 mLCat. No. Description UnitASTM-P-0071-BL Benzene Blank 1 x 1 mLASTM-P-0071-01 Nitrogen @ 0.25 µg/g & Sulfur @ 0.25 µg/g in Benzene 1 x 1 mLASTM-P-0071-02 Nitrogen @ 0.50 µg/g & Sulfur @ 0.50 µg/g in Benzene 1 x 1 mLASTM-P-0071-03 Nitrogen @ 1.00 µg/g & Sulfur @ 1.00 µg/g in Benzene 1 x 1 mLTechnical NoteThe Nitrogen isintroduced usingAniline and the Sulfuris introduced usingn-Butyl sulfide.AccuPetroCheck and AccuPetroTest Real World Gasoline QC StandardsIn cooperation with ASTM D-02 subcommittee 3 and 4, AccuStandard ampulled 21 Real World gasoline reference fuels. Consensus Values havebeen determined for these reference fuels by various ASTM Round Robins to provide Petrochemical Laboratories with a source of wellcharacterized gasoline standards for use in QA/QC applications and as Single Blind test samples over an extended period of time. As new ASTMD-02.03 and D-02.04 Test methods are promulgated they require mandatory Quality Control testing of real world samples. AccuStandard’sAccuPetroTest & AccuPetroCheck standards are being successfully used to achieve these new Quality Control requirements.QC StandardsCARB Low Sulfur RFG QCStandardASTM-FUEL-QCS-01-PAK$ 60 / 5 x 15 mLParameter Method Value Conc.Total Aromatics D-1319 24.5 Vol.%Total Olefins D-1319 5.3 Vol.%Total Saturates D-1319 58.3 Vol.%Sulfur D-2622 0.0057 Wt.%Sulfur D-4294 0.0078 Wt.%Sulfur D-5453 55.76 µg/gSulfur D-6344 59.31 µg/gBenzene D-5769 0.80 Vol.%Toluene D-5769 4.92 Vol.%Total Aromatics D-5769 23.42 Vol.%Benzene D-6227 0.78 Vol.%Total Olefins D-6550 5.3 Vol.%Conventional Gasoline QCStandardASTM-FUEL-QCS-02-PAK$ 60 / 5 x 15 mLParameter Method Value Conc.Total Aromatics D-1319 34.6 Vol.%Total Olefins D-1319 12.4 Vol.%Total Saturates D-1319 62.8 Vol.%Sulfur D-2622 0.0338 Wt.%Sulfur D-4294 0.0368 Wt.%Sulfur D-5453 317.36 µg/gSulfur D-6344 338.78 µg/gBenzene D-5769 0.55 Vol.%Toluene D-5769 5.53 Vol.%Total Aromatics D-5769 32.51 Vol.%Benzene D-6227 0.52 Vol.%Total Olefins D-6550 12.4 Vol.%AccuPetroCheck QC StandardsTwo of the fuels are available as AccuPetroCheckConsensus Value QC Standards. TheAccuPetroCheck CARB and Conventionalgasoline reference materials have all parameterslisted on the certificate with the Consensus Valuesand the regression equations for reproducability.Use of these Reference Materials improve thequality of laboratory results. The ConsensusValues listed reflect initial statistical treatment ofthe data at the time the catalog was published.The actual certificate provided with theAccuPetroCheck QC standard will have theaccepted Consensus Value based on statisticaltreatment of the data.40TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Petrochemical StandardsMemberAccuPetroTestSulfur in Diesel Fuel QC StandardSBPT-SDF$ 25 / 2 x 15 mLParameterApprox. RangeSulfur20 - 11000 mg/kgSee ASTM Methods D-2622, D-3120, D-3246-92,D-4294, D-5453, for Sulfur Calibration StandardsAccuPetroTest GasolineSulfur in White Mineral Oil QCStandardSBPT-SWMO$ 25 / 2 x 15 mLParameterApprox. RangeSulfur20 - 11000 mg/kgSee ASTM Methods D-2622, D-3120,D-3246-92, D-4294, D-5453 for SulfurCalibration StandardsSulfur Single Blind AccuPetroTestAlternative Matrices StandardsAccuStandard has manufactured a number ofDiesel and White Mineral Oil quality controlproducts containing a gravimetrically preparedamount of Sulfur. Use of these alternativematrix materials can provide further evaluationof the QA/QC process in the laboratory. Twosamples will be sent for the test parameter anda separate sealed envelope containing thegravimetrically prepared sulfur values is alsoprovided. The second sample is forrepeatability testing or for use as a futureQA/QC reference.ASTMLow Sulfur QC SampleSBPT-LSGAS$ 25 / 2 x 15 mLParameter Method Approx. RangeSulfur 5453 0 - 50 µg/gOlefin QC SampleSBPT-OLEFINSFC$ 25 / 2 x 15 mLParameter Method Approx. RangeOlefins 6550 1 - 40 Vol.%AccuPetroTest Gasoline QCOlefins QC SampleSBPT-OLEFIN$ 25 / 2 x 15 mLParameter Method Approx. RangeTotal Aromatics D-1319 8-60 Vol.%Total Olefins D-1319 1 - 40 Vol.%Total Saturates D-1319 30-80 Vol. %See ASTM Method D-1319 for Sulfur CalibrationStandardsAromatics QC SampleSBPT-AROM$ 25 / 2 x 15 mLParameter Method Approx. RangeTotal Aromatics D-5769 8 - 60 Vol.%See ASTM Methods D-3606, D-5580-95, D-5769-95for Benzene Calibration StandardsSulfur QC SampleSBPT-SGAS$ 25 / 2 x 15 mLParameter Method Approx. RangeSulfur D-2622 0.0001 - 0.0930 Wt.%Sulfur D-4294 0.0016 - 0.0930 Wt.%Sulfur D-5453 4.0 - 500 µg/gSulfur D-XXXX 1.0 - 1000 µg/gSee ASTM Methods D-2622, D-3120, D-3246-92,D-4294, D-5453 for Sulfur Calibration StandardsBenzene/Toluene QC SampleSBPT-BENZ$ 25 / 2 x 15 mLParameter Method Approx. RangeBenzene D-5769 0.1 - 2.0 Vol.%Toluene D-5769 1.0 - 15 Vol.%See ASTM Methods D-3606, D-5580-95, D-5769-95for Benzene Calibration StandardsAccuPetroTest Single BlindStandardsPetrochemical Laboratories looking totest the performance of the laboratory fora specific parameter can order the SingleBlind AccuPetroTest sample for theparameter of interest. Two real worldgasoline samples will be sent for the testparameter requested and a separate sealedenvelope containing the determinedConsensus Value is also provided. Thesecond sample is for repeatability testingor as a future QA/QC reference.AccuPetroTest GasolineComprehensive Single Blind Gasoline QCSampleSBPT-COMP$ 50 / 2 x 15 mLParameter Method Approx. Range Conc.Total Aromatics D-1319 8 - 60 Vol.%Total Olefins D-1319 1 - 40 Vol.%Total Saturates D-1319 30 - 80 Vol.%Sulfur D-2622 0.0001 - 0.0930 Wt.%Sulfur D-4294 0.0016 - 0.0930 Wt.%Sulfur D-5453 0.5 -500 µg/gSulfur D-6344 1.0 - 1000 µg/gBenzene D-5769 0.1 - 2.0 Vol.%Toluene D-5769 1.0 - 15 Vol.%Total Aromatics D-5769 8 - 60 Vol.%Benzene D-6277 0.1 - 2.0 Vol.%Total Olefins D-6550 1 - 40 Vol.%Technical NoteOur new comprehensive singleblind gasoline QC sample tests formore parameters from a singlesample. The actual gasolinesample will have consensusvalues listed on the datasheet thatfall within the range listed for eachparameter.Test toLow ppbSulfurSee Pages 6-11Conducting a Petrochemical Round Robin for a new ASTM method?Select AccuStandard to prepare the necessary samples for the Round Robinstudy.TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 41


Method 5769ASTM StandardsMemberASTMASTM Method D-5769-98Benzene, Toluene, and Total Aromatics in Finished Gasoline by GC/MSASTM D-5769Benzene, Toluene & Total Aromatics in Finished Gasoline by GC/MSAll of your standards requirements for ASTM Method D-5769 have been put together in thefollowing 10 pages. These standards and methods are used in the monitoring of TotalAromatics according to the latest methods and amendments to the US Clean Air Act.A set of Amendments, containing more stringent specifications became effective January 1,1995 limiting the volatility and composition of reformulated gasoline.The D-02 Committee of the American Society of Testing Materials, developed a standard testmethod D-5769 for the determination of the analyte composition by GC/MS of reformulatedgasoline.Originally designed forD-5769-98Aromatic Product Line yields the following important benefitsFeatures:Benefits:Purity and Identity of all analytes verified .......... Impurity interferences in analyte retention timeunder identical operating conditionswindow are compensated.Certified method specific calibration standards . Increased confidence in analytical results.Eliminates preparation of calibration standards ..Time is utilized quantifying actual samples.Internal Standards Incorporated ......................... Saves time.Weights and weight percents provided .............. Ease of use in performing back calculations.Includes all necessary solutions .........................Complete single source for reference materials.Variations in packaging size .............................. Meet laboratory sample volumes and demands.Low Cost ............................................................ More economical to purchase than to prepare standards.Flexibility ............................................................ Meet your lab requirements/method changes.Only 5 standards needed for a 5 Point Curve ... Generate a full calibration curve in 1/2 the time of thetwo set version composed of 10 standards.No charge disk deliverable calibration curve .... Direct computer uploading eliminates the input of 135weights (CALAMTS)separate data points.42TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 5769MemberASTM D-5769Benzene, Toluene & Total Aromatics in Finished Gasoline by GC/MSOriginally designed forD-5769-95Standards Designed for ASTM D-5769 as published in the 1997 Annual Book of ASTM Standards, Vol.05.03 Petroleum Products and Lubricants (III): D-4636-latest; CatalystsThe following M-GRA catalog numbers contain the necessary calibration curves, daily quality control, andinternal standards designed to meet the promulgated GC/MS Aromatic method listed in the 1997 ASTMBook of Standards.AccuStandard offers two different versions of the M-GRA catalog numbers: M-GRA three componentinternal standard version, and the M-GRA four component internal standard version.The three component internal standard version contains the necessary deuterated analytes for fullqualitative and quantitative analysis of the 25 components listed in the published version.The four component internal standard version was designed at the request of the petroleum refinerylaboratories. This four internal standard version incorporates not only the Benzene-d 6 , Ethyl benzene-d 10 ,Naphthalene-d 8 , but also Toluene-d 8 . Incorporating the Toluene-d 8 as the internal standard for thequantification of gasolines with higher Toluene levels has improved analytical results for this analyte.Incorporation of a 6th Calibration StandardA 6th calibration standard has been formulated for the M-GRA product line to improve the linearity at thehigh end of the calibration curve see page 44. This sixth standard can be especially important in thequantification of gasoline samples containing high toluene levels. The formulation contains an analyteconcentration between the high level standard and the next level, which is standard two. Use of the sixthstandard provides an additional calibration point that is desirable when the calibration curve is developedusing a quadratic fit.ASTMM-GRA-K1 $ 600(Original Formulations)Kit includes: Units FunctionM-GRA-CAL/IS-SET 5 x 1 mL 5 Pt. Curve w/ 3 ISTD'sM-GRA-QC/IS-5ML 1 x 5 mL Daily QC w/ 3 ISTD'sM-GRA-IS-5ML 1 x 5 mL Internal Std. 3 comps.M-GRA-ST 1 x 1 mL Sensitivity Test SolutionSee page 44 for product description withanalytes & conc.Aromatics Kits for analysis by GC/MSFor your added convenience we haveprovided the following Aromatics Kits tomeet the analytical requirements for thismethod.M-GRA-K2 $ 700(Developed for improved high concentration linearity)Kit includes: Units FunctionM-GRA-CAL/IS-SET 5 x 1 mL 5 Pt. Curve w/ 3 ISTD'sM-GRA-ADD/IS 1 x 1 mL 6th Std. for revison 5 FM-GRA-QC/IS-5ML 1 x 5 mL Daily QC w/ 3 ISTD'sM-GRA-IS-5ML 1 x 5 mL Internal Std. 3 comps.M-GRA-ST 1 x 1 mL Sensitivity Test SolutionSee page 44 for product description withanalytes & conc.M-GRA-K4 $ 850(Used to meet the Toluene-d 8 internal standard versionrecommended by a network of major petroleum refineries)Kit includes: Units FunctionM-GRA-CAL-R/IS-R-SET 5 x 1 mL 5 Pt. Curve w/ 4 ISTD'sM-GRA-ADD/IS-R 1 x 1 mL 6th Standard for rev. 5 FM-GRA-QC-R/IS-R-5ML 1 x 5 mL Daily QC w/ 4 ISTD'sM-GRA-IS-R-10ML 1 x 10 mL Internal Std. 4 comps.M-GRA-ST 1 x 1 mL Sensitivity Test SolutionSee page 45 for product description withanalytes & conc.Cross Reference TableASTM IP ISO DIN JIS AFNOR sorted byASTM Method see beginning of CatalogTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 43


Method 5769ASTM StandardsMemberASTMASTM D-5769Calibration Curve with 3 Component Deuterated Internal Standard AddedAromatics Calibration Standards Kit(3 Internal Standard Version)M-GRA-CAL/IS-SET$ 375 / set of 5 x 1 mLCore Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 524 Comps. Target Vol. %Vol. % Vol. % Vol. % Vol. %Benzene 3 1.50 0.75 0.375 0.1875Toluene 19 9.50 4.75 2.375 1.1875Ethylbenzene 5 2.50 1.25 0.625 0.3125m-Xylene 6 3.00 1.50 0.750 0.3750p-Xylene 6 3.00 1.50 0.750 0.3750o-Xylene 6 3.00 1.50 0.750 0.3750Isopropylbenzene 3 1.50 0.75 0.375 0.1875n-Propylbenzene 3 1.50 0.75 0.375 0.18751-Methyl-3-ethylbenzene 3 1.50 0.75 0.375 0.18751-Methyl-4-ethylbenzene 3 1.50 0.75 0.375 0.18751,3,5-Trimethylbenzene 3 1.50 0.75 0.375 0.18751-Methyl-2-ethylbenzene 3 1.50 0.75 0.375 0.18751,2,4-Trimethylbenzene 5 2.50 1.25 0.625 0.31251,2,3-Trimethylbenzene 3 1.50 0.75 0.375 0.1875Indan 3 1.50 0.75 0.375 0.18751,4-Diethylbenzene 3 1.50 0.75 0.375 0.1875n-Butylbenzene 3 1.50 0.75 0.375 0.18751,2-Diethylbenzene 3 1.50 0.75 0.375 0.18751,2,4,5-Tetramethylbenzene 2 1.00 0.50 0.250 0.12501,2,3,5-Tetramethylbenzene 2 1.00 0.50 0.250 0.1250Naphthalene 2 1.00 0.50 0.250 0.1250Pentamethylbenzene 2 1.00 0.50 0.250 0.12501-Methylnaphthalene 2 1.00 0.50 0.250 0.12502-Methylnaphthalene 2 1.00 0.50 0.250 0.1250Isooctane -- Bal Bal Bal BalInternal Standard (M-GRA-IS)Benzene-d 6 2 2 2 2 2Ethylbenzene-d 10 2 2 2 2 2Naphthalene-d 8 1 1 1 1 1Optional Sixth Standardwith 3 Comp. DeuteratedInternal Standard AddedM-GRA-ADD/IS $ 100 / 1 x 1 mLCore Calibr. Mix Optional Std. 624 Comps. Target Vol. %Benzene 2.25Toluene 15Ethylbenzene 3.75m-Xylene 4.50p-Xylene 4.50o-Xylene 4.50Isopropylbenzene 2.25n-Proplylbenzene 2.253-Ethyltoluene 2.254-Ethyltoluene 2.251,3,5-Trimethylbenzene 2.252-Ethyltoluene 2.251,2,4-Trimethylbenzene 3.751,2,3-Trimethylbenzene 2.25Indan 2.251,4-Diethylbenzene 2.25n-Butylbenzene 2.251,2-Diethylbenzene 2.251,2,4,5-Tetramethylbenzene 4.01,2,3,5-Tetramethylbenzene 1.5Naphthalene 1.5Pentamethylbenzene 1.51-Methylnaphthalene 1.52-Methylnaphthalene 1.5IsooctaneBalInternal Standard (M-GRA-IS)Benzene-d 6 2Ethylbenzene-d 10 2Naphthalene-d 8 1Originally designed forD-5769-95Disk Deliverable(At no additional charge)Eliminates hand keyed-in data.CALAMTS(Disk containing “CalibrationAmounts”)Each analyte in each standardis individually weighed. Actualweights and weight percentsare provided.Daily Quality Control Standard(without Internal Standard)M-GRA-QC-10MLM-GRA-QC-10ML-PAKWt.Compound Ration-Hexane 12n-Heptane 17n-Octane 17n-Decane 12n-Dodecane 5Isooctane 12Benzene 1$ 125 / 1 x 10 mLSAVE 20% $ 500 / 5 x 10 mLWt.CompoundRatioToluene 9Ethylbenzene 3m-Xylene 3o-Xylene 31,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 313 Comp. Core Mix 100Technical NoteUse with any M-GRA Calibration Curve.Daily Quality Control Standard(with Internal Standard)M-GRA-QC/IS-5MLM-GRA-QC/IS-5ML-PAK$ 100 / 1 x 5 mLSAVE 20% $ 400 / 5 x 5 mLWt.Wt.Compound Ratio CompoundRation-Hexane 12 Toluene 9n-Heptane 17 Ethylbenzene 3n-Octane 17 m-Xylene 3n-Decane 12 o-Xylene 3n-Dodecane 5 1,2,4-Trimethylbenzene 3Isooctane 12 1,2,4,5-Tetramethylbenzene 3Benzene 113 Comp. Core Mix 100Includes M-GRA-IS (3 Comp. Internal Standards mix)combined with the above 13 Comp. Core QC Mix:M-GRA-QC in a 5 to 100 weight ratio. 16 comps.ASTM/EPA Sensitivity Test SolutionM-GRA-ST$ 10 / 1 x 1 mLM-GRA-ST-PAKSAVE 20% $ 40 / 5 x 1 mL100 µg/mL in Isooctane1,4-Diethyl benzene3 Comp. Deuterated Internal Std. MixM-GRA-IS-5MLM-GRA-IS-5ML-PAKCompound Mix RatioBenzene-d 6 2 mLEthylbenzene-d 10 2 mL$ 150 / 1 x 5 mLSAVE 20% $ 600 / 5 x 5 mL3 comps.Compound Mix RatioNaphthalene-d 8 1 gm44TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 5769MemberASTM D-5769Calibration Curve with 4 Component Deuterated Internal Standard AddedOriginally designed forD-5769-95Aromatics Calibration Standards Kit(4 Internal Standard Version)M-GRA-CAL-R/IS-R-SET$ 425 / set of 5 x 1 mLCore Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 524 Comps. Target Wt. %Wt. % Wt. % Wt. % Wt. %Optional Sixth Standardwith 4 Comp. DeuteratedInternal Standard AddedM-GRA-ADD/IS-R $ 100 / 1 x 1 mLCore Calibr. Mix Optional Std. 624 Comps. Target Wt. %ASTMBenzene 3.13 1.78 0.95 0.490 0.2490Toluene 19.65 11.11 5.90 3.058 1.5547Ethylbenzene 5.12 2.92 1.55 0.805 0.4090m-Xylene 6.27 3.50 1.86 0.962 0.4891p-Xylene 6.33 3.50 1.86 0.962 0.4891o-Xylene 6.51 3.56 1.89 0.980 0.4981Isopropylbenzene 3.06 1.74 0.93 0.480 0.2439n-Propylbenzene 3.04 1.74 0.93 0.480 0.24403-Ethyltoluene 3.08 1.75 0.93 0.481 0.24464-Ethyltoluene 3.05 1.74 0.93 0.479 0.24371,3,5-Trimethylbenzene 3.07 1.75 0.93 0.481 0.24482-Ethyltoluene 3.14 1.78 0.95 0.490 0.24921,2,4-Trimethylbenzene 5.18 2.95 1.57 0.812 0.41301,2,3-Trimethylbenzene 3.19 1.81 0.96 0.498 0.2530Indan 3.46 1.95 1.04 0.536 0.27261,4-Diethylbenzene 3.04 1.74 0.93 0.480 0.2439n-Butylbenzene 3.05 1.74 0.92 0.479 0.24341,2-Diethylbenzene 3.22 1.78 0.95 0.490 0.24891,2,4,5-Tetramethylbenzene 2.10 1.20 0.64 0.329 0.16741,2,3,5-Tetramethylbenzene 2.09 1.20 0.64 0.330 0.1679Naphthalene 2.35 1.34 0.71 0.369 0.1877Pentamethylbenzene 2.16 1.23 0.66 0.340 0.17271-Methylnaphthalene 2.32 1.34 0.71 0.369 0.18772-Methylnaphthalene 2.41 1.37 0.73 0.378 0.1922Isooctane ----- 43.47 69.96 84.441 92.0905Benzene 2.48Toluene 16.29Ethylbenzene 4.07m-Xylene 4.87p-Xylene 4.87o-Xylene 4.96Isopropylbenzene 2.43n-Propylbenzene 2.433-Ethyltoluene 2.444-Ethyltoluene 2.431,3,5-Trimethylbenzene 2.442-Ethyltoluene 2.481,2,4-Trimethylbenzene 4.111,2,3-Trimethylbenzene 2.52Indan 2.711,4-Diethylbenzene 2.43n-Butylbenzene 2.421,2-Diethylbenzene 2.481,2,4,5-Tetramethylbenzene 4.441,2,3,5-Tetramethylbenzene 1.67Naphthalene 1.87Pentamethylbenzene 1.721-Methylnaphthalene 1.872-Methylnaphthalene 1.91Isooctane 17.67Technical NoteThis set of calibration solutionswas formulated to improvequantification for Toluene byusing Toluene-d 8as anadditional Internal Standard.Internal Standard(M-GRA-IS-R) Mix RatioBenzene-d 6 (2 mL) 16.57 16.57 16.57 16.57 16.57Ethylbenzene-d 10 (2 mL) 16.76 16.76 16.76 16.76 16.76Naphthalene-d 8 (1 gm) 8.78 8.78 8.78 8.78 8.78Toluene-d 8 (7 mL) 57.88 57.88 57.88 57.88 57.88Internal Standard(M-GRA-IS-R) Mix RatioBenzene-d 6 (2 mL) 16.57Ethylbenzene-d 10 (2 mL) 16.76Naphthalene-d 8 (1 mL) 8.78Toluene-d 8 (7 mL) 57.88The 4 component internal standard mix (M-GRA-IS-R) is combined with the 25 component core calibrationcurve mixtures in a 12 to 100 weight ratio to formulate a complete calibration solution containing 29 comps.Daily Quality Control Standard(without Internal Standard)M-GRA-QC-10ML$ 125 / 1 x 10 mLM-GRA-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mLWt.Compound Ration-Hexane 12n-Heptane 17n-Octane 17n-Decane 12n-Dodecane 5Isooctane 12Benzene 1Compound Mix RatioBenzene-d 6 2 mLEthylbenzene-d 10 2 mLWt.CompoundRatioToluene 9Ethylbenzene 3m-Xylene 3o-Xylene 31,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 313 Comp. Core Mix 1004 Comp. Deuterated Internal Std. MixM-GRA-IS-R-10ML$ 225 / 1 x 10 mLM-GRA-IS-R-10ML-PAK SAVE 20% $ 900 / 5 x 10 mL4 comps.Technical NoteCompound Mix RatioNaphthalene-d 8 1 gmToluene-d 8 7 mLUse with any M-GRA Calibration Curve.Daily Quality Control Standard(with Internal Standard M-GRA-IS-R)M-GRA-QC/IS-R-5ML$ 125 / 1 x 5 mLM-GRA-QC/IS-R-5ML-PAKSAVE 20% $ 500 / 5 x 5mLWt.Wt.Compound Ratio CompoundRation-Hexane 12 Toluene 9n-Heptane 17 Ethylbenzene 3n-Octane 17 m-Xylene 3n-Decane 12 o-Xylene 3n-Dodecane 5 1,2,4-Trimethylbenzene 3Isooctane 12 1,2,4,5-Tetramethylbenzene 3Benzene 113 Comp. Core Mix 100Includes M-GRA-IS-R (4 Comp. Internal StandardsMix) combined with the above 13 Comp. Core QC Mix:M-GRA-QC in a 12 to 100 weight ratio. 17 comps.ASTM/EPA Sensitivity Test SolutionM-GRA-STM-GRA-ST-PAK100 µg/mL in Isooctane1,4-Diethyl benzene$ 10 / 1 x 1 mLSAVE 20% $ 40 / 5 x 1 mLStandards of InterestFor the mandatory real worldQC samples stipulated in theMethod, see pages 1-2TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 45


Method 5769ASTM StandardsMemberASTM D-5769Version with No Internal StandardOriginally designed forD-5769-98ASTMThe following D-5769 and M-GRA Standards were formulated to address proposed and promulgatedchanges to ASTM Method D-5769-98 Aromatics by GC/MS. Many of these changes were evaluated and/or adopted due to the results generated from the 1997 Round Robin, which used a select group of 21gasolines ampulized by AccuStandard.AccuStandard is committed to staying abreast of ASTM committee D-02 method developments. We askthat you contact us when your analytical group finds a beneficial procedure or modification.ModificationsA Sixth Standard was added to meet the latest D-5769 method requirements and provide improvedlinearity at the high end of the Calibration curveThe Calibration Curve was packaged in two convenient sizes without the internal standard. Thispackaging scheme allows for the addition of any ISTD formulation or oxygenate components.The Quality Control Standard was reformulated in the latest D-5769 revision. The formulation changesinclude reducing the 1,2,4,5-Tetramethylbenzene weight ratio and adding Naphthalene.The Benzene Target Weight % has been increased to meet the latest D-5769 method requirements.Pentamethylbenzene has now been removed from the analyte list.Calibration Curve with No Internal Std. AddedD-5769-CAL-SET-5MLD-5769-CAL-SET-10ML$ 1500 / Set of 5 x 5 mL$ 2750 / Set of 5 x 10 mLCore Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 523 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %Benzene 5.25 2.95 1.575 0.8144 0.4143Toluene 19.67 11.06 5.898 3.0505 1.5519Ethylbenzene 5.18 2.91 1.552 0.8026 0.4083m-Xylene 6.19 3.48 1.856 0.9598 0.4883p-Xylene 6.19 3.48 1.856 0.9598 0.4883o-Xylene 6.30 3.54 1.890 0.9776 0.4973Isopropylbenzene 3.09 1.74 0.925 0.4786 0.2435n-Propylbenzene 3.09 1.74 0.926 0.4787 0.24353-Ethyltoluene 3.10 1.74 0.928 0.4801 0.24424-Ethyltoluene 3.08 1.73 0.925 0.4782 0.24331,3,5-Trimethylbenzene 3.10 1.74 0.929 0.4804 0.24442-Ethyltoluene 3.15 1.77 0.945 0.4890 0.24881,2,4-Trimethylbenzene 5.23 2.94 1.567 0.8104 0.41231,2,3-Trimethylbenzene 3.20 1.80 0.960 0.4965 0.2526Indan 3.45 1.94 1.034 0.5350 0.27221,4-Diethylbenzene 3.09 1.74 0.925 0.4786 0.2435n-Butylbenzene 3.08 1.73 0.923 0.4776 0.24301,2-Diethylbenzene 3.15 1.77 0.945 0.4885 0.24851,2,4,5-Tetramethylbenzene 2.12 1.19 0.635 0.3284 0.16711,2,3,5-Tetramethylbenzene 2.12 1.19 0.637 0.3295 0.1676Naphthalene 2.37 1.34 0.712 0.3683 0.18741-Methylnaphthalene 2.37 1.34 0.712 0.3683 0.18742-Methylnaphthalene 2.43 1.37 0.730 0.3773 0.1919Isooctane ----- 43.77 70.015 84.4922 92.1105Optional Sixth StandardD-5769-ADD-5MLD-5769-ADD-10ML$ 150 / 1 x 5 mL$ 300 / 1 x 10 mLCore Calibration Mix Target23 Comps. Wt. %Benzene 4.16Toluene 16.41Ethylbenzene 4.10m-Xylene 4.91p-Xylene 4.91o-Xylene 5.00Isopropylbenzene 2.45n-Propylbenzene 2.453-Ethyltoluene 2.454-Ethyltoluene 2.441,3,5-Trimethylbenzene 2.462-Ethyltoluene 2.501,2,4-Trimethylbenzene 4.141,2,3-Trimethylbenzene 2.54Indan 2.731,4-Diethylbenzene 2.45n-Butylbenzene 2.441,2-Diethylbenzene 2.501,2,4,5-Tetramethylbenzene 1.681,2,3,5-Tetramethylbenzene 1.68Naphthalene 1.881-Methylnaphthalene 1.882-Methylnaphthalene 1.93Isooctane 19.92Disk Deliverable(At no additional charge)Eliminates hand keyed-in data.CALAMTS ®(Disk containing “CalibrationAmounts”)Each analyte in each standardis individually weighed. Actualweights and weight percentsare provided.4 Comp. Deuterated Internal Std. MixM-GRA-IS-R-10ML$ 225 / 1 x 10 mLM-GRA-IS-R-10ML-PAK SAVE 20% $ 900 / 5 x 10 mL4 comps.MixCompound RatioBenzene-d 6 2 mLEthylbenzene-d 10 2 mLCompoundBenzene-d 6Ethylbenzene-d 10Naphthalene-d 8CompoundNaphthalene-d 8Toluene-d 8MixRatio1 gm7 mL3 Comp. Deuterated Internal Std. MixM-GRA-IS-5MLM-GRA-IS-5ML-PAK$ 150 / 1 x 5 mLSAVE 20% $ 600 / 5 x 5 mL3 comps.Mix Ratio2 mL2 mL1 gmDaily Quality Control Standard(without Internal Standard)D-5769-QC-10MLD-5769-QC-10ML-PAKWt.Compound Ration-Hexane 12n-Heptane 17n-Octane 17n-Decane 12n-Dodecane 5Isooctane 12Benzene 1$ 125 / 1 x 10 mLSAVE 20% $ 500 / 5 x 10 mLWt.CompoundRatioToluene 9Ethylbenzene 3m-Xylene 3o-Xylene 31,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 2Naphthalene 114 Comp. Core Mix 10046TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 5769MemberASTM D-5769Version with 3 Internal StandardsCalibration Curve with a 3 Comp. DeuteratedInternal Standard addedD-5769-CAL/IS-SET $ 375 / 5 x 1 mLCore Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 524 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %Benzene 5.25 2.95 1.575 0.8144 0.4143Toluene 19.67 11.06 5.898 3.0505 1.5519Ethylbenzene 5.18 2.91 1.552 0.8026 0.4083m-Xylene 6.19 3.48 1.856 0.9598 0.4883p-Xylene 6.19 3.48 1.856 0.9598 0.4883o-Xylene 6.30 3.54 1.890 0.9776 0.4973Isopropylbenzene 3.09 1.74 0.925 0.4786 0.2435n-Propylbenzene 3.09 1.74 0.926 0.4787 0.24353-Ethyltoluene 3.10 1.74 0.928 0.4801 0.24424-Ethyltoluene 3.08 1.73 0.925 0.4782 0.24331,3,5-Trimethylbenzene 3.10 1.74 0.929 0.4804 0.24442-Ethyltoluene 3.15 1.77 0.945 0.4890 0.24881,2,4-Trimethylbenzene 5.23 2.94 1.567 0.8104 0.41231,2,3-Trimethylbenzene 3.20 1.80 0.960 0.4965 0.2526Indan 3.45 1.94 1.034 0.5350 0.27221,4-Diethylbenzene 3.09 1.74 0.925 0.4786 0.2435n-Butylbenzene 3.08 1.73 0.923 0.4776 0.24301,2-Diethylbenzene 3.15 1.77 0.945 0.4885 0.24851,2,4,5-Tetramethylbenzene 2.12 1.19 0.635 0.3284 0.16711,2,3,5-Tetramethylbenzene 2.12 1.19 0.637 0.3295 0.1676Naphthalene 2.37 1.34 0.712 0.3683 0.18741-Methylnaphthalene 2.37 1.34 0.712 0.3683 0.18742-Methylnaphthalene 2.43 1.37 0.730 0.3773 0.1919Isooctane ----- 43.77 70.015 84.4922 92.1105Optional Sixth Standardwith a 3 Comp. DeuteratedInternal Standard addedD-5769-ADD/IS $ 100 / 1 x 1 mLCore Calibration Mix Target24 Comps. Wt. %Benzene 4.16Toluene 16.41Ethylbenzene 4.10m-Xylene 4.91p-Xylene 4.91o-Xylene 5.00Isopropylbenzene 2.45n-Propylbenzene 2.453-Ethyltoluene 2.454-Ethyltoluene 2.441,3,5-Trimethylbenzene 2.462-Ethyltoluene 2.501,2,4-Trimethylbenzene 4.141,2,3-Trimethylbenzene 2.54Indan 2.731,4-Diethylbenzene 2.45n-Butylbenzene 2.441,2-Diethylbenzene 2.501,2,4,5-Tetramethylbenzene 1.681,2,3,5-Tetramethylbenzene 1.68Naphthalene 1.881-Methylnaphthalene 1.882-Methylnaphthalene 1.93Isooctane 19.92Originally designed forD-5769-98Test toLow ppbSulfurSee Pages 6-11ASTMInternal StandardM-GRA-ISCompoundBenzene-d 6Ethylbenzene-d 10Naphthalene-d 8Mix ratio2 mL2 mL1 gmThe 3 Comp. Internal Standard Mix (M-GRA-IS) iscombined with the 24 Comp. Core Calibration Curve Mixesabove in a 5 to 100 weight ratio to formulate these27 Comp. calibration solutions.Daily Quality Control Standard(with Internal Standard)D-5769-QC/IS-5ML$ 100 / 1 x 5 mLD-5769-QC/IS-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL17 comps.Wt.Wt.Compound Ratio CompoundRation-Hexane 12 Toluene 9n-Heptane 17 Ethylbenzene 3n-Octane 17 m-Xylene 3n-Decane 12 o-Xylene 3n-Dodecane 5 1,2,4-Trimethylbenzene 3Isooctane 12 1,2,4,5-Tetramethylbenzene 2Benzene 1 Naphthalene 1Includes M-GRA-IS (3 component mix)added in 5 to 100 weight ratio1003 Comp. Deuterated Internal Std. MixM-GRA-IS-5ML$ 150 / 1 x 5 mLM-GRA-IS-5ML-PAK SAVE 20% $ 600 / 5 x 5 mL3 comps.CompoundMix RatioBenzene-d 62 mLEthylbenzene-d 102 mLNaphthalene-d 81 gmSensitivity Test SolutionM-GRA-ST$ 10 / 1 x 1 mLM-GRA-ST-PAK SAVE 20% $ 40 / 5 x 1 mL100 µg/mL in Isooctane1,4-Diethyl benzeneResolution StandardM-GRA-RESM-GRA-RES-PAKWt. %1,3,5-Trimethylbenzene 3.01-Methyl-2-ethylbenzene 3.0Isooctane 94$ 30 / 1 x 1 mL$ 120 / 5 x 1 mL3 comps.Fragmentation Pattern StandardM-GRA-FP$ 20 / 1 x 1 mLM-GRA-FP-PAK SAVE 20% $ 80 / 5 x 1 mL3.0% w/w in Isooctane1,2,3-TrimethylbenzeneMass Scan Range StandardM-GRA-MSR$ 20 / 1 x 1 mLM-GRA-MSR-PAK SAVE 20% $ 80 / 5 x 1 mL3.0% w/w in IsooctaneTolueneTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 47


Method 5769ASTM StandardsMemberASTMASTM D-5769 4 Internal Standard Version (includes Toluene-d 8)Calibration Curve with a 4 Comp. DeuteratedInternal Standard addedD-5769-CAL/IS-R-SET$ 425 / 5 x 1 mLCore Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 524 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %Optional Sixth Standardwith a 4 Comp. DeuteratedInternal Standard addedD-5769-ADD/IS-R $ 100 / 1 x 1 mLCore Calibration Mix Target24 Comp. Wt. %Originally designed forD-5769-98Benzene 5.25 2.95 1.575 0.8144 0.4143Toluene 19.67 11.06 5.898 3.0505 1.5519Ethylbenzene 5.18 2.91 1.552 0.8026 0.4083m-Xylene 6.19 3.48 1.856 0.9598 0.4883p-Xylene 6.19 3.48 1.856 0.9598 0.4883o-Xylene 6.30 3.54 1.890 0.9776 0.4973Isopropylbenzene 3.09 1.74 0.925 0.4786 0.2435n-Propylbenzene 3.09 1.74 0.926 0.4787 0.24353-Ethyltoluene 3.10 1.74 0.928 0.4801 0.24424-Ethyltoluene 3.08 1.73 0.925 0.4782 0.24331,3,5-Trimethylbenzene 3.10 1.74 0.929 0.4804 0.24442-Ethyltoluene 3.15 1.77 0.945 0.4890 0.24881,2,4-Trimethylbenzene 5.23 2.94 1.567 0.8104 0.41231,2,3-Trimethylbenzene 3.20 1.80 0.960 0.4965 0.2526Indan 3.45 1.94 1.034 0.5350 0.27221,4-Diethylbenzene 3.09 1.74 0.925 0.4786 0.2435n-Butylbenzene 3.08 1.73 0.923 0.4776 0.24301,2-Diethylbenzene 3.15 1.77 0.945 0.4885 0.24851,2,4,5-Tetramethylbenzene 2.12 1.19 0.635 0.3284 0.16711,2,3,5-Tetramethylbenzene 2.12 1.19 0.637 0.3295 0.1676Naphthalene 2.37 1.34 0.712 0.3683 0.18741-Methylnaphthalene 2.37 1.34 0.712 0.3683 0.18742-Methylnaphthalene 2.43 1.37 0.730 0.3773 0.1919Isooctane ----- 43.77 70.015 84.4922 92.1105Benzene 4.16Toluene 16.41Ethylbenzene 4.10m-Xylene 4.91p-Xylene 4.91o-Xylene 5.00Isopropylbenzene 2.45n-Propylbenzene 2.453-Ethyltoluene 2.454-Ethyltoluene 2.441,3,5-Trimethylbenzene 2.462-Ethyltoluene 2.501,2,4-Trimethylbenzene 4.141,2,3-Trimethylbenzene 2.54Indan 2.731,4-Diethylbenzene 2.45n-Butylbenzene 2.441,2-Diethylbenzene 2.501,2,4,5-Tetramethylbenzene 1.681,2,3,5-Tetramethylbenzene 1.68Naphthalene 1.881-Methylnaphthalene 1.882-Methylnaphthalene 1.93Isooctane 19.92Internal StandardM-GRA-IS-RCompound Mix ratioBenzene-d 6 2 mLEthylbenzene-d 10 2 mLNaphthalene-d 8 1 gmToluene-d 8 7 mLThe 4 Comp. Internal Standard Mix (M-GRA-IS-R) iscombined with the 24 component core calibrationcurve mixtures above in a 12 to 100 weight ratio toformulate these 28 component calibration solutions.Daily Quality Control Standard(with Internal Standard)D-5769-QC/IS-R-5ML$ 100 / 1 x 5 mLD-5769-QC/IS-R-5ML-PAK SAVE 20% $ 400/5 x 5 mL18 comps.Wt.Compound Ration-Hexane 12n-Heptane 17n-Octane 17n-Decane 12n-Dodecane 5Isooctane 12Benzene 1Compound Mix RatioBenzene-d 6 2 mLEthylbenzene-d 10 2 mLWt.CompoundRatioToluene 9Ethylbenzene 3m-Xylene 3o-Xylene 31,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 2Naphthalene 1Includes M-GRA-IS-R (4 component mix)added in 12 to 100 weight ratio4 Comp. Deuterated Internal Std. Mix100M-GRA-IS-R-10ML$ 225 / 1 x 10 mLM-GRA-IS-R-10ML-PAK SAVE 20% $ 900/ 5 x 10 mLCompound Mix RatioNaphthalene-d 8 1 gmToluene-d 8 7 mLSensitivity Test SolutionM-GRA-STM-GRA-ST-PAK100 µg/mL in Isooctane1,4-Diethyl benzeneResolution StandardM-GRA-RESM-GRA-RES-PAKCompound Wt. %1,3,5-Trimethylbenzene 3.01-Methyl-2-ethylbenzene 3.0Isooctane 94$ 30 / 1 x 1 mLSAVE 20% $ 120 / 5 x 1 mL3 comps.Fragmentation Pattern StandardM-GRA-FPM-GRA-FP-PAK3.0 w/w in Isooctane1,2,3-Trimethylbenzene$ 10 / 1 x 1 mLSAVE 20% $ 40 / 5 x 1 mL$ 20 / 1 x 1 mLSAVE 20% $ 80 / 5 x 1 mL48TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 5769MemberASTM D-5769New Proposed / Promulgated Method ModificationsCalibration Curve with a 3 Comp. ChlorinatedInternal Standard addedD-5769-CAL/IS-R2-SET$ 375 / 5 x 1 mLCore Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 524 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %Benzene 5.25 2.95 1.575 0.8144 0.4143Toluene 19.67 11.06 5.898 3.0505 1.5519Ethylbenzene 5.18 2.91 1.552 0.8026 0.4083m-Xylene 6.19 3.48 1.856 0.9598 0.4883p-Xylene 6.19 3.48 1.856 0.9598 0.4883o-Xylene 6.30 3.54 1.890 0.9776 0.4973Isopropylbenzene 3.09 1.74 0.925 0.4786 0.2435n-Propylbenzene 3.09 1.74 0.926 0.4787 0.24353-Ethyltoluene 3.10 1.74 0.928 0.4801 0.24424-Ethyltoluene 3.08 1.73 0.925 0.4782 0.24331,3,5-Trimethylbenzene 3.10 1.74 0.929 0.4804 0.24442-Ethyltoluene 3.15 1.77 0.945 0.4890 0.24881,2,4-Trimethylbenzene 5.23 2.94 1.567 0.8104 0.41231,2,3-Trimethylbenzene 3.20 1.80 0.960 0.4965 0.2526Indan 3.45 1.94 1.034 0.5350 0.27221,4-Diethylbenzene 3.09 1.74 0.925 0.4786 0.2435n-Butylbenzene 3.08 1.73 0.923 0.4776 0.24301,2-Diethylbenzene 3.15 1.77 0.945 0.4885 0.24851,2,4,5-Tetramethylbenzene 2.12 1.19 0.635 0.3284 0.16711,2,3,5-Tetramethylbenzene 2.12 1.19 0.637 0.3295 0.1676Naphthalene 2.37 1.34 0.712 0.3683 0.18741-Methylnaphthalene 2.37 1.34 0.712 0.3683 0.18742-Methylnaphthalene 2.43 1.37 0.730 0.3773 0.1919Isooctane ----- 43.77 70.015 84.4922 92.1105Internal StandardM-GRA-IS-R2CompoundMix ratioChlorobenzene2 mL1,2-Dichlorobenzene 2 mL1,2,4-Trichlorobenzene 1 mLOptional Sixth Standard witha 3 Comp. ChlorinatedInternal Standard addedD-5769-ADD/IS-R2 $ 100 / 1 x 1 mLCore Calibration Mix Target24 Component Wt.%Benzene 4.16Toluene 16.41Ethylbenzene 4.10m-Xylene 4.91p-Xylene 4.91o-Xylene 5.00Isopropylbenzene 2.45n-Propylbenzene 2.453-Ethyltoluene 2.454-Ethyltoluene 2.441,3,5-Trimethylbenzene 2.462-Ethyltoluene 2.501,2,4-Trimethylbenzene 4.141,2,3-Trimethylbenzene 2.54Indan 2.731,4-Diethylbenzene 2.45n-Butylbenzene 2.441,2-Diethylbenzene 2.501,2,4,5-Tetramethylbenzene 1.681,2,3,5-Tetramethylbenzene 1.68Naphthalene 1.881-Methylnaphthalene 1.882-Methylnaphthalene 1.93Isooctane 19.92The 3 Comp. Internal Standard Mix (M-GRA-IS-R2)is combined with the 24 Comp. Core CalibrationCurve mixtures above in a 5 to 100 weight ratio toformulate these 27 Comp. calibration solutions.Originally designed forD-5769-98Disk Deliverable(At no additional charge)Eliminates hand keyed-in data.CALAMTS ®(Disk containing “CalibrationAmounts”)Each analyte in each standardis individually weighed. Actualweights and weight percentsare provided.ASTMDaily Quality Control Standard(with Internal Standard)D-5769-QC/IS-R2-5ML$ 100 / 1 x 5 mLD-5769-QC/IS-R2-5ML-PAK SAVE 20% $400/5 x 5 mL17 comps.Wt.Wt.Compound Ratio CompoundRation-Hexane 12 Toluene 9n-Heptane 17 Ethylbenzene 3n-Octane 17 m-Xylene 3n-Decane 12 o-Xylene 3n-Dodecane 5 1,2,4-Trimethylbenzene 3Isooctane 12 1,2,4,5-Tetramethylbenzene 2Benzene 1 Naphthalene 1Sensitivity Test SolutionM-GRA-ST$ 10 / 1 x 1 mLM-GRA-ST-PAK SAVE 20% $ 40 / 5 x 1 mL100 µg/mL in Isooctane1,4-Diethyl benzeneFragmentation Pattern StandardM-GRA-FP$ 20 / 1 x 1 mLM-GRA-FP-PAK SAVE 20% $ 80 / 5 x 1 mL3.0 w/w in Isooctane1,2,3-TrimethylbenzeneStandards of InterestFor the mandatory real worldQC samples stipulated in theMethod, see pages 1-2Includes M-GRA-IS-R2 (3 component mix)added in 5 to 100 weight ratio1003 Comp. Chlorinated Internal Std. MixM-GRA-IS-R2-SETM-GRA-IS-R2-25MLCompoundChlorobenzene1,2-Dichlorobenzene1,2,4-Trichlorobenzene$125 / set of 25 x 1 mL$ 100 / 1 x 25 mL3 comps.Mix Ratio2 mL2 mL1 mLResolution StandardM-GRA-RESM-GRA-RES-PAKCompound Wt. %1,3,5-Trimethylbenzene 3.01-Methyl-2-ethylbenzene 3.0Isooctane 94$ 30 / 1 x 1 mLSAVE 20% $ 120 / 5 x 1 mL3 comps.TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 49


Method 5769ASTM StandardsMemberASTM D-5769Special QA/QC FormulationsOriginally designed forD-5769-98ASTMDaily Quality Control Standard(without Internal Standard)M-GRA-QC-R-10ML$ 125 / 1 x 10 mLM-GRA-QC-R-10ML-PAK SAVE 20% $ 500 / 5 x 10 mLWt.Compound Ration-Hexane 12n-Heptane 17n-Octane 17n-Decane 12n-Dodecane 5Isooctane 12Benzene 1Toluene 9Wt.CompoundRatioEthylbenzene 3m-Xylene 3o-Xylene 31,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 1Pentamethylbenzene 11-Methylnaphthalene 115 Comp. Core Mix 100Technical NoteSpecially formulated Daily Quality ControlStandards originally designed in response toclient requests for QC mixes that bracket thecurve and contain more C9+ analytes to verifythe instrument and QC solution integrity.Save 20-40%Buy AccuPAKsFor use with any M-GRACalibration CurveDaily Quality Control Standard(with Internal Standard M-GRA-IS)M-GRA-QC-R/IS-5ML$ 100 / 1 x 5 mLM-GRA-QC-R/IS-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL18 comps.Wt.Wt.Compound Ratio CompoundRation-Hexane 12 Ethylbenzene 3n-Heptane 17 m-Xylene 3n-Octane 17 o-Xylene 3n-Decane 12 1,2,4-Trimethylbenzene 3n-Dodecane 5 1,2,4,5-Tetramethylbenzene 1Isooctane 12 Pentamethylbenzene 1Benzene 1 1-Methylnaphthalene 1Toluene 9Includes M-GRA-IS (3 Comp. Internal StandardsMix) combined with the above 15 Comp. Core QCMix: M-GRA-QC-R in a 5 to 100 weight ratio100Daily Quality Control Standard(with Internal Std. M-GRA-IS-R)M-GRA-QC-R/IS-R-5ML$ 125 / 1 x 5 mLM-GRA-QC-R/IS-R-5ML-PAK SAVE $ 500 / 5 x 5 mL19 comps.Wt.Wt.Compound Ratio CompoundRation-Hexane 12 Ethylbenzene 3n-Heptane 17 m-Xylene 3n-Octane 17 o-Xylene 3n-Decane 12 1,2,4-Trimethylbenzene 3n-Dodecane 5 1,2,4,5-Tetramethylbenzene 1Isooctane 12 Pentamethylbenzene 1Benzene 1 1-Methylnaphthalene 1Toluene 9100Includes M-GRA-IS-R (4 Comp. InternalStandards mix) combined with the above 15 Comp.Core QC Mix: M-GRA-QC-R in a 12 to 100 Wt. ratioAccuPAK ®Reduce reordering frequencyReduce data entry time forCalibration tables due toLot No. consistencyEconomical3 Comp. Deuterated Internal Std. MixM-GRA-IS-5ML$ 150 / 1 x 5 mLM-GRA-IS-5ML-PAK SAVE 20% $ 600 / 5 x 5 mL3 comps.Compound Mix RatioBenzene-d 62 mLEthylbenzene-d 10 2 mLNaphthalene-d 8 1 gm4 Comp. Deuterated Internal Std. MixM-GRA-IS-R-10ML$ 225 / 1 x 10 mLM-GRA-IS-R-10ML-PAK SAVE 20% $ 900 / 5 x 10 mL4 comps.Compound Mix RatioBenzene-d 62 mLEthylbenzene-d 10 2 mLNaphthalene-d 8 1 gmToluene-d 87 mLCustom Ampulling for Bulk Quantity RequirementsFill Volumes from 0.2 mL to 20 mL• FlammablesQC Services availableAccuStandard has the resources and equipment to meet your custom packagingrequirements. Our full automated filler-sealer can accommodate a fill range from0.5 to 20 mL, and ampule sizes from 1 mL to 20 mL.AccuStandard has extensive experience with Round Robin samples for ASTMcommittees.Call our Technical Department for a quotation.50TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 5769MemberThrough a collaborative effort involving the instrument manufactures, Petrochemical end users, and Chemical Reference Standard manufacturers,the following proposed D-5769 method is under consideration. A number of end users would like to evaluate this proposed D-5769 method andhave asked AccuStandard to make the standards. We have formulated the following certified standards to meet those requests.Summary Proposed Modifications for D-5769• Calibration standards when combined with internal standards are diluted into significantly more isooctane.• The analytes in the Performance Standard have been expanded to better tune the GC/MS system for optimum performance.• The number of components in the QA/QC mix has been reduced with new QA/QC tolerances.• The number of analytes in the calibration mix has been reduced.• Samples that exceed the linear range are to be diluted, reducing the number of extra calibration points required.ASTMASTM D-5769-XXASTM-P-0140-SETCalibration Curve with No Internal Standard Added$ 1500 / Set of 5 x 5 mLASTM-P-0140-05ASTM-P-0140-04ASTM-P-0140-03ASTM-P-0140-02ASTM-P-0140-01Core Calibr. Mix Level 1 Level 2 Level 3 Level 4 Level 5Compound Target Mass % Mass % Mass % Mass % Mass %Benzene 5 3 1 0.5 0.1Toluene 12 9 6 3 0.5Ethylbenzene 5 3.75 2.5 1.25 0.21,3-Dimethylbenzene 10 7.5 5 2.5 0.21,4-Dimethylbenezene 5 3.75 2.5 1.25 0.21,2-Dimethylbenezene 5 3.75 2.5 1.25 0.2(1-Methylethyl)-benzene 3 2.25 1.5 0.75 0.21-Methyl-3-ethylbenzene 3 2.25 1.5 0.75 0.21-Methyl-4-ethylbenzene 3 2.25 1.5 0.75 0.21,3,5-Trimethylbenzene 3 2.25 1.5 0.75 0.21-Methyl-2-ethylbenzene 3 2.25 1.5 0.75 0.21,2,4-Trimethylbenzene 6 4.5 3 1.5 0.21,2,3-Trimethylbenzene 3 2.25 1.5 0.75 0.2Indan 3 2.25 1.5 0.75 0.21,2-Diethylbenzene 2 1.5 1 0.5 0.2Naphthalene A 2 1.5 1 0.5 0.12-Methylnaphthalene A 2 1.5 1 0.5 0.11-Methylnaphthalene A 2 1.5 1 0.5 0.1Isooctane (solvent) * balance balance balance balance balance4 Comp. Deuterated Internal Std. MixASTM-P-0140-ISASTM-P-0140-IS-PAKCompound Mass %Benzene-d 6 2Ethylbenzene-d 10 2$ 75 / 1 x 10 mL$ 300 / 5 x 10 mL4 comps.Compound Mass %Naphthalene-d 8 1Isooctane * balance4 Comp. Deuterated Internal Std. MixASTM-P-0140-IS2ASTM-P-0140-IS2-PAKCompound Mass %Benzene-d 6 2Ethylbenzene-d 10 2A = This component is a solid at roomtemperature$ 95 / 1 x 10 mL$ 380 / 5 x 10 mL5 comps.Compound Mass %Naphthalene-d 8 1Toluene-d 8 7Isooctane * balanceTechnical Note* The isooctane balance is theamount of material to make upa 100 mL calibration standard.Certificate will reflect actualweight of each component inthe 100 mL batch including theisooctane.Performance Evalutation StandardASTM-P-0140-PESASTM-P-0140-PES-PAKTargetCompound Mass %Benzene 11,2-Diethylbenzene 0.0051,3,5-Trimethylbenzene 11-Methyl-2-ethylbenzene 1Styrene 0.1Indene 0.1Biphenyl 0.11,2,4,5-Tetramethylbenzene 11,2,3,5-Tetramethylbenzene 1Hexadecane 1Isooctane:Toluene(1:1) * balance$ 55 / 1 x 1 mL$ 220 / 5 x 1 mL11 comps.Composition of Daily QC StandardASTM-P-0140-QC$ 125 / 1 x 10 mLASTM-P-0140-QC-PAK$ 500 / 5 x 10 mL9 comps.TargetCompound Mass %Benzene 1Toluene 10Ethylbenzene 31,3-Dimethylbenzene 61,2-Dimethylbenzene 31,2,4-Trimethylbenzene 31,2-Diethylbenzene 0.02Naphthalene 1Isooctane (solvent) * balanceTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 51


Method 577157725773Member 5863ASTM StandardsASTM D-5771Cloud Point of Petroleum ProductsSee page 5 for AccuStandard’s comprehensive line of certified Cloud Point Standards.ASTMASTM D-5772Cloud Point of Petroleum Products (Linear Cooling Rate Method)See page 5 for AccuStandard’s comprehensive line of certified Cloud Point Standards.ASTM D-5773Cloud Point of Petroleum Products (Constant Cooling Rate Method)See page 5 for AccuStandard’s comprehensive line of certified Cloud Point Standards.WEAR METALSASTM D-5863µg/mLIron 100Nickel 200Nickel, Vanadium, Iron, & Sodium in Crude Oils & Residual Fuels byFlame AA SpectrometryTest Method A - Sample Decomposition with Acid for Total Ni, V and FeDeterminationStock Multi-ElementAqueous StandardD-5863-95A-10X-1$ 75 / 1 x 100 mL2-5% HNO 3 3 comps.µg/mLVanadium 200Matrix BlankNitric Acid BlankCLP-BLN-5CLP-BLN-LIndividual High Concentration Elements in Aqueous Matrix1,000 µg/mL Conc.Element Matrix Unit Cat. No. PriceIron Fe 500 mL ICP-27N-5 $ 67in HNO 3Nickel Ni 500 mL ICP-37N-5 67in HNO 3Vanadium V 2 O 5 500 mL ICP-67N-5 67in HNO 35% HNO 3 in ASTM Type I Water$ 30 / 500 mLSAVE 33% $ 45 / L (2 x 500 mL)Originally designed forD-5863-00Standards of InterestSee page 73-75 for additionalTrace Metal Standards by AA.Test Method B - Sample Dilution with Organic Solvent for the Determination of Ni, Vand Na using Oil-Soluble Metals as Calibrants.Stock Multi-Element Standard in MineralOilD-5863-95B-10XAt stated conc. in 20 cst Mineral Oilµg/gSodium 50Nickel 200$ 160 / 1 x 4 oz3 comps.µg/gVanadium 150Standards of InterestSee pages 59-65 for AccuStandard’scomprehensive line of Certified Oil DissolvedWear Metal calibration standards designed forflame AA Applications.52TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 5901 -5986MemberASTM D-5901Freezing Point Aviation Fuels (Automated Optical Method)See page 5 for AccuStandard’s comprehensive line of Certified Freezing Point Standards.Standards of InterestAlso see Cloud Pointstandards used for ASTMMethod D-2500 on page 5.ASTM D-5972Freezing Point Aviation Fuels (Automated Phase Transition Method)ASTMSee page 5 for AccuStandard’s comprehensive line of Certified Freezing Point Standards.ASTM D-5986Daily Quality Control Standard(without Internal Standard)Wt.Compound Ration-Hexane 12n-Heptane 17n-Octane 17n-Decane 12n-Dodecane 5Isooctane 12Benzene 1Oxygenates, Benzene, Toluene, C 8 -C 12 , Aromatics & Total Aromatics in Finished Gasolines by GC/FTIRM-GRA-QC-10ML$ 125 / 1 x 10 mLM-GRA-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mLWt.CompoundRatioToluene 9Ethylbenzene 3m-Xylene 3o-Xylene 31,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 313 Comp. Core Mix 100Technical NoteAccuStandard formulated this quality controlstandard to meet Section 11 of ASTM D-5986-96specifications stipulating to “analyze the qualitycontrol reference material before every batch ofsamples. Bracket the samples with the referencematerials”.Oxygenate QC samples are available on pages 1-2 or can be custom formulated.Originally designed forD-5986-96Standards of InterestSee page 34 for OxygenateCalibration Curve (Cat. No.M-GRO-CAL-SET) and page 46for AccuStandard’s AromaticCalibration Curve (Cat. No.D-5769-CAL-SET-5ML).Cross Reference TableASTM IP ISO DIN JIS AFNOR sorted byASTM Method see beginning of CatalogTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 53


Method 616062586277ASTM StandardsMemberASTMASTM D-6160Polychlorinated Biphenyls (PCBs in Waste Materials by GC)Aroclor Solutions (Individual and Kit)SAVE 20%in PAK(35 µg/mL in (35 µg/mL in (35 µg/mL inIsooctane) MeOH) Hexane) 1 x 1 mL 5 x 1 mLAroclor # Cat. No. Cat. No. Cat. No. Price Cat. No. PriceAroclor 1016 C-216S C-216S-M C-216S-H-10X $ 15 Cat. #-PAK $ 60Aroclor 1221 C-221S C-221S-M C-221S-H-10X 15 Cat. #-PAK 60Aroclor 1232 C-232S C-232S-M C-232S-H-10X 15 Cat. #-PAK 60Aroclor 1242 C-242S C-242S-M C-242S-H-10X 15 Cat. #-PAK 60Aroclor 1248 C-248S C-248S-M C-248S-H-10X 15 Cat. #-PAK 60Aroclor 1254 C-254S C-254S-M C-254S-H-10X 15 Cat. #-PAK 60Aroclor 1260 C-260S C-260S-M C-260S-H-10X 15 Cat. #-PAK 60Aroclor 1262 C-262S C-262S-M C-262S-H-10X 15 Cat. #-PAK 60Aroclor 1268 C-268S C-268S-M C-268S-H-10X 15 Cat. #-PAK 60Kit of all 9 above Z-008S Z-008S-M Z-008S-H-10X $ 78 / 9 x 1 mLOriginally designed forD-6160-98Additional Ready-to-Inject PCBAroclor CalibrationCurves available in our OrganicCatalogASTM D-6258Stock Solvent Red 26 StandardD-6258-CONC-5MLSolvent Red 164 Dye Concentration in Diesel Fuels$ 45 / 1 x 5 mLOriginally designed forD-6258-98Solvent Red 26 @ 300 µg/mL in XyleneD-6258 Calibration CurveD-6258-CAL-SET-5ML$ 125 / set of 6 x 5 mLSet includes the following Cat. No.’sCat. No. Description UnitD-6258-BL Xylene Blank 1 x 5 mLD-6258-01 Solvent Red 26 Dye @ 3 µg/mL in Xylene 1 x 5 mLD-6258-02 Solvent Red 26 Dye @ 6 µg/mL in Xylene 1 x 5 mLD-6258-03 Solvent Red 26 Dye @ 9 µg/mL in Xylene 1 x 5 mLD-6258-04 Solvent Red 26 Dye @ 12 µg/mL in Xylene 1 x 5 mLD-6258-05 Solvent Red 26 Dye @ 15 µg/mL in Xylene 1 x 5 mLASTM D-6277Benzene in Spark - Ignition Engine Fuels using Mid Infrared SpectroscopySee page 1 for AccuStandard’s QA/QC material reference in the method.Technical NoteSolvent Red 26 is the azo dyestandard against which theconcentration of Solvent Red164 is measured. The visiblespectrum of Solvent Red 164 isvirtually identical to thespectrum of Solvent Red 26.MemberAccuStandard is an active member in ASTM andstrives to keep abreast of ASTM method revisions. Ifour listed formulation does not meet the most recentmethod revision, please contact Technical Support,ext. 117 for an updated product.54TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 62936296MemberASTM D-6293Oxygenates & Paraffin, Olefin, Naphthene, Aromatics (O-PONA) Hydrocarbontypes in Low-Olefin Spark-Ignition Engine Fuels by GCO-PONA System Validation MixtureASTM-P-0080ASTM-P-0080-PAKWt./Wt. %Cyclopentane 1.5n-Pentane 1.5Cyclohexane 2.02,3-Dimethylbutane 2.0n-Hexane 2.01-Hexene 1.5Methylcyclohexane 3.54-Methyl-1-hexene 1.5n-Heptane 3.0cis-1,2-Dimethylcyclohexane 4.5Isooctane 4.0n-Octane 4.01,2,4-Trimethylcyclohexane 3.5n-Nonane 3.0n-Decane 3.5n-Undecane 2.0n-Dodecane 2.0$ 135 / 1 x 1 mLSAVE 26% $ 500 / 5 x 1 mL33 comps.Wt./Wt. %Benzene 2.5Toluene 2.5trans-Decahydronaphthelene 3.5n-Tetradecane 2.0Ethylbenzene 3.5o-Xylene 3.0n-Propylbenzene 3.51,2,4-Trimethylbenzene 3.01,2,3-Trimethylbenzene 2.01,2,4,5-Tetramethylbenzene 2.0Pentamethylbenzene 2.5Ethanol 5.0t-Butanol 4.0MtBE 8.0ETBE 3.0TAME 5.0O-PONA Olefin MixASTM-P-0081 $ 45 / 1 x 1 mLASTM-P-0081-PAK $ 180 / 5 x 1 mLAt stated conc. in Hexane : Heptane (1:1)5 comps.Wt./Wt. %1-Pentene 5.01-Hexene 2.01-Heptene 2.01-Octene 2.01-Nonene 3.0O-PONA Paraffin MixASTM-P-0082 $ 25 / 1 x 1 mLASTM-P-0082-PAK $ 100 / 5 x 1 mLAt stated conc. in Hexane : Heptane (1:1)2 comps.Wt./Wt. %n-Nonane 5.0n-Decane 2.0Originally designed forD-6293-98ASTMStandards of InterestFor the mandatory real worldQC samples stipulated inQA/QC section 8.6 of themethod see pages 1-2.O-PONA Paraffin MixASTM-P-0082-R1 $ 25 / 1 x 1 mLASTM-P-0082-R1-PAK $ 100 / 5 x 1 mLAt stated conc. in Hexane : Heptane (1:1)2 comps.Wt./Wt. %n-Nonane 3.0n-Decane 3.0ASTM D-6296Total Olefins in Spark-Ignition Engine Fuels by Multidimensional GCSystem Setup & Verification StandardsD-6296-VER-SET$ 40 / 2 x 1 mLSet contains 1 ampule of each Cat. No. listed belowD-6296-VER-SET-PAK SAVE 23% $ 150 / 5 x (2 x 1 mL)5 sets containing 1 ampule of each Cat. No. listed belowOriginally designed forD-6296-98System Setup & Verification StandardsD-6296-VER1Wt. %MTBE 5%Isooctane 95%1 x 1 mL2 comps.System Setup & Verification StandardsD-6296-VER2Wt. %ETBE 5%Isooctane 95%1 x 1 mL2 comps.Calibration Standard with MTBED-6296-CAL1D-6296-CAL1-PAKWt. %Pentene 1.0Hexene 1.0Heptene 1.0Octene 1.0Nonene 1.0$ 65 / 1 x 1 mLSAVE 23% $ 250 / 5 x 1 mL10 comps.Wt. %Decene 1.0Undecane 1.0Dodecane 1.0Isooctane 87.0MTBE 5.0Calibration Standard with ETBED-6296-CAL2D-6296-CAL2-PAKWt. %Pentene 1.0Hexene 1.0Heptene 1.0Octene 1.0Nonene 1.0Decene 1.0$ 65 / 1 x 1 mLSAVE 23% $ 250 / 5 x 1 mL11 comps.Wt. %Decane 1.0Undecane 1.0Dodecane 1.0Isooctane 86.0ETBE 5.0Isooctane Blank Compensation StandardD-6296-BL$ 15 / 1 x 5 mLIsooctane (Neat)TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 55


Method 630463346352ASTM StandardsMemberASTM D-6304Determination of Water in Petroleum Products Lubricating oil, andadditives by Coulometric Karl Fischer TitrationASTMSee page 5 for AccuStandard’s comprehensive line of Certified Water Standards, forKarl Fischer Analysis.ASTM D-6334Sulfur in Gasoline by Wavelength Dispersive X-Ray FluorescenceSee Sulfur Standards Group listing in the Table of Contents for AccuStandard’s comprehensiveline of Certified Sulfur Calibration Standards.ASTM D-6352Polywax 500 ®ASTM-P-0051N-2GPolywax 500Polywax 655 ®ASTM-P-0053N-2GPolywax 655Boiling Range Distribution of Petroleum Distillates from 174 to 700ºC by GC$ 20 / 2 grams$ 20 / 2 gramsPolywax 850 ®ASTM-P-0137N-2GPolywax 850Polywax 1000 ®ASTM-P-0138N-2GPolywax 1000$ 20 / 2 grams$ 20 / 2 gramsOriginally designed forD-6352-98Standards of InterestContact AccuStandard’sTechnical Department regardingthe availability of a QA/QCReference Oil Sample underdevelopment in ASTM.Hydrocarbon WindowDefining Standard*DRH-008S-R2$ 65 / 1 x 1 mLDRH-008S-R2-PAK SAVE 20% $ 260 / 5 x 1 mL500 µg/mL each in Chloroform 35 comps.OctaneNonaneDecaneUndecaneDodecaneTridecaneTetradecanePentadecaneHexadecaneHeptadecaneOctadecanePristaneNonadecanePhytaneEicosaneHeneicosaneDocosaneTricosaneTetracosanePentacosaneHexacosaneHeptacosaneOctacosaneNonacosaneTriacontanen-HentriacontaneDotriacontaneTritriacontaneTetratriacontanePentatriacontaneHexatriacontaneHeptatriacontaneOctatriacontaneNonatriacontaneTetracontane* Can be shipped by Air and SeaCalibration MixDRH-002NDRH-002N-10XWt. %n-Hexane 6n-Heptane 6n-Octane 8n-Nonane 8n-Decane 12n-Undecane 12n-Dodecane 12n-Tetradecane 12n-Hexadecane 10Column Test Mixture$ 10 / 100 mg$ 40 / 1 gm17 comps.Wt. %n-Octadecane 5n-Eicosane 2n-Tetracosane 2n-Octacosane 1n-Dotriacontane 1n-Hexatriacontane 1n-Tetracontane 1n-Tetratetracontane 1ASTM-D2887$ 10 / 1 x 1 mL1% v/v in n-Octane 2 comps.n-Hexadecanen-OctadecaneASTM D-6378Vapor Pressure (VPx) of Petroleum Products, Hydrocarbons, &Hydrocarbon-Oxygenate Mixtures (Triple Expansion Method)See pages 29 & 32 for AccuStandard’s comprehensive line of Vapor Pressure Standards &Instrument Quality Control Samples.56TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM StandardsMethod 6379IP 3916417Member 6428ASTM D-6379 Aromatic Hydrocarbon Types in Aviation Fuels & Petroleum Distillates -HPLC method with Refractive IndexOriginally designed forD-6379-99System Resolution StandardD-6379-SRS$ 40 / 1 x 1 mLD-6379-SRS-PAK SAVE 30% $ 140 / 5 x 1 mLAt stated Conc. in n-Heptane 3 comps.D-6379 Calibration CurveD-6379-SET$ 100 / 4 x 1 mLD-6379-SET-PAK SAVE 30% $ 350 / 5 x (4 x 1 mL)At stated Conc. in n-HeptaneASTMCyclohexaneo-Xylene1-Methyl naphthalene10 mg/mL0.5 mg/mL0.05 mg/mLAnalyte Std. 1 Std. 2 Std. 3 Std. 4(mg/mL) (mg/mL) (mg/mL) (mg/mL)Cyclohexane 5 2 0.5 0.1o-Xylene 15 5 1.0 0.11-Methyl naphthalene 5 1.0 0.2 0.05D-6591 Aromatic Hydrocarbon Types in Middle Distillates -IP 391 HPLC method with Refractive Index DetectionSystem Performance StandardASTM-P-0135$ 75 / 1 x 5 mLASTM-P-0135-PAK SAVE 20% $ 300 / 5 x 5 mLAt stated Conc. in n-Heptane 4 comps.Cyclohexaneo-XyleneDibenzothiophene9-Methylanthracene10 mg/mL5.0 mg/mL0.5 mg/mL0.5 mg/mLIP 391-95 Calibration CurveASTM-P-0136-SETAt stated Conc. in n-Heptane$ 145 / 4 x 1 mLAnalyte Std. 1 Std. 2 Std. 3 Std. 4(mg/mL) (mg/mL) (mg/mL) (mg/mL)Cyclohexane 50 20 5 1o-Xylene 40 10 2.5 0.51-Methyl naphthalene 40 10 2.5 0.2Phenanthrene 4 2 0.5 0.1ASTM D-6417 Estimation of Engine Oil Volatility by Capillary GCSee page 15 for Alkane and Polywax standards suitable for D-6417.ASTM D-6428 Sulfur by Combustion and Electrochemical DetectionNEWStandards of InterestSee ASTM Methods D-3710,D-5307, D-5442, D-6352 foradditional calibration standardsfor hydrocarbon analysis.D-6428-R1-4-SETD-6428-R1-SETSulfur as Dibenzothiophene$ 300 / 7 x 4 oz$ 65 / 7 x 1 mLD-6428-R1-4-SETD-6428-R1-SETDescription Cat. No. Unit Cat. No. UnitSulfur Blank D-6428-BL-4 4 oz D-6428-BL 1 mLSulfur @ 0.1 µg/g D-6428-0.1X-4 4 oz D-6428-0.1X 1 mLSulfur @ 0.5 µg/g D-6428-0.5X-4 4 oz D-6428-0.5X 1 mLSulfur @ 1.0 µg/g D-6428-1X-4 4 oz D-6428-1X 1 mLSulfur @ 2.5 µg/g D-6428-2.5X-4 4 oz D-6428-2.5X 1 mLSulfur @ 5.0 µg/g D-6428-5X-4 4 oz D-6428-5X 1 mLSulfur @ 10 µg/g D-6428-10X-4 4 oz D-6428-10X 1 mLD-6428-R2-4-SETD-6428-R2-SETSulfur as Dibenzothiophene$ 275 / 6 x 4 oz$ 65 / 6 x 1 mLD-6428-R2-4-SETD-6428-R2-SETDescription Cat. No. Unit Cat. No. UnitSulfur Blank D-6428-BL-4 4 oz D-6428-BL 1 mLSulfur @ 10 µg/g D-6428-10X-4 4 oz D-6428-10X 1 mLSulfur @ 25 µg/g D-6428-25X-4 4 oz D-6428-25X 1 mLSulfur @ 50 µg/g D-6428-50X-4 4 oz D-6428-50X 1 mLSulfur @ 75 µg/g D-6428-75X-4 4 oz D-6428-75X 1 mLSulfur @ 100 µg/g D-6428-100X-4 4 oz D-6428-100X 1 mLTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 57


Method 644364816550ASTM StandardsMemberASTMASTM D-6443Ca, Cl, Cu, Mg, P, S, Zn in Unused Lubricating Oils & Additives byWavelength Dispersive X-ray Fluorescence & SpectrometryLubricating Oil, Elements, WLXRF ASTM Method (Nominal Value) Wt.% listed belowASTM-P-0117-SET$ 2100 / 10 x 100 mLCa Cl Cu Mg P S ZnCat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0117-01 0.020 0.030 0.010 0.200 0.250 1.000 0.020ASTM-P-0117-02 0.020 0.020 0.050 0.200 0.020 0.020 0.250ASTM-P-0117-03 0.020 0.200 0.010 0.040 0.250 0.150 0.250ASTM-P-0117-04 0.020 0.200 0.050 0.040 0.020 1.000 0.020ASTM-P-0117-05 0.400 0.020 0.010 0.040 0.020 1.000 0.250ASTM-P-0117-06 0.400 0.020 0.050 0.040 0.250 0.020 0.020ASTM-P-0117-07 0.400 0.200 0.010 0.200 0.020 0.020 0.050ASTM-P-0117-08 0.400 0.200 0.050 0.200 0.250 1.000 0.250ASTM-P-0117-09 0.200 0.100 0.025 0.080 0.150 0.500 0.100ASTM-P-0117-10 0.000 0.000 0.000 0.000 0.000 0.000 0.000Originally designed forD-6443-99Standards of InterestSee the Wear Metal Grouplisting in the Table of Contentsfor a comprehensive line ofCertified Oil Dissolved WearMetal Calibration Standards.WEAR METALSASTM D-6445ASTM D-6481Sulfur in Gasoline by ED - XRFSee the Sulfur Standards Group listing in the Table of Contents for AccuStandard’scomprehensive line of Certified Sulfur Calibration Standards.P, S, Ca and Zn in Lube Oils by ED-XRFLubricating Oil, Elements, EDXRF ASTM Method(Nominal Value) Wt.% listed belowASTM-P-0114-SET$ 1900 / 17 x 100 mLCa P S ZnCat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0114-01 0.005 0.005 0.050 0.050ASTM-P-0114-02 0.600 0.000 0.000 0.000ASTM-P-0114-03 0.000 0.300 0.000 0.000ASTM-P-0114-04 1.000 0.000 1.000 0.000ASTM-P-0114-05 0.000 0.000 0.000 0.300ASTM-P-0114-06 0.005 0.250 0.800 0.300ASTM-P-0114-07 0.500 0.150 0.500 0.150ASTM-P-0114-08 0.010 0.200 0.100 0.250ASTM-P-0114-09 0.050 0.010 0.400 0.075ASTM-P-0114-10 0.100 0.150 0.200 0.200ASTM-P-0114-11 0.200 0.200 0.800 0.100ASTM-P-0114-12 0.400 0.005 0.800 0.300ASTM-P-0114-13 0.600 0.100 0.500 0.050ASTM-P-0114-14 0.800 0.010 0.050 0.100ASTM-P-0114-15 1.000 0.300 1.000 0.150ASTM-P-0114-16 0.400 0.050 0.600 0.250ASTM-P-0114-17 0.000 0.000 0.000 0.000Originally designed forD-6481-99ASTM D-6550Wt. %1-Nonene 2.5Cyclohexene 51-Hexene 51-Octene 51-Decene 52-Methyl-1,3-butadiene 54-Methyl-1-pentene 51,5-Hexadiene 3Olefin Content of Gasolines by SFCStock Olefin Calibration StandardD-6550-CONCD-6550-CONC-5MLAt stated Conc. by Wt. %$ 80 / 1 x 1 mL$ 350 / 1 x 5 mL15 comps.Wt. %3-Methyl-1,3-pentadiene 22-Methyl-1-butene 252-Methyl-2-pentene 101-Heptene 102-Methyl-1-octene 2.52-Methyl-1-heptene 55-Methyl-1-hexene 10Originally designed forD-6550-00Technical NoteAccuStandard worked inconjunction with the D-02technical committee and ShellOil to develop this stock OlefinStandard proven useful increating the required calibrationcurve.Standards of InterestSee page 2 for consensusvalue QA/QC material availablefor this method.58TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM-FUEL-QCS-01-PAK:40ASTM-FUEL-QCS-02-PAK:40ASTM-P-0051N-2G:56ASTM-P-0053N-2G:56ASTM-P-0061-SET:37ASTM-P-0062-SET:37ASTM-P-0063-SET:37ASTM-P-0064-SET:37ASTM-P-0065-SET:37ASTM-P-0066-SET:37ASTM-P-0067-SET:37ASTM-P-0068-SET:37ASTM-P-0069-SET:37ASTM-P-0070-10X:40ASTM-P-0070-1X:40ASTM-P-0070-20X:40ASTM-P-0070-2X:40ASTM-P-0070-4X:40ASTM-P-0070-BL:40ASTM-P-0070-SET:40ASTM-P-0071-01:40ASTM-P-0071-02:40ASTM-P-0071-03:40ASTM-P-0071-BL:40ASTM-P-0071-SET:40ASTM-P-0080:55ASTM-P-0080-PAK:55ASTM-P-0081:55ASTM-P-0081-PAK:55ASTM-P-0082:55ASTM-P-0082-PAK:55ASTM-P-0082-R1:55ASTM-P-0082-R1-PAK:55ASTM-P-0091-01-10X:38ASTM-P-0091-02-10X:38ASTM-P-0091-03-10X:38ASTM-P-0091-04-10X:38ASTM-P-0091-05-10X:38ASTM-P-0091-06-10X:38ASTM-P-0091-07-10X:38ASTM-P-0091-08-10X:38ASTM-P-0091-09-10X:38ASTM-P-0091-10-10X:38ASTM-P-0091-10X-SET:38ASTM-P-0091-11-10X:38ASTM-P-0091-12-10X:38ASTM-P-0091-13-10X:38ASTM-P-0091-14-10X:38ASTM-P-0091-15-10X:38ASTM-P-0091-16-10X:38ASTM-P-0091-17-10X:38ASTM-P-0091-18-10X:38ASTM-P-0091-19-10X:38ASTM-P-0091-20-10X:38ASTM-P-0091-21-10X:38ASTM-P-0091-22-10X:38ASTM-P-0102-SET:39ASTM-P-0103-01:39ASTM-P-0103-02:39ASTM-P-0103-03:39ASTM-P-0103-04:39ASTM-P-0103-05:39ASTM-P-0103-06:39ASTM-P-0103-07:39ASTM-P-0103-08:39ASTM-P-0103-09:39ASTM-P-0103-10:39ASTM-P-0103-11:39ASTM-P-0103-12:39ASTM-P-0103-SET:39ASTM-P-0114-01:58ASTM-P-0114-02:58ASTM-P-0114-03:58ASTM-P-0114-04:58ASTM-P-0114-05:58ASTM-P-0114-06:58ASTM-P-0114-07:58ASTM-P-0114-08:58ASTM-P-0114-09:58ASTM-P-0114-10:58ASTM-P-0114-11:58ASTM-P-0114-12:58ASTM-P-0114-13:58ASTM-P-0114-14:58ASTM-P-0114-15:58ASTM-P-0114-16:58ASTM-P-0114-17:58ASTM-P-0114-SET:58ASTM-P-0117-01:58ASTM-P-0117-02:58ASTM-P-0117-03:58ASTM-P-0117-04:58ASTM-P-0117-05:58ASTM-P-0117-06:58ASTM-P-0117-07:58ASTM-P-0117-08:58ASTM-P-0117-09:58ASTM-P-0117-10:58ASTM-P-0117-SET:58ASTM-P-0135:57ASTM-P-0135-PAK:57ASTM-P-0136-SET:57ASTM-P-0137N-2G:56ASTM-P-0138N-2G:56ASTM-P-0140-01:51ASTM-P-0140-02:51ASTM-P-0140-03:51ASTM-P-0140-04:51ASTM-P-0140-05:51ASTM-P-0140-IS:51ASTM-P-0140-IS-PAK:51ASTM-P-0140-IS2:51ASTM-P-0140-IS2-PAK:51ASTM-P-0140-PES:51ASTM-P-0140-PES-PAK:51ASTM-P-0140-QC:51ASTM-P-0140-QC-PAK:51ASTM-P-124-01:32ASTM-P-124-02:32ASTM-P-124-03:32ASTM-P-124-04:32ASTM-P-124-05:32ASTM-P-124-06:32C-216S:54C-216S-H-10X:54C-216S-M:54C-221S:54C-221S-H-10X:54C-221S-M:54C-232S:54C-232S-H-10X:54C-232S-M:54C-242S:54C-242S-H-10X:54C-242S-M:54C-248S:54


Petrochemical StandardsCertified Petroleum Reference Materials (CPRM)ASTM Methods for Organometallics, Aromatics, Olefins, Saturates, Sulfur, Nitrogen &Oxygenates in Refinery ProductsTable of ContentspageWear Metals 46-52Organometallic Wear Metals Single and Multi-Element 46Organometallic Single Element Concentrates & Stock Solutions Sulfur Free 47Stabilization Solutions 47, 52Wear Metals Multi-Element Sulfur Free 48Sulfur & Metals in Oil 49ISO / CD 14597 Vanadium & Nickel in Oil 49Lubricating Oil Standards 50-52Metal Working Fluids 52Looking for a methodnumber you can’t find in theIndex or Table of Contents?There are more on ourWebsite.Petrochemical & ASTMSulfur Standards 53-55Sulfur in Mineral Oil 53Sulfur in Diesel Fuel 53Sulfur in Kerosene, Refinery Oils & Aromatics 54Sulfur in Isooctane for Gasoline Analysis (D-2622, D-4294, D-3120, D-3246) 55Petroleum QC Standards 56ASTM MethodsD-3230 Salts in Crude Oil 57D-3231 Phosphorus in Gasoline 57For our complete line of standards forover 100 ASTM Methods, request ourPetroleum catalog.D-3237 Lead in Gasoline 57D-3605 Trace Metals in Gas Turbine Fuels 57D-3610 Cobalt Oxide Standard 57D-3831 Manganese in Gasoline 57D-4628 Barium, Calcium, Magnesium & Zinc in unused Lubricating Oil 57D-4629 Nitrogen in Petroleum Hydrocarbons 58D-4927 Wear Metals in Lubricating Oil 59D-4929 Organic Chlorides in Crude Oil 59D-4951 Additive Elements in Lubricating Oil 59D-5056 Trace Metals in Petroleum Coke 59D-5059 Lead in Gasoline 60D-5184 Aluminum & Silicon in Fuel Oils 60D-5185 Additive Elements, Wear Metals & Contaminants in used Lubricating Oils 60D-5453 Sulfur in Light Hydrocarbons, Motor Fuels & Oils 61D-5600 Trace Metals in Petroleum Coke 61D-5708 Nickel, Vanadium & Iron in Crude Oils & Residual Fuels 62D-5762 Nitrogen in Petroleum & Petroleum Products 63D-5863 Nickel, Vanadium, Iron & Sodium in Crude Oils & Residual Fuels 63MEMBERTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 45


Traceable Organometallic Standards forAA, ICP, DCP & XRF AnalysisThese Standards were formulated for the analysis of metals in oils and other organic matrices. These Standards and curves provide a convenientway to analyze for metals (wear metals, additives and contaminants) in lubricating oils, gasolines, residual oils, crude oils, turbine fuels andenvironmental samples. All standards undergo rigorous quality assurance checks. Major constituents in the final Standard are typically analyzed byboth plasma emission and rotrode techniques. Organometallic Standards listed on this page may contain sulfur which can be introduced by possiblesulfonate starting materials used to formulate the actual organometallic standard. We developed a Premium Organometallic line for preferring tohave organometallic standards with


Organometallic StandardsPremium Sulfur-FreeThese highly concentrated stabilized solutions can be used for customer specific formulations of additive elements in lubricating oils, iron, nickel andvanadium in residual oil, and wear metals in oils. These organometallic solutions can also be used to prepare single element or multi-elementstandards for plasma emission (ICP or DCP), rotating disk (rotrode), or atomic absorption spectroscopy (AA). The starting materials are PUREREAGENTS and have been certified against NIST SRM’s whenever available. THEY DO NOT CONTAIN PHOSPHORUS OR SULFUR.Highly Concentrated Liquid Organometallic StandardsStabilizedOrganometallic Single Element ConcentratesSulfur/Phosphorous free (< 1 ppm)Ready for UseElement Conc. (Wt. %) Cat. No. (25 grams) Price Cat. No. (50 grams) PriceAluminum 3 WM-NMS-01-30X-25G $ 150 WM-NMS-01-30X-50G $ 210Antimony NEW 2 WM-NMS-02-20X-25G 120 WM-NMS-02-20X-50G 165Barium 12.5 WM-NMS-04-125X-25G 540 WM-NMS-04-125X-50G 780Boron 2.5 WM-NMS-07-25X-25G 130 WM-NMS-07-25X-50G 180Cadmium 10 WM-NMS-08-100X-25G 510 WM-NMS-08-100X-50G 710Calcium 5 WM-NMS-09-50X-25G 250 WM-NMS-09-50X-50G 355Cerium NEW 5 WM-NMS-11-50X-25G 250 WM-NMS-11-50X-50G 350Chromium 3.5 WM-NMS-13-35X-25G 175 WM-NMS-13-35X-50G 265Cobalt 7.5 WM-NMS-14-75X-25G 330 WM-NMS-14-75X-50G 450Copper 6 WM-NMS-15-60X-25G 250 WM-NMS-15-60X-50G 355Iron 4 WM-NMS-27-40X-25G 220 WM-NMS-27-40X-50G 300Lead 20 WM-NMS-29-200X-25G 900 WM-NMS-29-200X-50G 1260Lithium NEW 1.5 WM-NMS-30-15X-25G 155 WM-NMS-30-15X-50G 215Magnesium 3 WM-NMS-32-30X-25G 180 WM-NMS-32-30X-50G 252Manganese 6 WM-NMS-33-60X-25G 280 WM-NMS-33-60X-50G 450Molybdenum 5 WM-NMS-35-50X-25G 215 WM-NMS-35-50X-50G 294Nickel 5 WM-NMS-37-50X-25G 250 WM-NMS-37-50X-50G 350Phosphorus 5 WM-NMS-41-50X-25G 250 WM-NMS-41-50X-50G 350Potassium NEW 7.5 WM-NMS-43-75X-25G 330 WM-NMS-43-75X-50G 450Praseodymium 3 WM-NMS-44-30X-25G 175 WM-NMS-44-30X-50G 240Selenium 3.5 WM-NMS-51-35X-25G 200 WM-NMS-51-35X-50G 270Silicon NEW 7.5 WM-NMS-52-75X-25G 330 WM-NMS-52-75X-50G 450Sodium NEW 2.5 WM-NMS-54-25X-25G 180 WM-NMS-54-25X-50G 252Strontium 10 WM-NMS-55-100X-25G 510 WM-NMS-55-100X-50G 710Thallium 5 WM-NMS-60-50X-25G 265 WM-NMS-60-50X-50G 360Tin NEW 7.5 WM-NMS-63-75X-25G 330 WM-NMS-63-75X-50G 450Titanium 5 WM-NMS-64-50X-25G 215 WM-NMS-64-50X-50G 295Vanadium 4 WM-NMS-67-40X-25G 210 WM-NMS-67-40X-50G 325Yttrium NEW 2.5 WM-NMS-69-25X-25G 180 WM-NMS-69-25X-50G 252Zinc 6 WM-NMS-70-60X-25G 270 WM-NMS-70-60X-50G 380Zirconium 5 WM-NMS-71-50X-25G 250 WM-NMS-71-50X-50G 355These products do not requireHazardous Shipping charges at thistime.PremiumSulfur-FreeSulfur belowdetection limitsStabilization SolutionsThe solutions were specificallydesigned for chelating & solubilizingour line of Sulfur-Free OrganometallicStandards. Contact Tech Service foradditional information.Stabilizer Solution AASTM-P-0122-0.5ASTM-P-0122-1Stabilizer Solution BASTM-P-0123-0.5ASTM-P-0123-1$ 80 / 50 mL$ 120 / 100 mL$ 80 / 50 mL$ 120 / 100 mLOrganometallicOrganometallic Single Element Stock StandardsSulfur free @ 1000 µg/g Price @ 5000 µg/g PriceElement Cat. No. 50 mL Cat. No. 50 mLAluminum WM-NMS-01 $ 50 WM-NMS-01-5X $ 90Antimony WM-NMS-02 50 WM-NMS-02-5X 90Arsenic NEW WM-NMS-03 50 WM-NMS-03-5X 90Barium WM-NMS-04 50 WM-NMS-04-5X 90Beryllium NEW WM-NMS-05 75 WM-NMS-05-5X 110Cadmium WM-NMS-08 50 WM-NMS-08-5X 90Calcium WM-NMS-09 50 WM-NMS-09-5X 90Chromium WM-NMS-13 50 WM-NMS-13-5X 90Cobalt WM-NMS-14 50 WM-NMS-14-5X 90Copper WM-NMS-15 50 WM-NMS-15-5X 90Gallium NEW WM-NMS-20 75 WM-NMS-20-5X 110Gold NEW WM-NMS-22 120 ---------- ----Iron WM-NMS-27 50 WM-NMS-27-5X 90Lead WM-NMS-29 50 WM-NMS-29-5X 90Lithium NEW WM-NMS-30 75 WM-NMS-30-5X 110Magnesium WM-NMS-32 50 WM-NMS-32-5X 90Manganese WM-NMS-33 50 WM-NMS-33-5X 90Mercury NEW WM-NMS-34 75 WM-NMS-34-5X 110Molybdenum WM-NMS-35 50 WM-NMS-35-5X 90Nickel WM-NMS-37 50 WM-NMS-37-5X 90Phosphorous WM-NMS-41 50 WM-NMS-41-5X 90Potassium WM-NMS-43 50 WM-NMS-43-5X 90Selenium WM-NMS-51 60 WM-NMS-51-5X 100Silicon WM-NMS-52 75 WM-NMS-52-5X 110Silver NEW WM-NMS-53 75 WM-NMS-53-5X 110Sodium WM-NMS-54 50 WM-NMS-54-5X 90Strontium WM-NMS-55 50 WM-NMS-55-5X 90Thallium WM-NMS-60 60 WM-NMS-60-5X 100Tin NEW WM-NMS-63 50 WM-NMS-63-5X 90Titanium WM-NMS-64 50 WM-NMS-64-5X 90Vanadium WM-NMS-67 50 WM-NMS-67-5X 90Yttrium WM-NMS-68 60 WM-NMS-68-5X 100Zinc WM-NMS-70 50 WM-NMS-70-5X 90Zirconium WM-NMS-71 50 WM-NMS-71-5X 90Stabilizer Solution CASTM-P-0124-0.5ASTM-P-0124-1Stabilizer Solution DASTM-P-0125-0.5ASTM-P-0125-1ContainsNo Metallic SulfonatesTechnical Note$ 80 / 50 mL$ 120 / 100 mL$ 80 / 50 mL$ 120 / 100 mLThese standards are sulfur free(below detection limits)organometallic standards for X-rayFluorescence (XRF), plasmaemission (ICP or DCP), rotatingdisk (rotrode), or atomicabsorption (AA). They arestabilized for blending togetherwith other Analytes to preparemulti-element standards.TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 47


Organometallic StandardsNo Metallic Sulfonates11 Wear Metal Multi-ElementWear Metals Multi-Element12 Wear Metal Multi-ElementContainsNo Metallic SulfonatesOrganometallicConc.(µg/g) Unit Cat. No. Price10 100 mL WM-11-NMS-1X-1 $ 13030 100 mL WM-11-NMS-3X-1 13050 100 mL WM-11-NMS-5X-1 130100 100 mL WM-11-NMS-10X-1 140300 100 mL WM-11-NMS-30X-1 165500 100 mL WM-11-NMS-50X-1 245900 100 mL WM-11-NMS-90X-1 325Al (Aluminum)Cr (Chromium)Cu (Copper)Fe (Iron)Mg (Magnesium)Na (Sodium)WM-11-NMS-1-SET $ 1100set of above 7 x 100 mLEach Wear Metal Standard contains 11 elements inhydrocarbon oil at the stated concentration.Ni (Nickel)Pb (Lead)Si (Silicon)Sn (Tin)Ti (Titanium)Conc.(µg/g) Unit Cat. No. Price10 100 mL WM-12-NMS-1X-1 $ 13530 100 mL WM-12-NMS-3X-1 13550 100 mL WM-12-NMS-5X-1 135100 100 mL WM-12-NMS-10X-1 145300 100 mL WM-12-NMS-30X-1 170500 100 mL WM-12-NMS-50X-1 250Each Wear Metal Standard contains 12 elements inhydrocarbon oil at the stated concentration.Ag (Silver)Al (Aluminum)Cr (Chromium)Cu (Copper)Fe (Iron)Mg (Magnesium)WM-12-NMS-1-SET $ 850set of above 6 x 100 mLNa (Sodium)Ni (Nickel)Pb (Lead)Si (Silicon)Sn (Tin)Ti (Titanium)PremiumSulfur-FreeSulfur belowdetection limits20 Wear Metal Multi-Element 21 Wear Metal Multi-ElementConc.(µg/g) Unit Cat. No. Price10 100 mL WM-20-NMS-1X-1 $ 15030 100 mL WM-20-NMS-3X-1 15050 100 mL WM-20-NMS-5X-1 150100 100 mL WM-20-NMS-10X-1 170300 100 mL WM-20-NMS-30X-1 230500 100 mL WM-20-NMS-50X-1 350900 100 mL WM-20-NMS-90X-1 500Each Wear Metal Standard contains 20 elements inhydrocarbon oil at the stated concentration.Al (Aluminum)B (Boron)Ba (Barium)Ca (Calcium)Cd (Cadmium)Cr (Chromium)Cu (Copper)Fe (Iron)Mg (Magnesium)Mn (Manganese)WM-20-NMS-1-SET $ 1450set of above 7 x 100 mLMo (Molybdenum)Na (Sodium)Ni (Nickel)P (Phosphorus)Pb (Lead)Si (Silicon)Sn (Tin)Ti (Titanium)V (Vanadium)Zn (Zinc)Conc.(µg/g) Unit Cat. No. Price10 100 mL WM-21-NMS-1X-1 $ 16030 100 mL WM-21-NMS-3X-1 16050 100 mL WM-21-NMS-5X-1 160100 100 mL WM-21-NMS-10X-1 180300 100 mL WM-21-NMS-30X-1 240500 100 mL WM-21-NMS-50X-1 350Each Wear Metal Standard contains 21 elements inhydrocarbon oil at the stated concentration.Ag (Silver)Al (Aluminum)B (Boron)Ba (Barium)Ca (Calcium)Cd (Cadmium)Cr (Chromium)Cu (Copper)Fe (Iron)Mg (Magnesium)Mn (Manganese)WM-21-NMS-1-SET $ 1050set of above 6 x 100 mLMo (Molybdenum)Na (Sodium)Ni (Nickel)P (Phosphorus)Pb (Lead)Si (Silicon)Sn (Tin)Ti (Titanium)V (Vanadium)Zn (Zinc)e-Standards Just a click awayThese products do not require Hazardous Shippingcharges at this time.AccuStandard.comThis is the easier way to getChemical Reference Standards48TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Traceable Organometallic Standards forAA, ICP, DCP & XRF AnalysisSulfur and Metals in Mineral OilASTM-P-0100-SET$ 1650 / 12 x 100 mLSulfur Nickel Vanadium 100 mLCat. No. (Wt. %) (µg/g) (µg/g) PriceASTM-P-0100-01 0.00 0 0 $ 200ASTM-P-0100-02 0.50 10 500 200ASTM-P-0100-03 1.00 100 25 200ASTM-P-0100-04 1.50 80 250 200ASTM-P-0100-05 2.00 40 100 200ASTM-P-0100-06 2.50 5 400 200ASTM-P-0100-07 3.00 60 300 200ASTM-P-0100-08 3.50 0 200 200ASTM-P-0100-09 4.00 100 0 200ASTM-P-0100-10 4.50 50 250 200ASTM-P-0100-11 5.00 20 500 200ASTM-P-0100-12 5.50 100 50 200Sulfur and Metals in OilSulfur and Metals in Residual Fuel OilASTM-P-0101-SET$ 1800 / 12 x 100 mLSulfur Nickel Vanadium 100 mLCat. No. (Wt. %) (µg/g) (µg/g) PriceASTM-P-0101-01 0.00 0 0 $ 200ASTM-P-0101-02 0.50 10 500 200ASTM-P-0101-03 1.00 100 25 200ASTM-P-0101-04 1.50 80 250 200ASTM-P-0101-05 2.00 40 100 200ASTM-P-0101-06 2.50 5 400 200ASTM-P-0101-07 3.00 60 300 200ASTM-P-0101-08 3.50 0 200 200ASTM-P-0101-09 4.00 100 0 200ASTM-P-0101-10 4.50 50 250 200ASTM-P-0101-11 5.00 20 500 200ASTM-P-0101-12 5.50 100 50 200OrganometallicSulfur and Metals in Mineral OilDesigned for ASTM D-5708-95aASTM-P-0102-SET $ 1850 / 12 x 100 mLSulfur Iron Nickel Vanadium 100 mLCat. No. (Wt. %) (µg/g) (µg/g) (µg/g) PriceASTM-P-0102-01 0.00 0 0 0 $ 200ASTM-P-0102-02 0.50 300 10 500 200ASTM-P-0102-03 1.00 500 100 25 200ASTM-P-0102-04 ----- 100 80 250 200ASTM-P-0102-05 2.00 200 40 100 200ASTM-P-0102-06 2.50 400 5 400 200ASTM-P-0102-07 3.00 0 60 300 200ASTM-P-0102-08 3.50 500 0 200 200ASTM-P-0102-09 ----- 100 100 0 200ASTM-P-0102-10 4.50 300 50 250 200ASTM-P-0102-11 5.00 200 20 500 200ASTM-P-0102-12 5.50 50 100 50 200Sulfur and Metals in Residual Fuel OilASTM-P-0103-SET$ 2100 / 12 x 100 mLSulfur Iron Nickel Vanadium 100 mLCat. No. (Wt. %) (µg/g) (µg/g) (µg/g) PriceASTM-P-0103-01 0.00 0 0 0 $ 200ASTM-P-0103-02 0.50 300 10 500 200ASTM-P-0103-03 1.00 500 100 25 200ASTM-P-0103-04 ----- 100 80 250 200ASTM-P-0103-05 2.00 200 40 100 200ASTM-P-0103-06 2.50 400 5 400 200ASTM-P-0103-07 3.00 0 60 300 200ASTM-P-0103-08 3.50 500 0 200 200ASTM-P-0103-09 ----- 100 100 0 200ASTM-P-0103-10 4.50 300 50 250 200ASTM-P-0103-11 5.00 200 20 500 200ASTM-P-0103-12 5.50 50 100 50 200ISO/CD 14597 Vanadium and Nickel Standards with Manganese (Internal Standard)Designed for ASTMD-5708-95aVanadium Standards - Low Range for ISO/CD14597 with 0.05% Manganese Internal Standardin Xylene-Mineral OilASTM-P-0104-SET $ 1050 / 9 x 100 mLVanadium PriceCat. No. Conc. (Wt.%) 100 mLASTM-P-0104-01 0.0005 $ 150ASTM-P-0104-02 0.0025 150ASTM-P-0104-03 0.0050 150ASTM-P-0104-04 0.0075 150ASTM-P-0104-05 0.0100 150ASTM-P-0104-06 0.0125 150ASTM-P-0104-07 0.0150 150ASTM-P-0104-08 0.0175 150ASTM-P-0104-09 0.0200 150Vanadium Standards - High Range for ISO/CD14597 with 0.05% Manganese Internal Standardin Xylene-Mineral OilASTM-P-0105-SET $ 780 / 7 x 100 mLVanadium PriceCat. No. Conc. (Wt.%) 100 mLASTM-P-0105-01 0.0000 $ 135ASTM-P-0105-02 0.0300 135ASTM-P-0105-03 0.0400 135ASTM-P-0105-04 0.0500 135ASTM-P-0105-05 0.0600 135ASTM-P-0105-06 0.0800 135ASTM-P-0105-07 0.1000 135Internal StandardASTM-P-0107-5$ 235 / 500 mLManganese @ 0.05 Wt. % in Xylene-Mineral OilNickel Standards for ISO/CD 14597 with 0.05%Manganese Internal Standard in Xylene-Mineral OilASTM-P-0106-SET $ 780 / 7 x 100 mLNickel PriceCat. No. Conc. (Wt.%) 100 mLASTM-P-0106-01 0.0000 $ 135ASTM-P-0106-02 0.0005 135ASTM-P-0106-03 0.0010 135ASTM-P-0106-04 0.0025 135ASTM-P-0106-05 0.0050 135ASTM-P-0106-06 0.0075 135ASTM-P-0106-07 0.0100 135TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 49


Traceable Organometallic Standards forAA, ICP, DCP & XRF AnalysisLubricating Oil StandardsASTM-P-0108-SET$ 1900 / 17 x 100 mLASTM-P-0109-SET$ 1600 / 17 x 100 mLDesigned forASTM D-6481-99OrganometallicCat. No. Ca P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0108-01 0.600 0.005 0.175 0.060ASTM-P-0108-02 0.500 0.200 0.050 0.080ASTM-P-0108-03 0.400 0.150 0.300 0.180ASTM-P-0108-04 0.260 0.250 0.150 0.120ASTM-P-0108-05 0.005 0.005 0.450 0.070ASTM-P-0108-06 0.400 0.025 0.350 0.100ASTM-P-0108-07 0.300 0.060 0.250 0.120ASTM-P-0108-08 0.200 0.100 0.450 0.100ASTM-P-0108-09 0.060 0.080 0.300 0.130ASTM-P-0108-10 0.060 0.050 0.200 0.050ASTM-P-0108-11 0.050 0.120 0.100 0.075ASTM-P-0108-12 0.025 0.150 0.200 0.130ASTM-P-0108-13 0.005 0.200 0.400 0.150ASTM-P-0108-14 0.170 0.250 0.550 0.110ASTM-P-0108-15 0.100 0.100 0.200 0.200ASTM-P-0108-16 0.010 0.010 0.600 0.250ASTM-P-0108-17 0.000 0.000 0.000 0.000Cat. No. Ca Cl P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0109-01 0.600 0.100 0.005 0.175 0.060ASTM-P-0109-02 0.500 0.000 0.200 0.050 0.080ASTM-P-0109-03 0.400 0.010 0.150 0.300 0.180ASTM-P-0109-04 0.260 0.500 0.250 0.150 0.120ASTM-P-0109-05 0.005 1.000 0.005 0.450 0.070ASTM-P-0109-06 0.400 0.400 0.025 0.350 0.100ASTM-P-0109-07 0.300 0.100 0.060 0.250 0.120ASTM-P-0109-08 0.200 0.010 0.100 0.450 0.100ASTM-P-0109-09 0.060 0.050 0.080 0.300 0.130ASTM-P-0109-10 0.060 0.200 0.050 0.200 0.050ASTM-P-0109-11 0.050 0.500 0.120 0.100 0.075ASTM-P-0109-12 0.025 0.800 0.150 0.200 0.130ASTM-P-0109-13 0.005 1.000 0.200 0.400 0.150ASTM-P-0109-14 0.170 0.600 0.250 0.550 0.110ASTM-P-0109-15 0.100 0.200 0.100 0.200 0.200ASTM-P-0109-16 0.010 0.400 0.010 0.600 0.250ASTM-P-0109-17 0.000 0.000 0.000 0.000 0.000ASTM-P-0110-SET$ 2300 / 17 x 100 mLDesigned forASTM D-4927-96Cat. No. Ba Ca P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0110-01 0.100 0.600 0.005 0.175 0.060ASTM-P-0110-02 0.175 0.500 0.200 0.050 0.080ASTM-P-0110-03 0.000 0.400 0.150 0.300 0.180ASTM-P-0110-04 0.025 0.260 0.250 0.150 0.120ASTM-P-0110-05 0.150 0.005 0.005 0.450 0.070ASTM-P-0110-06 0.000 0.400 0.025 0.350 0.100ASTM-P-0110-07 0.200 0.300 0.060 0.250 0.120ASTM-P-0110-08 0.000 0.200 0.100 0.450 0.100ASTM-P-0110-09 0.100 0.060 0.080 0.300 0.130ASTM-P-0110-10 0.050 0.060 0.050 0.200 0.050ASTM-P-0110-11 0.075 0.050 0.120 0.100 0.075ASTM-P-0110-12 0.010 0.025 0.150 0.200 0.130ASTM-P-0110-13 0.005 0.005 0.200 0.400 0.150ASTM-P-0110-14 0.000 0.170 0.250 0.550 0.110ASTM-P-0110-15 0.000 0.100 0.100 0.200 0.200ASTM-P-0110-16 0.005 0.010 0.010 0.600 0.250ASTM-P-0110-17 0.000 0.000 0.000 0.000 0.000ASTM-P-0111-SET$ 2800 / 17 x 100 mLDesigned forASTM D-4927-96Cat. No. Ba Ca Cl P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0111-01 0.100 0.600 0.100 0.005 0.175 0.060ASTM-P-0111-02 0.175 0.500 0.000 0.200 0.050 0.080ASTM-P-0111-03 0.000 0.400 0.010 0.150 0.300 0.180ASTM-P-0111-04 0.025 0.260 0.500 0.250 0.150 0.120ASTM-P-0111-05 0.150 0.005 1.000 0.005 0.450 0.070ASTM-P-0111-06 0.000 0.400 0.400 0.025 0.350 0.100ASTM-P-0111-07 0.200 0.300 0.100 0.060 0.250 0.120ASTM-P-0111-08 0.000 0.200 0.010 0.100 0.450 0.100ASTM-P-0111-09 0.100 0.060 0.050 0.080 0.300 0.130ASTM-P-0111-10 0.050 0.060 0.200 0.050 0.200 0.050ASTM-P-0111-11 0.075 0.050 0.500 0.120 0.100 0.075ASTM-P-0111-12 0.010 0.025 0.800 0.150 0.200 0.130ASTM-P-0111-13 0.005 0.005 1.000 0.200 0.400 0.150ASTM-P-0111-14 0.000 0.170 0.600 0.250 0.550 0.110ASTM-P-0111-15 0.000 0.100 0.200 0.100 0.200 0.200ASTM-P-0111-16 0.005 0.010 0.400 0.010 0.600 0.250ASTM-P-0111-17 0.000 0.000 0.000 0.000 0.000 0.000ASTM-P-0112-SET$ 2300 / 17 x 100 mLASTM-P-0113-SET$ 2850 / 17 x 100 mLDesigned forASTM D-4628-97 & D-4927-96Cat. No. Ca Mg P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0112-01 0.600 0.100 0.005 0.175 0.060ASTM-P-0112-02 0.500 0.150 0.200 0.050 0.080ASTM-P-0112-03 0.400 0.350 0.150 0.300 0.180ASTM-P-0112-04 0.260 0.225 0.250 0.150 0.120ASTM-P-0112-05 0.005 0.450 0.005 0.450 0.070ASTM-P-0112-06 0.400 0.500 0.025 0.350 0.100ASTM-P-0112-07 0.300 0.325 0.060 0.250 0.120ASTM-P-0112-08 0.200 0.250 0.100 0.450 0.100ASTM-P-0112-09 0.060 0.100 0.080 0.300 0.130ASTM-P-0112-10 0.060 0.400 0.050 0.200 0.050ASTM-P-0112-11 0.050 0.300 0.120 0.100 0.075ASTM-P-0112-12 0.025 0.200 0.150 0.200 0.130ASTM-P-0112-13 0.005 0.375 0.200 0.400 0.150ASTM-P-0112-14 0.170 0.175 0.250 0.550 0.110ASTM-P-0112-15 0.100 0.425 0.100 0.200 0.200ASTM-P-0112-16 0.010 0.275 0.010 0.600 0.250ASTM-P-0112-17 0.000 0.000 0.000 0.000 0.000Cat. No. Ba Ca Mg P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0113-01 0.025 0.600 0.100 0.005 0.175 0.060ASTM-P-0113-02 0.000 0.500 0.150 0.200 0.050 0.080ASTM-P-0113-03 0.100 0.400 0.350 0.150 0.300 0.180ASTM-P-0113-04 0.175 0.260 0.225 0.250 0.150 0.120ASTM-P-0113-05 0.150 0.005 0.450 0.005 0.450 0.070ASTM-P-0113-06 0.000 0.400 0.500 0.025 0.350 0.100ASTM-P-0113-07 0.100 0.300 0.325 0.060 0.250 0.120ASTM-P-0113-08 0.200 0.200 0.250 0.100 0.450 0.100ASTM-P-0113-09 0.050 0.060 0.100 0.080 0.300 0.130ASTM-P-0113-10 0.075 0.060 0.400 0.050 0.200 0.050ASTM-P-0113-11 0.010 0.050 0.300 0.120 0.100 0.075ASTM-P-0113-12 0.000 0.025 0.200 0.150 0.200 0.130ASTM-P-0113-13 0.175 0.005 0.375 0.200 0.400 0.150ASTM-P-0113-14 0.005 0.170 0.175 0.250 0.550 0.110ASTM-P-0113-15 0.000 0.100 0.425 0.100 0.200 0.200ASTM-P-0113-16 0.005 0.010 0.275 0.010 0.600 0.250ASTM-P-0113-17 0.000 0.000 0.000 0.000 0.000 0.000These products do not require Hazardous Shippingcharges at this time.50TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Traceable Organometallic Standards forAA, ICP, DCP & XRF AnalysisLubricating Oil Standards (Continued)ASTM-P-0114-SET$ 1900 / 17 x 100 mLEDXRF ASTM MethodDesigned for ASTM D-6481-99Cat. No. Ca P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0114-01 0.005 0.005 0.050 0.050ASTM-P-0114-02 0.600 0.000 0.000 0.000ASTM-P-0114-03 0.000 0.300 0.000 0.000ASTM-P-0114-04 1.000 0.000 1.000 0.000ASTM-P-0114-05 0.000 0.000 0.000 0.300ASTM-P-0114-06 0.005 0.250 0.800 0.300ASTM-P-0114-07 0.500 0.150 0.500 0.150ASTM-P-0114-08 0.010 0.200 0.100 0.250ASTM-P-0114-09 0.050 0.010 0.400 0.075ASTM-P-0114-10 0.100 0.150 0.200 0.200ASTM-P-0114-11 0.200 0.200 0.800 0.100ASTM-P-0114-12 0.400 0.005 0.800 0.300ASTM-P-0114-13 0.600 0.100 0.500 0.050ASTM-P-0114-14 0.800 0.010 0.050 0.100ASTM-P-0114-15 1.000 0.300 1.000 0.150ASTM-P-0114-16 0.400 0.050 0.600 0.250ASTM-P-0114-17 0.000 0.000 0.000 0.000ASTM-P-0115-SET$ 2300 / 17 x 100 mLCat. No. Ca P S Zn MgNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0115-01 0.005 0.005 0.050 0.050 0.100ASTM-P-0115-02 0.600 0.000 0.000 0.000 0.150ASTM-P-0115-03 0.000 0.300 0.000 0.000 0.350ASTM-P-0115-04 1.000 0.000 1.000 0.000 0.225ASTM-P-0115-05 0.000 0.000 0.000 0.300 0.450ASTM-P-0115-06 0.005 0.250 0.800 0.300 0.500ASTM-P-0115-07 0.500 0.150 0.500 0.150 0.325ASTM-P-0115-08 0.010 0.200 0.100 0.250 0.250ASTM-P-0115-09 0.050 0.010 0.400 0.075 0.050ASTM-P-0115-10 0.100 0.150 0.200 0.200 0.400ASTM-P-0115-11 0.200 0.200 0.800 0.100 0.300ASTM-P-0115-12 0.400 0.005 0.800 0.300 0.200ASTM-P-0115-13 0.600 0.100 0.500 0.050 0.375ASTM-P-0115-14 0.800 0.010 0.050 0.100 0.175ASTM-P-0115-15 1.000 0.300 1.000 0.150 0.425ASTM-P-0115-16 0.400 0.050 0.600 0.250 0.275ASTM-P-0115-17 0.000 0.000 0.000 0.000 0.000Organometallic StandardsASTM-P-0116-SET$ 2450 / 11 x 100 mLDesigned for ASTM D-6481-99AdditivesCat. No. Ca P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0116-01 0.500 1.000 0.500 0.500ASTM-P-0116-02 3.000 1.000 3.000 2.000ASTM-P-0116-03 2.000 1.250 1.000 1.500ASTM-P-0116-04 5.000 1.500 0.500 1.200ASTM-P-0116-05 4.000 0.500 1.500 0.750ASTM-P-0116-06 2.500 0.750 4.000 1.000ASTM-P-0116-07 4.000 0.500 2.000 1.250ASTM-P-0116-08 0.500 2.000 5.000 1.000ASTM-P-0116-09 1.000 0.750 2.000 1.500ASTM-P-0116-10 2.500 1.200 3.000 0.500ASTM-P-0116-11 0.000 0.000 0.000 0.000ASTM-P-0117-SET$ 2100 / 10 x 100 mLWLXRF ASTM MethodDesigned forASTM D-6443-99Cat. No. Ca Cl Cu Mg P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0117-01 0.020 0.030 0.010 0.200 0.250 1.000 0.020ASTM-P-0117-02 0.020 0.020 0.050 0.200 0.020 0.020 0.250ASTM-P-0117-03 0.020 0.200 0.010 0.040 0.250 0.150 0.250ASTM-P-0117-04 0.020 0.200 0.050 0.040 0.020 1.000 0.020ASTM-P-0117-05 0.400 0.020 0.010 0.040 0.020 1.000 0.250ASTM-P-0117-06 0.400 0.020 0.050 0.040 0.250 0.020 0.020ASTM-P-0117-07 0.400 0.200 0.010 0.200 0.020 0.020 0.050ASTM-P-0117-08 0.400 0.200 0.050 0.200 0.250 1.000 0.250ASTM-P-0117-09 0.200 0.100 0.025 0.080 0.150 0.500 0.100ASTM-P-0117-10 0.000 0.000 0.000 0.000 0.000 0.000 0.000ASTM-P-0118-SET$ 2400 / 10 x 100 mLDesigned for ASTM D-4628-97, D-4927-96, D-4951-96, D-6443-99WLXRF ASTM MethodCat. No. Ba Ca Cl Cu Mg P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0118-01 0.020 0.020 0.030 0.010 0.200 0.250 1.000 0.020ASTM-P-0118-02 0.250 0.020 0.020 0.050 0.200 0.020 0.020 0.250ASTM-P-0118-03 0.020 0.020 0.200 0.010 0.040 0.250 0.150 0.250ASTM-P-0118-04 0.250 0.020 0.200 0.050 0.040 0.020 1.000 0.020ASTM-P-0118-05 0.020 0.400 0.020 0.010 0.040 0.020 1.000 0.250ASTM-P-0118-06 0.250 0.400 0.020 0.050 0.040 0.250 0.020 0.020ASTM-P-0118-07 0.020 0.400 0.200 0.010 0.200 0.020 0.020 0.050ASTM-P-0118-08 0.250 0.400 0.200 0.050 0.200 0.250 1.000 0.250ASTM-P-0118-09 0.130 0.200 0.100 0.025 0.080 0.150 0.500 0.100ASTM-P-0118-10 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000Lubricating Oil Standards continued on next pageTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 51


Traceable Organometallic Standards forAA, ICP, DCP & XRF AnalysisOrganometallicASTM-P-0119-SETLubricating Oil Standards (Continued)$ 2900 / 22 x 100 mLDesigned for ASTM D-4628-97, D-4927-96, D-4951-96, D-6443-99Cat. No. Ca Cl Cu Mg P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0119-01 0.300 0.080 0.030 0.060 0.060 0.275 0.060ASTM-P-0119-02 0.250 0.100 0.000 0.010 0.150 0.000 0.150ASTM-P-0119-03 0.500 0.000 0.035 0.160 0.150 0.000 0.020ASTM-P-0119-04 0.350 0.010 0.000 0.120 0.080 0.200 0.000ASTM-P-0119-05 0.110 0.000 0.015 0.100 0.100 0.300 0.050ASTM-P-0119-06 0.200 0.100 0.000 0.200 0.050 0.250 0.150ASTM-P-0119-07 0.000 0.050 0.025 0.000 0.000 0.450 0.020ASTM-P-0119-08 0.150 0.030 0.000 0.100 0.030 0.400 0.040ASTM-P-0119-09 0.250 0.150 0.010 0.160 0.000 0.350 0.080ASTM-P-0119-10 0.110 0.150 0.040 0.005 0.030 0.750 0.150ASTM-P-0119-11 0.260 0.050 0.000 0.000 0.000 0.750 0.000ASTM-P-0119-12 0.200 0.000 0.005 0.140 0.080 0.500 0.080ASTM-P-0119-13 0.000 0.000 0.005 0.020 0.020 0.200 0.020ASTM-P-0119-14 0.070 0.150 0.020 0.080 0.140 0.650 0.150ASTM-P-0119-15 0.050 0.000 0.000 0.000 0.150 0.000 0.000ASTM-P-0119-16 0.400 0.000 0.001 0.080 0.000 0.500 0.020ASTM-P-0119-17 0.180 0.020 0.020 0.000 0.020 0.600 0.060ASTM-P-0119-18 0.400 0.010 0.001 0.010 0.020 0.000 0.000ASTM-P-0119-19 0.010 0.020 0.040 0.010 0.020 0.200 0.100ASTM-P-0119-20 0.050 0.005 0.050 0.000 0.008 0.000 0.120ASTM-P-0119-21 0.200 0.050 0.020 0.080 0.050 0.275 0.050ASTM-P-0119-22 0.000 0.000 0.000 0.000 0.000 0.000 0.000Standards of InterestConcentration for the sets on pages50-52 are targets. Actual productionlots may vary.These products do not require Hazardous Shippingcharges at this time.ASTM-P-0120-SET$ 3100 / 23 x 100 mLCat. No. Ba Ca Cl Cu Mg P S ZnNominal Value (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0120-01 0.100 0.300 0.080 0.030 0.060 0.060 0.275 0.060ASTM-P-0120-02 0.175 0.250 0.100 0.000 0.010 0.150 0.000 0.150ASTM-P-0120-03 0.040 0.500 0.000 0.035 0.160 0.150 0.000 0.020ASTM-P-0120-04 0.020 0.350 0.010 0.000 0.120 0.080 0.200 0.000ASTM-P-0120-05 0.150 0.110 0.000 0.015 0.100 0.100 0.300 0.050ASTM-P-0120-06 0.000 0.200 0.100 0.000 0.200 0.050 0.250 0.150ASTM-P-0120-07 0.200 0.000 0.050 0.025 0.000 0.000 0.450 0.020ASTM-P-0120-08 0.000 0.150 0.030 0.000 0.100 0.030 0.400 0.040ASTM-P-0120-09 0.000 0.250 0.150 0.010 0.160 0.000 0.350 0.080ASTM-P-0120-10 0.000 0.110 0.150 0.040 0.005 0.030 0.750 0.150ASTM-P-0120-11 0.100 0.260 0.050 0.000 0.000 0.000 0.750 0.000ASTM-P-0120-12 0.050 0.200 0.000 0.005 0.140 0.080 0.500 0.080ASTM-P-0120-13 0.000 0.000 0.000 0.005 0.020 0.020 0.200 0.020ASTM-P-0120-14 0.080 0.070 0.150 0.020 0.080 0.140 0.650 0.150ASTM-P-0120-15 0.010 0.050 0.000 0.000 0.000 0.150 0.000 0.000ASTM-P-0120-16 0.000 0.400 0.000 0.001 0.080 0.000 0.500 0.020ASTM-P-0120-17 0.000 0.180 0.020 0.020 0.000 0.020 0.600 0.060ASTM-P-0120-18 0.000 0.400 0.010 0.001 0.010 0.020 0.000 0.000ASTM-P-0120-19 0.150 0.010 0.020 0.040 0.010 0.020 0.200 0.100ASTM-P-0120-20 0.005 0.050 0.005 0.050 0.000 0.008 0.000 0.120ASTM-P-0120-21 0.100 0.200 0.050 0.020 0.080 0.050 0.275 0.050ASTM-P-0120-22 0.120 0.200 0.000 0.000 0.000 0.000 0.750 0.000ASTM-P-0120-23 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000ASTM-P-0121-SETMetal Working Fluids$ 1300 / 13 x 100 mLCat. No. Cl P SNominal Value (Wt.%) (Wt.%) (Wt.%)ASTM-P-0121-01 0.000 0.000 0.000ASTM-P-0121-02 0.750 0.025 0.500ASTM-P-0121-03 0.050 0.100 3.000ASTM-P-0121-04 1.000 0.500 2.500ASTM-P-0121-05 0.100 0.005 2.000ASTM-P-0121-06 1.500 0.200 1.000ASTM-P-0121-07 2.000 0.005 3.000ASTM-P-0121-08 1.000 0.050 0.100ASTM-P-0121-09 0.500 0.400 0.000ASTM-P-0121-10 2.000 0.200 1.500ASTM-P-0121-11 0.000 0.500 1.500ASTM-P-0121-12 1.250 0.010 0.050ASTM-P-0121-13 0.050 0.300 0.050Stabilizer Solution AASTM-P-0122-0.5 $ 80 / 50 mLASTM-P-0122-1 $ 120 / 100 mLStabilizer Solution BASTM-P-0123-0.5 $ 80 / 50 mLASTM-P-0123-1 $ 120 / 100 mLStabilization SolutionsThe solutions were specifically designed for chelating & solubilizing our line of Sulfur-Free Organometallic Standards. Contact Tech Service for additional information.Stabilizer Solution CASTM-P-0124-0.5ASTM-P-0124-1Stabilizer Solution DASTM-P-0125-0.5ASTM-P-0125-1$ 80 / 50 mL$ 120 / 100 mL$ 80 / 50 mL$ 120 / 100 mL52TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM-P-0100-SET:49ASTM-P-0101-SET:49ASTM-P-0102-SET:49ASTM-P-0103-SET:49ASTM-P-0104-SET:49ASTM-P-0105-SET:49ASTM-P-0106-SET:49ASTM-P-0107-5:49ASTM-P-0108-SET:50ASTM-P-0109-SET:50ASTM-P-0110-SET:50ASTM-P-0111-SET:50ASTM-P-0112-SET:50ASTM-P-0113-SET:50ASTM-P-0114-SET:51ASTM-P-0115-SET:51ASTM-P-0116-SET:51ASTM-P-0117-SET:51ASTM-P-0118-SET:51ASTM-P-0119-SET:52ASTM-P-0120-SET:52ASTM-P-0121-SET:52ASTM-P-0122-0.5:47, 52ASTM-P-0122-1:47, 52ASTM-P-0123-0.5:47, 52ASTM-P-0123-1:47, 52ASTM-P-0124-0.5:52ASTM-P-0124-1:52ASTM-P-0125-0.5:52ASTM-P-0125-1:52MA-900-4:46MA-900-8:46MOSOL-20:46MOSOL-75:46WC-STAB:46WM-11-NMS-1-SET:48WM-11-NMS-10X-1:48WM-11-NMS-1X-1:48WM-11-NMS-30X-1:48WM-11-NMS-3X-1:48WM-11-NMS-50X-1:48WM-11-NMS-5X-1:48WM-11-NMS-90X-1:48WM-12-10X-4:46WM-12-10X-8:46WM-12-1X-4:46WM-12-1X-8:46WM-12-30X-4:46WM-12-30X-8:46WM-12-3X-4:46WM-12-3X-8:46WM-12-4-SET:46WM-12-50X-4:46WM-12-50X-8:46WM-12-5X-4:46WM-12-5X-8:46WM-12-8-SET:46WM-12-90X-4:46WM-12-90X-8:46WM-12-NMS-1-SET:48WM-12-NMS-10X-1:48WM-12-NMS-1X-1:48WM-12-NMS-30X-1:48WM-12-NMS-3X-1:48WM-12-NMS-50X-1:48WM-12-NMS-5X-1:48WM-20-NMS-1-SET:48WM-20-NMS-10X-1:48WM-20-NMS-1X-1:48WM-20-NMS-30X-1:48WM-20-NMS-3X-1:48WM-20-NMS-50X-1:48WM-20-NMS-5X-1:48WM-20-NMS-90X-1:48WM-20CST-01:46WM-20CST-02:46WM-20CST-03:46WM-20CST-04:46WM-20CST-05:46WM-20CST-06:46WM-20CST-07:46WM-20CST-08:46WM-20CST-09:46WM-20CST-13:46WM-20CST-14:46WM-20CST-15:46WM-20CST-28:46WM-20CST-29:46WM-20CST-30:46WM-20CST-32:46WM-20CST-33:46WM-20CST-34:46WM-20CST-35:46WM-20CST-37:46WM-20CST-41:46WM-20CST-43:46WM-20CST-50:46WM-20CST-51:46WM-20CST-52:46WM-20CST-53:46WM-20CST-54:46WM-20CST-55:46WM-20CST-56:46WM-20CST-60:46WM-20CST-63:46WM-20CST-64:46WM-20CST-69:46WM-20CST-70:46WM-20CST-71:46WM-21-10X-4:46WM-21-10X-8:46WM-21-1X-4:46WM-21-1X-8:46WM-21-30X-4:46WM-21-30X-8:46WM-21-3X-4:46WM-21-3X-8:46WM-21-4-SET:46WM-21-50X-4:46WM-21-50X-8:46WM-21-5X-4:46WM-21-5X-8:46WM-21-8-SET:46WM-21-90X-4:46WM-21-90X-8:46WM-21-NMS-1-SET:48WM-21-NMS-10X-1:48WM-21-NMS-1X-1:48WM-21-NMS-30X-1:48WM-21-NMS-3X-1:48WM-21-NMS-50X-1:48WM-21-NMS-5X-1:48WM-75CST-01-5X:46WM-75CST-02-5X:46WM-75CST-04-5X:46WM-75CST-06-5X:46WM-75CST-07-5X:46WM-75CST-08-5X:46WM-75CST-09-5X:46WM-75CST-13-5X:46WM-75CST-14-5X:46WM-75CST-15-5X:46WM-75CST-27:46WM-75CST-27-5X:46WM-75CST-29-5X:46WM-75CST-30-5X:46WM-75CST-32-5X:46WM-75CST-33-5X:46WM-75CST-35-5X:46WM-75CST-37-5X:46WM-75CST-41-5X:46WM-75CST-43-5X:46WM-75CST-51-5X:46WM-75CST-52-5X:46WM-75CST-53-5X:46WM-75CST-54-5X:46WM-75CST-56-5X:46WM-75CST-63-5X:46WM-75CST-64-5X:46WM-75CST-67:46WM-75CST-67-5X:46WM-75CST-69-5X:46WM-75CST-70-5X:46WM-75CST-71-5X:46WM-NMS-01:47WM-NMS-01-30X-25G:47WM-NMS-01-30X-50G:47WM-NMS-01-5X:47WM-NMS-02:47WM-NMS-02-20X-25G:47WM-NMS-02-20X-50G:47WM-NMS-02-5X:47WM-NMS-03:47WM-NMS-03-5X:47WM-NMS-04:47WM-NMS-04-125X-25G:47WM-NMS-04-125X-50G:47WM-NMS-04-5X:47WM-NMS-05:47WM-NMS-05-5X:47WM-NMS-07-25X-25G:47WM-NMS-07-25X-50G:47WM-NMS-08:47WM-NMS-08-100X-25G:47WM-NMS-08-100X-50G:47WM-NMS-08-5X:47WM-NMS-09:47WM-NMS-09-50X-25G:47WM-NMS-09-50X-50G:47WM-NMS-09-5X:47WM-NMS-11-50X-25G:47WM-NMS-11-50X-50G:47WM-NMS-13:47WM-NMS-13-35X-25G:47WM-NMS-13-35X-50G:47WM-NMS-13-5X:47WM-NMS-14:47WM-NMS-14-5X:47WM-NMS-14-75X-25G:47WM-NMS-14-75X-50G:47WM-NMS-15:47WM-NMS-15-5X:47WM-NMS-15-60X-25G:47WM-NMS-15-60X-50G:47WM-NMS-20:47WM-NMS-20-5X:47WM-NMS-22:47WM-NMS-27:47WM-NMS-27-40X-25G:47WM-NMS-27-40X-50G:47WM-NMS-27-5X:47WM-NMS-29:47WM-NMS-29-200X-25G:47WM-NMS-29-200X-50G:47WM-NMS-29-5X:47WM-NMS-30:47WM-NMS-30-15X-25G:47WM-NMS-30-15X-50G:47WM-NMS-30-5X:47WM-NMS-32:47WM-NMS-32-30X-25G:47WM-NMS-32-30X-50G:47WM-NMS-32-5X:47WM-NMS-33:47WM-NMS-33-5X:47WM-NMS-33-60X-25G:47WM-NMS-33-75X-50G:47WM-NMS-34:47WM-NMS-34-5X:47WM-NMS-35:47WM-NMS-35-50X-25G:47WM-NMS-35-50X-50G:47WM-NMS-35-5X:47WM-NMS-37:47WM-NMS-37-50X-25G:47WM-NMS-37-50X-50G:47WM-NMS-37-5X:47WM-NMS-41:47WM-NMS-41-50X-25G:47WM-NMS-41-50X-50G:47WM-NMS-41-5X:47WM-NMS-43:47WM-NMS-43-5X:47WM-NMS-43-75X-25G:47WM-NMS-43-75X-50G:47WM-NMS-44-30X-25G:47WM-NMS-44-30X-50G:47WM-NMS-51:47WM-NMS-51-35X-25G:47WM-NMS-51-35X-50G:47WM-NMS-51-5X:47WM-NMS-52:47WM-NMS-52-5X:47WM-NMS-52-75X-25G:47WM-NMS-52-75X-50G:47WM-NMS-53:47WM-NMS-53-5X:47WM-NMS-54:47WM-NMS-54-25X-25G:47WM-NMS-54-25X-50G:47WM-NMS-54-5X:47WM-NMS-55:47WM-NMS-55-100X-25G:47WM-NMS-55-100X-50G:47WM-NMS-55-5X:47WM-NMS-60:47WM-NMS-60-50X-25G:47WM-NMS-60-50X-50G:47WM-NMS-60-5X:47WM-NMS-63:47WM-NMS-63-5X:47WM-NMS-63-75X-25G:47WM-NMS-63-75X-50G:47WM-NMS-64:47WM-NMS-64-50X-25G:47WM-NMS-64-50X-50G:47WM-NMS-64-5X:47WM-NMS-67:47WM-NMS-67-40X-25G:47WM-NMS-67-40X-50G:47WM-NMS-67-5X:47WM-NMS-68:47WM-NMS-68-5X:47WM-NMS-69-25X-25G:47WM-NMS-69-25X-50G:47WM-NMS-70:47WM-NMS-70-5X:47WM-NMS-70-60X-25G:47WM-NMS-70-60X-50G:47WM-NMS-71:47WM-NMS-71-50X-25G:47WM-NMS-71-50X-50G:47WM-NMS-71-5X:47


Traceable Sulfur Calibration StandardsSulfur Calibration StandardsSulfur Standards for ASTM D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 & Proposed ASTM Sulfur MethodsSulfur in Heavy Weight Mineral Oil (75 cSt)Sulfur inReady-to-UseConcentration White Mineral Oil Sulfur AccuShotsµg/g Wt. % Cat. No. Cat. No.Blank 0.000 SWMO-BL-4 SWMO-BL-20ML-PAK100 0.010 SWMO-1X-4 SWMO-1X-20ML-PAK200 0.020 SWMO-2X-4 SWMO-2X-20ML-PAK300 0.030 SWMO-3X-4 SWMO-3X-20ML-PAK400 0.040 SWMO-4X-4 SWMO-4X-20ML-PAK500 0.050 SWMO-5X-4 SWMO-5X-20ML-PAK750 0.075 SWMO-7.5X-4 SWMO-7.5X-20ML-PAK1,000 0.10 SWMO-10X-4 SWMO-10X-20ML-PAK1,500 0.15 SWMO-15X-4 SWMO-15X-20ML-PAK2,000 0.20 -------------------- --------------------------3,000 0.30 SWMO-30X-4 SWMO-30X-20ML-PAK4,000 0.40 -------------------- --------------------------5,000 0.50 SWMO-50X-4 SWMO-50X-20ML-PAK7,000 0.70 SWMO-70X-4 SWMO-70X-20ML-PAK10,000 1.00 SWMO-100X-4 SWMO-100X-20ML-PAK15,000 1.50 SWMO-150X-4 SWMO-150X-20ML-PAK20,000 2.00 SWMO-200X-4 SWMO-200X-20ML-PAK30,000 3.00 SWMO-300X-4 SWMO-300X-20ML-PAK40,000 4.00 SWMO-400X-4 SWMO-400X-20ML-PAK50,000 5.00 SWMO-500X-4 SWMO-500X-20ML-PAK60,000 6.00 SWMO-600X-4 SWMO-600X-20ML-PAKSulfur in Mineral OilSulfur in Light Weight Mineral Oil (20 cSt)Sulfur inReady-to-UseConcentration White Mineral Oil Sulfur AccuShotsµg/g Wt. % Cat. No. Cat. No.Blank 0.000 SWMO-LT-BL-4 SWMO-LT-BL-20ML-PAK100 0.010 SWMO-LT-1X-4 SWMO-LT-1X-20ML-PAK200 0.020 SWMO-LT-2X-4 SWMO-LT-2X-20ML-PAK300 0.030 SWMO-LT-3X-4 SWMO-LT-3X-20ML-PAK400 0.040 SWMO-LT-4X-4 SWMO-LT-4X-20ML-PAK500 0.050 SWMO-LT-5X-4 SWMO-LT-5X-20ML-PAK750 0.075 SWMO-LT-7.5X-4 SWMO-LT-7.5X-20ML-PAK1,000 0.10 SWMO-LT-10X-4 SWMO-LT-10X-20ML-PAK1,500 0.15 SWMO-LT-15X-4 SWMO-LT-15X-20ML-PAK2,000 0.20 -------------------- --------------------------3,000 0.30 SWMO-LT-30X-4 SWMO-LT-30X-20ML-PAK4,000 0.40 -------------------- --------------------------5,000 0.50 SWMO-LT-50X-4 SWMO-LT-50X-20ML-PAK7,000 0.70 SWMO-LT-70X-4 SWMO-LT-70X-20ML-PAK10,000 1.00 SWMO-LT-100X-4 SWMO-LT-100X-20ML-PAK15,000 1.50 SWMO-LT-150X-4 SWMO-LT-150X-20ML-PAK20,000 2.00 SWMO-LT-200X-4 SWMO-LT-200X-20ML-PAK30,000 3.00 SWMO-LT-300X-4 SWMO-LT-300X-20ML-PAK40,000 4.00 SWMO-LT-400X-4 SWMO-LT-400X-20ML-PAK50,000 5.00 SWMO-LT-500X-4 SWMO-LT-500X-20ML-PAK60,000 6.00 SWMO-LT-600X-4 SWMO-LT-600X-20ML-PAKSulfur MethodsSet of above SWMO-CAL-4-SET 5 x 20 mL ampules atCat. No.’s 19 x 4 oz. $ 850 stated conc. for $ 60Individual Sulfur 1-10 units 10+unitsStandards 4 oz. Bottle $ 55 ea $ 50 eaSet of aboveSWMO-LT-CAL-4-SET5 x 20 mL ampules atCat. No.’s 19 x 4 oz. $ 850 stated conc. for $ 60Individual Sulfur 1-10 units 10+unitsStandards 4 oz. Bottle $ 55 ea $ 50 eaSulfur in #2 Diesel FuelSulfur inReady-to-UseConcentration #2 Diesel Fuel Sulfur AccuShotsµg/g Wt. % Cat. No. Cat. No.Blank 0.000 SDF-BL-4 SDF-BL-20ML-PAK100 0.010 SDF-1X-4 SDF-1X-20ML-PAK200 0.020 SDF-2X-4 SDF-2X-20ML-PAK300 0.030 SDF-3X-4 SDF-3X-20ML-PAK400 0.040 SDF-4X-4 SDF-4X-20ML-PAK500 0.050 SDF-5X-4 SDF-5X-20ML-PAK750 0.075 SDF-7.5X-4 SDF-7.5X-20ML-PAK1,000 0.10 SDF-10X-4 SDF-10X-20ML-PAK1,500 0.15 SDF-15X-4 SDF-15X-20ML-PAK2,000 0.20 ------------- -------------3,000 0.30 SDF-30X-4 SDF-30X-20ML-PAK4,000 0.40 ------------- -------------5,000 0.50 SDF-50X-4 SDF-50X-20ML-PAK7,000 0.70 SDF-70X-4 SDF-70X-20ML-PAK10,000 1.00 SDF-100X-4 SDF-100X-20ML-PAK15,000 1.50 SDF-150X-4 SDF-150X-20ML-PAK20,000 2.00 SDF-200X-4 SDF-200X-20ML-PAK30,000 3.00 SDF-300X-4 SDF-300X-20ML-PAK40,000 4.00 SDF-400X-4 SDF-400X-20ML-PAK50,000 5.00 SDF-500X-4 SDF-500X-20ML-PAK60,000 6.00 SDF-600X-4 SDF-600X-20ML-PAKSet of above SDF-CAL-4-SET 5 x 20 mL ampules atCat. No.’s 19 x 4 oz. $ 850 stated conc. for $ 60Individual Sulfur 1-10 units 10+unitsStandards 4 oz. Bottle $ 55 ea $ 50 eaTechnical NoteSulfur concentration calculated from % sulfur in di-n-butyl sulfide.These products require a Hazardous Shipping ChargeReady-to-UseAccuStandard is the first standard manufacturer to provide sulfurstandards in convenient and Ready-to-Aspirate AccuShot 20 mLsealed ampules. Each 20 mL AccuShot provides the necessarymaterial for calibration curve development or daily QA/QC. Bypurchasing AccuShots the analytical chemist can open a fresh shotfor each analysis which eliminates opening and pipetting repeatedlyfrom a stock bottle. This minimizes contamination and evaporation.These ship with no haz fee for additional savings.• Ultra Low Sulfur Matrices • Convenient Packaging •Wide Variety of MatricesAccuStandard's Technical Service Dept. can provideReady-to-Inject working level calibration standards tomeet unique laboratory applications call or fax us yourstandard requirements.Working Level Standards &Continuing Calibration Check (CCC)TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3 53


Traceable Sulfur Calibration StandardsSulfur Calibration StandardsSulfur Standards for ASTM D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 & Proposed ASTM Sulfur MethodsSulfur MethodsSulfur in Light Distillate KeroseneSulfur in KeroseneSulfur in Light Ready-to-UseConcentration Distillate Kerosene Sulfur AccuShotsµg/g Wt. % Cat. No. Cat. No.Blank 0.000 SK-BL-4 SK-BL-20ML-PAK100 0.010 SK-1X-4 SK-1X-20ML-PAK200 0.020 --------------- ---------------300 0.030 SK-3X-4 SK-3X-20ML-PAK400 0.040 --------------- ---------------500 0.050 SK-5X-4 SK-5X-20ML-PAK750 0.075 SK-7.5X-4 SK-7.5X-20ML-PAK1,000 0.10 SK-10X-4 SK-10X-20ML-PAK1,500 0.15 --------------- ---------------2,000 0.20 SK-20X-4 SK-20X-20ML-PAK3,000 0.30 SK-30X-4 SK-30X-20ML-PAK4,000 0.40 SK-40X-4 SK-40X-20ML-PAK5,000 0.50 SK-50X-4 SK-50X-20ML-PAK7,000 0.70 --------------- ---------------10,000 1.00 SK-100X-4 SK-100X-20ML-PAK15,000 1.50 --------------- ---------------20,000 2.00 SK-200X-4 SK-200X-20ML-PAK30,000 3.00 --------------- ---------------40,000 4.00 --------------- ---------------50,000 5.00 --------------- ---------------60,000 6.00 --------------- ---------------Sulfur in Heavy Distillate KeroseneSulfur in HeavyConcentration Distillate Keroseneµg/g Wt. % Cat. No.Blank 0.000 SK-HD-BL-4100 0.010 SK-HD-1X-4200 0.020 SK-HD-2X-4300 0.030 SK-HD-3X-4400 0.040 SK-HD-4X-4500 0.050 SK-HD-5X-4750 0.075 SK-HD-7.5X-41,000 0.10 SK-HD-10X-41,500 0.15 SK-HD-15X-42,000 0.20 SK-HD-20X-43,000 0.30 SK-HD-30X-44,000 0.40 SK-HD-40X-45,000 0.50 SK-HD-50X-47,000 0.70 SK-HD-70X-410,000 1.00 SK-HD-100X-415,000 1.50 SK-HD-150X-420,000 2.00 SK-HD-200X-430,000 3.00 SK-HD-300X-440,000 4.00 SK-HD-400X-450,000 5.00 SK-HD-500X-460,000 6.00 SK-HD-600X-4Technical NoteSulfur concentrationcalculated from % sulfur indi-n-butyl sulfide.Standards of InterestFor the mandatory realworld QC samplesstipulated in the Method,see pages 56.Set of above SK-CAL-4-SET 5 x 20 mL ampules atCat. No.’s 12 x 4 oz. $ 500 stated conc. for $ 60Individual Sulfur 1-10 units 10+unitsStds. 4 oz. Bottle $ 55 ea $ 50 eaSet of above SK-HD-CAL-4-SETCat. No.’s 21 x 4 oz. $ 950Individual Sulfur 1 -10 units10 +unitsStds. 4 oz. Bottle $ 55 ea $ 50 eaSulfur in Crude Oil StandardsConcentration Sulfur in Crude Oilµg/g Wt. % Cat. No.1,000 0.10 SCO-10X-42,500 0.25 SCO-25X-45,000 0.50 SCO-50X-410,000 1.00 SCO-100X-420,000 2.00 SCO-200X-430,000 3.00 SCO-300X-440,000 4.00 SCO-400X-450,000 5.00 SCO-500X-4Set of aboveSCO-CAL-4-SETCat. No.’s 8 x 4 oz. $ 500Individual Sulfur 1 -10 units 10 +unitsStandards 4 oz. Bottle $ 75 ea $ 65 eaSulfur in Crude Oil and Residual OilSulfur in Residual Oil StandardsConcentration Sulfur in Crude Oilµg/g Wt. % Cat. No.3,500 0.35 SRO-35X-47,000 0.70 SRO-70X-410,000 1.00 SRO-100X-415,000 1.50 SRO-150X-420,000 2.00 SRO-200X-430,000 3.00 SRO-300X-440,000 4.00 SRO-400X-4Set of aboveSRO-CAL-4-SETCat. No.’s 7 x 4 oz. $ 450Individual Sulfur 1 -10 units 10 +unitsStandards 4 oz. Bottle $ 75 ea $ 65 eaTotal Sulfur in Aromatic Compounds byHydrogenolysis and RateometricColorimetryASTM-P-0010-PAK1000 µg/mL in TolueneProposed ASTM Methods Sulfur Calibration Standards$ 75 / 5 x 1 mLTrace Quantities of Sulfur in LiquidAromatic Hydrocarbons byOxidative MicrocoulometryASTM-P-0020-PAK1000 µg/mL in Xylenes$ 75 / 5 x 1 mLSulfur (as Thiophene)Technical NoteWell characterized Thiophene is used in a lowsulfur Toluene matrix for this stock calibrationstandard.Sulfur (as Dibenzothiophene)Technical NoteWell characterized Dibenzothiophene is usedin a low sulfur Xylene matrix for this stockcalibration standard.These products require a Hazardous Shipping Charge54TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Traceable Standards for ASTM MethodsSulfur Calibration StandardsSulfur Calibration Standards in Isooctane forGasoline & Reformulated Gasoline AnalysisCat. No. Sulfur Conc. Sulfur Wt. % UnitSTP-BL-4 Blank 0.0 4 oz.STP-1X-4 10 µg/g 0.001 4 oz.STP-2X-4 20 µg/g 0.002 4 oz.STP-3X-4 30 µg/g 0.003 4 oz.STP-5X-4 50 µg/g 0.005 4 oz.STP-10X-4 100 µg/g 0.010 4 oz.STP-20X-4 200 µg/g 0.020 4 oz.STP-30X-4 300 µg/g 0.030 4 oz.STP-40X-4 400 µg/g 0.040 4 oz.STP-60X-4 600 µg/g 0.060 4 oz.STP-100X-4 1000 µg/g 0.10 4 oz.STP-200X-4 2000 µg/g 0.20 4 oz.STP-300X-4 3000 µg/g 0.30 4 oz.STP-CAL-SETIn IsooctaneASTM D-2622, D-4294$ 650 / set of 13 x 4 oz.Set contains the above 13 individual bottlesStandards can be mixed for quantity discounts1 to 4 units $ 60 each per Sulfur Standard5 to 10 units $ 55 each per Sulfur Standardmore than 10 units $ 50 each per Sulfur StandardDesigned forD-2622-98D-4294-98ASTM D-2622, D-6334, D-6445Low Level Sulfur Calibration Standardsfor use on XRF Energy Dispersive orWavelength InstrumentsCat. No. Sulfur Conc. Sulfur Wt. % UnitD-2622-LL-BL-4 Blank 0.0 4 oz.D-2622-LL-5X-4 5 µg/g 0.0005 4 oz.D-2622-LL-10X-4 10 µg/g 0.0010 4 oz.D-2622-LL-30X-4 30 µg/g 0.0030 4 oz.D-2622-LL-50X-4 50 µg/g 0.0050 4 oz.D-2622-LL-75X-4 75 µg/g 0.0075 4 oz.D-2622-LL-100X-4 100 µg/g 0.010 4 oz.D-2622-LL-300X-4 300 µg/g 0.030 4 oz.D-2622-LL-500X-4 500 µg/g 0.050 4 oz.D-2622-LL-1000X-4 1000 µg/g 0.100 4 oz.D-2622-LL-CAL-SET$ 450 / 10 x 4 oz.In Isooctane : Toluene (3:1)Set contains the above 10 individual bottlesStandards can be mixed for quantity discounts1 to 4 units $ 60 each per Sulfur Standard5 to 10 units $ 55 each per Sulfur Standardmore than 10 units $ 50 each per Sulfur StandardDesigned forD-2622-98D-6334-98D-6445-99Sulfur MethodsTechnical NoteA well characterized di-n-butyl sulfide starting material is used witha low sulfur Isooctane matrix for RFG/gasoline sulfur standards.Technical NoteWell characterized Thiophene & 2-Methyl thiophene are used in alow sulfur Isooctane/Toluene matrix for this calibration set.Designed forASTM D-3120, D-3246D-3120-96Sulfur Calibration SetD-3120-92-CAL-SETD-3246-96$ 75 / set of 8 x 1 mLIn IsooctaneCat. No. Sulfur Conc. Sulfur Wt. %D-3120-92-BL Blank ———D-3120-92-1X 1 µg/g 0.0001D-3120-92-3X 3 µg/g 0.0003D-3120-92-10X 10 µg/g 0.0010D-3120-92-30X 30 µg/g 0.0030D-3120-92-50X 50 µg/g 0.0050D-3120-92-75X 75 µg/g 0.0075D-3120-92-100X 100 µg/g 0.010Mid Level Sulfur Calibration Standards for use on XRFEnergy Dispersive or Wavelength InstrumentsCat. No. Sulfur Conc. Sulfur Wt. % UnitD-2622-LL-200X-4 200 µg/g 0.020 4 ozD-2622-LL-400X-4 400 µg/g 0.040 4 ozD-2622-LL-600X-4 600 µg/g 0.060 4 ozD-2622-LL-700X-4 700 µg/g 0.070 4 ozD-2622-LL-800X-4 800 µg/g 0.080 4 ozD-2622-LL-900X-4 900 µg/g 0.090 4 ozD-2622-LL-1100X-4 1100 µg/g 0.110 4 ozD-2622-LL-1200X-4 1200 µg/g 0.120 4 ozStandards can be mixed for quantity discounts1 to 4 units $ 60 each per Sulfur Standard5 to 10 units $ 55 each per Sulfur Standardmore than 10 units $ 50 each per Sulfur StandardTechnical NoteWell characterized di-n-butyl sulfide is used in a low sulfurIsooctane matrix for this calibration set.These products require a Hazardous Shipping ChargeStandards of InterestFor the mandatory real world QC samples stipulated in manyASTM Sulfur Methods, see page 56.MemberAccuStandard is an active member in ASTM andstrives to keep abreast of ASTM method revisions. Ifour listed formulation does not meet the most recentmethod revision, please contact Technical Support foran updated product.TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3 55


Traceable Standards for ASTM MethodsSulfur in Gasoline QA/QC StandardsASTM Sulfur QA/QCAccuPetroCheck and AccuPetroTest Real World Gasoline QC StandardsIn cooperation with ASTM D-02 subcommittee 3 and 4, AccuStandard ampuled 21 Real World gasoline reference fuels. Consensus Values havebeen determined for these reference fuels by various ASTM Round Robins to provide Petrochemical Laboratories with a source of well characterizedgasoline standards for use in QA/QC applications and as Single Blind test samples over an extended period of time. As new ASTM D-02.03 andD-02.04 Test methods are promulgated they require mandatory Quality Control testing of real world samples. AccuStandard’s AccuPetroTest &AccuPetroCheck standards are being successfully used to achieve these new Quality Control requirements.QC StandardsCARB Low Sulfur RFG QC StandardASTM-FUEL-QCS-01-PAK $ 60 / 5 x 15 mLParameter Method Value Conc.Total Aromatics D-1319 24.5 Vol.%Total Olefins D-1319 5.3 Vol.%Total Saturates D-1319 58.3 Vol.%Sulfur D-2622 0.0057 Wt.%Sulfur D-4294 0.0078 Wt.%Sulfur D-5453 55.76 µg/gSulfur D-6344 59.31 µg/gBenzene D-5769 0.80 Vol.%Toluene D-5769 4.92 Vol.%Total Aromatics D-5769 23.42 Vol.%Benzene D-6227 0.78 Vol.%Total Olefins D-6550 5.3 Vol.%Conventional Gasoline QC StandardASTM-FUEL-QCS-02-PAK $ 60 / 5 x 15 mLParameter Method Value Conc.Total Aromatics D-1319 34.6 Vol.%Total Olefins D-1319 12.4 Vol.%Total Saturates D-1319 62.8 Vol.%Sulfur D-2622 0.0338 Wt.%Sulfur D-4294 0.0368 Wt.%Sulfur D-5453 317.36 µg/gSulfur D-6344 338.78 µg/gBenzene D-5769 0.55 Vol.%Toluene D-5769 5.53 Vol.%Total Aromatics D-5769 32.51 Vol.%Benzene D-6227 0.52 Vol.%Total Olefins D-6550 12.4 Vol.%AccuPetroCheck QC StandardsTwo of the fuels are available asAccuPetroCheck Consensus Value QCStandards. The AccuPetroCheck CARBand Conventional gasoline referencematerials have all parameters listed on thecertificate with the Consensus Values andthe regression equations forreproducability. Use of these ReferenceMaterials improve the quality of laboratoryresults. The Consensus Values listedreflect initial statistical treatment of thedata at the time the catalog was published.The actual certificate provided with theAccuPetroCheck QC standard will havethe accepted Consensus Value based onstatistical treatment of the data.AccuPetroTestSulfur in Diesel Fuel QC StandardSBPT-SDFParameterSulfurLow Sulfur QC Sample$ 25 / 2 x 15 mLApprox. Range20 - 11000 mg/kgSee ASTM Methods D-2622, D-3120, D-3246-92,D-4294, D-5453, for Sulfur Calibration StandardsAccuPetroTest GasolineSBPT-LSGAS$ 25 / 2 x 15 mLParameter Method Approx. RangeSulfur 5453 0 - 50 µg/gSulfur in White Mineral Oil QC StandardSBPT-SWMOParameterSulfur$ 25 / 2 x 15 mLApprox. Range20 - 11000 mg/kgSee ASTM Methods D-2622, D-3120, D-3246-92,D-4294, D-5453 for Sulfur Calibration StandardsOlefin QC SampleSBPT-OLEFINSFC$ 25 / 2 x 15 mLParameter Method Approx. RangeOlefins 6550 1 - 40 Vol.%Sulfur Single BlindAccuPetroTest AlternativeMatrices StandardsAccuStandard has manufactured anumber of Diesel and White MineralOil quality control products containinga gravimetrically prepared amount ofSulfur. Use of these alternativematrix materials can provide furtherevaluation of the QA/QC process inthe laboratory. Two samples will besent for the test parameter and aseparate sealed envelope containingthe gravimetrically prepared sulfurvalues is also provided. The secondsample is for repeatability testing orfor use as a future QA/QC reference.AccuPetroTest Gasoline QCOlefins QC SampleSBPT-OLEFIN$ 25 / 2 x 15 mLParameter Method Approx. RangeTotal Aromatics D-1319 8-60 Vol.%Total Olefins D-1319 1 - 40 Vol.%Total Saturates D-1319 30-80 Vol. %See ASTM Method D-1319 for Sulfur CalibrationStandardsAromatics QC SampleSBPT-AROM$ 25 / 2 x 15 mLParameter Method Approx. RangeTotal Aromatics D-5769 8 - 60 Vol.%See ASTM Methods D-3606, D-5580-95, D-5769-95 forBenzene Calibration StandardsSulfur QC SampleSBPT-SGAS$ 25 / 2 x 15 mLParameter Method Approx. RangeSulfur D-2622 0.0001 - 0.0930 Wt.%Sulfur D-4294 0.0016 - 0.0930 Wt.%Sulfur D-5453 4.0 - 500 µg/gSulfur D-XXXX 1.0 - 1000 µg/gSee ASTM Methods D-2622, D-3120, D-3246-92,D-4294, D-5453 for Sulfur Calibration StandardsBenzene/Toluene QC SampleSBPT-BENZ$ 25 / 2 x 15 mLParameter Method Approx. RangeBenzene D-5769 0.1 - 2.0 Vol.%Toluene D-5769 1.0 - 15 Vol.%See ASTM Methods D-3606, D-5580-95, D-5769-95 forBenzene Calibration StandardsAccuPetroTest Single BlindStandardsPetrochemical Laboratories looking totest the performance of the laboratoryfor a specific parameter can order theSingle Blind AccuPetroTest samplefor the parameter of interest. Tworeal world gasoline samples will besent for the test parameter requestedand a separate sealed envelopecontaining the determinedConsensus Value is also provided.The second sample is forrepeatability testing or as a futureQA/QC reference.56TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


ASTM-FUEL-QCS-01-PAK:56ASTM-FUEL-QCS-02-PAK:56ASTM-P-0010-PAK:54ASTM-P-0020-PAK:54D-2622-LL-1000X-4:55D-2622-LL-100X-4:55D-2622-LL-10X-4:55D-2622-LL-1100X-4:55D-2622-LL-1200X-4:55D-2622-LL-200X-4:55D-2622-LL-300X-4:55D-2622-LL-30X-4:55D-2622-LL-400X-4:55D-2622-LL-500X-4:55D-2622-LL-50X-4:55D-2622-LL-5X-4:55D-2622-LL-600X-4:55D-2622-LL-700X-4:55D-2622-LL-75X-4:55D-2622-LL-800X-4:55D-2622-LL-900X-4:55D-2622-LL-BL-4:55D-2622-LL-CAL-SET:55D-3120-92-CAL-SET:55SBPT-AROM:56SBPT-BENZ:56SBPT-LSGAS:56SBPT-OLEFIN:56SBPT-OLEFINSFC:56SBPT-SDF:56SBPT-SGAS:56SBPT-SWMO:56SCO-100X-4:54SCO-10X-4:54SCO-200X-4:54SCO-25X-4:54SCO-300X-4:54SCO-400X-4:54SCO-500X-4:54SCO-50X-4:54SCO-CAL-4-SET:54SDF-100X-20ML-PAK:53SDF-100X-4:53SDF-10X-20ML-PAK:53SDF-10X-4:53SDF-150X-20ML-PAK:53SDF-150X-4:53SDF-15X-20ML-PAK:53SDF-15X-4:53SDF-1X-20ML-PAK:53SDF-1X-4:53SDF-200X-20ML-PAK:53SDF-200X-4:53SDF-2X-20ML-PAK:53SDF-2X-4:53SDF-300X-20ML-PAK:53SDF-300X-4:53SDF-30X-20ML-PAK:53SDF-30X-4:53SDF-3X-20ML-PAK:53SDF-3X-4:53SDF-400X-20ML-PAK:53SDF-400X-4:53SDF-4X-20ML-PAK:53SDF-4X-4:53SDF-500X-20ML-PAK:53SDF-500X-4:53SDF-50X-20ML-PAK:53SDF-50X-4:53SDF-5X-20ML-PAK:53SDF-5X-4:53SDF-600X-20ML-PAK:53SDF-600X-4:53SDF-7.5X-20ML-PAK:53SDF-7.5X-4:53SDF-70X-20ML-PAK:53SDF-70X-4:53SDF-BL-20ML-PAK:53SDF-BL-4:53SDF-CAL-4-SET:53SK-100X-20ML-PAK:54SK-100X-4:54SK-10X-20ML-PAK:54SK-10X-4:54SK-1X-20ML-PAK:54SK-1X-4:54SK-200X-20ML-PAK:54SK-200X-4:54SK-20X-20ML-PAK:54SK-20X-4:54SK-30X-20ML-PAK:54SK-30X-4:54SK-3X-20ML-PAK:54SK-3X-4:54SK-40X-20ML-PAK:54SK-40X-4:54SK-50X-20ML-PAK:54SK-50X-4:54SK-5X-20ML-PAK:54SK-5X-4:54SK-7.5X-20ML-PAK:54SK-7.5X-4:54SK-BL-20ML-PAK:54SK-BL-4:54SK-CAL-4-SET:54SK-HD-100X-4:54SK-HD-10X-4:54SK-HD-150X-4:54SK-HD-15X-4:54SK-HD-1X-4:54SK-HD-200X-4:54SK-HD-20X-4:54SK-HD-2X-4:54SK-HD-300X-4:54SK-HD-30X-4:54SK-HD-3X-4:54SK-HD-400X-4:54SK-HD-40X-4:54SK-HD-4X-4:54SK-HD-500X-4:54SK-HD-50X-4:54SK-HD-5X-4:54SK-HD-600X-4:54SK-HD-7.5X-4:54SK-HD-70X-4:54SK-HD-BL-4:54SK-HD-CAL-4-SET:54SRO-100X-4:54SRO-150X-4:54SRO-200X-4:54SRO-300X-4:54SRO-35X-4:54SRO-400X-4:54SRO-70X-4:54SRO-CAL-4-SET:54STP-100X-4:55STP-10X-4:55STP-1X-4:55STP-200X-4:55STP-20X-4:55STP-2X-4:55STP-300X-4:55STP-30X-4:55STP-3X-4:55STP-40X-4:55STP-5X-4:55STP-60X-4:55STP-BL-4:55STP-CAL-SET:55SWMO-100X-20ML-PAK:53SWMO-100X-4:53SWMO-10X-20ML-PAK:53SWMO-10X-4:53SWMO-150X-20ML-PAK:53SWMO-150X-4:53SWMO-15X-20ML-PAK:53SWMO-15X-4:53SWMO-1X-20ML-PAK:53SWMO-1X-4:53SWMO-200X-20ML-PAK:53SWMO-200X-4:53SWMO-2X-20ML-PAK:53SWMO-2X-4:53SWMO-300X-20ML-PAK:53SWMO-300X-4:53SWMO-30X-20ML-PAK:53SWMO-30X-4:53SWMO-3X-20ML-PAK:53SWMO-3X-4:53SWMO-400X-20ML-PAK:53SWMO-400X-4:53SWMO-4X-20ML-PAK:53SWMO-4X-4:53SWMO-500X-20ML-PAK:53SWMO-500X-4:53SWMO-50X-20ML-PAK:53SWMO-50X-4:53SWMO-5X-20ML-PAK:53SWMO-5X-4:53SWMO-600X-20ML-PAK:53SWMO-600X-4:53SWMO-7.5X-20ML-PAK:53SWMO-7.5X-4:53SWMO-70X-20ML-PAK:53SWMO-70X-4:53SWMO-BL-20ML-PAK:53SWMO-BL-4:53SWMO-CAL-4-SET:53SWMO-LT-100X-20ML-PAK:53SWMO-LT-100X-4:53SWMO-LT-10X-20ML-PAK:53SWMO-LT-10X-4:53SWMO-LT-150X-20ML-PAK:53SWMO-LT-150X-4:53SWMO-LT-15X-20ML-PAK:53SWMO-LT-15X-4:53SWMO-LT-1X-20ML-PAK:53SWMO-LT-1X-4:53SWMO-LT-200X-20ML-PAK:53SWMO-LT-200X-4:53SWMO-LT-2X-20ML-PAK:53SWMO-LT-2X-4:53SWMO-LT-300X-20ML-PAK:53SWMO-LT-300X-4:53SWMO-LT-30X-20ML-PAK:53SWMO-LT-30X-4:53SWMO-LT-3X-20ML-PAK:53SWMO-LT-3X-4:53SWMO-LT-400X-20ML-PAK:53SWMO-LT-400X-4:53SWMO-LT-4X-20ML-PAK:53SWMO-LT-4X-4:53SWMO-LT-500X-20ML-PAK:53SWMO-LT-500X-4:53SWMO-LT-50X-20ML-PAK:53SWMO-LT-50X-4:53SWMO-LT-5X-20ML-PAK:53SWMO-LT-5X-4:53SWMO-LT-600X-20ML-PAK:53SWMO-LT-600X-4:53SWMO-LT-7.5X-20ML-PAK:53SWMO-LT-7.5X-4:53SWMO-LT-70X-20ML-PAK:53SWMO-LT-70X-4:53SWMO-LT-BL-20ML-PAK:53SWMO-LT-BL-4:53SWMO-LT-CAL-4-SET:53


Traceable Standards for ASTM MethodsASTM D-3230 Salts in Crude OilMixed Salt SolutionD-3230-89-1$ 75 / 100 mLD-3230-89-5$ 150 / 500 mLAt stated conc. in Alcohol Solution (1-butanol:MeOH)(63:37) tr. H 2O 3 comps.Calcium chlorideMagnesium chloride10 µg/mL20 µg/mLSodium chlorideASTM D-3231 Phosphorus in GasolineD3231 Meets EPA Guidelines for RFG AnalysisOriginally designed for D3230-9970 µg/mLOriginally designed for D3231-99Element Quantity Cat. No. PriceMatrixConc.Phosphorus 100 mL ICP-41W-1 $ 34H 2O1000 µg/mLPhosphorus 500 mL ICP-41W-5 $ 67H 2O1000 µg/mLASTM D-3237 Lead in Gasoline by AA SpectroscopyD3237 Meets EPA Guidelines for RFG AnalysisLead Standard Calibration CurveOriginally designed for D3237-97D-3237-CAL-SET$ 210 / 4 x 100 mLSet includes the following Catalog Numbers:Cat. No.Price / UnitBlank 1% Aliquot 336/MIBK D-3237-01 $ 20 / 100 mL0.02 g Pb / gal ( 5.3 mg Pb/ L) D-3237-02 80 / 100 mLin 1% Aliquat 336 / MIBK0.05 g Pb / gal ( 13.2 mg Pb/ L) D-3237-03 80 / 100 mLin 1% Aliquat 336 / MIBK0.10 g Pb / gal ( 26.4 mg Pb/ L) D-3237-04 80 / 100 mLin 1% Aliquat 336 / MIBKASTM D-3605 (Reapproved ‘95) Trace Metals in GasTurbine Fuels by AA & Flame Emission SpectroscopyD-3605-91 Trace Metals StandardD-3605-91-1At stated conc. in 1,2,3,4-TetrahydronaphthaleneNa (Sodium)Pb (Lead)250 µg/mL250 µg/mLCa (Calcium)V (Vanadium)Originally designed for D3605-91$ 165 / 1 x 100 mL4 comps.250 µg/mL250 µg/mLASTM D-3610 Total Cobalt in Alumina-Base Cobalt-Molybdenum Catalyst by Potentiometric TitrationCobalt Oxide StandardD-3610-93-1Cobalt oxide @ 1500 µg/mL in WaterOriginally designed for D3610-88 (re-approved 1993)$ 50 / 1 x 100 mLASTM D-3831 Manganese in Gasoline by AA SpectroscopyOriginally designed for D3831-98Manganese Stock SolutionD-3831 $ 65 / 1 x 100 mLManganese @ 1.0 g Mn / gal (264.2 mg Mn / L) in Methyl isobutyl ketoneASTM D-4628 Barium, Calcium, Magnesium & ZincAnalysis of Ba, Ca, Mg & Zn in Unused Lubricating Oil.See page 46-52 for AccuStandard’s comprehensive line of CertifiedOil Dissolved Wear Metal Calibration Standards.ASTM MethodsASTM D-4628 Barium, Calcium, Magnesium & Zinc in Unused Lubricating OilLubricating Oil, Elements (Nominal Value) Wt.%ASTM-P-0113-SETOriginally designed for D4628-97$ 2850 / 17 x 100 mLBa Ca Mg P S ZnCat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)ASTM-P-0113-01 0.025 0.600 0.100 0.005 0.175 0.060ASTM-P-0113-02 0.000 0.500 0.150 0.200 0.050 0.080ASTM-P-0113-03 0.100 0.400 0.350 0.150 0.300 0.180ASTM-P-0113-04 0.175 0.260 0.225 0.250 0.150 0.120ASTM-P-0113-05 0.150 0.005 0.450 0.005 0.450 0.070ASTM-P-0113-06 0.000 0.400 0.500 0.025 0.350 0.100ASTM-P-0113-07 0.100 0.300 0.325 0.060 0.250 0.120ASTM-P-0113-08 0.200 0.200 0.250 0.100 0.450 0.100ASTM-P-0113-09 0.050 0.060 0.100 0.080 0.300 0.130ASTM-P-0113-10 0.075 0.060 0.400 0.050 0.200 0.050ASTM-P-0113-11 0.010 0.050 0.300 0.120 0.100 0.075ASTM-P-0113-12 0.000 0.025 0.200 0.150 0.200 0.130ASTM-P-0113-13 0.175 0.005 0.375 0.200 0.400 0.150ASTM-P-0113-14 0.005 0.170 0.175 0.250 0.550 0.110ASTM-P-0113-15 0.000 0.100 0.425 0.100 0.200 0.200ASTM-P-0113-16 0.005 0.010 0.275 0.010 0.600 0.250ASTM-P-0113-17 0.000 0.000 0.000 0.000 0.000 0.000These products require a Hazardous Shipping ChargeWorking Level Standards &Continuing Calibration Check (CCC)TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 57


Traceable Standards for ASTM MethodsASTM D-4629 Trace Nitrogen in Liquid Petroleum Hydrocarbons by Syringe/Inlet OxidativeCombustion and Chemiluminescence Detection. IP Designation 379/88ASTM MethodsMethod D4629 is used to determine trace total nitrogen naturally found in liquid hydrocarbons boiling from 50to 400°C with viscosities between 0.2 and 10 cSt. This method monitors feed stocks for nitrogen to prevent thepoisoning of some process catalysts when trace nitrogenous materials are present.Stock Nitrogen Solution for Low Boiling SolventsD-4629-91-LB-CON$ 20 / 1 x 1 mLTechnical NoteD-4629-91-LB-CON-PAKNitrogen @ 1000 µg/mL in IsooctanePyridine @ 5.65 mg/mL in IsooctaneStock Nitrogen Solution for High Boiling SolventsD-4629-91-HB-COND-4629-91-HB-CON-PAKNitrogen @ 1000 µg/mL in Toluene : Acetone (9:1)Carbazole @ 11.95 mg/mL in Toluene : Acetone (9:1)SAVE 20% $ 80 / 5 x 1 mLNitrogen Calibration Set for Low Boiling SolventsD-4629-91-LB-CAL-SET$ 75 / set of 7 x 1 mLCat. No. Description Concentration Price / UnitD-4629-91-LB-0.3X Nitrogen @ 0.3 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-1X Nitrogen @ 1 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-10X Nitrogen @ 10 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-25X Nitrogen @ 25 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-50X Nitrogen @ 50 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-75X Nitrogen @ 75 µg/mL in Isooctane $ 20 / 1 x 1 mLD-4629-91-LB-100X Nitrogen @ 100 µg/mL in Isooctane $ 20 / 1 x 1 mL$ 20 / 1 x 1 mLSAVE 20% $ 80 / 5 x 1 mLOriginally designed for D4629-96Nitrogen is introduced usingPyridine.Technical NoteNitrogen is introducedusing Carbazole.Ready-to-Inject PetrochemicalStandards & Calibration CurvesReduce CostsIncrease Time Spent forSample AnalysisAre Validated AgainstIndependent LotsInclude Internal Standardsor SurrogatesFollow ASTM MethodGuidelinesAllow Direct Transfer toAutosampler VialsNitrogen Calibration Set for High Boiling SolventsD-4629-91-HB-CAL-SET$ 75 / set of 7 x 1 mLCat. No. Description Concentration Price / UnitD-4629-91-HB-0.3X Nitrogen @ 0.3 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-1X Nitrogen @ 1 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-10X Nitrogen @ 10 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-25X Nitrogen @ 25 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-50X Nitrogen @ 50 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-75X Nitrogen @ 75 µg/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-100X Nitrogen @ 100 µg/mL in Toluene $ 20 / 1 x 1 mLLow level Nitrogen Calibration SetASTM-P-0070-SET$ 75 / 6 x 1 mLCat. No. Description Concentration UnitASTM-P-0070-BL Isooctane Blank 1 x 1 mLASTM-P-0070-1X Nitrogen @ 0.5 µg/g in Isooctane 1 x 1 mLASTM-P-0070-2X Nitrogen @ 1.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-4X Nitrogen @ 2.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-10X Nitrogen @ 5.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-20X Nitrogen @ 10.0 µg/g in Isooctane 1 x 1 mLTechnical NoteNitrogen is introducedusing Aniline.Low level Nitrogen & Sulfur Calibration SetASTM-P-0071-SET$ 50 / 4 x 1 mLCat. No. Description UnitASTM-P-0071-BL Benzene Blank 1 x 1 mLASTM-P-0071-01 Nitrogen @ 0.25 µg/g & Sulfur @ 0.25 µg/g in Benzene 1 x 1 mLASTM-P-0071-02 Nitrogen @ 0.50 µg/g & Sulfur @ 0.50 µg/g in Benzene 1 x 1 mLASTM-P-0071-03 Nitrogen @ 1.00 µg/g & Sulfur @ 1.00 µg/g in Benzene 1 x 1 mLTechnical NoteThe Nitrogen isintroduced using Anilineand the Sulfur isintroduced using di-n-Butyl sulfide.58TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Traceable Standards for ASTM MethodsASTM D-4927 Elemental Analysis of Lubricant and Additive Components - Ba, Ca, P, S and Znby WD-XRF SpectroscopySee pages 46 to 52 for AccuStandard's comprehensive line of Certified Oil Dissolved Wear Metalcalibration standards designed for XRF Applications.ASTM D-4929 Organic Chloride Content in Crude Oil - Test Method B Combustion andMicrocoulometryOriginally designed for D4929-99Working Level Chlorine StandardD-4929-94D-4929-94-PAK$ 10 / 1 x 5 mLSAVE $ 40 / 5 x 5 mLStock Chlorine StandardD-4929-94-100XD-4929-94-100X-PAK$ 15 / 1 x 5 mLSAVE $ 60 / 5 x 5 mLASTM MethodsChlorine @ 10 µg/mL in IsooctaneChlorine @ 1000 µg/mL in IsooctaneASTM D-4951 Additive Elements in Lubricating Oils by Inductively Coupled Plasma AtomicEmission SpectrometryOriginally designed for D4951-9620 Wear Metal Multi-Element Standardcontaining no metallic sulfonatesConc.(µg/g) Cat. No. Price10 WM-20-NMS-1X-1 $ 15030 WM-20-NMS-3X-1 15050 WM-20-NMS-5X-1 150100 WM-20-NMS-10X-1 170300 WM-20-NMS-30X-1 230500 WM-20-NMS-50X-1 350900 WM-20-NMS-90X-1 500WM-20-NMS-1-SET $ 1450set of above 7 x 100 mLEach Wear Metal Standard contains thebelow list of 20 elements in hydrocarbon oil at thestated concentrationAl (Aluminum)B (Boron)Ba (Barium)Ca (Calcium)Cd (Cadmium)Cr (Chromium)Cu (Copper)Fe (Iron)Mg (Magnesium)Mn (Manganese)Mo (Molybdenum)Na (Sodium)Ni (Nickel)P (Phosphorus)Pb (Lead)Si (Silicon)Sn (Tin)Ti (Titanium)V (Vanadium)Zn (Zinc)Recommended Internal Standard (IS)Sulfur free Organometallic (IS) Sulfur free Organometallic (IS)Element 1000 µg/g Price 5000 µg/g PriceCat. No. 50 mL Cat. No. 50 mLCobalt WM-NMS-14 $ 75 WM-NMS-14-5X $ 110ASTM D-5056 Trace Metals in Petroleum Coke by Atomic AbsorptionOriginally designed for D5056-96Element @ 1000 µg/mL Unit Cat. No. PriceMatrixAluminum 100 mL AA01N-1 $ 13HNO 3500 mL AA01N-5 33Calcium 100 mL AA09N-1 12HNO 3500 mL AA09N-5 30Iron 100 mL AA27N-1 12HNO 3500 mL AA27N-5 30Nickel 100 mL AA37N-1 12HNO 3500 mL AA37N-5 30Element @ 1000 µg/mL Unit Cat. No. PriceMatrixSilicon 100 mL AA52W-1 $ 13H 2O tr. NaOH 500 mL AA52W-5 33Sodium 100 mL AA54N-1 13HNO 3500 mL AA54N-5 33Vanadium 100 mL AA67N-1 13HNO 3500 mL AA67N-5 33These products require a Hazardous Shipping ChargeTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 59


Traceable Standards for ASTM MethodsASTM MethodsASTM D-5059 Lead in Gasoline by X-Ray Spectroscopy IP Designation 228/79D5059 Meets EPA Guidelines for RFG AnalysisPart A - Lead in Gasoline StandardsD-5059-A-CAL-SET$ 450 / set of 7 x 4 ozThe Set contains the following 7 solutions in isooctaneCat. No. Lead Concentration Price /g Pb/US gal g Pb/ UK gal mg Pb/mL UnitD-5059-A-01 0.0000 0.000 0.000 $ 10 / 4 ozD-5059-A-02 0.1000 0.120 0.026 80 / 4 ozD-5059-A-03 1.0000 1.200 0.264 80 / 4 ozD-5059-A-04 2.0000 2.400 0.528 80 / 4 ozD-5059-A-05 3.0000 3.600 0.793 80 / 4 ozD-5059-A-06 4.0000 4.800 1.057 80 / 4 ozD-5059-A-07 5.0000 6.000 1.321 80 / 4 ozPart C - Lead in Gasoline StandardsD-5059-C-CAL-SET$ 450 / set of 7 x 4 ozThe Set contains the following 7 solutions in isooctaneCat. No. Lead Concentration Price /g Pb/US gal g Pb/ UK gal µg Pb/mL UnitD-5059-C-01 0.0000 0.000 0.000 $ 10 / 4 ozD-5059-C-02 0.0010 0.001 0.264 80 / 4 ozD-5059-C-03 0.0050 0.006 1.321 80 / 4 ozD-5059-C-04 0.0100 0.012 2.642 80 / 4 ozD-5059-C-05 0.0500 0.060 13.209 80 / 4 ozD-5059-C-06 0.1000 0.120 26.417 80 / 4 ozD-5059-C-07 0.3000 0.360 79.252 80 / 4 ozInternal StandardD-5059-IS-4D-5059-IS-10ML-PAKOriginally designed for D-5059-98$ 80 / 1 x 4 ozbottle$ 60 / 5 x 10 mLampulesBismuth @ 0.793 mg/mL (3.00 g/US gal)(3.60 g/UK gal) in Mineral oilTechnical NoteAll D-5059 Certificates have theconcentrations for the Standard listedin three convenient Lead Concentrationunits.Technical NoteThese standards areformulated to measure the leadcontent in gasoline for both highand low concentrations usingbismuth as an internal standard.For long term stability and easeof use the internal standard isprovided in two convenientpackaging sizes. The bulk 100mL (4 oz.) bottles are designedfor laboratories analyzing manysamples while the 10 mLampules are for laboratoriesthat have limited requests forthe test method. For bulkquantities of the internalstandard packaged in singleuseampules, contact ourtechnical department for aquotation. Bulk volumes of 250mL or more can be sealed intoampules (up to 20 mL size).Use of our ampulling servicescan provide substantial savingsfor the Laboratory.ASTM D-5184 (Reapproved 1995) Aluminum and Silicon in Fuel Oils by Ashing, Fusion, ICP-AES Spectrometry & AA SpectrometryOriginally designed for D5184-91Tartaric Acid / Hydrochloric AcidSolutionD-5184-91-TA-5Tartaric acid @ 0.5% w/v in 4% HClSilicon Standard SolutionD-5184-91-SI-1D-5184-91-SI-5Silicon @ 1000 µg/mL in trace NaOH$ 20 / 1 x 500 mL$ 34 / 1 x 100 mL$ 67 / 1 x 500 mLAluminum Standard SolutionD-5184-91-AL-1D-5184-91-AL-5Al @ 1000 µg/mL in 5 % HCl$ 34 / 1 x 100 mL$ 67 / 1 x 500 mLTechnical NoteContact us by phone/e-mail attechservice@accustandard.comand the our TechnicalDepartment for Ready-to-Aspirate working levelcalibration curves designed foryour laboratories' specificcalibration ranges.These products require a Hazardous Shipping ChargeASTM D-5185 Additive Elements, Wear Metals, & Contaminants in Used Lubricating Oils byICP-AESOriginally designed for D5185-9721 Wear Metal Multi-Element StandardContaining No Metallic SulfonatesConc.(µg/g) Cat. No. Price10 WM-21-NMS-1X-1 $ 16030 WM-21-NMS-3X-1 16050 WM-21-NMS-5X-1 160100 WM-21-NMS-10X-1 180300 WM-21-NMS-30X-1 240500 WM-21-NMS-50X-1 350WM-21-NMS-1-SET $ 1050set of above 6 x 100 mLRecommended Internal Standard (IS)Sulfur free Organometallic (IS) Sulfur free Organometallic (IS)Element @ 1000 µg/g Price @ 5000 µg/g PriceCat. No. 50 mL Cat. No. 50 mLCobalt WM-NMS-14 $ 75 WM-NMS-14-5X $ 110Each Wear Metal Standard containsthe below list of 21 elements in hydrocarbon oilat the stated concentrationAg (Silver)Al (Aluminum)B (Boron)Ba (Barium)Ca (Calcium)Cd (Cadmium)Cr (Chromium)Cu (Copper)Fe (Iron)Mg (Magnesium)Mn (Manganese)Mo (Molybdenum)Na (Sodium)Ni (Nickel)P (Phosphorus)Pb (Lead)Si (Silicon)Sn (Tin)Ti (Titanium)V (Vanadium)Zn (Zinc)Technical NoteThis calibration curve has beenformulated with startingmaterials containing no metalsulfonates. So a sulfurcalibration curve can easily bedeveloped using a highconcentration sulfur standard.60TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Traceable Standards for ASTM MethodsASTM D-5453 Total Sulfur in Light Hydrocarbons, Motor Fuels and Oils byUltraviolet FluorescenceD5059 Meets EPA Guidelines for RFG AnalysisLow Level Sulfur SetD-5453-LL-SET$ 90 / 5 x 2 mLThe set contains the following 5 standards in IsooctaneCat. No. Description UnitD-5453-LL-BL Sulfur Blank 2 mLD-5453-LL-01 Sulfur @ 0.5 ng/µL 2 mLD-5453-LL-02 Sulfur @ 2.5 ng/µL 2 mLD-5453-LL-03 Sulfur @ 5.0 ng/µL 2 mLD-5453-LL-04 Sulfur @ 10.0 ng/µL 2 mLMid Level Sulfur SetD-5453-ML-SET$ 90 / 6 x 2 mLThe set contains the following 5 standards in IsooctaneCat. No. Description UnitD-5453-ML-BL Sulfur Blank 2 mLD-5453-ML-01 Sulfur @ 5.0 ng/µL 2 mLD-5453-ML-02 Sulfur @ 25 ng/µL 2 mLD-5453-ML-03 Sulfur @ 50 ng/µL 2 mLD-5453-ML-04 Sulfur @ 100 ng/µL 2 mLD-5453-ML-05 Sulfur @ 200 ng/µL 2 mLReal World Sulfur in Various Gasoline &Fuels QC SamplesSBPT-LSGAS$ 25 / 2 x 15 mLParameter Method Approx .RangeSulfur D-5453-00 0 - 50 µg/gHigh Level Sulfur SetOriginally designed for D5453-00D-5453-HL-SET$ 90 / 5 x 2 mLThe set contains the following 5 standards in IsooctaneCat. No. Description UnitD-5453-HL-BL Sulfur Blank 2 mLD-5453-HL-01 Sulfur @ 100 ng/µL 2 mLD-5453-HL-02 Sulfur @ 250 ng/µL 2 mLD-5453-HL-03 Sulfur @ 500 ng/µL 2 mLD-5453-HL-04 Sulfur @ 1000 ng/µL 2 mLD5453 Meets EPA Guidelines forRFG AnalysisASTM MethodsASTM D-5600 Trace Metals in Petroleum Coke by ICP-AESMulti-Element Calibration StandardD-5600-01-1$ 225 / 1 x 100 mL500 µg/mL each in 2-5% HNO 3tr. HF 12 comps.AluminumBariumCalciumIronMagnesiumManganeseNickelSiliconSodiumTitaniumVanadiumZincThese products require a Hazardous Shipping ChargeHydrochloric Acid DiluentD-5600-BLH-5D-5600-BLH-L-VAP20% HCl in ASTM Type II waterLithium Borate DiluentD-5600-LIB-1D-5600-LIB-52.0% Lithium Borate in 10% HClOriginally designed for D5600-98$ 50 / 1 x 500 mL$ 65 / L (2 x 500 mL)$ 125 / 1 x 100 mL$ 180 / 1 x 500 mLTechnical NoteD-5600 Ready-to-AspirateStandardsAccuStandard has formulated thefollowing stock standards forASTM Method D-5600. We haveprepared numerous Ready-to-Aspirate ICP multi-elementsolutions. Should your companywant to eliminate the preparationprocess for Inorganic standardscontact our Technical Departmentfor a quote on a Ready-to-Aspirate working level Inorganicstandard.Tens of thousands of Standards Ready-to-ShipTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 61


Traceable Standards for ASTM MethodsASTM MethodsASTM D-5708 Nickel, Vanadium, & Iron in Crude Oils & Residual Fuels by ICP-AESTest Method A - ICP with an Organic Solvent Specimen SolutionSulfur and Metals in Mineral OilASTM-P-0102-SET$ 1850 / 100 mLSulfur Iron Nickel VanadiumCat. No. Conc. Conc. Conc. Conc. Price(Wt. %) (µg/g) (µg/g) (µg/g) 100 mLASTM-P-0102-01 0.00 0 0 0 $ 200ASTM-P-0102-02 0.50 300 10 500 200ASTM-P-0102-03 1.00 500 100 25 200ASTM-P-0102-04 - 100 80 250 200ASTM-P-0102-05 2.00 200 40 100 200ASTM-P-0102-06 2.50 400 5 400 200ASTM-P-0102-07 3.00 0 60 300 200ASTM-P-0102-08 3.50 500 0 200 200ASTM-P-0102-09 - 100 100 0 200ASTM-P-0102-10 4.50 300 50 250 200ASTM-P-0102-11 5.00 200 20 500 200ASTM-P-0102-12 5.50 50 100 50 200Sulfur and Metals in Residual Fuel OilASTM-P-0103-SET$ 2100 / 100 mLSulfur Iron Nickel VanadiumCat. No. Conc. Conc. Conc. Conc. Price(Wt. %) (µg/g) (µg/g) (µg/g) 100 mLASTM-P-0103-01 0.00 0 0 0 $ 200ASTM-P-0103-02 0.50 300 10 500 200ASTM-P-0103-03 1.00 500 100 25 200ASTM-P-0103-04 - 100 80 250 200ASTM-P-0103-05 2.00 200 40 100 200ASTM-P-0103-06 2.50 400 5 400 200ASTM-P-0103-07 3.00 0 60 300 200ASTM-P-0103-08 3.50 500 0 200 200ASTM-P-0103-09 - 100 100 0 200ASTM-P-0103-10 4.50 300 50 250 200ASTM-P-0103-11 5.00 200 20 500 200ASTM-P-0103-12 5.50 50 100 50 200Test Method B - ICP after Acid Decomposition of SampleStock Multi-Element Aqueous StandardD-5708-B-10X-1D-5708-B-10X-5Each at 100 µg/mL in 2-5% HNO 3$ 60 / 100 mL$ 115 / 500 mL3 comps.Originally designed for D5708-95aStock Multi-Element inMineral OilD-5708-A-10X $ 150 / 100 mL100 µg/g in 20 cSt mineral oil3 comps.IronNickelVanadiumCustom StandardsWhen you have a need for unique AnalyticalStandards, let the experts at AccuStandardassist in designing your formulation. Ourtechnical group, with over 80 years ofcombined analytical experience, will reviewyour request, suggest the most economicaland stable formulation, and provide pricingall within 24 hours.For a Quick Quote, copy the custom quoteform in the back of catalog and fax it back.We will get right back to you.Plus we typically ship within one week afterorder receipt.IronNickelVanadiumWorking Level Multi-Element AqueousStandardD-5708-B-5Each at 10 µg/mL in 2-5% HNO 3IronNickelVanadium$ 105 / 500 mL3 comps.Nitric Acid BlankCLP-BLN-5CLP-BLN-L-SET$ 30 / 500 mL$ 45 / 1 L (2 x 500 mL)5% HNO 3in ASTM Type I WaterThese products require a Hazardous Shipping Charge62TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Traceable Standards for ASTM MethodsASTM D-5762 Nitrogen in Petroleum and Petroleum Products by Boat-InletChemiluminescenceOriginally designed for D5762-98Stock Nitrogen StandardD-5762-95-500X-PAK$ 45 / 5 x 1 mLNitrogen @ 500 µg/mL in Xylene (Acridine @ 6397 µg/mL)Nitrogen Calibration SetD-5762-95-CAL-SET$ 75 / 6 x 1 mLCat. No. Description UnitD-5762-95-BL Xylene Blank 1 x 1 mLD-5762-95-1X Nitrogen @ 1.0 µg/mL in Xylene 1 x 1 mLD-5762-95-5X Nitrogen @ 5.0 µg/mL in Xylene 1 x 1 mLD-5762-95-10X Nitrogen @ 10 µg/mL in Xylene 1 x 1 mLD-5762-95-50X Nitrogen @ 50 µg/mL in Xylene 1 x 1 mLD-5762-95-100X Nitrogen @ 100 µg/mL in Xylene 1 x 1 mLTechnical NoteNitrogen is introducedusing Aniline.ASTM MethodsLow level Nitrogen Calibration SetASTM-P-0070-SET$ 75 / 6 x 1 mLCat. No. Description UnitASTM-P-0070-BL Isooctane Blank 1 x 1 mLASTM-P-0070-1X Nitrogen @ 0.5 µg/g in Isooctane 1 x 1 mLASTM-P-0070-2X Nitrogen @ 1.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-4X Nitrogen @ 2.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-10X Nitrogen @ 5.0 µg/g in Isooctane 1 x 1 mLASTM-P-0070-20X Nitrogen @ 10.0 µg/g in Isooctane 1 x 1 mLTechnical NoteNitrogen is introducedusing Aniline.Low level Nitrogen & Sulfur Calibration SetASTM-P-0071-SET$ 50 / 4 x 1 mLCat. No. Description UnitASTM-P-0071-BL Benzene Blank 1 x 1 mLASTM-P-0071-01 Nitrogen @ 0.25 µg/g & Sulfur @ 0.25 µg/g in Benzene 1 x 1 mLASTM-P-0071-02 Nitrogen @ 0.50 µg/g & Sulfur @ 0.50 µg/g in Benzene 1 x 1 mLASTM-P-0071-03 Nitrogen @ 1.00 µg/g & Sulfur @ 1.00 µg/g in Benzene 1 x 1 mLTechnical NoteThe Nitrogen is introducedusing Aniline and the Sulfuris introduced usingn-Butyl sulfide.ASTM D-5863 Nickel, Vanadium, Iron, & Sodium in Crude Oils & Residual Fuels byFlame AA SpectrometryOriginally designed for D5863-00Test Method A - Sample Decomposition with Acid for Total Ni, V and Fe DeterminationStock Multi-ElementAqueous StandardD-5863-95A-10X-1$ 75 / 1 x 100 mL2-5% HNO 33 comps.µg/mLIron 100Nickel 200µg/mLVanadium 200Matrix BlankNitric Acid BlankCLP-BLN-5CLP-BLN-L-SETIndividual High Concentration Elements in Aqueous Matrix1,000 µg/mL Conc.Element Matrix Unit Cat. No. PriceIron Fe in HNO 3500 mL ICP-27N-5 $ 67Nickel Ni in HNO 3500 mL ICP-37N-5 67Vanadium V 2O 5in HNO 3500 mL ICP-67N-5 675% HNO 3in ASTM Type I Water$ 30 / 500 mLSAVE $ 45 / 1 L (2 x 500 mL)Test Method B - Sample Dilution with Organic Solvent for the Determination of Ni, V and Nausing Oil-Soluble Metals as Calibrants.Stock Multi-Element Standard in MineralOilD-5863-95B-10XAt stated conc. in 20 cst Mineral Oilµg/gSodium 50Nickel 200$ 160 / 1 x 4 oz3 comps.µg/gVanadium 150Standards of InterestSee Wear Metal section for additionalcalibration standards designed for flame AAApplications.These products require a Hazardous Shipping ChargeTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 63


AA01N-1:59AA01N-5:59AA09N-1:59AA09N-5:59AA27N-1:59AA27N-5:59AA37N-1:59AA37N-5:59AA52W-1:59AA52W-5:59AA54N-1:59AA54N-5:59AA67N-1:59AA67N-5:59ASTM-P-0070-SET:58, 63ASTM-P-0071-SET:58, 63ASTM-P-0102-01:62ASTM-P-0102-02:62ASTM-P-0102-03:62ASTM-P-0102-04:62ASTM-P-0102-05:62ASTM-P-0102-06:62ASTM-P-0102-07:62ASTM-P-0102-08:62ASTM-P-0102-09:62ASTM-P-0102-10:62ASTM-P-0102-11:62ASTM-P-0102-12:62ASTM-P-0102-SET:62ASTM-P-0103-01:62ASTM-P-0103-02:62ASTM-P-0103-03:62ASTM-P-0103-04:62ASTM-P-0103-05:62ASTM-P-0103-06:62ASTM-P-0103-07:62ASTM-P-0103-08:62ASTM-P-0103-09:62ASTM-P-0103-10:62ASTM-P-0103-11:62ASTM-P-0103-12:62ASTM-P-0103-SET:62ASTM-P-0113-SET:57CLP-BLN-5:62, 63CLP-BLN-L-SET:62, 63D-3230-89-1:57D-3230-89-5:57D-3237-01:57D-3237-02:57D-3237-03:57D-3237-04:57D-3237-CAL-SET:57D-3605-91-1:57D-3610-93-1:57D-3831:57D-4629-91-HB-0.3X:58D-4629-91-HB-100X:58D-4629-91-HB-10X:58D-4629-91-HB-1X:58D-4629-91-HB-25X:58D-4629-91-HB-50X:58D-4629-91-HB-75X:58D-4629-91-HB-CAL-SET:58D-4629-91-HB-CON:58D-4629-91-HB-CON-PAK:58D-4629-91-LB-0.3X:58D-4629-91-LB-100X:58D-4629-91-LB-10X:58D-4629-91-LB-1X:58D-4629-91-LB-25X:58D-4629-91-LB-50X:58D-4629-91-LB-75X:58D-4629-91-LB-CAL-SET:58D-4629-91-LB-CON:58D-4629-91-LB-CON-PAK:58D-4929-94:59D-4929-94-100X:59D-4929-94-100X-PAK:59D-4929-94-PAK:59D-5059-A-01:60D-5059-A-02:60D-5059-A-03:60D-5059-A-04:60D-5059-A-05:60D-5059-A-06:60D-5059-A-07:60D-5059-A-CAL-SET:60D-5059-C-01:60D-5059-C-02:60D-5059-C-03:60D-5059-C-04:60D-5059-C-05:60D-5059-C-06:60D-5059-C-07:60D-5059-C-CAL-SET:60D-5059-IS-10ML-PAK:60D-5059-IS-4:60D-5184-91-AL-1:60D-5184-91-AL-5:60D-5184-91-SI-1:60D-5184-91-SI-5:60D-5184-91-TA-5:60D-5453-HL-SET:61D-5453-LL-SET:61D-5453-ML-SET:61D-5600-01-1:61D-5600-BLH-5:61D-5600-BLH-L-VAP:61D-5600-LIB-1:61D-5600-LIB-5:61D-5708-A-10X:62D-5708-B-10X-1:62D-5708-B-10X-5:62D-5708-B-5:62D-5762-95-500X-PAK:63D-5762-95-CAL-SET:63D-5863-95A-10X-1:63D-5863-95B-10X:63ICP-27N-5:63ICP-37N-5:63ICP-41W-1:57ICP-41W-5:57ICP-67N-5:63SBPT-LSGAS:61WM-20-NMS-1-SET:59WM-20-NMS-10X-1:59WM-20-NMS-1X-1:59WM-20-NMS-30X-1:59WM-20-NMS-3X-1:59WM-20-NMS-50X-1:59WM-20-NMS-5X-1:59WM-20-NMS-90X-1:59WM-21-NMS-1-SET:60WM-21-NMS-10X-1:60WM-21-NMS-1X-1:60WM-21-NMS-30X-1:60WM-21-NMS-3X-1:60WM-21-NMS-50X-1:60WM-21-NMS-5X-1:60WM-NMS-14:59, 60WM-NMS-14-5X:59, 60


Fuel & Hydrocarbon StandardsFuels & Hydrocarbon Standards (in 1 mL of solvent, unless otherwise noted)Individual Fuel & HydrocarbonsFUEL & HYDROCARBON STANDARDS CAS NO. QTY./CONC. MATRIX CAT. NO. UNIT PRICE5-alpha Androstane 438-22-2 1 mg/mL CH 2 Cl 2 GRH-IS 1 mL 1510 mg/mL CH 2 Cl 2 GRH-IS-10X 1 mL 30Arctic Diesel Fuel 68334-30-5-AR 0.5 mg/mL MeOH FU-023 1 mL 1020 mg/mL MeOH FU-023-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-023-D-40X 1 mL 20Aviation (gas) grade 100-LL 0.5 mg/mL MeOH GA-004 1 mL 1020 mg/mL MeOH GA-004-40X 1 mL 2020 mg/mL CH 2 Cl 2 GA-004-D-40X 1 mL 20p-Bromofluorobenzene 460-00-4 2.5 mg/mL Acetone GARH-SS 1 mL 201-Chloro-4-fluorobenzene 352-33-0 2 mg/mL MeOH AK-101.0-IS-10X 1 mL 201-Chlorooctadecane 3386-33-2 1 mg/mL Hexane DRH-007-SS 1 mL 151-Chloro-4-fluorobenzene 352-33-0 1 mg/mL CH 2 Cl 2 GARH-IS 1 mL 152,5-Dibromotoluene 615-59-8 50 µg/mL MeOH GRH-004-SS 1 mL 10500 µg/mL MeOH GRH-004-SS-10X 1 mL 205 mg/mL MeOH GRH-004-SS-100X 1 mL 20Diesel Fuel 0.5 mg/mL MeOH FU-009 1 mL 105 mg/mL CH 2 Cl 2 FU-009-D-10X 1 mL 2020 mg/mL MeOH FU-009-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-009-D-40X 1 mL 20#1 Diesel - Low Sulfur 0.5 mg/mL MeOH FU-013 1 mL 1020 mg/mL MeOH FU-013-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-013-D-40X 1 mL 20#2 Diesel Fuel 68334-30-5 50 mg/mL Acetone AK-102-LCS-R1-10X 1 mL 20#2 Diesel Fuel (Extra Low Sulfur) 68476-43-6 0.5 mg/mL MeOH FU-017 1 mL 105 mg/mL CH 2 Cl 2 FU-017-D-10X 1 mL 205 mg/mL Acetone AK-102.0-LCS 1 mL 1050 mg/mL Acetone AK-102.0-LCS-10X 1 mL 2020 mg/mL MeOH FU-017-40X 1 mL 2020 mg/mL CH2Cl2 FU-017-D-40X 1 mL 20#2 Diesel Fuel (Low Sulfur) - 25% Weathered 5 mg/mL CH 2 Cl 2 FD2-W25-10X 1 mL 25#2 Diesel Fuel (Low Sulfur) - 50% Weathered 5 mg/mL CH 2 Cl 2 FD2-W50-10X 1 mL 25#2 Diesel Fuel (Low Sulfur) - 75% Weathered 5 mg/mL CH 2 Cl 2 FD2-W75-10X 1 mL 25#2 Diesel Fuel - 25% Weathered 5 mg/mL CH 2 Cl 2 FD2-W25-R1-10X 1 mL 25#2 Diesel Fuel - 50% Weathered 5 mg/mL CH 2 Cl 2 FD2-W50-R1-10X 1 mL 25#2 Diesel Fuel - 75% Weathered 5 mg/mL CH 2 Cl 2 FD2-W75-R1-10X 1 mL 25Docosane 629-97-0 50 % w/w Toluene D-5186-91-PM 1 mL 20n-Dodecane 112-40-3 5 mg/mL MeOH AS-E0238 1 mL 321.5 % w/w Isooctane M-GRA-SCS-AS 1 mL 10#1 Fuel oil 70892-10-3 0.5 mg/mL MeOH FU-001 1 mL 1020 mg/mL MeOH FU-001-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-001-D-40X 1 mL 20#2 Fuel oil 68476-30-2 0.5 mg/mL MeOH FU-002 1 mL 1020 mg/mL MeOH FU-002-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-002-D-40X 1 mL 20#3 Fuel oil 0.5 mg/mL Hexane FU-003 1 mL 1020 mg/mL Hexane FU-003-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-003-D-40X 1 mL 20#4 Fuel oil 68476-31-3 0.5 mg/mL Hexane FU-004 1 mL 1020 mg/mL Hexane FU-004-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-004-D-40X 1 mL 20#5 Fuel Oil 0.5 mg/mL Hexane FU-007 1 mL 1020 mg/mL Hexane FU-007-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-007-D-40X 1 mL 20#6 Fuel Oil 68553-00-4 0.5 mg/mL Hexane FU-008 1 mL 1020 mg/mL Hexane FU-008-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-008-D-40X 1 mL 20Gasoline - Regular, unleaded 0.5 mg/mL MeOH GA-001 1 mL 105 mg/mL MeOH GA-001-10X 1 mL 2020 mg/mL MeOH GA-001-40X 1 mL 2220 mg/mL CH 2 Cl 2 GA-001-D-40X 1 mL 20Gasoline - Premium 0.5 mg/mL MeOH GA-003 1 mL 1020 mg/mL MeOH GA-003-40X 1 mL 2020 mg/mL CH 2 Cl 2 GA-003-D-40X 1 mL 20Hydraulic Fluid 64742-54-7 20 mg/mL CH 2 Cl 2 FU-020-D-40X 1 mL 20Jet Reference Fuel - Type I 0.5 mg/mL MeOH FU-011 1 mL 1020 mg/mL MeOH FU-011-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-011-D-40X 1 mL 20JP-4 (Jet Fuel) 0.5 mg/mL MeOH FU-010 1 mL 1020 mg/mL MeOH FU-010-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-010-D-40X 1 mL 20JP-5 Fuel 0.5 mg/mL MeOH FU-012 1 mL 1020 mg/mL MeOH FU-012-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-012-D-40X 1 mL 20JP-7 Fuel 0.5 mg/mL MeOH FU-014 1 mL 1020 mg/mL MeOH FU-014-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-014-D-40X 1 mL 20JP-8 Fuel 0.5 mg/mL MeOH FU-015 1 mL 1020 mg/mL MeOH FU-015-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-015-D-40X 1 mL 20JP-TS Aviation Fuel 64742-47-8 0.5 mg/mL MeOH FU-016 1 mL 1020 mg/mL MeOH FU-016-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-016-D-40X 1 mL 20118TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Fuel & Hydrocarbon StandardsFuels & Hydrocarbon Standards (in 1 mL of solvent, unless otherwise noted)FUEL & HYDROCARBON STANDARDS CAS NO. QTY./CONC. MATRIX CAT. NO. UNIT PRICEJP-10 Aviation Fuel 2825-82-3 0.5 mg/mL MeOH FU-022 1 mL 1020 mg/mL MeOH FU-022-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-022-D-40X 1 mL 20Kerosene - 25% Weathered 5 mg/mL CH 2 Cl 2 FK-W25-10X 1 mL 25Kerosene - 50% Weathered 5 mg/mL CH 2 Cl 2 FK-W50-10X 1 mL 25Kerosene - 75% Weathered 5 mg/mL CH 2 Cl 2 FK-W75-10X 1 mL 25Kerosene 8008-20-6 0.5 mg/mL MeOH FU-005 1 mL 1020 mg/mL MeOH FU-005-40X 1 mL 205 mg/mL CH 2 Cl 2 FU-005-D-10X 1 mL 2020 mg/mL CH 2 Cl 2 FU-005-D-40X 1 mL 20Lacquer Thinner 1 gram Neat HS-001N 1 gram 200.5 mg/mL MeOH HS-001S 1 mL 1020 mg/mL MeOH HS-001S-40X 1 mL 2020 mg/mL CH 2 Cl 2 HS-001S-D-40X 1 mL 20Mineral Spirits 8030-30-6 1 gram Neat HS-002N 1 gram 200.5 mg/mL MeOH HS-002S 1 mL 1020 mg/mL MeOH HS-002S-40X 1 mL 2020 mg/mL CH 2 Cl 2 HS-002S-D-40X 1 mL 20Naphtha 64742-89-8 1 gram Neat HS-003N 1 gram 200.5 mg/mL MeOH HS-003S 1 mL 1020 mg/mL MeOH HS-003S-40X 1 mL 2020 mg/mL CH 2 Cl 2 HS-003S-D-40X 1 mL 20Nonatriacontane 7194-86-7 750 µg/mL Chloroform DRH-FL-SS-R1 1 mL 601 mg/mL CS 2 DRH-FL-SS 1 mL 203 mg/mL CS 2 DRH-FL-SS-3X 1 mL 27n-Pentadecane 629-62-9 5 mg/mL MeOH AS-E0241 1 mL 32RFA Gasoline (oxygenate-free) 0.5 mg/mL MeOH GA-005 1 mL 1020 mg/mL MeOH GA-005-40X 1 mL 2020 mg/mL CH 2 Cl 2 GA-005-D-40X 1 mL 20RFA Gasoline 10 mL Neat M-GRO-BLNK-10ML 10 mL 10SAE 5W30 Motor Oil 0.5 mg/mL Hexane FU-025-H 1 mL 1020 mg/mL Hexane FU-025-H-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-025-D-40X 1 mL 20SAE 10W30 Motor Oil 0.5 mg/mL Hexane FU-026-H 1 mL 1020 mg/mL Hexane FU-026-H-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-026-D-40X 1 mL 20SAE 10W40 Motor Oil 0.5 mg/mL Hexane FU-027-H 1 mL 1020 mg/mL Hexane FU-027-H-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-027-D-40X 1 mL 20SAE 20W50 Motor Oil 0.5 mg/mL Hexane FU-028-H 1 mL 1020 mg/mL Hexane FU-028-H-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-028-D-40X 1 mL 20SAE 30W Motor Oil 0.5 mg/mL Hexane FU-018-H 1 mL 1020 mg/mL Hexane FU-018-H-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-018-D-40X 1 mL 20SAE 40W Motor Oil 0.5 mg/mL Hexane FU-019-H 1 mL 105 mg/mL Acetone AK-103.0-LCS 1 mL 1020 mg/mL Hexane FU-019-H-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-019-D-40X 1 mL 2025 mg/mL Acetone:CH 2 Cl 2 AK-103.0-LCS-5X 1 mL 20SAE 50W Motor Oil 20 mg/mL CH 2 Cl 2 FU-021-D-40X 1 mL 20Stoddard solvent 8052-41-3 1 gram Neat HS-005N 1 gram 200.5 mg/mL MeOH HS-005S 1 mL 105 mg/mL MeOH HS-005S-10X 1 mL 2020 mg/mL MeOH HS-005S-40X 1 mL 2020 mg/mL CH 2 Cl 2 HS-005S-D-40X 1 mL 20o-Terphenyl 84-15-1 200 µg/mL Acetone AK-102.0-SS 1 mL 101 mg/mL CH 2 Cl 2 DRH-006-SS 1 mL 152 mg/mL Acetone AK-102.0-SS-10X 1 mL 152 mg/mL Acetone GRH-SS 1 mL 17n-Tetradecane 629-59-4 5 mg/mL MeOH AS-E0240 1 mL 32Tetracosane 646-31-1 500 µg/mL CS 2 D-5480-C40-5ML 5 mL 15500 µg/mL Chloroform D-5480-C40-R1-5ML 5 mL 20n-Tridecane 629-50-5 5 mg/mL MeOH AS-E0239 1 mL 321,2,3-Trimethylbenzene 526-73-8 1 mg/mL CH 2 Cl 2 V-028S-D-10X 1 mL 20n-Triacontane-d 62 93952-07-9 500 µg/mL Acetone AK-103.0-SS 1 mL 205 mg/mL Acetone:THF (3:1) AK-103.0-SS-10X 1 mL 305 mg/mL THF DRH-SS 1 mL 30Turbine (Jet) fuel 0.5 mg/mL MeOH FU-006 1 mL 1020 mg/mL MeOH FU-006-40X 1 mL 2020 mg/mL CH 2 Cl 2 FU-006-D-40X 1 mL 20Turpentine 8006-64-2 1 gram Neat HS-004N 1 gram 200.5 mg/mL MeOH HS-004S 1 mL 1020 mg/mL MeOH HS-004S-40X 1 mL 2020 mg/mL CH 2 Cl 2 HS-004S-D-40X 1 mL 20Unleaded Gasoline - 25% Weathered 5 mg/mL MeOH GA-W25-10X 1 mL 25Unleaded Gasoline - 50% Weathered 5 mg/mL MeOH GA-W50-10X 1 mL 25Unleaded Gasoline - 75% Weathered 5 mg/mL MeOH GA-W75-10X 1 mL 25Individual Fuel & HydrocarbonsTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 119


Fuel & Hydrocarbon StandardsIndividual Fuel & HydrocarbonsTPH-SETMotor Fuels & Lubricating Oils SetTPH-001-SET$ 180 / 11 x 1 mLmg/mL Solv. Cat. No. PriceRegular unleaded 20 MeOH GA-001-40X 20Regular leaded 20 MeOH GA-002-40X 20Premium 20 MeOH GA-003-40X 20RFA Gasoline (oxygenate free) 20 MeOH GA-005-40X 20#2 Diesel (conventional) 20 CH 2 Cl 2 FU-009-D-40X 20#1 Diesel (low sulfur) 20 CH 2 Cl 2 FU-013-D-40X 20#2 Diesel (extra low sulfur) 20 CH 2 Cl 2 FU-017-D-40X 20Arctic Diesel 20 CH 2 Cl 2 FU-023-D-40X 20SAE 30 W motor oil 20 CH 2 Cl 2 FU-018-D-40X 20SAE 40 W motor oil 20 CH 2 Cl 2 FU-019-D-40X 20SAE 50 W motor oil 20 CH 2 Cl 2 FU-021-D-40X 20Heating Fuel Oils SetTPH-002-SETComplete Set of Total Petroleum Hydrocarbon (TPH) Pattern Recognition StandardsAccuStandard has assembled the following sets to identify specific petroleum product types found during LUFT/LUST investigations. The sets canbe purchased using one convenient Cat. No. or as individuals. Other concentrations are listed in the Individual Section on the previous pages.$ 115 / 7 x 1 mLmg/mL Solv. Cat. No. Price#1 Fuel Oil 20 CH 2 Cl 2 FU-001-D-40X 20#2 Fuel Oil 20 CH 2 Cl 2 FU-002-D-40X 20#3 Fuel Oil 20 CH 2 Cl 2 FU-003-D-40X 20#4 Fuel Oil 20 CH 2 Cl 2 FU-004-D-40X 20#5 Fuel Oil 20 CH 2 Cl 2 FU-007-D-40X 20#6 Fuel Oil 20 CH 2 Cl 2 FU-008-D-40X 20Kerosene 20 CH 2 Cl 2 FU-005-D-40X 20$ 535 / 33 x 1 mL (includes TPH-001-SET, TPH-002-SET, TPH-003-SET, TPH-004-SET)Aviation Fuels & Oils SetTPH-003-SET$ 160 / 10 x 1 mLmg/mL Solv. Cat. No. PriceAviation (gas) Grade 100 LL 20 CH 2 Cl 2 GA-004-D-40X 20JP-4 Fuel 20 CH 2 Cl 2 FU-010-D-40X 20JP-5 Fuel 20 CH 2 Cl 2 FU-012-D-40X 20JP-7 Fuel 20 CH 2 Cl 2 FU-014-D-40X 20JP-8 Fuel 20 CH 2 Cl 2 FU-015-D-40X 20JP-10 Fuel (Cruise Missile) 20 CH 2 Cl 2 FU-022-D-40X 20JP-TS 20 CH 2 Cl 2 FU-016-D-40X 20Jet Fuel (type 1) 20 CH 2 Cl 2 FU-011-D-40X 20Turbine (Jet A) Fuel 20 CH 2 Cl 2 FU-006-D-40X 20Hydraulic oil 20 CH 2 Cl 2 FU-020-D-40X 20Household & Industrial Solvent SetTPH-004-SET$ 80 / 5 x 1 mLmg/mL Solv. Cat. No. PriceLacquer thinner 20 CH 2 Cl 2 HS-001S-D-40X 20Mineral spirits 20 CH 2 Cl 2 HS-002S-D-40X 20Naphtha 20 CH 2 Cl 2 HS-003S-D-40X 20Turpentine 20 CH 2 Cl 2 HS-004S-D-40X 20Stoddard 20 CH 2 Cl 2 HS-005S-D-40X 20mg/mL Solv. Cat. No. PriceSAE 5W 30 Motor Oil 0.5 Hexane FU-025-H $ 1020.0 Hexane FU-025-H-40X 2020.0 CH 2 Cl 2 FU-025-D-40X 20SAE 10W 30 Motor Oil 0.5 Hexane FU-026-H 1020.0 Hexane FU-026-H-40X 2020.0 CH 2 Cl 2 FU-026-D-40X 20Motor Oil StandardsWeathered LUFT/LUST Fuel Setsmg/mL Solv. Cat. No. PriceSAE 10W 40 Motor Oil 0.5 Hexane FU-027-H $ 1020.0 Hexane FU-027-H-40X 2020.0 CH 2 Cl 2 FU-027-D-40X 20SAE 20W 50 Motor Oil 0.5 Hexane FU-028-H 1020.0 Hexane FU-028-H-40X 2020.0 CH 2 Cl 2 FU-028-D-40X 20Petroleum Products contain many different chemicals, plus synthetic product additives. Typically, these petroleum products are subdivided into twogroups based on their volatility: [a] gasoline related products (more volatile) and [b] fuel related products (less volatile such as kerosene, aviationfuels, diesel fuels and heating oils).Weathered Gasoline SetWGA-SET$ 85 / 4 x 1 mLGasoline - Regular, unleaded 5.0 mg/mL in MeOH GA-001-10X $ 20 / 1 x 1 mLGasoline - Regular, unleaded (25% Weathered) 5.0 mg/mL in MeOH GA-W25-10X $ 25 / 1 x 1 mLGasoline - Regular, unleaded (50% Weathered) 5.0 mg/mL in MeOH GA-W50-10X $ 25 / 1 x 1 mLGasoline - Regular, unleaded (75% Weathered) 5.0 mg/mL in MeOH GA-W75-10X $ 25 / 1 x 1 mLWeathered Kerosene SetWFK-SET$ 85 / 4 x 1 mLKerosene 5.0 mg/mL in CH 2 Cl 2 FU-005-D-10X $ 20 / 1 x 1 mLKerosene (25% Weathered) 5.0 mg/mL in CH 2 Cl 2 FK-W25-10X $ 25 / 1 x 1 mLKerosene (50% Weathered) 5.0 mg/mL in CH 2 Cl 2 FK-W50-10X $ 25 / 1 x 1 mLKerosene (75% Weathered) 5.0 mg/mL in CH 2 Cl 2 FK-W75-10X $ 25 / 1 x 1 mLWeathered #2 Diesel (extra Low Sulfur Content) SetWFD2-SET$ 85 / 4 x 1 mL#2 Diesel fuel (extra Low Sulfur) 5.0 mg/mL in CH 2 Cl 2 FU-017-D-10X $ 20 / 1 x 1 mL#2 Diesel fuel (extra Low Sulfur) (25% Weathered) 5.0 mg/mL in CH 2 Cl 2 FD2-W25-10X $ 25 / 1 x 1 mL#2 Diesel fuel (extra Low Sulfur) (50% Weathered) 5.0 mg/mL in CH 2 Cl 2 FD2-W50-10X $ 25 / 1 x 1 mL#2 Diesel fuel (extra Low Sulfur) (75% Weathered) 5.0 mg/mL in CH 2 Cl 2 FD2-W75-10X $ 25 / 1 x 1 mLWeathered #2 Diesel (Conventional) SetWFD2-R1-SET$ 85 / 4 x 1 mL#2 Diesel fuel (Conventional) 5.0 mg/mL in CH 2 Cl 2 FU-009-D-10X $ 20 / 1 x 1 mL#2 Diesel fuel (Conventional) (25% Weathered) 5.0 mg/mL in CH 2 Cl 2 FD2-W25-R1-10X $ 25 / 1 x 1 mL#2 Diesel fuel (Conventional) (50% Weathered) 5.0 mg/mL in CH 2 Cl 2 FD2-W50-R1-10X $ 25 / 1 x 1 mL#2 Diesel fuel (Conventional) (75% Weathered) 5.0 mg/mL in CH 2 Cl 2 FD2-W75-R1-10X $ 25 / 1 x 1 mLMost analytical methods forpetroleum products focus on severalitems: the level of BTEX, the totalpetroleum hydrocarbon number(TPH), and the fingerprint of thepetroleum product. Depending on thevolatility of the petroleum productspilled, the nature of thecontaminated soil, and the age of thespill, analysis becomes even moredifficult. Weathering, evaporation,and the migration of the lightervolatiles at the contamination site canaffect the fingerprint identificationportion of the fuel products analysis.AccuStandard designed theweathered fuel line to artificiallymimic the weathering, evaporation,and migration process. Use of thesestandards can help in theidentification of the fuel type if it hasbeen present in the ground for sometime, in a sandy type soil withpossible evaporation loss, or hasmigrated from the plume point oforigin.120TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Fuel & Hydrocarbon StandardsGasoline Range HydrocarbonAnalysisGasoline AdditivesGAD-001$ 20 / 1 x 1 mLGAD-001-PAKSAVE $ 80 / 5 x 1 mL0.2 mg/mL each in MeOH 4 comps.Dibromomethane1,2-Dibromoethane1,2-DichloroethaneMethyl t-butyl etherCertified BTEX in UnleadedGasolineGA-001-20X-BTEX10.0 mg/mL in MeOHRegular unleaded gasolineHexadecane Extraction VolatilesCLP-BTEX$ 30 / 1 x 1 mLCLP-BTEX-PAK SAVE $ 120 / 5 x 1 mL0.2 mg/mL each in MeOH 6 comps.CLP-BTEX-10X$ 30 / 1 x 1 mLCLP-BTEX-10X-PAK SAVE $ 120 / 5 x 1 mL2.0 mg/mL each in MeOH 6 comps.BenzeneEthyl benzeneTolueneo-Xylenem-Xylenep-XyleneTechnical NoteSimultaneous BTEX/Gasoline QA/QCAccuStandard's QA/QC department hascertified the benzene, toluene, ethylbenzene and xylene concentrations inour unleaded gasoline standard. Use ofGA-001-20X-BTEX allows the analyticalchemist in a single injection to verify thatQA/QC requirements are being met forthe BTEX analytes as well as thegasoline.$ 55 / 1 x 1 mLTotal Recoverable Petroleum Hydrocarbon (FTRPH) Standard &SurrogatesCalibration/Window DefiningHydrocarbon StandardDRH-004S-R1-5X$ 50 / 1 x 1 mLDRH-004S-R1-5X-PAK $ 200 / 5 x 1 mL1.0 mg/mL each in Chloroform 17 comps.Octane C 8Decane C 10Dodecane C 12Tetradecane C 14Hexadecane C 16Octadecane C 18Eicosane C 20Docosane C 22Tetracosane C 24Internal StandardGRH-ISGRH-IS-PAK1.0 mg/mL in CH 2 Cl 25-alpha AndrostaneSurrogate StandardsDRH-SSDRH-SS-PAK5.0 mg/mL in THFn-Triacontane-d 62GRH-SSGRH-SS-PAK2.0 mg/mL in Acetoneo-Terphenyl (OTP)Hexacosane C 26Octacosane C 28Triacontane C 30Dotriacontane C 32Tetratriacontane C 34Hexatricontane C 36Octatriacontane C 38Tetracontane C 40$ 15 / 1 x 1 mLSAVE $ 60 / 5 x 1 mL$ 30 / 1 x 1 mLSAVE $ 120 / 5 x 1 mL$ 17 / 1 x 1 mLSAVE $ 68 / 5 x 1 mLFTRPH Calibration / WindowDefining StandardDRH-FTRPH$ 35 / 1 x 1 mLDRH-FTRPH-PAK SAVE $ 150 / 5 x 1 mL500 µg/mL each in Hexane 17 comps.n-Octanen-Decanen-Dodecanen-Tetradecanen-Hexadecanen-Octadecanen-Eicosanen-Docosanen-TetracosaneTechnical NoteThe above FTRPH Calibration/WindowDefining Standard was formulated at alower concentration to insure solubility ofthe analytes & eliminate the odorcaused by the introduction of Carbondisulfide as a cosolvent.Multi-State MethodHydrocarbon Window DefiningDRH-008S-R2$ 65 / 1 x 1 mLDRH-008S-R2-PAK SAVE $ 260 / 5 x 1 mL500 µg/mL each in Chloroform 35 comps.OctaneNonaneDecaneUndecaneDodecaneTridecaneTetradecanePentadecaneHexadecaneHeptadecanePristaneOctadecanePhytaneNonadecaneEicosaneHeneicosaneDocosaneTricosanen-Hexacosanen-Octacosanen-Triacontanen-Dotriacontanen-Tetratriacontanen-Hexatriacontanen-Octatriacontanen-TetracontaneTetracosanePentacosaneHexacosaneHeptacosaneOctacosaneNonacosaneTriacontanen-HentriacontaneDotriacontaneTritriacontaneTetratriacontanePentatriacontaneHexatriacontaneHeptatriacontaneOctatriacontaneNonatriacontaneTetracontaneFuel & Hydrocarbon MixturesDRO Defining MixAK-102.0-NAS-10X$ 40 / 1 x 1 mLAK-102.0-NAS-10X-PAK $ 160 / 5 x 1 mL2.0 mg/mL each in CH 2 Cl 2 16 comps.n-Decanen-Undecanen-Dodecanen-Tridecanen-Tetradecanen-Pentadecanen-Hexadecanen-Heptadecanen-Octadecanen-Nonadecanen-Eicosanen-Heneicosanen-Docosanen-Tricosanen-Tetracosanen-PentacosaneTechnical NoteAccuStandard offers a hydrocarbonwindow defining standard with the C 8 toC 40 odd and even alkanes. Use of thisone standard should meet the numerousstate-to-state variations for hydrocarbonvalidation and reporting. As an addedbenefit, AccuStandard has includedPristane and Phytane in the formulation.Again, use of this one standard canmeet numerous LUFT/LUST programsrequiring that the C 17 (Pristane) and C 18(Phytane) ratio be used to estimatesubsurface degradation of fuel oil spills.Total Petroleum Hydrocarbon Pattern Recognition StandardsThis book contains chromatography for the various petroleum products typically found during LUFT/LUST siteinvestigations. The chromatography shows each fuel pattern in a 25 minute analytical run for early eluting petroleumproducts like gasoline to late eluting products like motor oil. In addition, an n-alkane standard (DRH-008S) analyzedunder identical conditions has been overlaid on each petroleum product chromatogram. Use of the book will assist thechemist’s identification of the fuel for pattern recognition.The n-alkane standard (DRH-008S) overlay provides n-alkane reference points between the standard and theunknown sample. These beginning and ending n-alkane reference points can be used to establish gross hydrocarbonconcentrations. By comparing the specific n-alkane range of the closest identified petroleum standard to that of theunknown sample, a reproducible gross hydrocarbon number can be achieved.To Order, BOOK-TPH $ 35TECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 121


Fuel & Hydrocarbon StandardsKits for Qualitative Analysis & IdentificationFuel & Hydrocarbon KitsAlkanes nC 6 -nC 19PS-211C$ 100 / 15 units2 mL each at the stated concentrations by weight% in Ethylbenzene solvent.(01) n-Hexane Neat(02) n-Heptane Neat(03) n-Octane Neat(04) n-Nonane Neat(05) n-Decane Neat(06) n-Undecane Neat(07) n-Dodecane Neat(08) n-Tridecane Neat(09) n-Tetradecane Neat(10) n-Pentadecane Neat(11) n-Hexadecane 10%(12) n-Heptadecane 10%(13) n-Octadecane 10%(14) n-Nonadecane 10%(15) Normal HydrocarbonsMixture PS-21CNeat at the stated weightn-Dodecane 24.6%n-Tridecane 24.9%n-Tetradecane 25.1%n-Hexadecane 25.4%Calibration MixturePS-21C$ 30 / 1 x 2 mLNeat at the stated weight % listed above.Alkanes nC 6 -nC 19 NEATPS-211CX $ 115Ampules 1 through 52 mL eachVials 6 through 10, & 152 mL eachVials 11 through 140.5 g eachAlkenes C 6 -C 10PS-231CNeat at the stated quantities.$ 180 / 15 units(01) Hexene-1 2 mL(02) Hexene-2 (cis, trans) 0.5 mL(03) 2-Methylpentene-1 2 mL(04) 4-Methylpentene-1 2 mL(05) 4-Methylpentene-2 (cis, trans) 0.5 mL(06) 2-Ethylbutene-1 0.5 mL(07) Heptene-1 2 mL(08) Heptene-2 (cis, trans) 0.5 mL(09) Heptene-3 (cis, trans) 0.5 mL(10) Octene-1 2 mL(11) Octene-2 2 mL(12) 2-Ethylhexene-1 0.5 mL(13) Nonene-1 2 mL(14) Decene-1 2 mL(15) 1-Olefins C 1 -C 9Mixture PS-23C2 mLNeat at the stated weight %.1-Pentene 14.65%1-Hexene 11.93%1-Heptene 37.53%1-Octene 15.38%1-Nonene 20.51%Branched Alkanes C 6 -C 9PS-221DNeat at stated quantities.$ 200 / 15 units(01) 2-Methylpentane 2 mL(02) 3-Methylpentane 2 mL(03) 2,2-Dimethylbutane 2 mL(04) 2,3-Dimethylbutane 2 mL(05) 3-Methylhexane 2 mL(06) 2,3-Dimethylpentane 2 mL(07) 2,4-Dimethylpentane 1 mL(08) 3-Methylheptane 2 mL(09) 2,5-Dimethylhexane 1 mL(10) 2,2,4-Trimethylpentane 2 mL(11) 2,3,4-Trimethylpentane 2 mL(12) 2,2,5-Trimethylhexane 1 mL(13) Cyclohexane 2 mL(14) Methylcyclohexane 2 mL(15) Branched ChainHydrocarbons Mixture PS-22D 2 mLNeat at the stated weight %2-Methylpentane 14%n-Hexane 24%2,3-Dimethylpentane 14%2,2,4-Trimethylpentane 33%2,5-Dimethylhexane 15%Calibration MixturePS-22D$ 30 / 1 x 2 mLNeat at the stated weight % listed above.Alkenes C 8 -C 22PS-241DNeat at the stated quantities.$ 175 / 15 units(01) 2,4,4-Trimethylpentene-1 2 mL(02) 2,4,4-Trimethylpentene-2 0.5 mL(03) Nonene-1 0.5 mL(04) Nonene-4 (cis, trans) 0.5 mL(05) 3,5,5-Trimethyl-1-hexene 0.5 mL(06) Decene-1 2 mL(07) Undecene-1 0.5 mL(08) Dodecene-1 2 mL(09) Tridecene-1 2 mL(10) Tetradecene-1 2 mL(11) Hexadecene-1 2 mL(12) Octadecene-1 2 mL(13) Eicosene-1 2 mL(14) Docosene-1 0.5 mL(15) 1-Olefins C 12 -C 18Mixture PS-24D2 mLNeat at the stated weight %Decene- 1 10%Dodecene-1 15%Tetradecene-1 20%Hexadecene-1 25%Octadecene-1 30%Calibration MixturePS-24D$ 30 / 1 x 2 mLNeat at the stated weight % listed above.Alkanes nC 19 -nC 40PS-261C$ 220 / 15 units2 mL at the stated concentrations byweight % in Ethylbenzene solvent.(01) n-Nonadecane 10%(02) n-Eicosane 10%(03) n-Heneicosane 10%(04) n-Docosane 10%(05) n-Tricosane 10%(06) n-Tetracosane 10%(07) n-Pentacosane 10%(08) n-Hexacosane 10%(09) n-Octacosane 10%(10) n-Triacontane 1%(11) n-Dotriacontane 1%(12) n-Hexatriacontane 1%(13) n-Octatriacontane 1%(14) n-Tetracontane 1%(15) Normal HydrocarbonsMixture PS-26C2 mLAt the stated concentrations.Ethylbenzene 80%n-Octadecane 2%n-Nonadecane 5%n-Heneicosane 6%n-Docosane 7%Calibration MixturePS-26C$ 30 / 1 x 2 mLNeat at the stated weight % listed above.Alkanes nC 19 -nC 40 , NEATPS-261CX $ 345Vials 1 through 140.5 g eachVial 152 mLNaphthenes C 5 -C 10PS-281C2 mL each. Neat.$ 110 / 15 units(01) Cyclopentane(02) Methylcyclopentane(03) Cyclohexane(04) Methylcyclohexane(05) cis-1,2-Dimethylcyclohexane(06) trans-1,2-Dimethylcyclohexane(07) cis and trans-1,3-Dimethylcyclohexane(08) cis and trans-1,4-Dimethylcyclohexane(09) Ethylcyclohexane(10) n-Propylcyclohexane(11) iso-Propylcyclohexane(12) n-Butylcyclohexane(13) iso-Butylcyclohexane(14) tert-Butylcyclohexane(15) Branched chainHydrocarbons Mixture PS-28DNeat at the stated weight %Methylcyclopentane 16%Cyclohexane 17%Methylcyclohexane 17%Ethylcyclohexane 17%n-Propylcyclohexane 17%n-Butylcyclohexane 16%Calibration MixturePS-23C$ 30 / 1 x 2 mLNeat at the stated weight % listed above.Calibration MixturePS-28D$ 30 / 1 x 2 mLNeat at the stated weight % listed above.122TECHLAB 4C La Tannerie - BP 30055 - 57072 - METZ cedex 3


Fuel & Hydrocarbon StandardsLeaking Underground Storage Tank Retention Time StandardThis product can be used to screen a sample to determine what typeof petroleum spill that may have caused the contamination.Retention Time StandardDRH-010S$ 20 / 1 x 1 mLDRH-010S-PAKSAVE $ 80 / 5 x 1 mL25 µg/mL each in CH 2 Cl 2 7 comps.n-Hexanen-Decanen-Dodecanen-TetracosaneVPH SolutionTechnical Noten-Octacosanen-Triacontanen-TetracontaneA sample showing peaks in the C 6 -C 10 range generally indicates agasoline spill. Samples with the peaks in the C 24 -C 12 range are indicativeof a diesel spill while samples with the higher carbon numbers above C 24are typically oils or lubricants. Once the initial screen is complete, moredetailed work can be done to further identify the contaminant.WA-VPH$ 30 / 1 x 1 mLWA-VPH-PAKSAVE $ 120 / 5 x 1 mL200 µg/mL each in MeOH 15 comps.Determination of Aromatic & Aliphatic Hydrocarbons in GasolineRange OrganicsAK101AA Aromatics MixAK-101AA-ARO$ 30 / 1 x 1 mLAK-101AA-ARO-PAKSAVE $ 120 / 5 x 1 mL2000 µg/mL each in MeOH 14 comps.BenzeneTolueneEthylbenzenem-Xylenep-Xyleneo-Xylene1,2,3-TrimethylbenzeneSurrogate StandardM-602-SSM-602-SS-PAK0.2 mg/mL in MeOHα,α,α-Trifluorotoluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzenem-Ethyltoluenep-Ethyltolueneo-Ethyltoluenen-Propylbenzene$ 20 / 1 x 1 mLSAVE $ 80 / 5 x 1 mLFuel & Hydrocarbons MixturesBenzeneEthylbenzeneTolueneo-Xylenem-Xylenep-XyleneMtBEn-Pentanen-Hexanen-Octanen-Decanen-Dodecane1-MethylnaphthaleneNaphthalene1,2,3-TrimethylbenzeneCanadian Ministry of the Environment Brownfield RegulationsBrownfield Regulation for Light Petroleum FractionCCME-LPF-SET$ 95 / 5 x 1 mLAt stated conc. in MeOH8 comps.CCME-LPF-0.05X CCME-LPF-0.1X CCME-LPF-0.25X CCME-LPF-0.5X CCME-LPFµg/mL µg/mL µg/mL µg/mL µg/mLn-Decane 12.5 25 50 125 250n-Hexane 12.5 25 50 125 250Toluene 12.5 25 50 125 250Benzene 12.5 25 50 125 250o-Xylene 12.5 25 50 125 250m-Xylene 6.25 12.5 25 62.5 125p-Xylene 6.25 12.5 25 62.5 125Ethylbenzene 12.5 25 50 125 250Approved by the Canadian Ministry ofthe Environment as of October 1, 2004.Brownfield Regulation for Medium & Heavy Petroleum FractionCCME-MHPF-SET$ 75 / 3 x 1 mLAt stated conc. in n-Hexane3 comps.CCME-MHPF-0.1X CCME-MHPF-0.5X CCME-MHPFµg/mL µg/mL µg/mLn-Decane 40 200 400n-Hexadecan 40 200 400n-Tetratriacontane 40 200 400Brownfield Regulation Performance Check StandardCCME-QCCCME-QC-PAKAt 40 µg/mL each in n-Hexane:Cyclohexanen-Pentacontanen-TetracontaneBrownfield Regulation SpikeCCME-SPIKEAt 2500 µg/mL each in n-HexaneSAE 30W Motor Oil - Non-Detergent Formula#2 Diesel Fuel - 50% Weathered$ 45 / 1 x 1 mL$ 180 / 5 x 1 mL2 comps.$ 30 / 1 x 1 mL2 comps.Hydrocarbon StandardBrownfield RegulationD-5442-R1$ 60 / 1 x 1 mL100 µg/mL each in Cyclohexane 18 comps.n-Decanen-Dodecanen-Tetradecanen-Hexadecanen-Octadecanen-Eicosanen-Docosanen-Tetracosanen-Hexacosanen-Octacosanen-Triacontanen-Dotriacontanen-Tetratriacontanen-Hexatriacontanen-Octatriacontanen-Tetracontanen-Tetratetracontanen-PentacontaneTECHLAB Tél. 03 87 75 54 29 • Fax 03 87 36 23 90 • Web www.techlab.fr 123


112-40-3:1182825-82-3:1183386-33-2:118352-33-0:118438-22-2:118460-00-4:118526-73-8:119615-59-8:118629-50-5:119629-59-4:119629-62-9:119629-97-0:118646-31-1:11964742-47-8:11864742-54-7:11864742-89-8:11968334-30-5:11868476-30-2:11868476-31-3:11868476-43-6:11868553-00-4:11870892-10-3:1187194-86-7:1198006-64-2:1198008-20-6:1198030-30-6:1198052-41-3:11984-15-1:11993952-07-9:119AK-101.0-IS-10X:118AK-101AA-ARO:123AK-101AA-ARO-PAK:123AK-102-LCS-R1-10X:118AK-102.0-LCS:118AK-102.0-LCS-10X:118AK-102.0-NAS-10X:121AK-102.0-NAS-10X-PAK:121AK-102.0-SS:119AK-102.0-SS-10X:119AK-103.0-LCS:119AK-103.0-LCS-5X:119AK-103.0-SS:119AK-103.0-SS-10X:119AS-E0238:118AS-E0239:119AS-E0240:119AS-E0241:119BOOK-TPH:121CCME-LPF-SET:123CCME-MHPF-SET:123CCME-QC:123CCME-QC-PAK:123CCME-SPIKE:123CLP-BTEX:121CLP-BTEX-10X:121CLP-BTEX-10X-PAK:121CLP-BTEX-PAK:121D-5186-91-PM:118D-5442-R1:123D-5480-C40-5ML:119D-5480-C40-R1-5ML:119DRH-004S-R1-5X:121DRH-004S-R1-5X-PAK:121DRH-006-SS:119DRH-007-SS:118DRH-008S-R2:121DRH-008S-R2-PAK:121DRH-010S:123DRH-010S-PAK:123DRH-FL-SS:119DRH-FL-SS-3X:119DRH-FL-SS-R1:119DRH-FTRPH:121DRH-FTRPH-PAK:121DRH-SS:119, 121DRH-SS-PAK:121FD2-W25-10X:118, 120FD2-W25-R1-10X:118, 120FD2-W50-10X:118, 120FD2-W50-R1-10X:118, 120FD2-W75-10X:118, 120FD2-W75-R1-10X:118, 120FK-W25-10X:119,120FK-W50-10X:119,120FK-W75-10X:119,120FU-001:118FU-001-40X:118FU-001-D-40X:118FU-002:118FU-002-40X:118FU-002-D-40X:118FU-003:118FU-003-40X:118FU-003-D-40X:118FU-004:118FU-004-40X:118FU-004-D-40X:118FU-005:119FU-005-40X:119FU-005-D-10X:119, 120FU-005-D-40X:119FU-006:119FU-006-40X:119FU-006-D-40X:119FU-007:118FU-007-40X:118FU-007-D-40X:118FU-008:118FU-008-40X:118FU-008-D-40X:118FU-009:118FU-009-40X:118FU-009-D-10X:118, 120FU-009-D-40X:118FU-010:118FU-010-40X:118FU-010-D-40X:118FU-011:118FU-011-40X:118FU-011-D-40X:118FU-012:118FU-012-40X:118FU-012-D-40X:118FU-012N:118FU-013:118FU-013-40X:118FU-013-D-40X:118FU-014:118FU-014-40X:118FU-014-D-40X:118FU-015:118FU-015-40X:118FU-015-D-40X:118FU-016:118FU-016-40X:118FU-016-D-40X:118FU-017:118FU-017-40X:118FU-017-D-10X:118, 120FU-017-D-40X:118FU-018-D-40X:119FU-018-H:119FU-018-H-40X:119FU-019-D-40X:119FU-019-H:119FU-019-H-40X:119FU-020-D-40X:118FU-021-D-40X:119FU-022:118FU-022-40X:119FU-022-D-40X:119FU-023:118FU-023-40X:118FU-023-D-40X:118FU-025-D-40X:119FU-025-H:119FU-025-H-40X:119FU-026-D-40X:119FU-026-H:119FU-026-H-40X:119FU-027-D-40X:119FU-027-H:119FU-027-H-40X:119FU-028-D-40X:119FU-028-H:119FU-028-H-40X:119GA-001:118GA-001-10X:118,120GA-001-20X-BTEX:121GA-001-40X:118GA-001-D-40X:118GA-003:118GA-003-40X:118GA-003-D-40X:118GA-004:118GA-004-40X:118GA-004-D-40X:118GA-005:119GA-005-40X:119GA-005-D-40X:119GA-W25-10X:119, 120GA-W50-10X:119, 120GA-W75-10X:119, 120GAD-001:121GAD-001-PAK:121GARH-IS:118GARH-SS:118GRH-004-SS:118GRH-004-SS-100X:118GRH-004-SS-10X:118GRH-IS:118, 121GRH-IS-10X:118GRH-IS-PAK:121GRH-SS:119,121GRH-SS-PAK:121HS-001N:119HS-001S:119


HS-001S-40X:119HS-001S-D-40X:119HS-002N:119HS-002S:119HS-002S-40X:119HS-002S-D-40X:119HS-003N:119HS-003S:119HS-003S-40X:119HS-003S-D-40X:119HS-004N:119HS-004S:119HS-004S-40X:119HS-004S-D-40X:119HS-005N:119HS-005S:119HS-005S-10X:119HS-005S-40X:119HS-005S-D-40X:119M-602-SS:123M-602-SS-PAK:123M-GRA-SCS-AS:118M-GRO-BLNK-10ML:119PS-211C:122PS-211CX:122PS-21C:122PS-221D:122PS-22D:122PS-23C:122PS-241D:122PS-24D:122PS-261C:122PS-261CX:122PS-26C:122PS-281C:122PS-28D:122TPH-001-SET:120TPH-002-SET:120TPH-003-SET:120TPH-004-SET:120TPH-SET:120V-028S-D-10X:119WA-VPH:123WA-VPH-PAK:123

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