A+RI Standard 700-2006 - Informative - AHRI
A+RI Standard 700-2006 - Informative - AHRI
A+RI Standard 700-2006 - Informative - AHRI
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2008 Appendix D to ARI <strong>Standard</strong> <strong>700</strong>-<strong>2006</strong>2008 Appendix D for Gas Chromatograms forARI <strong>Standard</strong><strong>700</strong>-<strong>2006</strong> - <strong>Informative</strong>
IMPORTANTSAFETY DISCLAIMER<strong>AHRI</strong> does not set safety standards and does not certify or guarantee the safety of any products,components or systems designed, tested, rated, installed or operated in accordance with thisstandard/guideline. It is strongly recommended that products be designed, constructed, assembled,installed and operated in accordance with nationally recognized safety standards and code requirementsappropriate for products covered by this standard/guideline.<strong>AHRI</strong> uses its best efforts to develop standards/guidelines employing state-of-the-art and acceptedindustry practices. <strong>AHRI</strong> does not certify or guarantee that any tests conducted under itsstandards/guidelines will be non-hazardous or free from risk.FOREWORDThe intent of this informative appendix is to provide figures for the gas chromatograms used withAppendix C, Analytical Procedures for ARI <strong>Standard</strong> <strong>700</strong>-<strong>2006</strong> - Normative.Note:This Appendix is a new appendix.Price $15.00 (Members) $30.00 (Non-Members)Printed in U. S.A.©Copyright 2008, by Air-Conditioning, Heating and Refrigeration InstituteRegistered United States Patent and Trademark Office
FIGURESPAGEFigure 1 Gas Chromatogram of Non-Condensable Gas ...................................................2Figure 2 Gas Chromatogram of R-11 ...............................................................................3Figure 3 Gas Chromatogram of R-12 ...............................................................................4Figure 4 Gas Chromatogram of R-13 ...............................................................................5Figure 5 Gas Chromatogram of R-22 (Packed) ................................................................6Figure 6 Gas Chromatogram of R-22 (Capillary).............................................................7Figure 7 Gas Chromatogram of R-23 ...............................................................................8Figure 8 Gas Chromatogram of R-32 ...............................................................................9Figure 9 Gas Chromatogram of R-113 ...........................................................................10Figure 10 Gas Chromatogram of R-114 ...........................................................................11Figure 11 Gas Chromatogram of R-115 ...........................................................................12Figure 12 Gas Chromatogram of R-116 .......................................................................... 13Figure 13 Gas Chromatogram of R-123 (Packed) ........................................................... 14Figure 14 Gas Chromatogram of R-123 (Capillary)........................................................ 15Figure 15 Gas Chromatogram of R-124 .......................................................................... 16Figure 16 Gas Chromatogram of R-125 .......................................................................... 17Figure 17 Gas Chromatogram of R-134a ......................................................................... 18Figure 18 Gas Chromatogram of R-141b ........................................................................ 19Figure 19 Gas Chromatogram of R-142b ........................................................................ 20Figure 20 Gas Chromatogram of R-143a ......................................................................... 21Figure 21 Gas Chromatogram of R-152a ......................................................................... 22Figure 22 Gas Chromatogram of R-218 .......................................................................... 23Figure 23 Gas Chromatogram of R-245fa ....................................................................... 24Figure 24 Gas Chromatogram of R-290 .......................................................................... 25Figure 25 Gas Chromatogram of R-401 .......................................................................... 26Figure 26 Gas Chromatogram of R-402 .......................................................................... 27Figure 27 Gas Chromatogram of R-403 .......................................................................... 28Figure 28 Gas Chromatogram of R-404 .......................................................................... 29Figure 29 Gas Chromatogram of R-406 .......................................................................... 30Figure 30 Gas Chromatogram of R-407 .......................................................................... 31Figure 31 Gas Chromatogram of R-408 .......................................................................... 32Figure 32 Gas Chromatogram of R-409 .......................................................................... 33Figure 33 Gas Chromatogram of R-410 .......................................................................... 34Figure 34 Gas Chromatogram of R-411 .......................................................................... 35Figure 35 Gas Chromatogram of R-412 .......................................................................... 36Figure 36 Gas Chromatogram of R-413 .......................................................................... 37Figure 37 Gas Chromatogram of R-414 .......................................................................... 38Figure 38 Gas Chromatogram of R-416 .......................................................................... 39Figure 39 Gas Chromatogram of R-417 .......................................................................... 40i
Figure 40 Gas Chromatogram of R-422 .......................................................................... 41Figure 41 Gas Chromatogram of R-500 .......................................................................... 42Figure 42 Gas Chromatogram of R-502 .......................................................................... 43Figure 43 Gas Chromatogram of R-503 .......................................................................... 44Figure 44 Gas Chromatogram of R-507 .......................................................................... 45Figure 45 Gas Chromatogram of R-508 .......................................................................... 46Figure 46 Gas Chromatogram of R-509 .......................................................................... 47Figure 47 Gas Chromatogram of R-600 .......................................................................... 48ii
2008 APPENDIX D TO ARI STANDARD <strong>700</strong>-<strong>2006</strong>Gas Chromatogram FiguresSection 1. PurposeThe purpose of this informative appendix is to provide figures for the gas chromatograms used withAppendix C, Analytical Procedures for <strong>AHRI</strong> <strong>Standard</strong> <strong>700</strong>-<strong>2006</strong> - Normative.Section 2. DefinitionsNote for all figures:2.1 Ret. Time = Retention Time2.2 Comp. = Component_____________________________________________________________________________
6.05.50.445.04.54.0Response - MilliVolts3.53.02.52.01.51.00.50.0AirCO2C=0.040.67C=0.01.33C=0.01.75C=0.02.050.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0Time - MinutesRun Time = 5.791479 minutes Data Sampling Rate = 5.001601 points/secRet. Time Component0.44 Air0.67 CO21.331.752.05
10010.689080Response - MilliVolts706050403020104.33 4.48 R226.13R127.61 R133a8.02 R218.69 CH2CL29.13 R114/ACETONESBNR11R123aR12311.7412.37CHCL3SBN13.98R11315.13317.11R140aCCL418.1318.983M7100#220.09TCE24.22R11227.230 5 10 15 20 25 30Time - MinutesRun Time = 32.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component4.334.48 R226.13 R127.61 R133a8.02 R218.69 CH2CL29.13 R114/ACETONE10.68 R1111.74 R123a12.37 R12313.98 CHCL315.13 R11317.11 3M7100#118.13 R140a18.98 CCL420.09 3M7100#224.22 TCE27.23 R112
Figure 3: Gas Chromatogram of R-12Response - MilliVolts10090807060504030201002.63CH43.23R233.96C2H4C2H64.635.285.87 R13 6.166.69R143a7.54 R152a8.07 R134aR407.87R228.6710.75 C3H6 11.02 R11512.53R12R142b13.37SBN14.83 R12415.47 R133a16.10 R2116.52 ISOB.R114R114A18.01 N-BUTANE18.66 2-BUT-TSBN0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30Time - MinutesRun Time = 30 minutes Data Sampling Rate = 5 points/sec17.45SUM+SUM-R1119.5020.53R12321.2023.41 MEK24.11 R113 24.38 2-BUT.N-PENTANE25.18Ret. Time Component2.633.23 CH43.96 R234.63 C2H45.28 C2H65.87 R136.166.69 R143a7.54 R152a7.87 R408.07 R134a8.67 R2210.75 C3H611.02 R11512.53 R1213.37 R142b14.83 R12415.47 R133a16.10 R2116.52 ISOB.17.45 R114R114A18.01 N-BUTANE18.66 2-BUT-T19.50 R1120.53Ret. Time Component21.20 R12323.41 MEK24.11 R11324.38 2-BUT.25.18 N-PENTANE
Figure 4: Gas Chromatogram of R-132406.32220200180Response - MilliVolts16014012010080604020INT-R143.69INT+R234.47R1166.05R13SBNR1259.53R22R13B110.4811.01R11512.9914.65 R12SBNSBNR114R114a19.38R1121.760 2 4 6 8 10 12 14 16 18 20 22 24Time - MinutesRun Time = 24 minutes Data Sampling Rate = 5 points/secRet. Time Component3.69 R144.47 R236.05 R1166.32 R139.53 R12510.48 R2211.01 R13B112.99 R11514.65 R1219.38 R114R114a21.76 R11
Figure 5: Gas Chromatogram of R-22 (Packed)75708.4765605550Response - MilliVolts454035302520151050CH43.23R23R323.97C2H4C2H64.635.28R135.87R143a6.697.53 R152a R125R134a8.057.76R22C3H6 R11510.77 11.02SBNR12R142b12.7313.41R21ISOB.14.84 R12415.48 R133a16.1116.53R114R114aN-BUTANESUM+18.01SUM-2-BUT-T17.4618.67SBNR12319.50 R1119.9420.54 R123a21.200 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30Time - MinutesRun Time = 30 minutes Data Sampling Rate = 5 points/secR11324.11Ret. Time Component3.23 CH43.97 R23R324.63 C2H45.28 C2H65.87 R136.69 R143a7.53 R152a7.76 R1258.05 R134a8.47 R2210.77 C3H611.02 R11512.73 R1213.41 R142b14.84 R12415.48 R133a16.11 R2116.53 ISOB.17.46 R114R114a18.01 N-BUTANE18.67 2-BUT-T19.50 R1119.9420.54 R123a21.20 R123
Figure 6: Gas Chromatogram of R-22 (Capillary)201817.8716Response - MilliVolts14121086R23/R11513.46R143A R3214.4014.51R1217.40R4020.67R31R2126.72R11327.9742SKIM22.460R2212 14 16 18 20 22 24 26 28 30Time - MinutesRun Time = 31 minutes Data Sampling Rate = 20 points/secRet. Time Component13.46 R23/R11514.40 R143A14.51 R3217.40 R1217.87 R2220.67 R4022.46 R3126.72 R2127.97 R113
R-2312.67R-32R-134ASBNR-12R-2213.4720.076.66.46.2Response - MilliVolts6.05.85.65.45.25.04.84.6R-1270R-4023.30R-31R-141b12 14 16 18 20 22 24 26 28 30 32 34Time - MinutesRun Time = 34.99917 minutes Data Sampling Rate = 20 points/secRet. Time Component12.67 R-2313.47 R-3220.07 R-2223.30 R-40
Figure 9: Chromatogram of R-1132018R12318.2323.90Response - MilliVolts1614121086R11511.51R111312.12R12 R2212.29 12.4112.92 R114R216ba R133a14.3114.071112a318mbb15.2515.74R1116.42C-31617.5117.0417.72R123aSUM+SUM-18.78R22519.35CCL423.70SBNR112 TCE25.02 25.1425.41PCE29.054R113R12210 12 14 16 18 20 22 24 26 28 30 32Time - MinutesRun Time = 30.27 minutes Data Sampling Rate = 20 points/secRet. Time Component11.51 R11512.12 R111312.29 R1212.41 R2212.92 R11414.07 R216ba14.31 R133a15.25 1112a15.74 318mbb16.42 R1117.04 C-31617.51 R123a17.72 R12318.23 R11318.7819.35 R22523.70 CCL423.90 R12225.0225.14 R11225.41 TCE29.05 PCE
Figure 10: Gas Chromatogram of R-11415014018.54130120110100Response - MilliVolts90807060504030201000.921.97R233.374.225.906.63 R137.33 7.588.51R134aR152a9.12R22R13019.7710.31R11512.2513.93 R1214.62 14.78 15.24 R124a15.95 R12416.2616.55R133a17.33 R217ba17.90 PW+ PW+R114/R114aPW- SBN0 5 10 15 20 25 30 35Time - MinutesRun Time = 37 minutes Data Sampling Rate = 5 points/secR133aB1R1119.7820.64R1112a/R123a22.32SUM+SUM-21.65R12323.15R113 R113a25.23 25.69R12231.3533.58TCE34.26Ret. Time Component0.921.973.374.22 R235.906.63 R137.337.588.51 R152a9.12 R134a9.77 R2210.31 R130112.25 R11513.93 R1214.6214.7815.24 R124a15.95 R12416.2616.55 R133a17.33 R217ba17.9018.54 R114/R114a19.78 R133aB120.64 R11
Figure 11: Gas Chromatogram of R-11550458.189.0811.5414.1615.354035R114/R114AResponse - MilliVolts302520R1213.1817.831510R143.93 R23R1166.08 R13SKIMR1119.7953.245.297.85SKIMPW+0R125R22R115R1113R1240 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30Time - MinutesRun Time = 30 minutes Data Sampling Rate = 5 points/secRet. Time Component3.24 R143.93 R235.29 R1166.08 R137.858.18 R1259.08 R2211.54 R11513.18 R1214.16 R111315.35 R12417.83 R114/R114A19.79 R11
Figure 12: Gas Chromatogram of R-1162004.928.021807.14160140Response - MilliVolts12010080R13R229.26606.24402003.36R234.12R116R143aR152a0 2 4 6 8 10 12 14 16 18 20Time - MinutesRun Time = 20 minutes18.62Data Sampling Rate = 5 points/secRet. Time Component3.364.12 R234.92 R1166.24 R137.14 R143a8.02 R152a9.26 R2218.6221.65 R1112a/R123a22.32 R12323.1525.23 R11325.69 R113a31.35 R12233.5834.26 TCE
Figure 14: Gas Chromatogram of R-123 (Capillary)2043.98 44181132aResponse - MilliVolts161412108623.4924.241225zc111326.5027.1027.41 27.62R1229.041336mzz R2229.24R11430.0831.63 112232.44 R124a33.16 R124216ba34.3134.73132636.97133a 1112a37.96 38.25111239.2140.02 124B140.68 R11R2142.2243.13 R141b 43.42 R11343.63R30R123b147.69 111145.7446.1046.6247.364R123bR123aR12322 24 26 28 30 32 34 36 38 40 42 44 46 48 50Time - MinutesRun Time = 50 minutes Data Sampling Rate = 5 points/secRet. Time Component23.4924.24 1132a26.50 1225zc27.10 111327.41 R1227.6229.04 1336mzz29.24 R2230.08 R11431.63 112232.44 R124a33.16 R12434.31 216ba34.7336.97 132637.96 133a38.25 1112a39.21 111240.02 124B140.68 R1142.22 R2143.13 R141b43.42 R11343.63 R123b43.98 R123a44.16 R12345.7446.10 R3046.62Ret. Time Component47.36 R123b147.69 1111
Figure 15: Gas Chromatogram of R-1241009014.0314.4980Response - MilliVolts7060504030201003.30R234.00R143a6.76R152a R1258.16 R134a7.627.86R22R318.779.43R11511.1312.23R1212.74111313.6013.37SKIMR124aR124R133a15.460 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30Time - MinutesRun Time = 30 minutes Data Sampling Rate = 5 points/sec1318-T16.44SBNR114 1318-C17.48 17.67R1118.8719.5520.58R12321.26R11324.1826.2827.12Ret. Time Component3.304.00 R236.76 R143a7.62 R152a7.86 R1258.16 R134a8.77 R229.43 R3111.13 R11512.2312.74 R1213.3713.60 111314.03 R124a14.49 R12415.46 R133a16.44 1318-T17.48 R11417.67 1318-C18.8719.55 R1120.5821.26 R12324.18 R11326.2827.12
Figure 16: Gas Chromatogram of R-1251007.718.469.9812.5116.4719.109080R123Response - Picoamps706050403020100CH43.45R23\R324.03 4.40R1165.91R136.787.20R143aR125R22R130110.48R115R1214.231113R124a15.1615.710 5 10 15 20 25 30Time - MinutesRun Time = 30.49667 minutes Data Sampling Rate = 5 points/secR124R133a17.1218.07SUM-R114\R114a19.30SUM-19.7521.1022.39 22.6923.5224.6126.34R11327.0428.0829.71Ret. Time Component3.45 CH44.034.40 R23\R325.91 R1166.78 R137.207.71 R143a8.46 R1259.98 R2210.48 R130112.51 R11514.23 R1215.16 111315.71 R124a16.47 R12417.12 R133a18.0719.1019.30 R114\R114a19.7521.1022.3922.6923.52 R12324.61Ret. Time Component26.3427.04 R11328.0829.71
Figure 17: Gas Chromatogram of R-134asRun Time = 33.99667 Data Sampling Rate = 20Run Time = 33.99667 minutesData Sampling Rate = 20 points/secRet. Time Component13.01 R11513.59 R143a13.89 R12515.34 R245CB15.47 R134a17.14 R16117.25 R152a17.73 R1218.60 R13420.07 R2222.76 R114/R114a23.27 R4023.60 112224.87 R12425.2225.46 114025.88 R3126.76 1131-t28.31 R133a30.87 1131-c33.07 R123
Figure 18: Gas Chromatogram of R-141b201816.3224.431130a31.53Response - MilliVolts161412108642012.89 R143a19.03 19.28 33.78 34.1114.41 R1215.85 1131aR142b17.1017.481363mz20.17 365mfc20.86 21.21151a21.80 392 ISOMERS22.5523.89R141b24.88 25.09 25.1725.7626.44 26.33 1121-t27.06 27.42 364132b27.8428.5829.03 150a29.5731.14R140a32.0232.5412 14 16 18 20 22 24 26 28 30 32 34 36Time - MinutesRun Time = 36.00333 minutes Data Sampling Rate = 10 points/secRet. Time Component12.89 R143a14.41 R1215.85 1131a16.32 R142b17.1017.4819.0319.28 1363mz20.17 365mfc20.86 151a21.2121.80 392 ISOMERS22.5523.8924.43 R141b24.8825.0925.17 1130a25.7626.33 1121-t26.4427.06 36427.42 132b27.8428.5829.03 150a29.5731.1431.53 R140aRet. Time Component32.0232.5433.7834.11
Figure 19: Gas Chromatogram of R-142b2011.8712.2015.2023.1224.1018161131aResponse - MilliVolts141210864INT+1132aR143a13.40 R152a13.65 R1214.07 R2215.03R142bSBN16.6819.33R16020.31R1121.63R141b1130a12 14 16 18 20 22 24 26Time - MinutesRun Time = 26.99833 minutes Data Sampling Rate = 10 points/secRet. Time Component11.87 1132a12.20 R143a13.40 R152a13.65 R1214.07 R2215.03 1131a15.20 R142b16.6819.3320.31 R16021.63 R1123.12 R141b24.10 1130a32.0232.5433.7834.11
Figure 20: Gas Chromatogram of R-143a2007.058.16180Response - MilliVolts160140120100806040200INT-INT+3.35R413.78R23R324.11C2H44.87C2H6/1132a5.60R143a SKIMR40/R125R134a8.42R152a8.77R229.39R115/C3H811.850 2 4 6 8 10 12 14 16 18 20 22 24Time - MinutesRun Time = 24 minutes Data Sampling Rate = 5 points/secR1213.49R142b14.17111314.47R12415.68R133a16.30ISOB.17.32N-BUTANE18.84R141b20.36365mfc21.06Ret. Time Component3.353.78 R414.11 R23R324.87 C2H45.60 C2H6/1132a7.05 R143a8.16 R152a8.42 R40/R1258.77 R134a9.39 R2211.85 R115/C3H813.49 R1214.17 R142b14.47 111315.68 R12416.30 R133a17.32 ISOB.18.84 N-BUTANE20.36 R141b21.06 365mfc
Figure 21: Gas Chromatogram of R-152a506.34454035Response - MilliVolts302520151050CH42.60C2H43.74C2H64.265.40R1615.70R152aC3H6C3H88.688.970 2 4 6 8 10 12 14 16 18 20Time - MinutesRun Time = 20 minutes Data Sampling Rate = 5 points/sec10.63SBNISOB.12.9013.55N-BUTANE13.9515.18Ret. Time Component2.60 CH43.74 C2H44.26 C2H65.405.70 R1616.34 R152a8.68 C3H68.97 C3H810.6312.90 ISOB.13.5513.95 N-BUTANE15.18
Figure 22: Gas Chromatogram of R-218757010.5612.9665605550121613.33Response - MilliVolts45403530R227ea15.3725201510508.799.38R218CF8S11.77245cbC-31813.9314.4314.8416.2016.9717.42C5F1018.0118.6720.2010 12 14 16 18 20 22 24 26 28 30Time - MinutesRun Time = 29.99667 minutes Data Sampling Rate = 5 points/sec20.80Ret. Time Component3.425.638.799.3810.56 R21811.77 CF8S12.96 245cb13.33 121613.93 C-31814.4314.8415.37 R227ea16.2016.9717.4218.01 C5F1018.6720.2020.80
Figure 23: Gas Chromatogram of R-245fa504525.894035Response - MilliVolts302520151050R-245faR-123426.65R-22621 22 23 24 25 26 27 28 29 30 31 32 33 34 35Time - MinutesRun Time = 34.99667 minutes Data Sampling Rate = 10 points/secR-1224 Isom129.46R-1233R-123530.58R-1224 Isom2 R-133a30.99 31.1833.38R-11R-141bR-123aR-113R-12333.49R-30Ret. Time Component25.89 R-245fa26.65 R-123429.46 R-1224 Isom130.58 R-123530.99 R-1224 Isom231.18 R-133a33.38 R-12333.49 R-113
Figure 24: Gas Chromatogram of R-290100905.5311.6817.1218.628070Response - MilliVolts6050403020100CH43.23C2H68.63C3H811.40C3H6SBN0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30Time - MinutesRun Time = 30 minutes Data Sampling Rate = 5 points/secISOB.N-BUTANE19.7320.3524.1226.4829.68Ret. Time Component3.23 CH45.53 C2H68.6311.40 C3H811.68 C3H617.12 ISOB.18.62 N-BUTANE19.7320.3524.1226.4829.6824.11 R113
Figure 25: Gas Chromatogram of R-4012409.5911.4619.99220200180Response - MilliVolts160140120100R134a10.61R1217.80R124a19.3380604020INT-INT+R152aR22SBNSBNSBNSBNR1240 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component9.59 R152a10.61 R134a11.46 R2217.80 R1219.33 R124a19.99 R124
Figure 26: Gas Chromatogram of R-4022409.9611.4815.89220200180Response - MilliVolts16014012010080604020INT-INT+R125R22R290SBNSBNSBN0 2 4 6 8 10 12 14 16 18 20 22 24 26Time - MinutesRun Time = 25.99333 minutes Data Sampling Rate = 5 points/secRet. Time Component9.96 R12511.48 R2215
Figure 27: Gas Chromatogram of R-40324011.3214.4015.82220200180Response - MilliVolts16014012010080604020INT-INT+R22R218R290SBNSBNSBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component11.32 R2214.40 R21815.82 R290
Figure 28: Gas Chromatogram of R-4042402202008.2710.01R134a10.59180Response - MilliVolts16014012010080R2211.64R11515.83R1217.79604020INT-INT+R143aR125SBNSBNSBN0 2 4 6 8 10 12 14 16 18 20 22 24 26Time - MinutesRun Time = 26 minutes Data Sampling Rate = 5 points/secRet. Time Component8.27 R143a10.01 R12510.59 R134a11.64 R2215.83 R11517.79 R12
Figure 29: Gas Chromatogram of R-406750<strong>700</strong>11.3418.55650600Response - MilliVolts550500450400350300R600a21.4025020015010050INT-INT+R22R142bSBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component11.34 R2218.55 R142b21.40 R600a
Figure 30: Gas Chromatogram of R-407750<strong>700</strong>4.389.9710.47650600550500Response - MilliVolts45040035030025020015010050INT-INT+R32R125R134aR2211.54R11515.76SBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component4.38 R329.97 R12510.47 R134a11.54 R2215.76 R115
Figure 31: Gas Chromatogram of R-408750<strong>700</strong>8.2211.40650600550500Response - MilliVolts450400350300R12510.10250200R115150SBNR1210050INT-INT+R143aR2215.79SBN17.76SBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component8.22 R143a10.10 R12511.40 R2215.79 R11517.76 R12
Figure 32: Gas Chromatogram of R-409750<strong>700</strong>11.3318.5019.97650600550500Response - MilliVolts450400350300250200150R12R124aSBNSBN10017.7619.3050INT-INT+R22R142bR1240 5 10 15 20 25 30Time - MinutesRun Time = 32 minutes Data Sampling Rate = 5 points/secRet. Time Component11.33 R2217.76 R1218.50 R142b19.30 R124a19.97 R124
Figure 33: Gas Chromatogram of R-410750<strong>700</strong>4.369.97650600550500Response - MilliVolts45040035030025020015010050INT-INT+4.02 R41R32R125R2211.56R11515.78SBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component4.02 R414.36 R329.97 R12511.56 R2215.78 R115
Figure 34: Gas Chromatogram of R-411750<strong>700</strong>11.28650600550500R152a9.49Response - MilliVolts450400350300250200127015.4115010050INT-INT+R22SBN17.76SBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component9.49 R152a11.28 R2215.41 127017.76
Figure 35: Gas Chromatogram of R-412750<strong>700</strong>11.3018.51650600550500Response - MilliVolts450400350300250200R21814.3415010050INT-INT+R22SBNR142bSBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99333 minutes Data Sampling Rate = 5 points/secRet. Time Component11.30 R2214.34 R21818.51 R142b
Figure 36: Gas Chromatogram of R-413750<strong>700</strong>10.48650600Response - MilliVolts550500450400350300R21814.34R600a21.3925020015010050INT-INT+R134aSBNSBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99333 minutes Data Sampling Rate = 5 points/secRet. Time Component10.48 R134a14.34 R21821.39 R600a
Figure 37: Gas Chromatogram of R-414750<strong>700</strong>11.3318.4719.93650600550500Response - MilliVolts450400350300R600a250R124a21.4020015019.2810050INT-INT+R22SBNR142bSBNR1240 5 10 15 20 25 30Time - MinutesRun Time = 31.99333 minutes Data Sampling Rate = 5 points/secRet. Time Component11.33 R2218.47 R142b19.28 R124a19.93 R12421.40 R600a
Figure 38: Gas Chromatogram of R-41624010.5319.9422.80220200180R124aResponse - MilliVolts16014012010019.3080604020INT-INT+R134aSBNSBNR124N-BUTANE0 2 4 6 8 10 12 14 16 18 20 22 24 26Time - MinutesRun Time = 25.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component10.53 R134a19.30 R124a19.94 R12422.80 N-BUTANE
Figure 39: Gas Chromatogram of R-417750<strong>700</strong>9.8910.50650600Response - MilliVolts550500450400350300R60022.7925020015010050INT-INT+R125R134a12.1015.79SBNSBN20.0321.4022.210 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component9.89 R12510.50 R134a12.1015.7920.0321.4022.2122.79 R600
Figure 40: Gas Chromatogram of R-4225004509.9210.6821.51400350Response - MilliVolts300250200150100500INT-INT+R125R134a0 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secR11515.91SBNSBN SBN SBN SBN SBN SBNSBNR600a22.90Ret. Time Component9.92 R12510.68 R134a15.91 R11521.51 R600a22.90
Figure 41: Gas Chromatogram of R50030028010.0717.76260240220200Response - MilliVolts1801601401201008060R324.39R137.04R143a8.17SKIMR134aR2210.6811.56R11515.72SKIMR142b18.50R12420.02R2121.02R114/R114a22.23R1124.15R12326.01R11328.984020INT-INT+R152aSBNR120 5 10 15 20 25 30Time - MinutesRun Time = 31.99333 minutes Data Sampling Rate = 5 points/secRet. Time Component4.39 R327.04 R138.17 R143a10.07 R152a10.68 R134a11.56 R2215.72 R11517.76 R1218.50 R142b20.02 R12421.02 R2122.23 R114/R114a24.15 R1126.01 R12328.98 R113
Figure 42: Gas Chromatogram of R-502Response - MilliVolts50045040035030025020015010050INT-INT+R324.356.02R137.00R143a8.119.49 R152a9.98 R125 10.40 R134aR2210.80SKIM15.99R11517.75 R1218.45 R142bSBNR12420.03R2121.02R114/R114a22.21R1124.11R12326.01R11328.890 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component4.35 R326.027.00 R138.11 R143a9.49 R152a9.98 R12510.40 R134a10.80 R2215.99 R11517.75 R1218.45 R142b20.03 R12421.02 R2122.21 R114/R114a24.11 R1126.01 R12328.89 R113
Figure 43: Gas Chromatogram of R-503Response - MilliVolts50045040035030025020015010050INT-3.63 INT+ 3.844.32R236.98R13SBNSBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component3.633.844.32 R236.98 R13
Figure 44: Gas Chromatogram of R-5072408.5610.34220200180Response - MilliVolts16014012010080604020INT-INT+R143aR1259.8912.07R11516.11R1218.03SBNSBN0 2 4 6 8 10 12 14 16 18 20 22 24 26Time - MinutesRun Time = 26 minutes Data Sampling Rate = 5 points/secRet. Time Component8.56 R143a9.89 R12510.3412.0716.1118.03 R12
Figure 45: Gas Chromatogram of R-5085004.336.03450400350Response - MilliVolts300250200150100INT+3.8550INT-R23R116SBNSBN0 5 10 15 20 25 30Time - MinutesRun Time = 32 minutes Data Sampling Rate = 5 points/secRet. Time Component3.854.33 R236.03 R116
Figure 46: Gas Chromatogram of R-50950045011.3314.44400350Response - MilliVolts30025020015010050INT-INT+R22R218SBNSBN0 5 10 15 20 25 30Time - MinutesRun Time = 31.99667 minutes Data Sampling Rate = 5 points/secRet. Time Component11.33 R2214.44 R21832.0232.5433.7834.11
Figure 47: Gas Chromatogram of R-60050045011.7217.1018.5120.3724.12400Response - MilliVolts350300250200N-PENTANE26.46150100500CH43.38C2H65.637.19R29016.23ISOBUTANE17.6418.16N-BUTANE0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30Time - MinutesRun Time = 29.99 minutes Data Sampling Rate = 5 points/sec19.35NEOPENTANE21.65ISOPENTANERet. Time Component3.38 CH45.63 C2H67.1911.72 R29016.2317.10 ISOBUTANE17.6418.1618.51 N-BUTANE19.3520.37 NEOPENTANE21.6524.12 ISOPENTANE26.46 N-PENTANE
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