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5<br />
www.pfeiffer-vacuum.net<br />
Leak detection<br />
5.1 General<br />
5.1.1 Leaks and leak detection<br />
What is a leak? A leak, also referred to as leakage, enables a substance to flow toward a<br />
pressure gradient. Expressed in simpler terms, leaks are small holes through which gases or<br />
liquids flow from the side of higher pressure to the side of lower pressure. This can involve<br />
simple, harmless leaks, such as a dripping water faucet, or hazardous toxic substances that<br />
escape through leaks.<br />
Any number of technical products will not function, or will not function for an adequate period<br />
of time, if they have leaks. Examples include: The refrigerant circulation system in refrigerators,<br />
air conditioning systems in cars, automobile tires, automotive fuel tanks or home fuel<br />
oil tanks, as well as distillation systems in the chemical or pharmaceutical industries. In many<br />
cases, the leak-tightness of machines and systems in the production process is an indispensable<br />
prerequisite for the quality of the manufactured products.<br />
Returning to the original definition of a leak, we thus find that it is impossible to completely<br />
prevent substances from flowing through a wall. The term ”tight“ therefore refers to the<br />
requirements of the respective machine, plant or vessel, and must be quantified accordingly.<br />
5.1.2 Leakage rate<br />
Let us consider a bicycle tube having a volume V = 41. It has been inflated to a pressure of<br />
three bar, and without any additional inflation should have a maximum pressure loss of<br />
�p = 1,000 mbar after time t (30 days).<br />
The leakage rate has already been defined in 1.3.3: (Formula 1-27).<br />
Or to illustrate: The leakage rate of a vessel having a volume of 1 liter is 1 mbar . �p<br />
l / s if the<br />
interior pressure increases or decreases by 1 mbar in 1 second. Please refer to Table 1.6 for<br />
conversion to other customary units. Inserting the values for our bicycle tube then yields<br />
the permissible leakage rate:<br />
. V<br />
Q = l �t<br />
1,000 mbar . 4 l mbar . l<br />
Q = = 1.5 l . - 3 10<br />
30 . 24 . 3,600 s s<br />
and we find that the bicycle tube with this leakage rate is sufficiently tight.<br />
These kinds of leakage rates can be found by means of the well-known bubble test method<br />
(Figure 5.1).<br />
Now let us consider a refrigerator in which a loss of 10 g of refrigerant having a molecular<br />
weight of 102 g / mol, i.e. around 2.24 bar . l, is allowable over a ten-year period. This results<br />
in a permissible leakage rate of<br />
2.24 l . 1,000 mbar mbar . l<br />
Q = = 7.1 l . - 6 10<br />
10 . 365 . 24 . 3,600 s s<br />
These kinds of leakage rates can only be localized and quantified by means of extremely<br />
sensitive measuring methods, for example with mass spectrometry and test gases that are<br />
not present in the atmosphere.<br />
Page 113<br />
<strong>Vacuum</strong><br />
<strong>Technology</strong>