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Vacuum Technology Know How - Triumf

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5<br />

www.pfeiffer-vacuum.net<br />

Leak detection<br />

5.1 General<br />

5.1.1 Leaks and leak detection<br />

What is a leak? A leak, also referred to as leakage, enables a substance to flow toward a<br />

pressure gradient. Expressed in simpler terms, leaks are small holes through which gases or<br />

liquids flow from the side of higher pressure to the side of lower pressure. This can involve<br />

simple, harmless leaks, such as a dripping water faucet, or hazardous toxic substances that<br />

escape through leaks.<br />

Any number of technical products will not function, or will not function for an adequate period<br />

of time, if they have leaks. Examples include: The refrigerant circulation system in refrigerators,<br />

air conditioning systems in cars, automobile tires, automotive fuel tanks or home fuel<br />

oil tanks, as well as distillation systems in the chemical or pharmaceutical industries. In many<br />

cases, the leak-tightness of machines and systems in the production process is an indispensable<br />

prerequisite for the quality of the manufactured products.<br />

Returning to the original definition of a leak, we thus find that it is impossible to completely<br />

prevent substances from flowing through a wall. The term ”tight“ therefore refers to the<br />

requirements of the respective machine, plant or vessel, and must be quantified accordingly.<br />

5.1.2 Leakage rate<br />

Let us consider a bicycle tube having a volume V = 41. It has been inflated to a pressure of<br />

three bar, and without any additional inflation should have a maximum pressure loss of<br />

�p = 1,000 mbar after time t (30 days).<br />

The leakage rate has already been defined in 1.3.3: (Formula 1-27).<br />

Or to illustrate: The leakage rate of a vessel having a volume of 1 liter is 1 mbar . �p<br />

l / s if the<br />

interior pressure increases or decreases by 1 mbar in 1 second. Please refer to Table 1.6 for<br />

conversion to other customary units. Inserting the values for our bicycle tube then yields<br />

the permissible leakage rate:<br />

. V<br />

Q = l �t<br />

1,000 mbar . 4 l mbar . l<br />

Q = = 1.5 l . - 3 10<br />

30 . 24 . 3,600 s s<br />

and we find that the bicycle tube with this leakage rate is sufficiently tight.<br />

These kinds of leakage rates can be found by means of the well-known bubble test method<br />

(Figure 5.1).<br />

Now let us consider a refrigerator in which a loss of 10 g of refrigerant having a molecular<br />

weight of 102 g / mol, i.e. around 2.24 bar . l, is allowable over a ten-year period. This results<br />

in a permissible leakage rate of<br />

2.24 l . 1,000 mbar mbar . l<br />

Q = = 7.1 l . - 6 10<br />

10 . 365 . 24 . 3,600 s s<br />

These kinds of leakage rates can only be localized and quantified by means of extremely<br />

sensitive measuring methods, for example with mass spectrometry and test gases that are<br />

not present in the atmosphere.<br />

Page 113<br />

<strong>Vacuum</strong><br />

<strong>Technology</strong>

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