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Vacuum Technology Know How - Triumf

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www.pfeiffer-vacuum.net<br />

Analytical applications<br />

In many cases, mass spectrometers are used in analysis devices today. Fluids are often<br />

injected and evaporated in the inlet chamber of the vacuum system. Pressure is reduced in<br />

several stages, and the individual chambers are isolated from one another by orifices. Since<br />

each chamber must be pumped, the objective is to combine the gas flows via taps on the<br />

turbopump through skillful combination of backing pumps and turbopumps. Specially modified<br />

turbopumps with taps are used for series applications.<br />

Helium leak detectors, too, are equipped with turbopumps. In this case, the counter-flow<br />

principle is often used; i.e. a mass spectrometer is arranged on the high vacuum side of the<br />

pump. Due to the lower compression ratios of turbopumps for helium than for nitrogen or<br />

oxygen, the pump acts as a selective amplifier for the helium partial pressure.<br />

Pumps with high gas loads in vacuum processes<br />

The turbopump offers two advantages when pumping high gas loads for vacuum processes:<br />

It generates clean vacuum at the beginning of each process step, and can then pump down<br />

process gas without any harmful backflow. In the second step, the primary objective is to<br />

maintain the given pressure at which the desired vacuum process should run. In this process,<br />

gas throughputs and working pressure will be determined by the application in question; i.e.<br />

a given volume flow rate will be pumped at a given gas throughput. Moreover, it should be<br />

possible to quickly achieve clean intermediate vacuum when changing workpieces. Since<br />

these are conflicting requirements, a turbopump of sufficient size for the required gas throughput<br />

and the required intermediate vacuum will be selected. The process pressure will be<br />

regulated via an inlet (butterfly) valve. An example of how to dimension this kind of pumping<br />

station is shown in Chapter 7. The maximum permissible gas loads specified in the technical<br />

data should be taken to mean permissible continuous loads. This applies subject to the<br />

assurance of sufficient cooling in accordance with the specification and a backing pressure<br />

that is less than 50 % of the critical backing pressure.<br />

Pumping corrosive and abrasive substances<br />

When pumping corrosive gases, measures must be taken to protect the motor / bearing areas<br />

and the rotor, in particular, against corrosion. To do this, all surfaces that come into contact<br />

with corrosive gas are either provided with a coating or made from materials that can withstand<br />

attacks by these gases. A defined inert gas flow is admitted into the motor / bearing<br />

area in the backing-vacuum via a special sealing gas valve. From there, the gas flows through<br />

labyrinth seals to the backing-vacuum area, mixes with the corrosive gas and is pumped<br />

down together with the corrosive gas.<br />

The blades can wear mechanically should dust accumulate; this could necessitate repairs and<br />

replacement of the rotor. It should also be noted that deposits can be expected to form in the<br />

pump, which will necessitate shorter service intervals. In particular, it is necessary to ensure<br />

that deposits in the pump do not react with the moisture in the air to become aggressive<br />

substances. Consequently, the pumps should be vented with dry inert gases only, and should<br />

be fitted with sealed backing-vacuum and high vacuum flanges. Turbopumps for these applications<br />

are always classical turbopumps without a Holweck stage, as the narrow gaps and<br />

pump channels in the Holweck stage would quickly clog with dust deposits and the<br />

rotor would seize.<br />

Page 65<br />

<strong>Vacuum</strong><br />

<strong>Technology</strong>

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