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P<br />

E<br />

T<br />

R<br />

O<br />

L<br />

E<br />

U<br />

M<br />

Certified<br />

Reference<br />

<strong>Standards</strong><br />

4th Edition<br />

Member<br />

Over 100<br />

<strong>ASTM</strong> Methods<br />

AccuStandard ®


Notice the Difference with AccuStandard<br />

Experience in Petrochemical Requirements<br />

•Years of Round Robin Studies with <strong>ASTM</strong><br />

•Ampulled over 300 gallons of <strong>ASTM</strong> fuel sets including<br />

over 35 gasoline and hydrocarbon blends<br />

• <strong>Standards</strong> for over 100 <strong>ASTM</strong> Methods<br />

• 17 years of Manufacturing, Organic & Inorganic <strong>Standards</strong><br />

• Synthesizes rare Hydrocarbons not otherwise available<br />

Involvement in the Petrochemical Industry<br />

• Participation in regular <strong>ASTM</strong> meetings<br />

• Active in D-02 and D-16 subcommittees<br />

• Provides support to several Petrochemical Instrument Manufacturers<br />

Resources<br />

• Low Sulfur Analyzers (such as XOS) for Measurements to ppb Levels<br />

• Instrumention for Analyzing <strong>Standards</strong> for ICP, ICP-MS, AA, GC/MS,<br />

GC/FID, GC/EC, GC/NPD, Karl Fischer Titrator, and others<br />

• NIST/NVLAP Accredited (Lab Code 200389-0) as a PT Provider<br />

• ISO 9001:2000 Certified (ISO 9001 for the last 10 years)<br />

• Extensive Inventory of <strong>ASTM</strong> and Related <strong>Standards</strong><br />

New Products in this Catalog<br />

• Low Sulfur and Nitrogen <strong>Standards</strong> (see pages 6-11)<br />

• LUFT/LUST <strong>Standards</strong> (see pages 81-98)<br />

• TPH <strong>Standards</strong> (see pages 81, 92-93, 96-97)<br />

• No Haz Fee ICP & AA <strong>Standards</strong> (see pages 67-75)<br />

• Additional New <strong>ASTM</strong> <strong>Standards</strong><br />

© AccuStandard, Inc. 2003<br />

PRINTED ON<br />

RECYCLED PAPER


<strong>ASTM</strong> # Method Description page<br />

Cross Reference Tables (<strong>ASTM</strong>,IP,ISO,DIN,JIS,AFNOR) II<br />

Analytical Capabilities III<br />

On-Line Ordering IV<br />

Quality Control 1-2<br />

D-56 Flash Point <strong>Standards</strong> 3<br />

D-86 Synthetic Distillation Standard 3<br />

D-92 Flash Point <strong>Standards</strong> (COC) 3<br />

D-93 Flash Point <strong>Standards</strong> (PMCC) 3<br />

D-445 Viscosity Calibration Standard 3<br />

D-611 Aniline Point Standard 4<br />

D-1015 Freezing Point <strong>Standards</strong> 4<br />

D-1319 Olefin Analysis by FIA 4<br />

D-1744 Water in Liquid Petroleum Products 5<br />

D-2386 Freezing Point Calibration <strong>Standards</strong> 5<br />

D-2500 Cloud Point Calibration <strong>Standards</strong> 5<br />

D-2622 Sulfur by XRF 10<br />

D-2789 Hydrocarbon Analysis in Gasoline by GC/MS 11<br />

PIANO, PONA, PNA by GC 12-13<br />

Proposed Method for Detailed Hydrocarbon Analysis 14<br />

Detailed Hydrocarbon Analysis PONA VI 14<br />

D-2887 Boiling Range by GC 14<br />

Simulated Distillation (SIM DIS) by GC 15<br />

D-3120 Sulfur by Oxidative Microcoulometry 16<br />

D-3230 Salts in Crude Oil 16<br />

D-3231 Phosphorus in Gasoline 16<br />

D-3237 Lead in Gasoline by AA 16<br />

D-3246 Sulfur in Petroleum Gas by Oxidative Microcoulometry 17<br />

D-3340 Li & Na in Lubricating Greases by Flame Photometer 17<br />

D-3524 Diesel Fuel Analysis by GC 17<br />

D-3605 Trace Metal in Gas Turbine Fuels by AA 17<br />

D-3606 Aromatics in Gasoline by GC 18<br />

D-3610 Total Co Analysis by Potentiometric Titration 18<br />

D-3710 Boiling Range by GC 20<br />

D-3798 p-Xylene Analysis by GC 20<br />

D-3831 Manganese in Gasoline by AA 20<br />

D-4059 PCB Analysis by GC 21<br />

D-4110 Ion Chrom 76<br />

D-4291 Ethylene Glycol by GC 21<br />

D-4294 Sulfur by ED-XRF 7-11, 21<br />

D-4377 Water in Liquid Petroleum Products 5, 21<br />

D-4420 Aromatics in Gasoline by GC 22<br />

D-4628 Wear Metals in Lube Oil 22<br />

D-4629 Nitrogen by Chemiluminescence 23<br />

D-4815 Oxygenates in Gasoline by GC 24<br />

D-4927 Wear Metals and Additives by WD-XRF 25,63<br />

D-4928 Water in Liquid Petroleum Products 6, 25<br />

D-4929 Chlorine in Crude Oil by Microcoulometry 25<br />

D-4951 Wear Metals and Additives by ICP 26<br />

D-5056 Trace Metals in Petroleum Coke by AA 26<br />

D-5059 Lead in Gasoline by X-Ray Spectroscopy 27<br />

D-5134 Petroleum Naphthas through n-Nonane by GC 27<br />

D-5184 Al and Si by ICP-AES & AA 28<br />

D-5185 Wear Metals and Additives by ICP 28<br />

D-5186 Aromatics by SFC 28<br />

D-5188 Vapor - Liquid Ratio Temperature 29<br />

D-5191 Vapor Pressure <strong>Standards</strong> 29<br />

D-5307 Boiling Range Distribution of Crude Petroleum by GC 29<br />

Sulfur <strong>Standards</strong> Group<br />

D-2622 Sulfur by XRF 10<br />

D-3120 Sulfur by Oxidative Microcoulometry 10, 17<br />

D-3246 Sulfur in Petro Gas by Oxidative Microcoulometry 6-11<br />

D-4294 Sulfur by ED-XRF 10<br />

D-5453 Sulfur by Ultra Violet Fluorescence 6-11, 31<br />

D-5623 Sulfur Compounds by Sulfur Selective Detection 38<br />

D-6334 Sulfur in Gasoline by Wavelength WD-XRF 6-11<br />

D-6445 Sulfur in Gasoline by ED-XRF 6-11<br />

Table of Contents<br />

<strong>ASTM</strong> # Method Description page<br />

D-5441 MtBE Analysis by GC 30<br />

D-5442 Petroleum Waxes by GC 31<br />

D-5443 PNA Analysis by Multidimensional GC 31<br />

D-5453 Sulfur by Ultra Violet Fluorescence 31<br />

D-5480 Engine Oil Volatility by GC 32<br />

D-5482 Vapor Pressure <strong>Standards</strong> 29, 32<br />

D-5501 Ethanol Analysis by GC 32<br />

D-5580 Aromatics by GC 32-33<br />

D-5599 Oxygenates by OFID 34-36<br />

D-5600 Trace Metals by ICP 37<br />

D-5622 Oxygenates by Reductive Pyrolysis 37<br />

D-5623 Sulfur Compounds by Sulfur Selective Detection 38<br />

D-5708 Trace Metals by ICP 39, 62<br />

D-5762 Nitrogen by Chemiluminescence 40<br />

D-5769 Aromatics by GC/MS 42-51<br />

D-5771 Cloud Point of Petro Products 52<br />

D-5772 Cloud Point of Petro Products (Linear Cooling Rate) 52<br />

D-5773 Cloud Point of Petro Products (Constant Cooling Rate) 52<br />

D-5863 Trace Metals by AA 52<br />

D-5901 Freezing Point Aviation Fuels (Auto Optical Method) 53<br />

D-5972 Freezing Point Aviation Fuels 53<br />

D-5986 Oxygenates and Aromatics by GC/FTIR 53<br />

D-6160 PCBs by GC 54<br />

D-6258 Solvent Red 164 Dye Concentration in Diesel Fuels 54<br />

D-6277 Benzene in Spark Ignition Fuels 54<br />

D-6293 Oxygenates (O-PONA) in Engine Fuels by GC 55<br />

D-6296 Total Olefins in Spark Ignition Engine Fuels by GC 55<br />

D-6304 Water in Liquid Petro Products 5<br />

D-6334 Sulfur in Gasoline by Wavelength WD-XRF 10, 56<br />

D-6352 Boiling Range Distribution of Petroleum 56<br />

D-6378 Vapor Pressure 56<br />

D-6379 Aromatic Hydrocarbon by HPLC 57<br />

D-6417 Engine Oil by GC 57<br />

D-6428 Sulfur by ECD 57<br />

D-6443 Metals in Oil 58-65<br />

D-6445 Sulfur in Gasoline by ED-XRF 10, 58<br />

D-6481 Lube Oils by ED-XRF 58, 63, 64<br />

D-6550 Olefin Content of Gasoline by SFC 58<br />

D-6591 Aromatic Hydrocarbon by HPLC 57<br />

(IP 391)<br />

E-1064 Water in Petroleum 6<br />

ISO/CD V & Ni with Mn 62<br />

Organometallic (Wear Metals) Analysis by AA, ICP, DCP, XRF 26, 28, 59-66<br />

Plasma Emission Spectroscopy (ICP) 67-71<br />

ICP (No Haz Fee) New 67-71<br />

Atomic Absorption Spectroscopy (AA) 67, 73-75<br />

AA (No Haz Fee) New 67, 73-75<br />

Plasma Emission / Mass Spectroscopy (ICP/MS) 72<br />

Trace Metals, Chlorine in Lube Oil, and Organo Tin New 66<br />

Ion Chrom 76-79<br />

LUFT/LUST and TPH (New Section) 81-98<br />

Index i-vii<br />

Quote Form back<br />

Order Information back<br />

Wear Metals Group<br />

D-3605 Trace Metals in Gas Turbine Fuel by AA 17<br />

D-4628 Wear Metals in Lube Oil 22<br />

D-4927 Wear Metals and Additives by WDXRF 25, 63-64<br />

D-4951 Wear Metals and Additives by ICP 26<br />

D-5185 Wear Metals and Additives by ICP 28<br />

D-5708 Trace Metals by ICP 39, 62<br />

D-5863 Trace Metals by AA 52<br />

D-6443 Metals in Oil 58, 64<br />

D-6481 Lube Oils by ED-XRF 58, 63-64<br />

Quality System is Certified to comply with the International ISO 9001:2000 Quality Standard<br />

QC<br />

<strong>ASTM</strong> SULFUR WEAR METALS PIANO ORGANOMETALLIC ICP & AA LUFT/LUST INDEX<br />

QUOTE FORM


II<br />

Cross Reference Table Sorted by <strong>ASTM</strong> Method<br />

Use the AccuStandard Cross<br />

Reference Tables to Match<br />

various International<br />

Methods for known<br />

Petrochemical analysis.<br />

MEMBER<br />

Fully Accredited<br />

For over 17 years<br />

AccuStandard has been the<br />

Leader in the Chemical<br />

<strong>Standards</strong> Industry in both<br />

Organic and Inorganic<br />

products. AccuStandard is<br />

ISO 9001:2000 registered<br />

and a NIST/NVLAP<br />

accredited Proficiency<br />

Testing provider (NVLAP<br />

Code 200389-0).<br />

ISO 9001:2000<br />

Certificate Number: 31692<br />

ANALYSIS <strong>ASTM</strong> IP ISO DIN JIS AFNOR PAGE<br />

Tag Flash Point D-56 51411 K 2580 M07-003 3<br />

Distillation D-86 123 3405 51751 K 2254 M07-002 3<br />

COC Flash Point D-92 36 2592 51376 K 2265 T60-118 3<br />

PMCC Flash Point D-93 34 2719 51758 K 2265 M07-019 3<br />

Kinematic Viscosity D-445 71-1 3104 51562 K 2283 T60-100 3<br />

Aniline Point D-611 2 2977 51775 M07-021 4<br />

Hydrocarbon Types by FID D-1319 156 3837 51791 K 2536 M07-024 4<br />

Water (Karl Fischer) D-1744 6296 T60-154 5<br />

Freezing Point D-2386 16 3013 51421 K 2276 M07-048 5<br />

Cloud Point D-2500 219 3015 51597 K 2269 T60-105 5<br />

Sulfur by XRF D-2622 51400T6 K 2541 10<br />

Boiling Range By GC D-2887 3924 14<br />

Sulfur by Oxidative Microcoulometry D-3120 16591 16<br />

Lead by AAS D-3237 428 16<br />

Sulfur by Oxidative Microcoulometry D-3246 373 M07-052 10<br />

Metals by AA D-3605 413 8691 51790T3 17<br />

Benzene by GC D-3606 425 18<br />

Sulfur by ED-XRF D-4294 336 8754 M07-053 21<br />

Water (Karl Fischer) D-4377 356 10336 5<br />

Metals by AA D-4628 308 51391T1 22<br />

Nitrogen by Chemiluminescence Detection D-4629 379 M07-058 23<br />

Metals by WD-XRF D-4927 407 51391T2 25, 63<br />

Water (Karl Fischer) D-4928 386 10337 5, 25<br />

Lead in Gas By X-Ray D-5059 228 27<br />

Vapor Pressure D-5191 394 M07-079 29, 32<br />

Oxygenates D-5599 408 34-36<br />

Cloud Point D-5771 444 52<br />

Cloud Point D-5772 445 52<br />

Cloud Point D-5773 446 52<br />

Freezing Point D-5901 434 53<br />

Auto-Freeze Point D-5972 435 53<br />

Hydrocarbons Automatic D-6379 436 57<br />

Hydrocarbons Automatic NEW D-6591 391 57<br />

Metals 14597 62<br />

This is a partial list of <strong>Standards</strong> available for <strong>ASTM</strong> Methods<br />

Tables Generated from<br />

(a) R.A. Nadkarni, “Guide to <strong>ASTM</strong> Test Methods for the Analysis of Petroleum Products and Lubricants”, Manual 44<br />

(200), <strong>ASTM</strong> West Conshohocken, PA<br />

(b) Annual Book of <strong>ASTM</strong> <strong>Standards</strong> 2000, Volumes 05.01 to 05.05<br />

Member<br />

AccuStandard is an active member in <strong>ASTM</strong> and<br />

strives to keep abreast of <strong>ASTM</strong> method revisions.<br />

If our listed formulation does not meet the most<br />

recent method revision, please contact Technical<br />

Support, ext. 117 for an updated product.


Analytical Capabilities<br />

Lab Resources<br />

Milligram to Kilogram Scale Glassware<br />

Equipment to work under N 2/Ar<br />

Flash and Liquid Solid Phase Chrom. (mg to 2 kg)<br />

Preparative TLC<br />

Buchi Rotary Evaporator<br />

Vacuum Drying Oven<br />

Parr Pressure Reactor (high pressure reaction, hydrogenation)<br />

Distillation Equipment - High Vacuum Distillation, Molecular<br />

Distillation (Kugelrohr), Spinning Band Columns,<br />

Packed and Vigreaux columns<br />

Melting Point Apparatus<br />

pH meter<br />

Viscometer<br />

Centrifuge<br />

Analytical Instruments<br />

Inorganic (ICP)<br />

PE Optima 3000<br />

Spectro FMD-07<br />

Organics<br />

GCs: (6) HP 5890 Series II, FID, NPD, ECD all with<br />

auto injectors<br />

GC/MS: (3) HP 5971A<br />

HP 5971A with OI Analytical Purge & Trap<br />

PE Q-Mass 910<br />

HPLC: Varian 5000 with Applied Bioscience Fluorescence<br />

detector and HP auto injector<br />

Sulfur (low level)<br />

XOS (XRF) with monochromatic wavelength disperser<br />

Antek 9000 Series (UVF)<br />

Miscellaneous<br />

Ion Chromatograph, Waters 600E with<br />

Conductivity detector 431, Alltech 335 Ion<br />

Suppressor<br />

Automatic Polarimeter, Zuzi W22<br />

Karl Fischer Titrator<br />

III


IV<br />

There is an easier way to get Chemical Reference <strong>Standards</strong><br />

e-<strong>Standards</strong> ®<br />

from AccuStandard.com<br />

5 Ways to Search<br />

“e-<strong>Standards</strong>” is the Fastest, Most Comprehensive Search Engine<br />

available and contains over 30,000 products.<br />

Search by:<br />

Catalog Number<br />

Single or Multiple Components,<br />

Method (EPA, <strong>ASTM</strong>, etc.)<br />

Chemical Category (Organic, Inorganic, Petroleum, etc.)<br />

Other Companys’ Part Number<br />

Log on to www.accustandard.com and see how easy it is.<br />

Easy Ordering 24/7<br />

Find It Fast...simply search for a product, select it for purchase &<br />

click - it's that easy! Discounts may apply to online orders, see<br />

details on website.<br />

On-Line Custom Services<br />

On-Line Ordering<br />

AccuStandard specializes in synthesizing chemicals of high purity<br />

to be used as reference standards, and offers custom synthesis<br />

capability for milligram to kilogram batches. If you can't find the<br />

specific standard you need, we can prepare Custom Formulations<br />

and Custom Packaging for both Organic and Inorganic needs.<br />

See our Website for more info.<br />

Custom Formulations<br />

Over 30,000 <strong>Standards</strong><br />

just a click away<br />

AccuStandard offers over 30,000 different standards, and if you can't find the specific standard you need, we will prepare a custom<br />

formulation. Our custom organic and inorganic standards are a fast, economical way to address your unique requirements. To<br />

make an inquiry for Custom Quotes visit our website.<br />

You can also Email your requirements to techservice@accustandard.com or Fax us at 203-786-5287. Please include the following<br />

information: List of analytes and concentrations, Solvent or matrix, Quantity required (milliliters), Packaging unit size (milliliters<br />

per ampule, bottle, or vial).<br />

Quality Control Options<br />

1. Gravimetric/Volumetric Certification: Each standard is measured gravimetrically and then QC’ed instrumentally (where<br />

available). Every component in the standard is guaranteed to be within ±0.5% of the requested value unless otherwise stated. The<br />

solutions are made up to volume using class A glassware. A certificate comes with each standard and documents the gravimetric<br />

values used.<br />

2. Quantitative Validation: Full QA/QC method includes extended GC analysis using both internal and calibration standards plus<br />

statistical analysis. A data package is provided containing analytical and gravimetric data (Organic customs only).<br />

Also available: OEM <strong>Standards</strong> - Privately labeled standards manufactured and tested to your specifications.


AccuPetroCheck Consensus Value QC <strong>Standards</strong><br />

CARB Low Sulfur RFG QC<br />

Standard<br />

<strong>ASTM</strong>-FUEL-QCS-01-PAK $ 60 / 5 x 15 mL<br />

Parameter Method Value Conc.<br />

Total Aromatics D-1319 24.5 Vol.%<br />

Total Olefins D-1319 5.3 Vol.%<br />

Total Saturates D-1319 58.3 Vol.%<br />

Sulfur D-2622 0.0057 Wt.%<br />

Sulfur D-4294 0.0078 Wt.%<br />

Sulfur D-5453 55.76 µg/g<br />

Sulfur D-6344 59.31 µg/g<br />

Benzene D-5769 0.80 Vol.%<br />

Toluene D-5769 4.92 Vol.%<br />

Total Aromatics D-5769 23.42 Vol.%<br />

Benzene D-6277 0.78 Vol.%<br />

Total Olefins D-6550 5.3 Vol.%<br />

AccuPetroTest<br />

Sulfur in Diesel Fuel QC Standard<br />

SBPT-SDF $ 25 / 2 x 15 mL<br />

Parameter Approx. Range<br />

Sulfur 20 - 11000 µg/g<br />

See <strong>ASTM</strong> Methods D-2622, D-3120, D-3246-92,<br />

D-4294, D-5453 for Sulfur Calibration <strong>Standards</strong><br />

AccuPetroTest Gasoline<br />

Low Sulfur QC Sample<br />

SBPT-LSGAS $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Sulfur D-5453 0 - 50 µg/g<br />

AccuPetroTest Gasoline<br />

Quality Control <strong>Standards</strong><br />

AccuPetroCheck and AccuPetroTest Real World Gasoline QC <strong>Standards</strong><br />

In cooperation with <strong>ASTM</strong> D-02 subcommittee 3 and 4, AccuStandard ampulled 21 Real World gasoline reference fuels. Consensus Values have<br />

been determined for these reference fuels by various <strong>ASTM</strong> Round Robins to provide Petrochemical Laboratories with a source of well<br />

characterized gasoline standards for use in QA/QC applications and as Single Blind test samples over an extended period of time. As new <strong>ASTM</strong><br />

D-02.03 and D-02.04 Test methods are promulgated they require mandatory Quality Control testing of real world samples. AccuStandard’s<br />

PetroTest & PetroCheck standards are being successfully used to achieve these new Quality Control requirements.<br />

Comprehensive Single Blind Gasoline QC Sample<br />

SBPT-COMP $ 50 / 2 x 15 mL<br />

Parameter Method Approx. Range Conc.<br />

Total Aromatics D-1319 8 - 60 Vol.%<br />

Total Olefins D-1319 1 - 40 Vol.%<br />

Total Saturates D-1319 30 - 80 Vol.%<br />

Sulfur D-2622 0.0001 - 0.0930 Wt.%<br />

Sulfur D-4294 0.0016 - 0.0930 Wt.%<br />

Sulfur D-5453 0.5 -500 µg/g<br />

Sulfur D-6344 1.0 - 1000 µg/g<br />

Benzene D-5769 0.1 - 2.0 Vol.%<br />

Toluene D-5769 1.0 - 15 Vol.%<br />

Total Aromatics D-5769 8 - 60 Vol.%<br />

Benzene D-6277 0.1 - 2.0 Vol.%<br />

Total Olefins D-6550 1 - 40 Vol.%<br />

Conventional Gasoline QC<br />

Standard<br />

<strong>ASTM</strong>-FUEL-QCS-02-PAK $ 60 / 5 x 15 mL<br />

Parameter Method Value Conc.<br />

Total Aromatics D-1319 34.6 Vol.%<br />

Total Olefins D-1319 12.4 Vol.%<br />

Total Saturates D-1319 62.8 Vol.%<br />

Sulfur D-2622 0.0338 Wt.%<br />

Sulfur D-4294 0.0368 Wt.%<br />

Sulfur D-5453 317.36 µg/g<br />

Sulfur D-6344 338.78 µg/g<br />

Benzene D-5769 0.55 Vol.%<br />

Toluene D-5769 5.53 Vol.%<br />

Total Aromatics D-5769 32.51 Vol.%<br />

Benzene D-6277 0.52 Vol.%<br />

Total Olefins D-6550 12.4 Vol.%<br />

Sulfur in White Mineral Oil QC<br />

Standard<br />

SBPT-SWMO $ 25 / 2 x 15 mL<br />

Parameter Approx. Range<br />

Sulfur 20 - 11000 µg/g<br />

See <strong>ASTM</strong> Methods D-2622, D-3120,<br />

D-3246-92, D-4294, D-5453 for Sulfur<br />

Calibration <strong>Standards</strong><br />

Olefin QC Sample<br />

SBPT-OLEFINSFC $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Total Olefins D-6550 1 - 40 Vol.%<br />

AccuPetroCheck QC <strong>Standards</strong><br />

Two of the fuels are available as<br />

AccuPetroCheck Consensus Value QC<br />

<strong>Standards</strong>. The AccuPetroCheck CARB and<br />

Conventional gasoline reference materials have<br />

all parameters listed on the certificate with the<br />

Consensus Values and the regression equations<br />

for reproducability. Use of these Reference<br />

Materials improve the quality of laboratory<br />

results. The Consensus Values listed reflect<br />

initial statistical treatment of the data at the time<br />

the catalog was published. The actual certificate<br />

provided with the AccuPetroCheck QC standard<br />

will have the accepted Consensus Value based on<br />

statistical treatment of the data.<br />

Sulfur Single Blind AccuPetroTest<br />

Alternative Matrices <strong>Standards</strong><br />

AccuStandard has manufactured a number of<br />

Diesel and White Mineral Oil QC products<br />

containing a gravimetrically prepared amount of<br />

Sulfur. Use of these alternative matrix materials<br />

can provide further evaluation of the QA/QC<br />

process in the laboratory. Two samples will be<br />

sent for the test parameter and a separate sealed<br />

envelope containing the gravimetrically prepared<br />

sulfur values is also provided. The second<br />

sample is for repeatability testing or for use as a<br />

future QA/QC reference.<br />

Technical Note<br />

This comprehensive<br />

single blind gasoline QC<br />

sample tests for more<br />

parameters from a single<br />

sample. The actual<br />

gasoline sample will have<br />

consensus values listed<br />

on the datasheet that fall<br />

within the range listed for<br />

each parameter.<br />

Quality Control <strong>Standards</strong><br />

continue on next page<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 1<br />

Real World<br />

Gasoline<br />

D-02.03 QC D-02.04<br />

QC


<strong>ASTM</strong> Round Robin<br />

&<br />

PT QC Samples<br />

QC<br />

AccuPetroTest Gasoline QC<br />

Olefins QC Sample<br />

SBPT-OLEFIN $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Total Aromatics D-1319 8-60 Vol.%<br />

Total Olefins D-1319 1 - 40 Vol.%<br />

Total Saturates D-1319 30-80 Vol. %<br />

See <strong>ASTM</strong> Method D-1319 for Sulfur Calibration<br />

<strong>Standards</strong><br />

Aromatics QC Sample<br />

SBPT-AROM $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Total Aromatics D-5769 8 - 60 Vol.%<br />

See <strong>ASTM</strong> Methods, D-3606, D-5580-95, D-5769-95<br />

for Benzene Calibration <strong>Standards</strong><br />

2<br />

Quality Control <strong>Standards</strong><br />

Conducting a Petrochemical Round Robin for a new <strong>ASTM</strong> method?<br />

Select AccuStandard to prepare the necessary samples for the Round Robin study<br />

AccuStandard has packaged for <strong>ASTM</strong> committee D-02 various select groups of gasoline fuels and hydrocarbon products for use in various<br />

Round Robin studies.<br />

Large Sample Offering<br />

AccuStandard was selected by <strong>ASTM</strong> committee D-02 to fill, seal and package an initial set of 21 different types of Round Robin Gasolines.<br />

Each gasoline was selected due to its unique properties. These unique properties will be determined by various <strong>ASTM</strong> methods under evaluation<br />

through <strong>ASTM</strong> subcommittees. AccuStandard has expanded this offering with additional materials blended for other <strong>ASTM</strong> Round Robins.<br />

Flexibility<br />

Use the original 21 gasoline samples to conduct a Round Robin and we can label the samples appropriately to protect the integrity of the Round<br />

Robin. In addition, we can easily add additional samples to your specific Round Robin study to expand the scope of the method for different<br />

matrices, concentrations or instrument types.<br />

Petro PT Samples<br />

Oxygenate PT Sample<br />

With MtBE contamination problems in drinking water, numerous states are<br />

now requiring certification for Oxygenate monitoring. Join AccuStandard’s<br />

next study for Oxygenate analysis. Our timely PT schedule easily allows<br />

your lab to be proactive in new regulatory requirements. The analytes in<br />

the standard and the PT sample have been drawn from the California list<br />

of known prevalent oxygenates in gasoline. These new Oxygenate PT<br />

samples and standards allow your Lab to:<br />

• Expand testing capabilities<br />

• Generate new testing revenue<br />

WS-PT Oxygenates<br />

*<br />

ETBE<br />

Diisopropylether<br />

Sulfur QC Sample<br />

SBPT-SGAS $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Sulfur D-2622 0.0001 - 0.0930 Wt.%<br />

Sulfur D-4294 0.0016 - 0.0930 Wt.%<br />

Sulfur D-5453 4.0 - 500 µg/g<br />

Sulfur D-6344 1.0 - 1000 µg/g<br />

See <strong>ASTM</strong> Methods D-2622, D-3120, D-3246-92,<br />

D-4294, D-5453 for Sulfur Calibration <strong>Standards</strong><br />

Benzene/Toluene QC Sample<br />

SBPT-BENZ $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Benzene D-5769 0.1 - 2.0 Vol.%<br />

Toluene D-5769 1.0 - 15 Vol.%<br />

See <strong>ASTM</strong> Methods, D-3606, D-5580-95, D-5769-95<br />

for Benzene Calibration <strong>Standards</strong><br />

• Eliminate standard preparation<br />

• Easily combine with other<br />

AccuStandard Volatile standards<br />

OPE-OXY-001-AS $ 47 / 2 mL<br />

OPE-OXY-001-AT $ 47 / 2 mL<br />

OPE-OXY-001-AV $ 47 / 2 mL<br />

Sample conc. after prep 5.0-50 µg/L<br />

Contains 4 analytes listed below<br />

MTBE<br />

TAME<br />

NEW<br />

NEW<br />

Suggested Calibration Standard<br />

Oxygenate Gasoline Additive Standard<br />

OGAD-001 $ 30 / 1 x 1 mL<br />

OGAD-001-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

At stated conc. in MeOH 5 comps.<br />

MtBE (2000 µg/mL) TAME (2000 µg/mL)<br />

ETBE (2000 µg/mL) t-Butanol (10000 µg/mL)<br />

Isopropyl ether (2000 µg/mL)<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

*<br />

AccuPetroTest Single Blind<br />

<strong>Standards</strong><br />

Petrochemical laboratories looking to test<br />

the performance of the laboratory for a<br />

specific parameter can order the Single<br />

Blind AccuPetroTest sample for the<br />

parameter of interest. Two real world<br />

gasoline samples will be sent for the test<br />

parameter requested and a separate sealed<br />

envelope containing the determined<br />

Consensus Value is also provided. The<br />

second sample is for repeatability testing<br />

or as a future QA/QC reference.<br />

WP-PT Oil, Grease & TPH<br />

IPE-OILG-001-AS *<br />

$ 32 / 5 mL<br />

IPE-OILG-001-AT $ 32 / 5 mL<br />

IPE-OILG-001-AV $ 32 / 5 mL<br />

Sample conc. after prep<br />

Contains 2 analytes listed below<br />

Analyte List Sample range<br />

Total Oil & Grease † 5-100 mg/L<br />

TPH 5-100 mg/L<br />

This PT sample can be used by gravimetric oil and grease<br />

methods. In addition, it can also be used for TPH analysis by<br />

gravimetric methods including the EPA method 1664. The<br />

sample contains real world material commonly found at<br />

petroleum containment sites.<br />

Suggested Calibration Standard<br />

Oil and Grease<br />

WC-OILG-10X-1 $ 45 / 100 mL<br />

1000 µg/mL Total Oil and Grease in n-Propanol<br />

Contains 500 µg/mL vegetable oil and 500 µg/mL of petroleum oil.<br />

Shake well before use.<br />

SUFFIX KEY<br />

"AS" = Formal PT Study<br />

"AT" = Pre-Test<br />

"AV" = Values Included<br />

Technical Note<br />

* Designed for NELAC/CA<br />

† Indicates that theses analytes are<br />

included in the NVLAP Scope of<br />

Accreditation, Lab Code 200389-0<br />

Lab Code 200389-0


<strong>ASTM</strong> D-56, D-92, D-93 Flash Point <strong>Standards</strong><br />

Verified by consensus analysis using <strong>ASTM</strong> Method # referenced<br />

Physical Properties<br />

Cat. No. <strong>ASTM</strong> # Nominal Flash Point Price / Unit<br />

<strong>ASTM</strong>-P-132-01 PMCC D93 65°C $ 110 / 250 mL<br />

<strong>ASTM</strong>-P-132-02 PMCC D93 93°C 110 / 250 mL<br />

<strong>ASTM</strong>-P-132-03 COC D92 200°C 110 / 250 mL<br />

<strong>ASTM</strong>-P-132-04 COC D92 230°C 110 / 250 mL<br />

Certified Flash Point <strong>Standards</strong><br />

The reference material is a stable, pure hydrocarbon with a method specific flash point<br />

determined by an inter-laboratory study using the <strong>ASTM</strong> Method # referenced.<br />

Cat. No. <strong>ASTM</strong> # Nominal Flash Point Price / Unit<br />

<strong>ASTM</strong>-P-133-01 PMCC D93 65°C $ 175 / 250 mL<br />

<strong>ASTM</strong>-P-133-02 PMCC D93 134°C 130 / 250 mL<br />

<strong>ASTM</strong>-P-133-03 COC D92 138°C 130 / 250 mL<br />

<strong>ASTM</strong>-P-133-04 TCC D56 67°C 175 / 250 mL<br />

<strong>ASTM</strong> D-86 Synthetic Distillation Standard<br />

The automatic distillation apparatus duplicates the distillation conditions of the manual method. The<br />

increased reliance on electronic control requires an independent standard to verify that the apparatus is<br />

performing correctly. This synthetic blend of hydrocarbons boil in the temperature range specified in<br />

<strong>ASTM</strong> D-86 distillation groups 1 and 2, and a fuel oil that meets the group 4 criteria.<br />

The group 1 and 2 standards cover the boiling range 129 - 368 °F (54 - 187 °C) and are verified by<br />

consensus analysis with twelve refinery laboratories. The group 4 standard covers the range from 410 -<br />

670 °F (210 - 355 °C). Products are packaged in convenient sizes to meet your laboratory sample<br />

analysis demands.<br />

Cat. No. Group Description Price / Unit<br />

<strong>ASTM</strong>-P-126-01 1, 2 Synthetic Distillation Standard $ 160 / 500 mL<br />

<strong>ASTM</strong>-P-126-SET 1, 2 Synthetic Distillation Standard 290 / 2 x 500 mL<br />

<strong>ASTM</strong>-P-127-01 4 Distillation Standard 160 / 250 mL<br />

<strong>ASTM</strong>-P-127-02 4 Distillation Standard 290 / 500 mL<br />

<strong>ASTM</strong> D-92 & Flash & Fire Points by Cleveland Open Cup (COC) &<br />

<strong>ASTM</strong> D-93 Flash Point by Pensky Martin Closed Cup (PMCC)<br />

See Method D-56 on this page for the comprehensive line of flash point standards<br />

<strong>ASTM</strong> D-445 Viscosity Calibration <strong>Standards</strong><br />

Cat. No. Viscosity @ 40 °C Price / Unit<br />

<strong>ASTM</strong>-P-128-01 4 Cst $ 60 / 500 mL<br />

<strong>ASTM</strong>-P-128-02 7 Cst 60 / 500 mL<br />

<strong>ASTM</strong>-P-128-03 19 Cst 60 / 500 mL<br />

<strong>ASTM</strong>-P-128-04 61 Cst 60 / 500 mL<br />

<strong>ASTM</strong>-P-128-05 180 Cst 60 / 500 mL<br />

<strong>ASTM</strong>-P-128-06 520 Cst 60 / 500 mL<br />

Originally designed for<br />

<strong>ASTM</strong> D-445-97<br />

Originally designed for<br />

<strong>ASTM</strong> D-56-98a,<br />

D-92-98a, D-93-99b<br />

Originally designed for<br />

<strong>ASTM</strong> D-86-99a<br />

Technical Note<br />

Oils are tested in<br />

accordance with<br />

<strong>ASTM</strong> D-445<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 3<br />

Method 56, 92, 93<br />

86<br />

445<br />

Member<br />

<strong>Standards</strong> of Interest<br />

Also see Cloud Point<br />

<strong>Standards</strong> used for <strong>ASTM</strong><br />

Method D-2500 on page 5<br />

QC<br />

<strong>ASTM</strong>


Method 611<br />

1015<br />

1319<br />

Member<br />

<strong>ASTM</strong><br />

<strong>ASTM</strong> D-611 (Reapproved 1998) Aniline Point <strong>Standards</strong><br />

The accuracy of automated aniline point apparatus can be verified using a range of standards whose<br />

aniline points are determined using <strong>ASTM</strong> D-611 (Method A) and <strong>ASTM</strong> D-611 (Method E). <strong>Standards</strong> are<br />

packaged in 20 mL ampules in an inert atmosphere.<br />

<strong>ASTM</strong> D-1015 Freezing Points of High Purity Hydrocarbons<br />

See Method D-2386 page 5 for AccuStandard’s new line of Freezing Point <strong>Standards</strong><br />

4<br />

Physical Properties<br />

Cat. No. Nominal Aniline Point Price / Unit<br />

D-611-SET Set include 5 <strong>Standards</strong> listed below<br />

Aniline Point Verification Set<br />

Method 611(A)<br />

$ 90 / 5 x 20 mL<br />

D-611-01 0°C 20 mL<br />

D-611-02 30°C 20 mL<br />

D-611-03 55°C 20 mL<br />

D-611-04 68°C 20 mL<br />

D-611-05 94°C 20 mL<br />

Cat. No. Nominal Aniline Point Price / Unit<br />

D-611E-SET Set include 3 <strong>Standards</strong> listed below<br />

Aniline Point Verification Set<br />

Method 611(E)<br />

$ 90 / 3 x 20 mL<br />

D-611E-01 43°C 20 mL<br />

D-611E-02 62°C 20 mL<br />

D-611E-03 77°C 20 mL<br />

Cat. No. Price / Unit<br />

<strong>ASTM</strong>-P-134-PAK Pure Aniline $ 30 / 5 x 15 mL<br />

<strong>ASTM</strong> D-1319 Calibration <strong>Standards</strong> by Fluorescent Indicator Adsorption FIA<br />

Olefin FIA Calibration Curve<br />

FIA-CAL-SET $ 300 / Set of 7 x 1 mL<br />

Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7<br />

Target Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %<br />

Total Olefins 2.0 4.0 5.0 6.0 8.0 10.0 12.0<br />

Total Paraffins 57.0 55.0 52.0 51.0 45.0 45.0 40.0<br />

Total Aromatics 23.0 24.0 25.0 26.0 29.0 28.0 30.0<br />

Total Oxygenate 18.0 17.0 18.0 17.0 18.0 17.0 18.0<br />

FIA Paraffin Standard<br />

FIA-PAR $ 30 / 1 x 1 mL<br />

FIA-PAR-5ML SAVE 33% $ 100 / 1 x 5 mL<br />

8 comps.<br />

Vol. %<br />

n-Pentane 8<br />

n-Hexane 9<br />

Cyclohexane 15<br />

n-Heptane 14<br />

mix ratio<br />

Benzene 4<br />

Toluene 32<br />

Ethylbenzene 8<br />

p-Xylene 8<br />

o-Xylene 8<br />

Vol. %<br />

2,3-Dimethylpentane 14<br />

Isooctane 16<br />

n-Octane 14<br />

n-Decane 7<br />

FIA Aromatic Standard<br />

FIA-ARO $ 30 / 1 x 1 mL<br />

FIA-ARO-5ML SAVE 33% $ 100 / 1 x 5 mL<br />

10 comps.<br />

mix ratio<br />

m-Xylene 16<br />

1,2,4-Trimethylbenzene 8<br />

1,3,5-Trimethylbenzene 8<br />

1,2,4,5-Tetramethylbenzene 4<br />

Naphthalene 4<br />

FIA Olefin Standard<br />

FIA-OLE $ 40 / 1 x 1 mL<br />

FIA-OLE-5ML SAVE 40% $ 120 / 1 x 5 mL<br />

3 comps.<br />

Vol. %<br />

1-Pentene 33.3<br />

2,3-Dimethyl-2-butene 33.3<br />

<strong>Standards</strong> of Interest<br />

Originally designed for<br />

D-611-82<br />

Originally<br />

designed for<br />

D-1319-99<br />

D-1319<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

Vol. %<br />

1-Heptene 33.3<br />

For the mandatory real world QC samples<br />

stipulated in the Method, see page 1-2<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Technical Note<br />

For routine purposes pure<br />

Aniline is packaged in ampules<br />

under dry nitrogen. This<br />

minimizes the risk of oxidation.<br />

Technical Note<br />

The following set of standards<br />

have been prepared for the<br />

determination of Aromatics,<br />

Olefins, Oxygenates and<br />

Saturates in petroleum fractions<br />

by Fluorescent Indicator<br />

Adsorption (FIA) IP designation<br />

156/95.<br />

The final certificate for the FIA<br />

calibration curve lists not only<br />

the volume percents for the<br />

hydrocarbon types, but also the<br />

individual volume percents for<br />

each analyte in the functional<br />

group.<br />

To further assist the<br />

Petrochemist, the weight fraction<br />

for each hydrocarbon type and<br />

individual analyte is listed on the<br />

final certificate. By providing the<br />

individual weights the<br />

Petrochemical chemist can use<br />

the FIA standards for other<br />

types of instrumentation<br />

measuring these Petroleum<br />

fractions.


<strong>ASTM</strong> D-1744, E-1064, D-4377 Water in Liquid Petroleum Products by<br />

D-4928, D-6304 Karl Fischer<br />

<strong>ASTM</strong> D-2386 Freezing Point Calibration <strong>Standards</strong><br />

<strong>ASTM</strong> D-2500 Cloud Point Calibration <strong>Standards</strong><br />

Physical Properties<br />

<strong>Standards</strong> are available for coulometric Karl Fischer titrations and are packaged in 2 mL, 5 mL, and 20 mL ampules in<br />

sets of 5 and 10. The following concentrations are available:<br />

Cat. No. Description Price / Unit<br />

KF-0.6X-5ML-VAP Water content 60 µg/g $ 65 / 10 x 5 mL<br />

KF-1X-2ML-VAP Water content 100 µg/g 40 / 10 x 2 mL<br />

KF-1X-5ML-VAP Water content 100 µg/g 45 / 10 x 5 mL<br />

KF-1X-20ML-PAK Water content 100 µg/g 50 / 5 x 20 mL<br />

KF-10X-2ML-VAP Water content 1000 µg/g 40 / 10 x 2 mL<br />

KF-10X-5ML-VAP Water content 1000 µg/g 45 / 10 x 5 mL<br />

KF-10X-20ML-PAK Water content 1000 µg/g 50 / 5 x 20 mL<br />

KF-50X-2ML-VAP Water content 5000 µg/g 40 / 10 x 2 mL<br />

KF-50X-5ML-VAP Water content 5000 µg/g 45 / 10 x 5 mL<br />

KF-50X-20ML-PAK Water content 5000 µg/g 50 / 5 x 20 mL<br />

Cat. No. Nominal Freezing Point Price / Unit<br />

<strong>ASTM</strong>-P-129-01 - 50 °C $ 110 / 250 mL<br />

<strong>ASTM</strong>-P-129-02 - 45 °C 110 / 250 mL<br />

Cat. No. Cloud Point, Approx. Value Price / Unit<br />

<strong>ASTM</strong>-P-131-01 + 5 °C $ 110 / 250 mL<br />

<strong>ASTM</strong>-P-131-02 - 2 °C 110 / 250 mL<br />

<strong>ASTM</strong>-P-131-03 - 10 °C 110 / 250 mL<br />

<strong>ASTM</strong>-P-131-04 - 15 °C 110 / 250 mL<br />

<strong>ASTM</strong>-P-131-05 - 20 °C 110 / 250 mL<br />

Value Added Paks (Cat. No.’s<br />

ending in -VAP) provide<br />

multiple single units packaged<br />

together for both greater<br />

stability and cost savings.<br />

Originally designed for<br />

D-2386-97<br />

Originally designed for<br />

D-2500-00<br />

Technical Note<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 5<br />

Method 1744-<br />

6304<br />

2386<br />

2500<br />

Member<br />

Many <strong>ASTM</strong> Petrochemical<br />

methods and specifications<br />

reference using QA/QC<br />

standards for water content<br />

measurements. AccuStandard<br />

has formulated a comprehensive<br />

range of water standards<br />

packaged in convenient sizes to<br />

meet the various referenced<br />

methods.<br />

Technical Note<br />

Verified by consensus analysis by<br />

<strong>ASTM</strong> Method D-2386<br />

Technical Note<br />

Verified by consensus analysis by<br />

<strong>ASTM</strong> Method D-2500<br />

<strong>ASTM</strong>


<strong>ASTM</strong> Methods for<br />

Sulfur<br />

Analysis<br />

<strong>ASTM</strong><br />

SULFUR<br />

6<br />

Sulfur <strong>Standards</strong><br />

D-2622-98, D-3120-96, D-3246-96, D-4294-98, D-5453-00, D-6334-98, D-6445-99 & Proposed <strong>ASTM</strong> Sulfur Methods<br />

AccuStandard offers the Petroleum Industry the most complete line of calibration standards designed for today’s Proposed &<br />

Promulgated test methods for Sulfur analysis. These calibration standards are designed specifically for the analysis of Sulfur in a<br />

wide variety of matrices such as #2 diesel fuel, white mineral oil, kerosene, gasoline, crude oil & residual oil.<br />

Traceability, Quality and Certification<br />

All Sulfur standards are manufactured from the highest quality raw materials, including well characterized starting materials & the<br />

lowest sulfur matrices available from the Petrochemical market. All standards are manufactured on a weight/weight basis using<br />

balances that are calibrated and verified daily against reference mass standards directly traceable to NIST under test No.<br />

822/254480. The concentration of these working level Sulfur standards have established traceability links to NIST SRM’s where<br />

available.<br />

Convenient Packaging<br />

Since applicable concentration ranges will vary based on the instrumentation used & the nature of the sample the standards can be<br />

ordered as complete sets, individual bottles, or Ready-to-Aspirate AccuShots.<br />

AccuShots... Packaged to improve analytical standard integrity<br />

AccuStandard is the first standard manufacturer to provide sulfur standards in convenient and Ready-to-Aspirate AccuShot 20 mL<br />

sealed ampules. Each 20 mL AccuShot provides the necessary material for calibration curve development or daily QA/QC. By<br />

purchasing AccuShots the analytical chemist can open a fresh shot for each analysis which eliminates opening and pipetting<br />

repeatedly from a stock bottle. This minimizes contamination and evaporation. These ship with no haz fee for additional savings.<br />

<strong>ASTM</strong> D-5453<br />

Test to Low ppb<br />

Sulfur<br />

Contact us for a copy of the<br />

Southwest Research Institute<br />

D-5453 Fitness for Use Report<br />

Low Sulfur <strong>Standards</strong> on following pages<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


X-Ray Optical Systems, Inc.<br />

15 Tech Valley Drive<br />

East Greenbush, NY 12061<br />

Tel. 518-880-1500<br />

website: www.xos.com<br />

Analytical Capabilities<br />

MWD XRF Sulfur Analyzer<br />

XOS SINDIE Analyzer<br />

X-Ray optics enable detection capability well<br />

beyond traditional XRF techniques. The<br />

same Monochromatic WD XRF technology<br />

of the SINDIE bench-top sulfur analyzer is<br />

available in an on-line sulfur analyzer.<br />

in Diesel and Gasoline Fuels<br />

Monochromatic WDXRF Technology<br />

Limits of Detection < 1 ppm<br />

Fast and easy sample preparation.<br />

Typical measurement time: 300 sec.<br />

Dynamic range: 0-1000 ppm in one<br />

calibration.<br />

No sample conversion or reagents<br />

required.<br />

Exceptional signal-to-background<br />

provides high sensitivity for<br />

low-level sulfur fuels<br />

SULFUR ANALYSIS IN<br />

ULTRA LOW SULFUR FUELS<br />

Repeatability:<br />

1 ppm 0.5 ppm<br />

10 ppm 1.7 ppm<br />

100 ppm 5.3 ppm<br />

500 ppm 11.7 ppm<br />

7<br />

SULFUR


Sulfur in<br />

Mineral Oil<br />

Diesel Fuel<br />

<strong>ASTM</strong><br />

SULFUR<br />

<strong>ASTM</strong> Methods Sulfur in Mineral Oil<br />

Sulfur in Heavy Weight Mineral Oil (75 cSt)<br />

Sulfur in Ready-to-Use<br />

Concentration White Mineral Oil Sulfur AccuShots<br />

µg/g Wt. % Cat. No. Cat. No.<br />

Blank 0.000 SWMO-BL-4 SWMO-BL-SHOT<br />

100 0.010 SWMO-1X-4 SWMO-1X-SHOT<br />

200 0.020 SWMO-2X-4 SWMO-2X-SHOT<br />

300 0.030 SWMO-3X-4 SWMO-3X-SHOT<br />

400 0.040 SWMO-4X-4 SWMO-4X-SHOT<br />

500 0.050 SWMO-5X-4 SWMO-5X-SHOT<br />

750 0.075 SWMO-7.5X-4 SWMO-7.5X-SHOT<br />

1,000 0.10 SWMO-10X-4 SWMO-10X-SHOT<br />

1,500 0.15 SWMO-15X-4 SWMO-15X-SHOT<br />

2,000 0.20 -------------------- --------------------------<br />

3,000 0.30 SWMO-30X-4 SWMO-30X-SHOT<br />

4,000 0.40 -------------------- --------------------------<br />

5,000 0.50 SWMO-50X-4 SWMO-50X-SHOT<br />

7,000 0.70 SWMO-70X-4 SWMO-70X-SHOT<br />

10,000 1.00 SWMO-100X-4 SWMO-100X-SHOT<br />

15,000 1.50 SWMO-150X-4 SWMO-150X-SHOT<br />

20,000 2.00 SWMO-200X-4 SWMO-200X-SHOT<br />

30,000 3.00 SWMO-300X-4 SWMO-300X-SHOT<br />

40,000 4.00 SWMO-400X-4 SWMO-400X-SHOT<br />

50,000 5.00 SWMO-500X-4 SWMO-500X-SHOT<br />

60,000 6.00 SWMO-600X-4 SWMO-600X-SHOT<br />

Set of above SWMO-CAL-SET-4 Each AccuShot product<br />

Cat. No.’s 19 x 4 oz. $ 850 contains 5 x 20 mL<br />

Individual Sulfur 1 -10 units 10 +units<br />

<strong>Standards</strong> 4 oz Bottle $ 55 ea $ 50 ea<br />

Sulfur conc. calculated from % sulfur in di-n-butyl sulfide<br />

8<br />

Technical Note<br />

Sulfur <strong>Standards</strong><br />

<strong>ASTM</strong> Methods<br />

Sulfur <strong>Standards</strong> for <strong>ASTM</strong> D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 &<br />

Proposed <strong>ASTM</strong> Sulfur Methods<br />

Individual Sulfur 1 -10 units 10 +units<br />

<strong>Standards</strong> 4 oz Bottle $ 55 ea $ 50 ea<br />

<strong>ASTM</strong> Methods Sulfur in #2 Diesel Fuel<br />

ampules at the stated<br />

conc. for $ 60<br />

Sulfur in Ready-to-Use<br />

Concentration #2 Diesel Fuel Sulfur AccuShots<br />

µg/g Wt. % Cat. No. Cat. No.<br />

Blank 0.000 SDF-BL-4 SDF-BL-SHOT<br />

100 0.010 SDF-1X-4 SDF-1X-SHOT<br />

200 0.020 SDF-2X-4 SDF-2X-SHOT<br />

300 0.030 SDF-3X-4 SDF-3X-SHOT<br />

400 0.040 SDF-4X-4 SDF-4X-SHOT<br />

500 0.050 SDF-5X-4 SDF-5X-SHOT<br />

750 0.075 SDF-7.5X-4 SDF-7.5X-SHOT<br />

1,000 0.10 SDF-10X-4 SDF-10X-SHOT<br />

1,500 0.15 SDF-15X-4 SDF-15X-SHOT<br />

2,000 0.20 ------------- -------------<br />

3,000 0.30 SDF-30X-4 SDF-30X-SHOT<br />

4,000 0.40 ------------- -------------<br />

5,000 0.50 SDF-50X-4 SDF-50X-SHOT<br />

7,000 0.70 SDF-70X-4 SDF-70X-SHOT<br />

10,000 1.00 SDF-100X-4 SDF-100X-SHOT<br />

15,000 1.50 SDF-150X-4 SDF-150X-SHOT<br />

20,000 2.00 SDF-200X-4 SDF-200X-SHOT<br />

30,000 3.00 SDF-300X-4 SDF-300X-SHOT<br />

40,000 4.00 SDF-400X-4 SDF-400X-SHOT<br />

50,000 5.00 SDF-500X-4 SDF-500X-SHOT<br />

60,000 6.00 SDF-600X-4 SDF-600X-SHOT<br />

Set of above SDF-CAL-SET-4 Each AccuShot product<br />

Cat. No.’s 19 x 4 oz. $ 850 contains 5 x 20 mL<br />

ampules at the stated<br />

conc. for $ 60<br />

Sulfur in Light Weight Mineral Oil (20 cSt)<br />

Sulfur in Ready-to-Use<br />

Concentration White Mineral Oil Sulfur AccuShots<br />

µg/g Wt. % Cat. No. Cat. No.<br />

Blank 0.000 SWMO-LT-BL-4 SWMO-LT-BL-SHOT<br />

100 0.010 SWMO-LT-1X-4 SWMO-LT-1X-SHOT<br />

200 0.020 SWMO-LT-2X-4 SWMO-LT-2X-SHOT<br />

300 0.030 SWMO-LT-3X-4 SWMO-LT-3X-SHOT<br />

400 0.040 SWMO-LT-4X-4 SWMO-LT-4X-SHOT<br />

500 0.050 SWMO-LT-5X-4 SWMO-LT-5X-SHOT<br />

750 0.075 SWMO-LT-7.5X-4 SWMO-LT-7.5X-SHOT<br />

1,000 0.10 SWMO-LT-10X-4 SWMO-LT-10X-SHOT<br />

1,500 0.15 SWMO-LT-15X-4 SWMO-LT-15X-SHOT<br />

2,000 0.20 -------------------- --------------------------<br />

3,000 0.30 SWMO-LT-30X-4 SWMO-LT-30X-SHOT<br />

4,000 0.40 -------------------- --------------------------<br />

5,000 0.50 SWMO-LT-50X-4 SWMO-LT-50X-SHOT<br />

7,000 0.70 SWMO-LT-70X-4 SWMO-LT-70X-SHOT<br />

10,000 1.00 SWMO-LT-100X-4 SWMO-LT-100X-SHOT<br />

15,000 1.50 SWMO-LT-150X-4 SWMO-LT-150X-SHOT<br />

20,000 2.00 SWMO-LT-200X-4 SWMO-LT-200X-SHOT<br />

30,000 3.00 SWMO-LT-300X-4 SWMO-LT-300X-SHOT<br />

40,000 4.00 SWMO-LT-400X-4 SWMO-LT-400X-SHOT<br />

50,000 5.00 SWMO-LT-500X-4 SWMO-LT-500X-SHOT<br />

60,000 6.00 SWMO-LT-600X-4 SWMO-LT-600X-SHOT<br />

Set of above SWMO-LT-CAL-SET-4 Each AccuShot product<br />

Cat. No.’s 19 x 4 oz. $ 850 contains 5 x 20 mL<br />

Individual Sulfur 1 -10 units 10 +units<br />

<strong>Standards</strong> 4 oz Bottle $ 55 ea $ 50 ea<br />

Ready-to-Use<br />

ampules at the stated<br />

conc. for $ 60<br />

AccuShots... Packaged to improve analytical<br />

standard integrity<br />

AccuStandard is the first standard manufacturer to<br />

provide sulfur standards in convenient and Ready-to-<br />

Aspirate AccuShot 20 mL sealed ampules. Each 20 mL<br />

AccuShot provides the necessary material for calibration<br />

curve development or daily QA/QC. By purchasing<br />

AccuShots the analytical chemist can open a fresh shot<br />

for each analysis which eliminates opening and pipetting<br />

repeatadly from a stock bottle. This minimizes<br />

contamination and evaporation. These ship with no haz<br />

fee for additional savings.<br />

Cross Reference Table<br />

<strong>ASTM</strong> IP ISO DIN JIS AFNOR sorted by<br />

<strong>ASTM</strong> Method see beginning of Catalog<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


Sulfur <strong>Standards</strong><br />

Method <strong>ASTM</strong> SulfurMethods for in<br />

Kerosene Sulfur<br />

<strong>ASTM</strong> Methods Sulfur in Kerosene<br />

Sulfur in Light Ready-to-Use<br />

Concentration Distillate Kerosene Sulfur AccuShots<br />

µg/g Wt. % Cat. No. Cat. No.<br />

Blank 0.000 SK-BL-4 SK-BL-SHOT<br />

100 0.010 SK-1X-4 SK-1X-SHOT<br />

200 0.020 ---------------<br />

300 0.030 SK-3X-4 SK-3X-SHOT<br />

400 0.040 ---------------<br />

500 0.050 SK-5X-4 SK-5X-SHOT<br />

750 0.075 SK-7.5X-4 SK-7.5X-SHOT<br />

1,000 0.10 SK-10X-4 SK-10X-SHOT<br />

1,500 0.15 ---------------<br />

2,000 0.20 SK-20X-4 SK-20X-SHOT<br />

3,000 0.30 SK-30X-4 SK-30X-SHOT<br />

4,000 0.40 SK-40X-4 SK-40X-SHOT<br />

5,000 0.50 SK-50X-4 SK-50X-SHOT<br />

7,000 0.70 ---------------<br />

10,000 1.00 SK-100X-4 SK-100X-SHOT<br />

15,000 1.50 ---------------<br />

20,000 2.00 SK-200X-4 SK-200X-SHOT<br />

30,000 3.00 ---------------<br />

40,000 4.00 ---------------<br />

50,000 5.00 ---------------<br />

60,000 6.00 ---------------<br />

Set of above SK-CAL-SET-4 Each AccuShot product<br />

Cat. No.’s 12 x 4 oz. $ 500 contains 5 x 20 mL<br />

Individual Sulfur 1 -10 units 10 +units<br />

<strong>Standards</strong> 4 oz Bottle $ 55 ea $ 50 ea<br />

ampules at the stated<br />

conc. for $ 60<br />

<strong>ASTM</strong> Methods<br />

Sulfur <strong>Standards</strong> for <strong>ASTM</strong> D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 &<br />

Proposed <strong>ASTM</strong> Sulfur Methods<br />

Sulfur in Light Distillate Kerosene<br />

Sulfur in Heavy Distillate Kerosene<br />

Concentration<br />

Sulfur in Heavy<br />

Distillate Kerosene<br />

µg/g Wt. % Cat. No.<br />

Blank 0.000 SK-HD-BL-4<br />

100 0.010 SK-HD-1X-4<br />

200 0.020 SK-HD-2X-4<br />

300 0.030 SK-HD-3X-4<br />

400 0.040 SK-HD-4X-4<br />

500 0.050 SK-HD-5X-4<br />

750 0.075 SK-HD-7.5X-4<br />

1,000 0.10 SK-HD-10X-4<br />

1,500 0.15 SK-HD-15X-4<br />

2,000 0.20 SK-HD-20X-4<br />

3,000 0.30 SK-HD-30X-4<br />

4,000 0.40 SK-HD-40X-4<br />

5,000 0.50 SK-HD-50X-4<br />

7,000 0.70 SK-HD-70X-4<br />

10,000 1.00 SK-HD-100X-4<br />

15,000 1.50 SK-HD-150X-4<br />

20,000 2.00 SK-HD-200X-4<br />

30,000 3.00 SK-HD-300X-4<br />

40,000 4.00 SK-HD-400X-4<br />

50,000 5.00 SK-HD-500X-4<br />

60,000 6.00 SK-HD-600X-4<br />

Set of above SK-HD-CAL-SET-4<br />

Cat. No.’s 21 x 4 oz. $ 950<br />

Individual Sulfur 1 -10 units 10 +units<br />

<strong>Standards</strong> 4 oz Bottle $ 55 ea $ 50 ea<br />

Technical Note<br />

Sulfur concentration<br />

calculated from % sulfur<br />

in di-n-butyl sulfide.<br />

<strong>Standards</strong> of Interest<br />

For the mandatory real<br />

world QC samples<br />

stipulated in the Method,<br />

see pages 1- 2.<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 9<br />

<strong>ASTM</strong> SULFUR


<strong>ASTM</strong> 2622-<br />

6445<br />

<strong>ASTM</strong><br />

SULFUR<br />

<strong>ASTM</strong> D-2622, D-4294 Sulfur Calibration <strong>Standards</strong> <strong>ASTM</strong> D-2622, D-6334, Low Level Sulfur<br />

D-6445 Calibration <strong>Standards</strong><br />

Sulfur Calibration <strong>Standards</strong> in Isooctane for<br />

Gasoline & Reformulated Gasoline Analysis<br />

<strong>Standards</strong> can be mixed for quantity discounts<br />

1 to 4 units $ 60 each per Sulfur Standard<br />

5 to 10 units $ 55 each per Sulfur Standard<br />

more than 10 units $ 50 each per Sulfur Standard<br />

Cat. No. Sulfur Conc. Sulfur Wt. % Unit<br />

STP-BL-4 Blank 0.0 4 oz.<br />

STP-1X-4 10 µg/g 0.001 4 oz.<br />

STP-2X-4 20 µg/g 0.002 4 oz.<br />

STP-3X-4 30 µg/g 0.003 4 oz.<br />

STP-5X-4 50 µg/g 0.005 4 oz.<br />

STP-10X-4 100 µg/g 0.010 4 oz.<br />

STP-20X-4 200 µg/g 0.020 4 oz.<br />

STP-30X-4 300 µg/g 0.030 4 oz.<br />

STP-40X-4 400 µg/g 0.040 4 oz.<br />

STP-60X-4 600 µg/g 0.060 4 oz.<br />

STP-100X-4 1000 µg/g 0.10 4 oz.<br />

STP-200X-4 2000 µg/g 0.20 4 oz.<br />

STP-300X-4 3000 µg/g 0.30 4 oz.<br />

STP-CAL-SET $ 650 / set of 13 x 4 oz.<br />

In Isooctane Set contains the above 13 individual bottles<br />

<strong>ASTM</strong> D-3120, D-3246 Sulfur Calibration Set<br />

10<br />

Technical Note<br />

A well characterized di-n-butyl sulfide starting mat’l is used with a<br />

low sulfur Isooctane matrix for RFG/gasoline sulfur standards.<br />

Sulfur Calibration Set<br />

D-3120-92-CAL-SET $ 75 / set of 8 x 1 mL<br />

In Isooctane<br />

Cat. No. Sulfur Conc. Sulfur Wt. %<br />

D-3120-92-BL Blank ———<br />

D-3120-92-1X 1 µg/g 0.0001<br />

D-3120-92-3X 3 µg/g 0.0003<br />

D-3120-92-10X 10 µg/g 0.0010<br />

D-3120-92-30X 30 µg/g 0.0030<br />

D-3120-92-50X 50 µg/g 0.0050<br />

D-3120-92-75X 75 µg/g 0.0075<br />

D-3120-92-100X 100 µg/g 0.010<br />

Technical Note<br />

Well characterized di-n-butyl sulfide is used in a low sulfur<br />

Isooctane matrix for this calibration set.<br />

<strong>Standards</strong> of Interest<br />

For the mandatory real world QC samples stipulated in many<br />

<strong>ASTM</strong> Sulfur Methods, see page 1-2<br />

Member<br />

Sulfur <strong>Standards</strong><br />

<strong>ASTM</strong> Methods<br />

Originally<br />

designed for<br />

D-2622-98<br />

D-4294-98<br />

Originally<br />

designed for<br />

D-3120-96<br />

D-3246-96<br />

Low Level Sulfur Calibration <strong>Standards</strong> for use on<br />

XRF Energy Dispersive or Wavelength Instruments<br />

<strong>Standards</strong> can be mixed for quantity discounts<br />

1 to 4 units $ 60 each per Sulfur Standard<br />

5 to 10 units $ 55 each per Sulfur Standard<br />

more than 10 units $ 50 each per Sulfur Standard<br />

Cat. No. Sulfur Conc. Sulfur Wt. % Unit<br />

D-2622-LL-BL-4 Blank 0.0 4 oz.<br />

D-2622-LL-5X-4 5 µg/g 0.0005 4 oz.<br />

D-2622-LL-10X-4 10 µg/g 0.0010 4 oz.<br />

D-2622-LL-30X-4 30 µg/g 0.0030 4 oz.<br />

D-2622-LL-50X-4 50 µg/g 0.0050 4 oz.<br />

D-2622-LL-75X-4 75 µg/g 0.0075 4 oz.<br />

D-2622-LL-100X-4 100 µg/g 0.010 4 oz.<br />

D-2622-LL-300X-4 300 µg/g 0.030 4 oz.<br />

D-2622-LL-500X-4 500 µg/g 0.050 4 oz.<br />

D-2622-LL-1000X-4 1000 µg/g 0.100 4 oz.<br />

D-2622-LL-CAL-SET $ 450 / 10 x 4 oz.<br />

In Isooctane : Toluene (3:1)<br />

Set contains the above 10 individual bottles<br />

Technical Note<br />

Well characterized Thiophene & 2-Methyl thiophene are used<br />

in a low sulfur Isooctane/Toluene matrix for this calibration set.<br />

<strong>ASTM</strong> D-2622, D-6334, Mid Level Sulfur<br />

D-6445 Calibration <strong>Standards</strong><br />

New Requested Additions for use on XRF Energy<br />

Dispersive or Wavelength Instruments<br />

<strong>Standards</strong> can be mixed for quantity discounts<br />

1 to 4 units $ 60 each per Sulfur Standard<br />

5 to 10 units $ 55 each per Sulfur Standard<br />

more than 10 units $ 50 each per Sulfur Standard<br />

Cat. No. Sulfur Conc. Sulfur Wt. % Unit<br />

D-2622-LL-200X-4 200 µg/g 0.020 4 oz<br />

D-2622-LL-400X-4 400 µg/g 0.040 4 oz<br />

D-2622-LL-600X-4 600 µg/g 0.060 4 oz<br />

D-2622-LL-700X-4 700 µg/g 0.070 4 oz<br />

D-2622-LL-800X-4 800 µg/g 0.080 4 oz<br />

D-2622-LL-900X-4 900 µg/g 0.090 4 oz<br />

D-2622-LL-1100X-4 1100 µg/g 0.110 4 oz<br />

D-2622-LL-1200X-4 1200 µg/g 0.120 4 oz<br />

Technical Note<br />

Well characterized Thiophene & 2-Methyl thiophene are used<br />

in a low sulfur Isooctane/Toluene matrix for this calibration set.<br />

AccuStandard is an active member in <strong>ASTM</strong> and<br />

strives to keep abreast of <strong>ASTM</strong> method revisions.<br />

If our listed formulation does not meet the most<br />

recent method revision, please contact Technical<br />

Support, ext. 117 for an updated product.<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Originally<br />

designed for<br />

D-2622-98<br />

D-6334-98<br />

D-6445-99<br />

Originally<br />

designed for<br />

D-2622-98<br />

D-6334-98<br />

D-6445-99


Individual Sulfur 1 -10 units 10 +units<br />

<strong>Standards</strong> 4 oz Bottle $ 75 ea $ 65 ea<br />

<strong>ASTM</strong> Methods Sulfur <strong>Standards</strong><br />

<strong>ASTM</strong>-SSTD-A/B-SET $ 100 / 10 x 2 mL<br />

The set contains the following 10 standards in isooctane<br />

<strong>ASTM</strong> D-2789 Hydrocarbon Types in Low Olefinic Gas by MS<br />

(Vol. %)<br />

2-Methylpentane 7.2<br />

2,4-Dimethylpentane 9.4<br />

n-Octane 16.6<br />

Methylcyclopentane 7.1<br />

Methylcyclohexane 10<br />

Sulfur <strong>Standards</strong><br />

<strong>ASTM</strong> Methods<br />

Sulfur <strong>Standards</strong> for <strong>ASTM</strong> D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 &<br />

Proposed <strong>ASTM</strong> Sulfur Methods<br />

<strong>ASTM</strong> Methods Sulfur Calibration <strong>Standards</strong><br />

Sulfur in Crude Oil <strong>Standards</strong><br />

Concentration Sulfur in Crude Oil<br />

µg/g Wt. % Cat. No.<br />

1,000 0.10 SCO-10X-4<br />

2,500 0.25 SCO-25X-4<br />

5,000 0.50 SCO-50X-4<br />

10,000 1.00 SCO-100X-4<br />

20,000 2.00 SCO-200X-4<br />

30,000 3.00 SCO-300X-4<br />

40,000 4.00 SCO-400X-4<br />

50,000 5.00 SCO-500X-4<br />

Set of above SCO-CAL-SET-4<br />

Cat. No.’s 8 x 4 oz. $ 500<br />

Total Sulfur in Aromatic Compounds<br />

by Hydrogenolysis & Rateometric<br />

Colorimetry<br />

<strong>ASTM</strong>-P-0010-PAK $ 75 / 5 x 1 mL<br />

1000 µg/mL in Toluene<br />

Sulfur (as Thiophene)<br />

Cat. No. Description Unit<br />

<strong>ASTM</strong>-SSTDA-BL Sulfur Blank 2 mL<br />

<strong>ASTM</strong>-SSTDA-01 Sulfur @ 0.5 µg/g in Isooctane 2 mL<br />

<strong>ASTM</strong>-SSTDA-02 Sulfur @ 1.0 µg/g in Isooctane 2 mL<br />

<strong>ASTM</strong>-SSTDA-03 Sulfur @ 2.5 µg/g in Isooctane 2 mL<br />

<strong>ASTM</strong>-SSTDA-04 Sulfur @ 5.0 µg/g in Isooctane 2 mL<br />

<strong>ASTM</strong>-SSTDB-BL Sulfur Blank 2 mL<br />

<strong>ASTM</strong>-SSTDB-04 Sulfur @ 5.0 µg/g in Isooctane 2 mL<br />

<strong>ASTM</strong>-SSTDB-05 Sulfur @ 10.0 µg/g in Isooctane 2 mL<br />

<strong>ASTM</strong>-SSTDB-06 Sulfur @ 25.0 µg/g in Isooctane 2 mL<br />

<strong>ASTM</strong>-SSTDB-07 Sulfur @ 50.0 µg/g in Isooctane 2 mL<br />

Composition Test Mix<br />

D-2789-CTM $ 40 / 1 x 1 mL<br />

D-2789-CTM-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

9 comps.<br />

(Vol. %)<br />

cis-1,2-Dimethylcyclohexane 15.5<br />

Benzene 7.7<br />

Toluene 10<br />

p-Xylene 16.5<br />

Sulfur in Residual Oil <strong>Standards</strong><br />

Concentration Sulfur in Crude Oil<br />

µg/g Wt. % Cat. No.<br />

3,500 0.35 SRO-35X-4<br />

7,000 0.70 SRO-70X-4<br />

10,000 1.00 SRO-100X-4<br />

15,000 1.50 SRO-150X-4<br />

20,000 2.00 SRO-200X-4<br />

30,000 3.00 SRO-300X-4<br />

40,000 4.00 SRO-400X-4<br />

Set of above SRO-CAL-SET-4<br />

Cat. No.’s 7 x 4 oz. $ 450<br />

Individual Sulfur 1 -10 units 10 +units<br />

<strong>Standards</strong> 4 oz Bottle $ 75 ea $ 65 ea<br />

Trace Quantities of Sulfur in Liquid<br />

Aromatic Hydrocarbons by Oxidative<br />

Microcoulometry<br />

<strong>ASTM</strong>-P-0020-PAK $ 75 / 5 x 1 mL<br />

1000 µg/mL in Xylenes<br />

Sulfur (as Dibenzothiophene)<br />

Originally<br />

designed for<br />

D-2789-95<br />

Technical Note<br />

AccuStandard's Technical<br />

Service Dept. can provide<br />

Ready-to-Inject working level<br />

calibration standards to meet<br />

unique laboratory applications.<br />

Call or fax us your standard<br />

requirements.<br />

Technical Note<br />

Both the actual volume %<br />

ratio and the final weight<br />

fractions for each analyte will<br />

be listed on the certificate.<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 11<br />

<strong>ASTM</strong> 2789<br />

<strong>ASTM</strong> SULFUR


PIANO<br />

PIONA<br />

PIANO, PONA, PNA Analysis<br />

12<br />

PIANO<br />

PONA<br />

PNA<br />

Low Aromatic PIAN Blend<br />

<strong>ASTM</strong>-P-0036 $ 120 / 100 µL<br />

110 comps.<br />

Low Aromatic blend contains the PIAN components<br />

blended to resemble a light naphtha. The actual certificate<br />

will have the exact weight % for each analyte accurate to<br />

four decimal places. Analyte list is drawn from<br />

Cat. No.’s: <strong>ASTM</strong>-P-0031, <strong>ASTM</strong>-P-0032,<br />

<strong>ASTM</strong>-P-0033, <strong>ASTM</strong>-P-0034<br />

PIANO, PONA, PNA<br />

AccuStandard has introduced the PIANO line of quantitative and qualitative Petrochemical <strong>Standards</strong> for class type analysis of petrochemical<br />

samples or product streams. PIANO analysis involves the determination of the percentage of the following five fractions Paraffins, Isoparaffins,<br />

Aromatics, Naphthenes, and Olefins.<br />

PONA analysis involves analyzing the naphtha sample for Paraffins, Olefins, Naphthenes, and Aromatics. If the Isoparaffins and Olefins are not<br />

present, the analysis is just for PNA.<br />

The PIANO line of standards is used to determine quantitative and qualitative retention times and indices as well as to monitor response factors<br />

within the hydrocarbon blend. These complex mixes are prepared from materials of the highest available purity, accurate to four decimal places,<br />

and include a detailed data sheet on the formulation composition. The typical range for the analytes in each formulation has been provided for<br />

each catalog item. The exact composition on a weight % basis for each analyte has been provided on the certificate, and a disk deliverable<br />

spreadsheet is available on request.<br />

Mini Inert Valves Seal<br />

The PIANO standards are supplied in convenient to use crimp top vials with Viton septa that resist<br />

mineral oil, aliphatic, aromatics hydrocarbons, and higher temperatures. Mini inert valve seals are<br />

available for an additional $ 25 vial. To order, add “-MIV” to any of the PIANO catalog numbers on<br />

this page.<br />

PIANO Mixture<br />

<strong>ASTM</strong>-P-0030 $ 250 / 100 µL<br />

135 comps.<br />

The PIANO formulation contains the n-Paraffins,<br />

Isoparaffins,Aromatics, Naphthenes, and Olefins from the<br />

five Cat. No.’s: <strong>ASTM</strong>-P-0031, <strong>ASTM</strong>-P-0032,<br />

<strong>ASTM</strong>-P-0033, <strong>ASTM</strong>-P-0034, <strong>ASTM</strong>-P-0035<br />

Approximate weight percentages for the total: n-Paraffins<br />

18.5%, Isoparaffins 17.9%, Aromatics 23.6%, Naphthenes<br />

20.9%, Olefins 19.0%.<br />

The actual certificate will list the weight % for all analytes<br />

in the formulation.<br />

High Aromatic PIAN Blend<br />

<strong>ASTM</strong>-P-0037 $ 120 / 100 µL<br />

110 comps.<br />

High Aromatic blend contains the PIAN components<br />

blended to resemble a reformate. The actual certificate<br />

will have the exact weight % for each analyte accurate<br />

to four decimal places. Analyte list is drawn from<br />

Cat. No.’s: <strong>ASTM</strong>-P-0031, <strong>ASTM</strong>-P-0032,<br />

<strong>ASTM</strong>-P-0033, <strong>ASTM</strong>-P-0034<br />

<strong>Standards</strong> of Interest<br />

For individual PIANO descriptions see next page<br />

AccuStandard, Your <strong>Standards</strong> and Technical Information Source!<br />

Total Petroleum<br />

Hydrocarbon Pattern<br />

Recognition <strong>Standards</strong><br />

BOOK-TPH $ 35<br />

Analytical <strong>Standards</strong> and<br />

Reference Material for all<br />

209 PCB Congeners<br />

S-3571 $ 25<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


PIANO, PONA, PNA Analysis<br />

PIANO Mix Set<br />

<strong>ASTM</strong>-PIANO-SET $ 700 / 6 x 100 µL<br />

Set includes the following Cat. No.:<br />

<strong>ASTM</strong>-P-0030, <strong>ASTM</strong>-P-0031, <strong>ASTM</strong>-P-0032,<br />

<strong>ASTM</strong>-P-0033, <strong>ASTM</strong>-P-0034, <strong>ASTM</strong>-P-0035<br />

PIANO n-Paraffins Mix<br />

<strong>ASTM</strong>-P-0031 $ 80 / 100 µL<br />

11 paraffins listed below at varying Wt. %<br />

typically in the range from 7.0 to 11.0 Wt. %.<br />

The actual certificate will have the exact Wt.<br />

% for each analyte.<br />

Typ. Wt. %<br />

n-Pentane 9.4375<br />

n-Hexane 9.5661<br />

n-Heptanea 9.8048<br />

n-Octane 9.5518<br />

n-Nonane 9.0482<br />

n-Decane 9.2517<br />

n-Undecane 9.3172<br />

n-Dodecane 9.1855<br />

n-Tridecane 8.9332<br />

n-Tetradecane 8.7989<br />

n-Pentadecane 7.1057<br />

PIANO Aromatics Mix<br />

<strong>ASTM</strong>-P-0033 $ 120 / 100 µL<br />

38 Aromatics listed below at varying Wt. %<br />

typically in the range from 0.2 to 7.0 Wt. %.<br />

The actual certificate will have the exact<br />

Wt. % for each analyte.<br />

Typ. Wt. %<br />

Benzene 7.1437<br />

Toluene 4.5738<br />

EthylBenzene 6.7670<br />

m-Xylene 2.2259<br />

p-Xylene 4.4815<br />

o-Xylene 2.2519<br />

Isopropylbenzene 2.2248<br />

n-Propylbenzene 4.4979<br />

1-Methyl-3-ethylbenzene 2.2243<br />

1-Methyl-4-ethylbenzene 2.2206<br />

1,3,5-Trimethylbenzene 1.1076<br />

1-Methyl-2-ethylbenzene 2.2611<br />

1,2,4-Trimethylbenzene 2.2535<br />

tert-Butylbenzene 4.5310<br />

Isobutylbenzene 4.4216<br />

sec-Butylbenzene 2.2368<br />

1-Methyl-3-isopropylbenzene 1.1066<br />

1-Methyl-4-isopropylbenzene 1.0668<br />

1-Methyl-2-isopropylbenzene 1.1241<br />

1-Methyl-3-n-propylbenzene 2.1135<br />

1-Methyl-4-n-propylbenzene 2.2336<br />

n-Butylbenzene 2.2087<br />

1,2-Diethylbenzene 1.0947<br />

1-Methyl-2-n-propylbenzene 2.2641<br />

1,4-Dimethyl-2-ethylbenzene 2.2803<br />

1,3-Dimethyl-5-ethylbenzene 2.2858<br />

1,2-Dimethyl-4-ethylbenzene 2.2558<br />

1,3-Dimethyl-2-ethylbenzene 1.1416<br />

1,2-Dimethyl-3-ethylbenzene 2.1864<br />

1,2,4,5-Tetramethylbenzene 0.2360<br />

2-Methylbutylbenzene 1.1453<br />

trans-1-Butyl-2-methylbenzene 0.7641<br />

n-Pentylbenzene 4.4828<br />

t-1-Butyl,3,5-dimethylbenzene 2.1641<br />

t-1-butyl-ethylbenzene 2.2322<br />

1,3,5-Triethylbenzene 4.5671<br />

1,2,4-Triethylbenzene 1.1087<br />

n-Hexylbenzene 4.5029<br />

PIANO, PONA, PNA<br />

Special Packaging<br />

Mini inert valve seals are available for an additional $ 25 / vial.<br />

To order, add “-MIV” to any of the PIANO cat.# on this page.<br />

PIANO Isoparaffins Mix<br />

<strong>ASTM</strong>-P-0032 $ 120 / 100 µL<br />

35 Isoparaffins listed below at varying Wt. % typically in the range from 0.5 to 6.0 Wt. %. The actual<br />

certificate will have the exact Wt. % for each analyte.<br />

Typ. Wt. %<br />

Isopentane 2.1928<br />

2,3-Dimethylbutane 0.4466<br />

2-Methylpentane 3.2815<br />

3-Methylpentane 5.3865<br />

2,2-Dimethylpentane 1.7747<br />

2,4-Dimethylpentane 3.6993<br />

2,2,3-Trimethylbutane 3.9291<br />

3,3-Dimethylpentane 1.1848<br />

2-Methylhexane 2.2384<br />

2,3-Dimethylpentane 1.7883<br />

3-Methylhexane 1.6708<br />

3-Ethylpentane 0.5080<br />

PIANO Naphthenes Mix<br />

<strong>ASTM</strong>-P-0034 $ 120 / 100 µL<br />

30 Napthenes listed below at varying Wt. %<br />

typically in the range from 0.5 to 8.0 Wt. %. The<br />

actual certificate will have the exact Wt. % for<br />

each analyte.<br />

Typ. Wt. %<br />

Cyclopentane 4.9143<br />

Methylcyclopentane 3.2829<br />

Cyclohexane 5.3268<br />

1,1-Dimethylcyclopentane 3.4612<br />

cis-1,3-Dimethylcyclopentane 0.5963<br />

trans-1,2-Dimethylcyclopentane 1.4715<br />

trans-1,3-Dimethylcyclopentane 2.7531<br />

Methylcyclohexane 5.6091<br />

Ethylcyclopentane 3.5534<br />

ctc-1,2,3-Trimethylcyclopentane 1.5859<br />

cct-1,2,4-Trimethylcyclopentane 3.7208<br />

ctc-1,2,4-Trimethylcyclopentane 1.6467<br />

trans-1,4-Dimethylcyclohexane 3.6499<br />

1-Ethyl-1-methylcyclopentane 1.0554<br />

trans-1,2-Dimethylcyclohexane 1.6537<br />

ccc-1,2,3-Trimethylcyclopentane 0.7971<br />

Isopropylcyclopentane 3.5042<br />

cis-1,2-Dimethylcyclohexane 3.7159<br />

n-Propylcyclopentane 3.6438<br />

ccc-1,3,5-Trimethylcyclohexane 3.5263<br />

1,1,4-Trimethylcyclohexane 3.6791<br />

ctt-1,2,4-Trimethylcyclohexane 3.6107<br />

ctc-1,2,4-Trimethylcyclohexane 3.5069<br />

1,1,2-Trimethylcyclohexane 3.3354<br />

Isobutylcyclopentane 3.7123<br />

Isopropylcyclohexane 5.7233<br />

n-Butylcyclopentane 3.6944<br />

Isobutylcyclohexane 5.6729<br />

t-1-Methyl-2-propylcyclohexane 3.8434<br />

t-1-Methyl-2-(4MP)cyclopentane 3.7534<br />

PIANO Mixture<br />

<strong>ASTM</strong>-P-0030 $ 250 / 100 µL (135 comps.)<br />

Typ. Wt. %<br />

2,2-Dimethylhexane 1.3061<br />

2,5-Dimethyl hexane 3.6975<br />

2,2,3-Trimethylpentane 1.7371<br />

2,4-Dimethylhexane 1.6252<br />

2,3-Dimethylhexane 1.6212<br />

2-Methylheptane 4.4073<br />

4-Methylheptane 3.2015<br />

3-Methylheptane 5.5186<br />

3-Ethylhexane 0.6999<br />

3,3-Dimethylheptane 1.7011<br />

2,5-Dimethylheptane 5.6731<br />

3,5-Dimethylheptane 0.7565<br />

Typ. Wt. %<br />

2,3-Dimethylheptane 1.4870<br />

3,4-Dimethylheptane 3.7450<br />

2-Methyloctane 3.7576<br />

3-Methyloctane 5.6020<br />

3,3-Diethylpentane 1.5755<br />

2,2-Dimethyloctane 3.4135<br />

3,3-Dimethyloctane 3.2582<br />

2,3-Dimethyloctane 3.8842<br />

3-Ethyloctane 3.7482<br />

2-Methylnonane 3.7144<br />

3-Methylnonane 5.7687<br />

PIANO Olefins Mix<br />

<strong>ASTM</strong>-P-0035 $ 120 / 100 µL<br />

25 Olefins listed below at varying Wt. %<br />

typically in the range from 1.2 to 9.0 Wt. %.<br />

The actual certificate will have the exact Wt. %<br />

for each analyte.<br />

Typ. Wt. %<br />

3-Methyl-1-butene 1.9396<br />

1-Pentene 4.1355<br />

2-Methyl-1-butene 1.4440<br />

2-Methyl-1,3-butadiene 2.3889<br />

trans-2-Pentene 1.8034<br />

cis-2-Pentene 1.9792<br />

4-Methylpentene-1 3.4372<br />

1-Hexene 7.0484<br />

trans-2-Hexene 1.7302<br />

2-Methylpentene-2 3.3901<br />

cis-2-Hexene 3.8765<br />

1-Heptene 7.6134<br />

trans-3-Heptene 3.3469<br />

cis-3-Heptene 5.8657<br />

trans-2-Heptene 3.7217<br />

cis-2-Heptene 5.7679<br />

1-Octene 7.6901<br />

trans-2-Octene 1.9432<br />

cis-2-Octene 3.9502<br />

1-Nonene 7.6425<br />

trans-3-Nonene 1.9972<br />

cis-3-Nonene 4.0042<br />

trans-2-Nonene 1.9848<br />

cis-2-Nonene 2.7952<br />

1-Decene 8.2053<br />

Production Note<br />

AccuStandard may add and/or subtract<br />

PIANO Analytes and vary the weight %<br />

for each Analyte. The certificate will<br />

reflect the exact Analyte composition.<br />

The PIANO formulation contains the n-Paraffins, Isoparaffins,Aromatics, Naphthenes, and Olefins from<br />

the Five Cat. No.’s: <strong>ASTM</strong>-P-0031, <strong>ASTM</strong>-P-0032, <strong>ASTM</strong>-P-0033, <strong>ASTM</strong>-P-0034, <strong>ASTM</strong>-P-0035<br />

Approximate weight %’s for the total: n-Paraffins 18.5%, Isoparaffins 17.9%, Aromatics 23.6%,<br />

Naphthenes 20.9%, Olefins 19.0%. The certificate lists the weight % for all analytes in the formulation.<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 13<br />

PIANO<br />

PIANO<br />

PONA<br />

PNA<br />

PIONA


Method 2887<br />

DHA<br />

Member<br />

<strong>ASTM</strong><br />

Detailed Hydrocarbon Analysis<br />

<strong>ASTM</strong> D-2887 Boiling Range Distribution of Petroleum Fractions by GC<br />

14<br />

Detailed Hydrocarbon Analysis<br />

Proposed <strong>ASTM</strong> Method for Detailed Hydrocarbon Analysis (DHA)<br />

Determination of Individual Components and Groups of Components in Spark Ignition Engine fuels by<br />

High Efficiency Open Tubular Column Gas Chromatography (Detailed Hydrocarbon Analysis)<br />

Detailed Hydrocarbon Analysis (includes oxygenates)<br />

<strong>ASTM</strong>-P-0038 $ 120 / 100 µL<br />

30 Analytes listed below at varying targeted weight %. The actual certificate will has the exact Wt. % for each analyte.<br />

Ethanol<br />

Pentane<br />

2-Methyl-2-propanol<br />

2-Methylbutene<br />

2,3-Dimethylbutane<br />

Methyl-t-butyl ether<br />

Hexane<br />

Methylcyclopentene<br />

Wt. %<br />

n-Hexane 6<br />

n-Heptane 6<br />

n-Octane 8<br />

n-Nonane 8<br />

n-Decane 12<br />

n-Undecane 12<br />

n-Dodecane 12<br />

n-Tetradecane 12<br />

n-Hexadecane 10<br />

Benzene<br />

Cyclohexane<br />

3-Ethylpentane<br />

t-1,2-Dimethylcyclopentane<br />

Heptane<br />

2,2,3-Trimethylpentane<br />

2,3,3-Trimethylpentane<br />

Toluene<br />

Calibration Mix<br />

DRH-002N $ 10 / 100 mg<br />

DRH-002N-10X $ 40 / 1 gm<br />

17 comps.<br />

Wt. %<br />

n-Octadecane 5<br />

n-Eicosane 2<br />

n-Tetracosane 2<br />

n-Octacosane 1<br />

n-Dotriacontane 1<br />

n-Hexatriacontane 1<br />

n-Tetracontane 1<br />

n-Tetratetracontane 1<br />

Column Test Mixture<br />

<strong>ASTM</strong>-D2887 $ 10 / 1 x 1 mL<br />

1% v/v in n-Octane 2 comps.<br />

n-Hexadecane n-Octadecane<br />

Fuel Oil Degradation/Retention<br />

Time Mix for Quantification of<br />

C 17/Pristane & C 18/Phytane ratios<br />

DRH-005S-10X $ 20 / 1 x 1 mL<br />

2.0 mg/mL each in CH 2Cl 2 : CS 2 (1:1) 4 comps.<br />

Heptadecane<br />

Octadecane<br />

Phytane (2,6,10,14-Tetramethylhexadecane)<br />

Pristane (2,6,10,14-Tetramethylpentadecane)<br />

Octane<br />

Nonane<br />

Decane<br />

Undecane<br />

Dodecane<br />

Tridecane<br />

Tetradecane<br />

Pentadecane<br />

Hexadecane<br />

Heptadecane<br />

Octadecane<br />

Pristane<br />

Calibration Solution *<br />

DRH-002S-R1 $ 50 / 1 x 1 mL<br />

DRH-002S-R1-PAK SAVE 20% $ 200 / 5 x 1 mL<br />

At stated conc. in Chloroform 17 comps.<br />

µg/mL<br />

n-Hexane 600<br />

n-Heptane 600<br />

n-Octane 800<br />

n-Nonane 800<br />

n-Decane 1200<br />

n-Undecane 1200<br />

n-Dodecane 1200<br />

n-Tetradecane 1200<br />

n-Hexadecane 1000<br />

µg/mL<br />

n-Octadecane 500<br />

n-Eicosane 200<br />

n-Tetracosane 200<br />

n-Octacosane 100<br />

n-Dotriacontane 100<br />

n-Hexatriacontane 100<br />

n-Tetracontane 100<br />

n-Tetratetracontane 100<br />

p-Xylene<br />

Ethylbenzene<br />

Octane<br />

2,3-Dimethylheptane<br />

Nonane<br />

5-Methylnonane<br />

1-Ethyl-2-methylbenzene<br />

Complete Hydrocarbon Analysis<br />

Hydrocarbon Window<br />

Defining Standard*<br />

DRH-008S-R2 $ 65 / 1 x 1 mL<br />

DRH-008S-R2-PAK SAVE 20% $ 260 / 5 x 1 mL<br />

500 µg/mL each in Chloroform 35 comps.<br />

Nonadecane<br />

Phytane<br />

Eicosane<br />

Heneicosane<br />

Docosane<br />

Tricosane<br />

Tetracosane<br />

Pentacosane<br />

Hexacosane<br />

Heptacosane<br />

Octacosane<br />

Nonacosane<br />

Decane<br />

Undecane<br />

1,2,3,5-Tetramethylbenzene<br />

Naphthalene<br />

Dodecane<br />

1-Methylnaphthalene<br />

Tridecane<br />

Triacontane<br />

n-Hentriacontane<br />

Dotriacontane<br />

Tritriacontane<br />

Tetratriacontane<br />

Pentatriacontane<br />

Hexatriacontane<br />

Heptatriacontane<br />

Octatriacontane<br />

Nonatriacontane<br />

Tetracontane<br />

Technical Note<br />

AccuStandard offers a hydrocarbon window defining standard with the C 8 to C 40 odd and<br />

even Alkanes. As an added benefit, AccuStandard included pristane and phytane in the<br />

formulation. Use of this one standard measuring the C 17/ pristane and C 18/ phytane ratio<br />

can be used to estimate degradation of fuel oil.<br />

If you prefer, AccuStandard has also developed a fuel oil degradation mixture containing<br />

just the four required analytes to determine the C 17/pristane and C 8/ phytane ratio<br />

Catalog Numbers DRH-005S-10X.<br />

NEW<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

DHA - PONA-VI (PONA 6) is a<br />

qualitative mixture of various<br />

gasoline and refinery materials<br />

prepared to provide nearly every<br />

component that may be encountered<br />

in feedstock and finished gasolines.<br />

Some oxygenates have been added<br />

to allow this blend to be used for<br />

DHA method setup. This blend<br />

contains approximately 450<br />

components (peaks).<br />

<strong>ASTM</strong>-P-0139 $ 120 / 100 µL<br />

Technical Note<br />

This sample is a petroleum fraction<br />

having a boiling range from 250°F to<br />

850°F, evaluated in round robin<br />

studies by the <strong>ASTM</strong> D-02<br />

committee. Use of this sample and<br />

the supplied <strong>ASTM</strong> boiling range<br />

consensus values helps to evaluate<br />

system performance<br />

Calibration Solution *<br />

DRH-002S-R2 $ 50 / 1 x 1 gm<br />

DRH-002S-R2-PAK SAVE 20% $ 200 / 5 x 1 gm<br />

1 % Wt./Wt. each in Chloroform 20 comps.<br />

n-Tetratetracontane<br />

n-Tetracontane<br />

n-Hexatriacontane<br />

n-Dotriacontane<br />

n-Octacosane<br />

n-Tetracosane<br />

n-Eicosane<br />

* Can be shipped by Air and Sea<br />

Originally designed for D-2887-99<br />

<strong>ASTM</strong> D-2887 Reference Gas<br />

Oil Sample Lot #2<br />

D-2887-REFOIL $ 35 / 1 x 1 mL<br />

n-Octadecane<br />

n-Hexadecane<br />

n-Tetradecane<br />

n-Dodecane<br />

n-Undecane<br />

n-Decane<br />

n-Nonane<br />

n-Octane<br />

n-Heptane<br />

n-Hexane<br />

n-Pentane<br />

n-Pentadecane<br />

n-Heptadecane<br />

NEW


SIM DIS <strong>Standards</strong> Simulated Distillation<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 15<br />

Method SIM DIS<br />

Simulated Distillation (SIM DIS) and Proposed Motor Oil Volatility Method<br />

AccuStandard has developed an extensive line of SIM DIS standards for normal and high temperature analytical requirements when generating<br />

boiling point versus retention time calibration curves. Since normal paraffins above Alkane C60 are not readily available, Polywax 500, Polywax<br />

655, Polywax 850 and Polywax 1000 standards have been incorporated to perform SIM DIS analysis of heavy petroleum fractions with boiling<br />

points up to 1350 °F. If you require additional analytes added to the formulations for extended SIM DIS work, use our custom quotation request<br />

form located in the back of the catalog.<br />

Stock SIM DIS Paraffin Solution<br />

<strong>ASTM</strong>-P-0050 $ 85 / 1 x 5 mL<br />

14 comps.<br />

Wt. %<br />

n-Pentane 6.66<br />

n-Hexane 6.66<br />

n-Heptane 6.66<br />

n-Octane 6.66<br />

n-Nonane 6.66<br />

n-Decane 6.66<br />

n-Undecane 6.66<br />

Polywax 500 ®<br />

<strong>ASTM</strong>-P-0051N-2G $ 20 / 2 grams<br />

Polywax 500<br />

Polywax 655 ®<br />

<strong>ASTM</strong>-P-0053N-2G $ 20 / 2 grams<br />

Polywax 655<br />

Petrochemical <strong>Standards</strong><br />

Wt. %<br />

n-Dodecane 13.33<br />

n-Tetradecane 6.66<br />

n-Pentadecane 6.66<br />

n-Hexadecane 6.66<br />

n-Heptadecane 6.66<br />

n-Octadecane 6.66<br />

n-Eicosane 6.66<br />

Wt. %<br />

n-Pentane 0.0333<br />

n-Hexane 0.0333<br />

n-Heptane 0.0333<br />

n-Octane 0.0333<br />

n-Nonane 0.0333<br />

n-Decane 0.0333<br />

n-Undecane 0.0333<br />

n-Dodecane 0.0666<br />

Polywax 850 ®<br />

<strong>ASTM</strong>-P-0137N-2G $ 20 / 2 grams<br />

Polywax 850<br />

Polywax 1000 ®<br />

<strong>ASTM</strong>-P-0138N-2G $ 20 / 2 grams<br />

Polywax 1000<br />

For our complete line of<br />

Organic <strong>Standards</strong>,<br />

request a copy of our<br />

Organic Catalog<br />

Working Level SIM DIS Paraffin Solution<br />

with Polywax 500<br />

<strong>ASTM</strong>-P-0052 $ 40 / 1 x 1 mL<br />

<strong>ASTM</strong>-P-0052-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

At stated conc. in Carbon disulfide 15 comps.<br />

Wt. %<br />

n-Tetradecane 0.0333<br />

n-Pentadecane 0.0333<br />

n-Hexadecane 0.0333<br />

n-Heptadecane 0.0333<br />

n-Octadecane 0.0333<br />

n-Eicosane 0.0333<br />

Polywax 500 0.5<br />

For our complete line of<br />

Inorganic <strong>Standards</strong>,<br />

request a copy of our<br />

Inorganics Catalog<br />

Member<br />

<strong>Standards</strong> of Interest<br />

See <strong>ASTM</strong> Methods D-3710,<br />

D-5307, D-5442, D-6352 for<br />

additional calibration<br />

standards for hydrocarbon<br />

analysis.<br />

Technical Note<br />

AccuStandard designed the<br />

following formulations for a<br />

Proposed <strong>ASTM</strong> Method under<br />

development for Motor Oil<br />

Volatility analysis & SIM DIS<br />

applications.<br />

<strong>ASTM</strong>


Method 3120<br />

3230<br />

,<br />

3231<br />

3237<br />

Member<br />

<strong>ASTM</strong><br />

<strong>ASTM</strong> D-3120 & D-3246 Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry<br />

Sulfur Calibration Set<br />

D-3120-92-CAL-SET $ 75 / set of 8 x 1 mL<br />

In Isooctane<br />

Cat. No. Sulfur Conc. Sulfur Wt.%<br />

D-3120-BL Blank Blank<br />

D-3120-92-1X 1 µg/g 0.0001<br />

D-3120-92-3X 3 µg/g 0.0003<br />

D-3120-92-10X 10 µg/g 0.0010<br />

D-3120-92-30X 30 µg/g 0.0030<br />

D-3120-92-50X 50 µg/g 0.0050<br />

D-3120-92-75X 75 µg/g 0.0075<br />

D-3120-92-100X 100 µg/g 0.010<br />

<strong>ASTM</strong> D-3230 Salts in Crude Oil<br />

Mixed Salt Solution<br />

D-3230-89-1 $ 75 / 100 mL<br />

D-3230-89-5 $ 150 / 500 mL<br />

At stated conc. in Alcohol Solution (1-butanol : MeOH) (ratio 63:37) tr. H 2O 3 comps.<br />

<strong>ASTM</strong> D-3231 Phosphorus in Gasoline<br />

<strong>ASTM</strong> D-3237 Lead in Gasoline by AA Spectroscopy<br />

16<br />

Calcium chloride 10 µg/mL<br />

Magnesium chloride 20 µg/mL<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Sodium chloride 70 µg/mL<br />

Technical Note<br />

Well characterized di-n-butyl sulfide is used<br />

in a low sulfur Isooctane matrix for this<br />

calibration set.<br />

Element Quantity Cat. No. Price<br />

Matrix Conc.<br />

Phosphorus 100 mL ICP-41W-1 $ 34<br />

H 2O 1000 µg/mL<br />

Phosphorus 500 mL ICP-41W-5 $ 67<br />

H 2O 1000 µg/mL<br />

Lead Standard Calibration Curve<br />

D-3237-CAL-SET $ 210 / 4 x 100 mL<br />

Set includes the following Catalog Numbers:<br />

Originally designed for<br />

D-3120-96<br />

D-3246-96<br />

Originally designed for D-3231-99<br />

Cat. No. Description Price / Unit<br />

D-3237-01 Blank 1% Aliquot 336/MIBK $ 20 / 100 mL<br />

D-3237-02 0.02 g Pb / gal ( 5.3 mg Pb/ L) in 1% Aliquat 336 / MIBK $ 80 / 100 mL<br />

D-3237-03 0.05 g Pb / gal ( 13.2 mg Pb/ L) in 1% Aliquat 336 / MIBK $ 80 / 100 mL<br />

D-3237-04 0.10 g Pb / gal ( 26.4 mg Pb/ L) in 1% Aliquat 336 / MIBK $ 80 / 100 mL<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

<strong>Standards</strong> of Interests<br />

See page 1 for AccuStandard’s<br />

comprehensive line of Certified<br />

Sulfur calibration standards,<br />

AccuPetroCheck, and<br />

AccuPetroTest quality control<br />

products.<br />

D-3231<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

D-3237<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

Ready-to-Inject Petrochemical <strong>Standards</strong> and Calibration Curves<br />

Reduce Costs<br />

Increase Time Spent for Sample Analysis<br />

Are Validated Against Independent Lots<br />

Include Internal <strong>Standards</strong> or Surrogates<br />

Follow <strong>ASTM</strong> Method Guidelines<br />

Allow Direct Transfer to Autosampler Vials<br />

Originally designed for<br />

D-3230-99<br />

Originally designed for<br />

D-3237-97<br />

Ready-to-Inject<br />

Working Level <strong>Standards</strong> &<br />

Continuing Calibration Check (CCC)


<strong>ASTM</strong> <strong>Standards</strong><br />

<strong>ASTM</strong> D-3246 Sulfur in Petroleum Gas by Oxidative Microcoulometry<br />

See pages 6 - 11 for Accu<strong>Standards</strong> comprehensive line of certified sulfur calibration standards<br />

<strong>ASTM</strong> D-3340 Lithium & Na in Lubricating Greases by Flame Photometer<br />

AccuStandard AccuTrace brand AA standards are produced under our rigorous ISO 9001 quality system to<br />

exacting specifications. Each standard is prepared from high purity starting materials; deionized water and<br />

high purity acids. Every standard is instrumentally assayed to verify 1000 ppm concentration of specified<br />

element; Actual Lot Analysis is provided on the label and a Certificate of Analysis is included for ease of<br />

record keeping and availability at audits.<br />

Element Unit Cat. No. Price<br />

Matrix 1,000 µg/mL<br />

Lithium * 100 mL AA30H-1 $ 12<br />

HCl 500 mL AA30H-5 30<br />

Sodium * 100 mL AA54H-1 13<br />

HCl 500 mL AA54H-5 33<br />

<strong>ASTM</strong> D-3524 (Reapproved 1999) Diesel Fuel Diluent in Used Diesel Engine Oils by GC<br />

D-3524 Calibration Curve<br />

D-3524-CAL-SET-5ML $ 150 / set of 6 x 5 mL<br />

D-3524-CAL-SET-10ML $ 250 / set of 6 x 10 mL<br />

Internal Standard Solution<br />

D-3524-IS-10ML $ 25 / 1 x 10 mL<br />

D-3524-IS-10ML-PAK SAVE 20% $ 100 / 5 x 10 mL<br />

At stated conc. in n-Heptane 2 comps.<br />

Wt. / Wt. %<br />

n-Decane 1.0<br />

n-Octadecane 0.2<br />

Column Resolution Mix<br />

D-3524-CR $ 10 / 1 x 1 mL<br />

D-3524-CR-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

At stated conc. in n-Heptane 2 comps.<br />

Wt. / Wt. %<br />

n-Hexadecane 1.0<br />

n-Octadecane 1.0<br />

<strong>ASTM</strong> D-3605 Trace Metals in Gas Turbine Fuels by AA &<br />

(Reapproved 1995) Flame Emission Spectroscopy<br />

Technical Note<br />

* For your convenience these elements are<br />

also available in HNO3. To order HNO3 change the H to N at the end of the Cat. No.<br />

Analyte Standard 1 Standard 2 Standard 3 Standard 4 Standard 5 Standard 6<br />

Target Wt. % Target Wt. % Target Wt. % Target Wt. % Target Wt. % Target Wt. %<br />

# 2 Diesel 10 7.5 5 2.5 1 0<br />

30 W Motor oil 90 92.5 95 97.5 99 100<br />

D-3605-91 Trace Metals Standard<br />

D-3605-91-1 $ 165 / 1 x 100 mL<br />

At stated conc. in 1,2,3,4-Tetrahydronaphthalene 4 comps.<br />

Na (Sodium) (250 µg/mL)<br />

Pb (Lead) (250 µg/mL)<br />

Ca (Calcium) (250 µg/mL)<br />

V (Vanadium) (250 µg/mL)<br />

Originally designed for<br />

D-3340-98<br />

Originally designed for<br />

D-3524-90<br />

Mid Level Daily QC Solution<br />

D-3524-QC-10ML $ 30 / 1 x 10 mL<br />

2 comps.<br />

Wt. / Wt. %<br />

# 2 Diesel 5.0<br />

30 W Motor oil 95<br />

Originally designed for<br />

D-3605-91<br />

Test to<br />

Low ppb<br />

Sulfur<br />

See Pages 6-11<br />

<strong>Standards</strong> of Interests<br />

See Table of Contents for the<br />

Wear Metals Group pages<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 17<br />

Method 3246<br />

3340<br />

3524<br />

3605<br />

Member<br />

<strong>ASTM</strong><br />

WEAR METALS


Method 3606<br />

3610<br />

,<br />

Member<br />

<strong>ASTM</strong><br />

18<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

<strong>ASTM</strong> D-3606 Benzene & Toluene in Finished Motor & Aviation Gasoline by GC<br />

Aromatics Quantitative Calibration Standard (without Internal <strong>Standards</strong>)<br />

D-3606-SET-25ML $ 800 / set of 7 x 25 mL<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7<br />

Calibr. range Target Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %<br />

Benzene 0.06 - 5.0 5.00 2.50 1.25 0.67 0.33 0.12 0.06<br />

Toluene 0.5 - 20 20.00 15.00 10.00 5.00 2.50 1.00 0.50<br />

Isooctane 75.00 82.50 88.75 94.33 97.17 98.88 99.44<br />

Aromatics Quantitative Calibration Standard (with Internal Standard: MEK)<br />

D-3606/IS-SET $ 115 / set of 7 x 1 mL<br />

D-3606/IS-SET-2ML $ 190 / set of 7 x 2 mL<br />

D-3606/IS-SET-2ML-PAK $ 760 / 5 x (7 x 2) mL<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7<br />

Calibr. range Target Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %<br />

Benzene 0.06 - 5.0 4.8 2.4 1.2 0.6432 0.3168 0.1152 0.0576<br />

Toluene 0.5 - 20 19.2 14.4 9.6 4.8000 2.4000 0.9600 0.4800<br />

Isooctane 72.0 79.2 85.2 90.5568 93.2832 94.9248 95.4624<br />

Methyl ethyl ketone (Internal Std.) 4.0 4.0 4.0 4.0 4.0 4.0 4.0<br />

Gasoline Refinery Quality Control <strong>Standards</strong><br />

Daily Quality Control Standard<br />

(with Internal Standard: MEK)<br />

D-3606-QC/IS-10ML $ 75 / 1 x 10 mL<br />

D-3606-QC/IS-10ML-PAK $ 300 / 5 x 10 mL<br />

Each at stated quantities 4 comps.<br />

Compound Target Vol. %<br />

Benzene 0.6432<br />

Toluene 4.8000<br />

Isooctane 90.5568<br />

Methyl ethyl ketone (ISTD) 4.0<br />

100<br />

Aromatics Quantitative Calibration Standard (w/ Internal Standard: sec Butanol)<br />

D-3606/IS2-SET $ 115 / set of 7 x 1 mL<br />

D-3606/IS2-SET-PAK $ 500 / 5 x (7 x 1) mL<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7<br />

Calibr. range Target Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %<br />

Benzene 0.06 - 5.0 4.8 2.4 1.2 0.6432 0.3168 0.1152 0.0576<br />

Toluene 0.5 - 20 19.2 14.4 9.6 4.8000 2.4000 0.9600 0.4800<br />

Isooctane 72.0 79.2 85.2 90.5568 93.2832 94.9248 95.4624<br />

sec Butanol (Internal Standard) 4.0 4.0 4.0 4.0 4.0 4.0 4.0<br />

Gasoline Refinery Quality Control <strong>Standards</strong><br />

Daily Quality Control Standard<br />

(with Internal Standard: sec Butanol)<br />

D-3606-QC-IS2-25ML $ 125 / 1 x 25 mL<br />

D-3606-QC-IS2-25ML-PAK $ 600 / 5 x 25 mL<br />

Each at stated quantities 4 comps.<br />

Compound Target Vol. %<br />

Benzene 0.6432<br />

Toluene 4.8000<br />

Isooctane 90.5568<br />

sec-Butanol (ISTD) 4.0<br />

100<br />

Daily Quality Control Standard<br />

(without Internal Standard)<br />

D-3606-QC-25ML $ 125 / 1 x 25 mL<br />

D-3606-QC-25ML-PAK $ 600 / 5 x 25 mL<br />

Each at stated quantities 3 comps.<br />

Compound Target Vol. %<br />

Benzene 0.67<br />

Toluene 5.00<br />

Isooctane 94.33<br />

Daily Quality Control Standard<br />

(without Internal Standard)<br />

D-3606-QC-25ML $ 125 / 1 x 25 mL<br />

D-3606-QC-25ML-PAK $ 600 / 5 x 25 mL<br />

Each at stated quantities 3 comps.<br />

Compound Target Vol. %<br />

Benzene 0.67<br />

Toluene 5.00<br />

Isooctane 94.33<br />

<strong>ASTM</strong> D-3610 Total Cobalt in Alumina-Base Cobalt-Molybdenum Catalyst by Potentiometric Titration<br />

Cobalt Oxide Standard<br />

D-3610-93-1 $ 50 / 1 x 100 mL<br />

Cobalt oxide @ 1500 µg/mL in Water<br />

Originally designed for<br />

D-3610-88 (Re-Approved 1993)<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

100<br />

100<br />

Originally designed for<br />

D-3606-99<br />

D-3606<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

Technical Note<br />

Due to changes in the possible<br />

use of other oxygenates like<br />

ethanol added to gasoline,<br />

AccuStandard formulated a<br />

new calibration curve using<br />

sec-butanol as an Internal<br />

Standard. The use of this new<br />

ISTD minimizes coelution<br />

caused by the oxygenate(s)<br />

and pre column - standard<br />

column configuration in the GC<br />

system.


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See our Website for more info.<br />

Cross Reference Table<br />

<strong>ASTM</strong> IP ISO DIN JIS AFNOR sorted by<br />

<strong>ASTM</strong> Method see beginning of Catalog<br />

Test to<br />

Low ppb<br />

Sulfur<br />

See Pages 6-11<br />

Over 30,000 <strong>Standards</strong><br />

just a click away<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 19<br />

<strong>ASTM</strong>


Method 3710<br />

3798<br />

, 3831<br />

Member<br />

<strong>ASTM</strong><br />

<strong>ASTM</strong> D-3710 (Reapproved 1999) Boiling Range Distribution of Gasoline & Gasoline Fractions by GC<br />

<strong>ASTM</strong> D-3831 Manganese in Gasoline by AA Spectroscopy<br />

Manganese Stock Solution<br />

D-3831 $ 65 / 1 x 100 mL<br />

Manganese @ 1.0 g Mn / gal (264.2 mg Mn / L) in Methyl isobutyl ketone<br />

20<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

This SIM DIS (Simulated Distillation or GCD) Method is used to determine the boiling range distribution of<br />

gasoline and gasoline components. <strong>ASTM</strong> Method D-3710 is used for petroleum products and fractions<br />

with a final boiling point of 500°F (260°C) or lower. By having an insight into the composition of the<br />

gasoline blend, essential data for the calculation of vapor pressure and a prediction of the D-86 distillation<br />

curve can be made.<br />

Qualitative Calibration Standard<br />

D-3710-QUAL $ 30 / 1 x 1 mL<br />

D-3710-QUAL-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

19 comps.<br />

Approx.<br />

Wt./ Wt. %<br />

n-Butane 4.5<br />

n-Butylbenzene 3.2<br />

n-Decane 3.2<br />

2,4-Dimethylpentane 5.4<br />

n-Dodecane 3.2<br />

n-Heptane 9.7<br />

n-Hexane 5.4<br />

2-Methylbutane 9.7<br />

2-Methylpentane 5.4<br />

2-Methylpropane 1.5<br />

Approx.<br />

Wt./ Wt. %<br />

n-Octane 5.4<br />

n-Pentadecane 2.2<br />

n-Pentane 7.6<br />

n-Propane 1.5<br />

n-Propylbenzene 4.3<br />

n-Tetradecane 2.2<br />

Toluene 10.8<br />

n-Tridecane 2.2<br />

p-Xylene 13<br />

<strong>ASTM</strong> D-3798 Analysis of p-Xylene by GC<br />

Quantitative Calibration Standard<br />

<strong>ASTM</strong>-D3710 $ 25 / 1 x 1 mL<br />

<strong>ASTM</strong>-D3710-PAK SAVE 36% $ 80 / 5 x 1 mL<br />

16 comps.<br />

Vol./Vol. %<br />

n-Butylbenzene 3.5<br />

n-Decane 3.5<br />

2,4-Dimethylpentane 5.8<br />

n-Dodecane 3.5<br />

n-Heptane 10.5<br />

n-Hexane 5.8<br />

2-Methylbutane 10.5<br />

2-Methylpentane 5.8<br />

Vol./Vol. %<br />

n-Octane 5.8<br />

n-Pentadecane 2.3<br />

n-Pentane 8.1<br />

n-Propylbenzene 4.7<br />

n-Tetradecane 2.3<br />

Toluene 11.6<br />

n-Tridecane 2.3<br />

p-Xylene 14.0<br />

<strong>ASTM</strong> D-2887-99 Boiling Range Distribution of Petroleum Fractions by GC<br />

Calibration Solution *<br />

DRH-002S-R1 $ 50 / 1 x 1 mL<br />

DRH-002S-R1-PAK SAVE 20% $ 200 / 5 x 1 mL<br />

At stated conc. in Chloroform 17 comps.<br />

µg/mL<br />

n-Hexane 600<br />

n-Heptane 600<br />

n-Octane 800<br />

n-Nonane 800<br />

n-Decane 1200<br />

AccuStandard’s R & D team has developed a special highly purified p-Xylene designed for <strong>ASTM</strong> Method<br />

D-3798 specifications. The incorporation of this p-Xylene into the formulation allows the analytical chemist<br />

to qualitatively and quantitatively measure the impurities in the p-Xylene feedstock streams.<br />

p-Xylene Impurity Standard<br />

with ISTD<br />

D-3798-IS $ 30 / 1 x 1 mL<br />

D-3798-IS-PAK SAVE 33% $ 100 / 5 x 1 mL<br />

At stated conc. by weight 11 comps.<br />

Wt./Wt. %<br />

n-Pentane 0.15<br />

n-Octane 0.15<br />

Benzene 0.15<br />

Toluene 0.15<br />

Ethylbenzene 0.15<br />

p-Xylene 98.65<br />

m-Xylene 0.15<br />

µg/mL<br />

n-Undecane 1200<br />

n-Dodecane 1200<br />

n-Tetradecane 1200<br />

n-Hexadecane 1000<br />

Wt./Wt. %<br />

o-Xylene 0.15<br />

Cumene 0.15<br />

Propylbenzene 0.15<br />

Total Analytes 100<br />

plus n-Undecane* (ISTD) 0.500<br />

grams<br />

µg/mL<br />

n-Octadecane 500<br />

n-Eicosane 200<br />

n-Tetracosane 200<br />

n-Octacosane 100<br />

p-Xylene Impurity Standard<br />

without ISTD<br />

D-3798-10ML $ 65 / 1 x 10 mL<br />

D-3798-10ML-PAK SAVE 20% $ 260 / 5 x 10 mL<br />

At stated conc. by weight 10 comps.<br />

Wt./Wt. %<br />

n-Pentane 0.15<br />

n-Octane 0.15<br />

Benzene 0.15<br />

Toluene 0.15<br />

Ethylbenzene 0.15<br />

NEW<br />

µg/mL<br />

n-Dotriacontane 100<br />

n-Hexatriacontane 100<br />

n-Tetracontane 100<br />

n-Tetratetracontane100<br />

* Can be shipped by Air and Sea<br />

Wt./Wt. %<br />

p-Xylene 98.65<br />

m-Xylene 0.15<br />

o-Xylene 0.15<br />

Cumene 0.15<br />

Propylbenzene 0.15<br />

Originally designed for<br />

D-3831-98<br />

Originally designed for<br />

D-3710-95<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

<strong>Standards</strong> of Interests<br />

See page 3 for AccuStandard’s<br />

new D-86 QA/QC <strong>Standards</strong>.<br />

Technical Note<br />

Bulk Packaged p-Xylene<br />

without Internal Standard<br />

Other suggested internal<br />

standards can be used in<br />

conjunction with the bulk<br />

packaged D-3789 1 x 10 mL<br />

ampule to meet your company’s<br />

application. If you prefer to<br />

eliminate making standards,<br />

contact AccuStandard’s<br />

Technical Department with your<br />

unique formulation for a custom<br />

quotation. The custom<br />

quotation request form is<br />

located in the back of this<br />

catalog.


<strong>ASTM</strong> D-4059 Polychlorinated Biphenyls in Insulating Liquids by GC<br />

Aroclor #<br />

Conc.<br />

(ppm w/w)<br />

Neat Individual Aroclors<br />

Aroclor # Cat. No. Price / Unit<br />

Z-008<br />

(Kit)<br />

Aroclor 1016 C-216N $ 25 / 100 mg 100 mg<br />

Aroclor 1221 C-221N 25 / 100 mg 100 mg<br />

Aroclor 1232 C-232N 25 / 10 mg 10 mg<br />

Aroclor 1242 C-242N 25 / 100 mg 100 mg<br />

Aroclor 1248 C-248N 25 / 10 mg 10 mg<br />

Aroclor 1254 C-254N 25 / 100 mg 100 mg<br />

Aroclor 1260 C-260N 25 / 100 mg 10 mg<br />

Aroclor 1262 C-262N 25 / 100 mg 10 mg<br />

Aroclor 1268 C-268N 25 / 10 mg 10 mg<br />

Kit of above 9 Aroclors Z-008 $ 125 / 9 vials<br />

<strong>ASTM</strong> D-4291 (Reapproved 1998) Trace Ethylene Glycol in Used Engine Oil<br />

Ethylene Glycol Stock Standard<br />

D-4291-93 $ 20 / 1 x 1 mL<br />

D-4291-93-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

Ethylene glycol @ 2000 µg/mL in water<br />

Cat. No.<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Aroclors in PCB-Free Transformer Oil (At 2 concentrations in Transcrest W130)<br />

1 x 1 mL<br />

Price<br />

PAK Cat. No.<br />

5 x 1 mL<br />

Price<br />

Aroclor 1016 50 C-216-ST-1 $ 25 C-216-ST-1-PAK $ 90<br />

Aroclor 1016 500 C-216-ST-2 30 C-216-ST-2-PAK 120<br />

Aroclor 1221 50 C-221-ST-1 25 C-221-ST-1-PAK 90<br />

Aroclor 1221 500 C-221-ST-2 30 C-221-ST-2-PAK 120<br />

Aroclor 1232 50 C-232-ST-1 25 C-232-ST-1-PAK 90<br />

Aroclor 1232 500 C-232-ST-2 30 C-232-ST-2-PAK 120<br />

Aroclor 1242 50 C-242-ST-1 25 C-242-ST-1-PAK 90<br />

Aroclor 1242 500 C-242-ST-2 30 C-242-ST-2-PAK 120<br />

Aroclor 1248 50 C-248-ST-1 25 C-248-ST-1-PAK 90<br />

Aroclor 1248 500 C-248-ST-2 30 C-248-ST-2-PAK 120<br />

Aroclor 1254 50 C-254-ST-1 25 C-254-ST-1-PAK 90<br />

Aroclor 1254 500 C-254-ST-2 30 C-254-ST-2-PAK 120<br />

Aroclor 1260 50 C-260-ST-1 25 C-260-ST-1-PAK 90<br />

Aroclor 1260 500 C-260-ST-2 30 C-260-ST-2-PAK 120<br />

Aroclor 1262 50 C-262-ST-1 25 C-262-ST-1-PAK 90<br />

Aroclor 1262 500 C-262-ST-2 30 C-262-ST-2-PAK 120<br />

Aroclor 1268 50 C-268-ST-1 25 C-268-ST-1-PAK 90<br />

Aroclor 1268 500 C-268-ST-2 30 C-268-ST-2-PAK 120<br />

<strong>ASTM</strong> D-4294 Sulfur in Petroleum Products by ED-XRF Spectroscopy<br />

Aroclor-free transformer oil<br />

also available as:<br />

T-W130 $ 5 / 1 x 1 mL<br />

Originally designed for<br />

D-4291-93<br />

See page 8-11 for AccuStandard’s comprehensive line of Certified Sulfur Calibration <strong>Standards</strong><br />

designed for matrix specific applications as described in Method D-4294 in section 9.0<br />

(Calibration & Standardization).<br />

<strong>ASTM</strong> D-4377 Water in Crude oils by Potentiometric Karl Fischer Titration<br />

See page 5 for AccuStandard’s comprehensive line of Certified Karl Fischer Water <strong>Standards</strong>.<br />

Originally designed for<br />

D-4059-96<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 21<br />

Method 4059<br />

4291<br />

4294<br />

4377<br />

Member<br />

Additional Aroclors and<br />

PCB Congener <strong>Standards</strong><br />

available in our Organic<br />

Catalog<br />

D-4294<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

<strong>ASTM</strong>


Method 4420<br />

4628<br />

,<br />

Member<br />

<strong>ASTM</strong><br />

WEAR METALS<br />

<strong>ASTM</strong> D-4420 Aromatics in Finished Gasolines by GC<br />

Aromatics in Gasoline by GC/TC<br />

D-4420-CAL-SET $ 105 / set of 7 x 1 mL<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7<br />

Target Target Target Target Target Target Target<br />

Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %<br />

Benzene 0.05 0.10 0.25 0.75 1.25 2.50 5.00<br />

Toluene 0.5 1.00 2.50 5.00 10.00 15.00 25.00<br />

Total Xylenes (C8 aromatics) 5 10.00 15.00 20.00 25.00 1.00 3.00<br />

n-Butylbenzene (C9 + aromatics) 30.00 25.00 20.00 10.00 5.00 15.00 2.50<br />

Isooctane 64.45 63.90 62.25 64.25 58.75 66.50 64.50<br />

Aromatics in Gasoline by GC/TX<br />

D-4420-94 $ 20 / 1 x 1 mL<br />

D-4420-94-PAK $ 80 / 5 x 1 mL<br />

5 comps.<br />

Vol. %<br />

Benzene 3.00<br />

Toluene 10.00<br />

Total Xylenes (C 8 aromatics) 15.00<br />

<strong>ASTM</strong> D-4628 Barium, Calcium, Magnesium & Zinc in Unused Lubricating Oil<br />

22<br />

Vol. %<br />

n-Butylbenzene(C 9 + aromatics) 15.00<br />

Isooctane 57.00<br />

Lubricating Oil, Elements (Nominal Value) Wt.% listed below<br />

<strong>ASTM</strong>-P-0113-SET $ 2850 / 17 x 100 mL<br />

Ba Ca Mg P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0113-01 0.025 0.600 0.100 0.005 0.175 0.060<br />

<strong>ASTM</strong>-P-0113-02 0.000 0.500 0.150 0.200 0.050 0.080<br />

<strong>ASTM</strong>-P-0113-03 0.100 0.400 0.350 0.150 0.300 0.180<br />

<strong>ASTM</strong>-P-0113-04 0.175 0.260 0.225 0.250 0.150 0.120<br />

<strong>ASTM</strong>-P-0113-05 0.150 0.005 0.450 0.005 0.450 0.070<br />

<strong>ASTM</strong>-P-0113-06 0.000 0.400 0.500 0.025 0.350 0.100<br />

<strong>ASTM</strong>-P-0113-07 0.100 0.300 0.325 0.060 0.250 0.120<br />

<strong>ASTM</strong>-P-0113-08 0.200 0.200 0.250 0.100 0.450 0.100<br />

<strong>ASTM</strong>-P-0113-09 0.050 0.060 0.100 0.080 0.300 0.130<br />

<strong>ASTM</strong>-P-0113-10 0.075 0.060 0.400 0.050 0.200 0.050<br />

<strong>ASTM</strong>-P-0113-11 0.010 0.050 0.300 0.120 0.100 0.075<br />

<strong>ASTM</strong>-P-0113-12 0.000 0.025 0.200 0.150 0.200 0.130<br />

<strong>ASTM</strong>-P-0113-13 0.175 0.005 0.375 0.200 0.400 0.150<br />

<strong>ASTM</strong>-P-0113-14 0.005 0.170 0.175 0.250 0.550 0.110<br />

<strong>ASTM</strong>-P-0113-15 0.000 0.100 0.425 0.100 0.200 0.200<br />

<strong>ASTM</strong>-P-0113-16 0.005 0.010 0.275 0.010 0.600 0.250<br />

<strong>ASTM</strong>-P-0113-17 0.000 0.000 0.000 0.000 0.000 0.000<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Originally designed for<br />

D-4420-94<br />

Ready-to-Inject Petrochemical <strong>Standards</strong><br />

and Calibration Curves<br />

Reduce Costs<br />

Increase Time Spent for Sample Analysis<br />

Are Validated Against Independent Lots<br />

Include Internal <strong>Standards</strong> or Surrogates<br />

Follow <strong>ASTM</strong> Method Guidelines<br />

Allow Direct Transfer to Autosampler Vials<br />

Originally designed for<br />

D-4628-97<br />

Cross Reference Table<br />

<strong>ASTM</strong> IP ISO DIN JIS AFNOR sorted by<br />

<strong>ASTM</strong> Method see beginning of Catalog<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

<strong>Standards</strong> of Interests<br />

See Table of Contents for the<br />

Wear Metals Group pages.


<strong>ASTM</strong> D-4629 Trace Nitrogen in Liquid Petroleum Hydrocarbons by Syringe/Inlet Oxidative<br />

Combustion and Chemiluminescence Detection. IP Designation 379/88<br />

Stock Nitrogen Solution for Low Boiling Solvents<br />

D-4629-91-LB-CON $ 20 / 1 x 1 mL<br />

D-4629-91-LB-CON-PAK $ 80 / 5 x 1 mL<br />

Nitrogen @ 1000 µg/mL in Isooctane<br />

(Pyridine @ 5.65 mg/mL in Isooctane)<br />

Technical Note<br />

Technical Note<br />

Nitrogen Calibration Set-High Boiling Solvents<br />

D-4629-91-HB-CAL-SET $ 75 / set of 7 x 1 mL<br />

Set includes the following Cat. No.s<br />

Nitrogen introduced using Carbazole<br />

Cat. No. Description Price / Unit<br />

D-4629-91-HB-0.3X Nitrogen @ 0.3 µg/mL in Toluene $ 20 / 1 x 1 mL<br />

D-4629-91-HB-1X Nitrogen @ 1 µg/mL in Toluene $ 20 / 1 x 1 mL<br />

D-4629-91-HB-10X Nitrogen @ 10 µg/mL in Toluene $ 20 / 1 x 1 mL<br />

D-4629-91-HB-25X Nitrogen @ 25 µg/mL in Toluene $ 20 / 1 x 1 mL<br />

D-4629-91-HB-50X Nitrogen @ 50 µg/mL in Toluene $ 20 / 1 x 1 mL<br />

D-4629-91-HB-75X Nitrogen @ 75 µg/mL in Toluene $ 20 / 1 x 1 mL<br />

D-4629-91-HB-100X Nitrogen @ 100 µg/mL in Toluene $ 20 / 1 x 1 mL<br />

Stock Nitrogen Solution for High Boiling Solvents<br />

D-4629-91-HB-CON $ 20 / 1 x 1 mL<br />

D-4629-91-HB-CON-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

Nitrogen @ 1000 µg/mL in Toluene : Acetone (9:1)<br />

(Carbazole @ 11.95 mg/mL in Toluene : Acetone (9:1) )<br />

Low level Nitrogen Calibration Set<br />

<strong>ASTM</strong>-P-0070-SET $ 75 / 6 x 1 mL<br />

Set includes the following Cat. No.s<br />

Low level Nitrogen &<br />

Sulfur Calibration Set<br />

<strong>ASTM</strong>-P-0071-SET $ 50 / 4 x 1 mL<br />

Set includes the following Cat. No.s<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Method D-4629 is used to determine trace total nitrogen naturally found in liquid hydrocarbons boiling from<br />

50 to 400°C with viscosities between 0.2 and 10 cSt. This method monitors feed stocks for nitrogen to<br />

prevent the poisoning of some process catalysts when trace nitrogenous materials are present.<br />

Nitrogen Calibration Set-Low Boiling Solvents<br />

D-4629-91-LB-CAL-SET $ 75 / set of 7 x 1 mL<br />

Set includes the following Cat. No.s<br />

Nitrogen introduced using Pyridine<br />

Cat. No. Description Price / Unit<br />

D-4629-91-LB-0.3X Nitrogen @ 0.3 µg/mL in Isooctane $ 20 / 1 x 1 mL<br />

D-4629-91-LB-1X Nitrogen @ 1 µg/mL in Isooctane $ 20 / 1 x 1 mL<br />

D-4629-91-LB-10X Nitrogen @ 10 µg/mL in Isooctane $ 20 / 1 x 1 mL<br />

D-4629-91-LB-25X Nitrogen @ 25 µg/mL in Isooctane $ 20 / 1 x 1 mL<br />

D-4629-91-LB-50X Nitrogen @ 50 µg/mL in Isooctane $ 20 / 1 x 1 mL<br />

D-4629-91-LB-75X Nitrogen @ 75 µg/mL in Isooctane $ 20 / 1 x 1 mL<br />

D-4629-91-LB-100X Nitrogen @ 100 µg/mL in Isooctane $ 20 / 1 x 1 mL<br />

Technical Note<br />

Nitrogen introduced using Aniline<br />

Cat. No. Description Unit<br />

<strong>ASTM</strong>-P-0070-BL Isooctane Blank 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-1X Nitrogen @ 0.5 µg/g in Isooctane 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-2X Nitrogen @ 1.0 µg/g in Isooctane 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-4X Nitrogen @ 2.0 µg/g in Isooctane 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-10X Nitrogen @ 5.0 µg/g in Isooctane 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-20X Nitrogen @ 10.0 µg/g in Isooctane 1 x 1 mL<br />

Technical Note<br />

The Nitrogen is introduced using Aniline and the<br />

Sulfur is introduced using di-n-Butyl sulfide<br />

Cat. No. Description Unit<br />

<strong>ASTM</strong>-P-0071-BL Benzene Blank 1 x 1 mL<br />

<strong>ASTM</strong>-P-0071-01 Nitrogen @ 0.25 µg/g & Sulfur @ 0.25 µg/g in Benzene 1 x 1 mL<br />

<strong>ASTM</strong>-P-0071-02 Nitrogen @ 0.50 µg/g & Sulfur @ 0.50 µg/g in Benzene 1 x 1 mL<br />

<strong>ASTM</strong>-P-0071-03 Nitrogen @ 1.00 µg/g & Sulfur @ 1.00 µg/g in Benzene 1 x 1 mL<br />

Originally designed for<br />

D-4629-96<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 23<br />

Method 4629<br />

Member<br />

<strong>ASTM</strong>


Method 4815<br />

,<br />

Member<br />

<strong>ASTM</strong><br />

<strong>ASTM</strong> D-4815 MtBE, EtBE, TAME, DIPE, Tertiary-amyl Alcohol and<br />

C 1 to C 4 Alcohols in Gasoline by GC<br />

24<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Oxygenate Quantitative Calibration Mixtures (without Internal Standard)<br />

D-4815-SET-10ML $ 300 / set of 5 x 10 mL of 5 component mix<br />

Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

Analyte Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Ethanol 3.00 0.10 6.00 9.00 12.00<br />

t-Butanol 0.10 3.00 6.00 8.00 12.00<br />

Methyl t-butyl ether (MtBE) 20.0 15.00 10.00 5.00 0.10<br />

t-Pentanol 1.25 5.00 2.50 3.75 0.10<br />

Isooctane/xylene (65:35) 75.65 76.90 75.50 74.25 75.80<br />

Oxygenate Quantitative Calibration Mixtures (with Internal Standard)<br />

D-4815/IS-SET of 6 component mix $ 125 / set of 5 x 1 mL<br />

D-4815/IS-SET-PAK $ 500 / set of 5 x (5 x 1 mL)<br />

Calibration Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

Analyte Range Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Ethanol 0.1 - 11.40 2.85 0.10 5.70 8.55 11.40<br />

t-Butanol 0.1 - 11.40 0.10 2.85 5.70 7.60 11.40<br />

Methyl t-butyl ether (MtBE) 0.1 - 19.0 19.00 14.25 9.50 4.75 0.10<br />

t-Pentanol 0.1 - 4.79 1.19 4.75 2.38 3.56 0.10<br />

1,2-Dimethoxyethane (DME) (Internal Std.) 5.00 5.00 5.00 5.00 5.00<br />

Isooctane/xylene (65:35) 71.87 73.06 71.73 70.54 72.0<br />

Total Oxgenates & Internal Standard 28.14 26.95 28.28 29.46 28.00<br />

Quantitative Peak ID and<br />

Retention Time Mixture<br />

D-4815-RT $ 25 / 1 x 1 mL<br />

D-4815-RT-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

Compound Wt. %<br />

Methylcyclopentane 4.00<br />

Methanol 7.30<br />

Ethanol 7.30<br />

Isopropanol 7.30<br />

tert-Butanol 7.30<br />

n-Propanol 7.30<br />

Methyl tert-butyl ether (MtBE) 4.00<br />

sec-Butanol 7.30<br />

Diisopropyl ether (DIPE) 4.00<br />

Isobutanol 7.30<br />

Ethyl tert-butyl ether (EtBE) 4.00<br />

tert-Pentanol 7.30<br />

1,2-Dimethoxyethane (ISTD) 6.00<br />

n-Butanol 7.30<br />

Benzene 5.00<br />

tert-Amyl methyl ether 7.30<br />

16 comp. core mix<br />

100<br />

Valve Timing Mixture<br />

D-4815-VT $ 25 / 1 x 1 mL<br />

D-4815-VT-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

5 comps.<br />

Compound Wt. %<br />

Methylcyclopentane 10.00<br />

Diisopropyl ether (DIPE) 10.00<br />

Ethyl tert-butyl ether (EtBE) 10.00<br />

Methyl tert-butyl ether (MtBE) 10.00<br />

n-Hexane 60.00<br />

Oxygenate Internal Standard Mixture<br />

M-GRO-IS-5ML $ 10 / 1 x 1 mL<br />

M-GRO-IS-5ML-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

1,2-Dimethoxyethane (ISTD) (neat)<br />

Oxygenate Free Refinery Gasoline<br />

Blank<br />

M-GRO-BLNK-10ML $ 10 / 1 x 10 mL<br />

M-GRO-BLNK-10ML-PAKSAVE 20% $ 40 / 5 x 10 mL<br />

RFA Gasoline (neat)<br />

Originally designed for<br />

D-4815-99<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

D-4815<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

Technical Note<br />

Additional Oxygenate<br />

calibration, check standards,<br />

and independent reference<br />

standards can be found in<br />

<strong>ASTM</strong> method D-5599 (pages<br />

34-36) or D-5622-94 (page 37)<br />

The required QA/QC procedures<br />

in EPA methods stipulate a<br />

calibration check standard be<br />

used once per analytical batch<br />

or per 10 sample set.<br />

AccuStandard has bulk<br />

packaged our check standards<br />

to meet this increased usage.<br />

Test to<br />

Low ppb<br />

Sulfur<br />

See Pages 6-11<br />

Custom Formulations<br />

AccuStandard offers over 30,000 different standards, and if you can't find the specific standard you need, we will prepare a custom formulation.<br />

Our custom organic and inorganic standards are a fast, economical way to address your unique requirements. To make an inquiry for Custom<br />

Quotes visit our website.<br />

You can also Email your requirements to techservice@accustandard.com or Fax us at 203-786-5287. Please include the following information:<br />

List of analytes and concentrations, Solvent or matrix, Quantity required (milliliters), Packaging unit size (milliliters per ampule, bottle, or vial).<br />

Quality Control Options<br />

1. Gravimetric/Volumetric Certification: Each standard is measured gravimetrically and then QC’ed instrumentally (where available). Every<br />

component in the standard is guaranteed to be within ±0.5% of the requested value unless otherwise stated. The solutions are made up to volume<br />

using class A glassware. A certificate comes with each standard and documents the gravimetric values used.<br />

2. Quantitative Validation: Full QA/QC method includes extended GC analysis using both internal and calibration standards plus statistical<br />

analysis. A data package is provided containing analytical and gravimetric data (Organic customs only).<br />

Also available: OEM <strong>Standards</strong> - Privately labeled standards manufactured and tested to your specifications.


<strong>ASTM</strong> D-4927 Elemental Analysis of Lubricant and Additive Components -<br />

Barium, Calcium,Phosphorus, Sulfur, and Zinc by WD-XRF Spectroscopy<br />

Lubricating Oil, Elements (Nominal Value) Wt.% listed below<br />

<strong>ASTM</strong>-P-0110-SET $ 2300 / 17 x 100 mL<br />

Ba Ca P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0110-01 0.100 0.600 0.005 0.175 0.060<br />

<strong>ASTM</strong>-P-0110-02 0.175 0.500 0.200 0.050 0.080<br />

<strong>ASTM</strong>-P-0110-03 0.000 0.400 0.150 0.300 0.180<br />

<strong>ASTM</strong>-P-0110-04 0.025 0.260 0.250 0.150 0.120<br />

<strong>ASTM</strong>-P-0110-05 0.150 0.005 0.005 0.450 0.070<br />

<strong>ASTM</strong>-P-0110-06 0.000 0.400 0.025 0.350 0.100<br />

<strong>ASTM</strong>-P-0110-07 0.200 0.300 0.060 0.250 0.120<br />

<strong>ASTM</strong>-P-0110-08 0.000 0.200 0.100 0.450 0.100<br />

<strong>ASTM</strong>-P-0110-09 0.100 0.060 0.080 0.300 0.130<br />

<strong>ASTM</strong>-P-0110-10 0.050 0.060 0.050 0.200 0.050<br />

<strong>ASTM</strong>-P-0110-11 0.075 0.050 0.120 0.100 0.075<br />

<strong>ASTM</strong>-P-0110-12 0.010 0.025 0.150 0.200 0.130<br />

<strong>ASTM</strong>-P-0110-13 0.005 0.005 0.200 0.400 0.150<br />

<strong>ASTM</strong>-P-0110-14 0.000 0.170 0.250 0.550 0.110<br />

<strong>ASTM</strong>-P-0110-15 0.000 0.100 0.100 0.200 0.200<br />

<strong>ASTM</strong>-P-0110-16 0.005 0.010 0.010 0.600 0.250<br />

<strong>ASTM</strong>-P-0110-17 0.000 0.000 0.000 0.000 0.000<br />

<strong>ASTM</strong> D-4928 Water in Crude Oils by Potentiometric Karl Fischer Titration<br />

See page 5 for AccuStandard’s new line of Karl Fischer Water <strong>Standards</strong>.<br />

<strong>ASTM</strong> D-4929 Organic Chloride Content in Crude Oil - Test Method B<br />

Combustion and Microcoulometry<br />

Working Level Chlorine Standard<br />

D-4929-94 $ 10 / 1 x 5 mL<br />

D-4929-94-PAK SAVE 20% $ 40 / 5 x 5 mL<br />

Chlorine @ 10 µg/mL in Isooctane<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Custom Ampulling for Bulk Quantity Requirements<br />

Automated ampule filling & sealing 0.2 mL up to 20 mL<br />

Quantities from 500 to over 500,000 ampules<br />

Homogeneity testing<br />

Amber ampules for added product stability<br />

Private labeling and packaging<br />

Originally designed for<br />

D-4927-96<br />

Stock Chlorine Standard<br />

D-4929-94-100X $ 15 / 1 x 5 mL<br />

D-4929-94-100X-PAK SAVE 20% $ 60 / 5 x 5 mL<br />

Chlorine @ 1000 µg/mL in Isooctane<br />

Originally designed for<br />

D-4929-99<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 25<br />

Method 4927<br />

4928<br />

4929<br />

Member<br />

<strong>Standards</strong> of Interests<br />

See Table of Contents for the<br />

Wear Metals Group pages<br />

<strong>Standards</strong> of Interests<br />

See page 66 for additional<br />

proposed and promulgated<br />

Chlorine in Lube Oil standards<br />

We can reduce your costs using the Cozzoli<br />

Auto Filling/ Sealing Machine to package just<br />

the right size product for your application.<br />

<strong>ASTM</strong><br />

WEAR METALS


Method 4951<br />

5056<br />

,<br />

Member<br />

<strong>ASTM</strong><br />

WEAR METALS<br />

<strong>ASTM</strong> D-4951 Additive Elements in Lubricating Oils by<br />

Inductively Coupled Plasma Atomic Emission Spectrometry<br />

20 Wear Metal Multi-Element Standard<br />

containing no metallic sulfonates<br />

Conc.<br />

(µg/g)<br />

Cat. No. Price<br />

10 WM-20-NMS-1X-1 $ 150<br />

30 WM-20-NMS-3X-1 150<br />

50 WM-20-NMS-5X-1 150<br />

100 WM-20-NMS-10X-1 170<br />

300 WM-20-NMS-30X-1 230<br />

500 WM-20-NMS-50X-1 350<br />

900 WM-20-NMS-90X-1 500<br />

WM-20-NMS-SET-1<br />

set of above 7 x 100 mL<br />

$ 1450<br />

Recommended Internal Standard (IS)<br />

<strong>ASTM</strong> D-5056 Trace Metals in Petroleum Coke by Atomic Absorption<br />

26<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Each Wear Metal Standard contains the below<br />

list of 20 elements in hydrocarbon oil at the<br />

stated concentration<br />

Al (Aluminum)<br />

B (Boron)<br />

Ba (Barium)<br />

Ca (Calcium)<br />

Cd (Cadmium)<br />

Cr (Chromium)<br />

Cu (Copper)<br />

Fe (Iron)<br />

Mg (Magnesium)<br />

Mn (Manganese)<br />

Sulfur free Organometallic (IS) Sulfur free Organometallic (IS)<br />

Element @ 1000 µg/g Price @ 5000 µg/g Price<br />

Cat. No. 50 mL Cat. No. 50 mL<br />

Cobalt WM-NMS-14 $ 75 WM-NMS-14-5X $ 110<br />

Element @ 1000 µg/mL Unit Cat. No. Price<br />

Matrix<br />

* Aluminum 100 mL AA01N-1 $ 13<br />

HNO3 500 mL AA01N-5 33<br />

* Calcium 100 mL AA09N-1 12<br />

HNO3 500 mL AA09N-5 30<br />

* Iron 100 mL AA27N-1 12<br />

HNO3 500 mL AA27N-5 30<br />

Nickel 100 mL AA37N-1 12<br />

HNO3 500 mL AA37N-5 30<br />

Mo (Molybdenum)<br />

Na (Sodium)<br />

Ni (Nickel)<br />

P (Phosphorus)<br />

Pb (Lead)<br />

Si (Silicon)<br />

Sn (Tin)<br />

Ti (Titanium)<br />

V (Vanadium)<br />

Zn (Zinc)<br />

Element @ 1000 µg/mL Unit Cat. No. Price<br />

Matrix<br />

Silicon 100 mL AA52W-1 $ 13<br />

H2O tr. NaOH 500 mL AA52W-5 33<br />

* Sodium 100 mL AA54N-1 13<br />

HNO3 500 mL AA54N-5 33<br />

Vanadium 100 mL AA67N-1 13<br />

HNO3 500 mL AA67N-5 33<br />

* For your convenience these elements are available<br />

in HCl. To order, change the N to H at the end of<br />

the catalog numbers.<br />

Cross Reference Table<br />

<strong>ASTM</strong> IP ISO DIN JIS AFNOR sorted by<br />

<strong>ASTM</strong> Method see beginning of Catalog<br />

Originally designed for<br />

D-4951-96<br />

Originally designed for<br />

D-5056-96<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

<strong>Standards</strong> of Interests<br />

See Table of Contents for the<br />

Wear Metals Group pages.<br />

Technical Notes<br />

This calibration curve has been<br />

formulated with starting<br />

materials containing no metal<br />

sulfonates. This way a sulfur<br />

calibration curve can easily be<br />

developed using a high<br />

concentration sulfur standard.


<strong>ASTM</strong> D-5059 Lead in Gasoline by X-Ray Spectroscopy IP Designation 228/79<br />

Technical Notes<br />

AccuStandard has formulated the following standards to measure the lead content in gasoline for both<br />

high and low concentrations using bismuth as an internal standard. For long term stability and ease of<br />

use AccuStandard provides the internal standard in two convenient packaging sizes. The bulk 4 oz.<br />

bottles are designed for laboratories analyzing many samples while the 10 mL ampules are for<br />

laboratories that have limited requests for the test method. Should you require bulk quantities of the<br />

internal standard conveniently packaged in single-use ampules, contact AccuStandard’s technical<br />

department for a quotation. Bulk volumes of 250 mL or more can be sealed into ampules (your choice<br />

up to 20 mL size). Use of our ampulling services can provide substantial saving for the Laboratory.<br />

Part A - Lead in Gasoline <strong>Standards</strong><br />

D-5059-A-CAL-SET $ 450 / set of 7 x 4 oz<br />

The Set contains the following 7 solutions in isooctane<br />

Cat. No. Lead Concentration Price /<br />

g Pb/US gal g Pb/ UK gal mg Pb/mL Unit<br />

D-5059-A-01 0.0000 0.000 0.000 $ 10 / 4 oz<br />

D-5059-A-02 0.1000 0.120 0.026 80 / 4 oz<br />

D-5059-A-03 1.0000 1.200 0.264 80 / 4 oz<br />

D-5059-A-04 2.0000 2.400 0.528 80 / 4 oz<br />

D-5059-A-05 3.0000 3.600 0.793 80 / 4 oz<br />

D-5059-A-06 4.0000 4.800 1.057 80 / 4 oz<br />

D-5059-A-07 5.0000 6.000 1.321 80 / 4 oz<br />

Part C - Lead in Gasoline <strong>Standards</strong><br />

D-5059-C-CAL-SET $ 450 / set of 7 x 4 oz<br />

The Set contains the following 7 solutions in isooctane<br />

Cat. No. Lead Concentration Price /<br />

g Pb/US gal g Pb/ UK gal µg Pb/mL Unit<br />

D-5059-C-01 0.0000 0.000 0.000 $ 10 / 4 oz<br />

D-5059-C-02 0.0010 0.001 0.264 80 / 4 oz<br />

D-5059-C-03 0.0050 0.006 1.321 80 / 4 oz<br />

D-5059-C-04 0.0100 0.012 2.642 80 / 4 oz<br />

D-5059-C-05 0.0500 0.060 13.209 80 / 4 oz<br />

D-5059-C-06 0.1000 0.120 26.417 80 / 4 oz<br />

D-5059-C-07 0.3000 0.360 79.252 80 / 4 oz<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

<strong>ASTM</strong> D-5134 Petroleum Naphthas through n-Nonane by Capillary GC<br />

Qualitative Reference Petroleum Set<br />

D-5134-92-SET $ 75 / 3 x 1 mL<br />

Column Evaluation Mix<br />

D-5134-92-CEM $ 35 / 1 x 1 mL<br />

Wt. / Wt. %<br />

Toluene 0.5<br />

n-Heptane 1.0<br />

2,3,3-Trimethylpentane 1.0<br />

2-Methylheptane 1.0<br />

7 comps.<br />

Wt. / Wt. %<br />

4-Methylheptane 1.0<br />

n-Octane 1.0<br />

2-Methylpentane 94.5<br />

Internal Standard<br />

D-5059-IS-4 $ 80 / 1 x 4 oz bottle<br />

D-5059-IS-10ML-PAK $ 60 / 5 x 10 mL amps<br />

Bismuth @ 0.793 mg/mL (3.00 g/US gal)<br />

(3.60 g/UK gal) in Mineral oil<br />

Technical Notes<br />

All D-5059 Certificates have the<br />

concentrations for the Standard listed<br />

in three convenient Lead<br />

Concentration units.<br />

Linearity Check Mix<br />

D-5134-92-LCM $ / 1 x 1 mL<br />

10% w/w each component 10 comps.<br />

Benzene<br />

2,4-Dimethylheptane<br />

2,4-Dimethylhexane<br />

n-Heptane<br />

n-Hexane<br />

Originally designed for<br />

D-5134-98<br />

Cat. No. Description Unit Price<br />

D-5134-92-ALK Qualitative Reference Alkylate Standard neat fraction<br />

approx. 30 components identified<br />

1 x 1 mL $ 30<br />

D-5134-92-NAP Qualitative Reference Naphtha Standard neat fraction<br />

approx. 70 components identified<br />

1 x 1 mL 30<br />

D-5134-92-REF Qualitative Reference Reformate Standard neat fraction<br />

approx. 100 components identified<br />

1 x 1 mL 30<br />

2-Methylheptane<br />

2-Methylhexane<br />

n-Nonane<br />

n-Octane<br />

Toluene<br />

Originally designed for<br />

D-5059-98<br />

D-5059<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 27<br />

Method 5059<br />

5134<br />

Member<br />

<strong>Standards</strong> of Interests<br />

See page 14 for additional<br />

Detailed Hydrocarbon Analysis<br />

(DHA) blends.<br />

<strong>ASTM</strong>


Method 5184<br />

5185<br />

, 5186<br />

Member<br />

<strong>ASTM</strong><br />

WEAR METALS<br />

<strong>ASTM</strong> D-5184 Aluminum and Silicon in Fuel Oils by<br />

(Reapproved 1995) Ashing, Fusion, ICP-AES Spectrometry & AA Spectrometry<br />

Tartaric Acid / Hydrochloric Acid<br />

Solution<br />

D-5184-91-TA-5 $ 20 / 1 x 500 mL<br />

Tartaric acid @ 0.5% w/v in 4% HCl<br />

Silicon Standard Solution<br />

D-5184-91-SI-1 $ 34 / 1 x 100 mL<br />

D-5184-91-SI-5 $ 67 / 1 x 500 mL<br />

Silicon @ 1000 µg/mL in trace NaOH<br />

<strong>ASTM</strong> D-5185 Additive Elements, Wear Metals, & Contaminants in Used Lubricating Oils by ICP-AES<br />

21 Wear Metal Multi-Element Standard<br />

Containing No Metallic Sulfonates<br />

Recommended Internal Standard (IS)<br />

<strong>ASTM</strong> D-5186 Aromatic Content & Polynuclear Aromatic Content of<br />

Diesel Fuels & Aviation Turbine Fuels by SFC<br />

Performance Solution<br />

D-5186-96-PM $ 25 / 1 x 1 mL<br />

D-5186-96-PM-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

4 comps.<br />

28<br />

Conc.<br />

(µg/g)<br />

Cat. No. Price<br />

10 WM-21-NMS-1X-1 $ 160<br />

30 WM-21-NMS-3X-1 160<br />

50 WM-21-NMS-5X-1 160<br />

100 WM-21-NMS-10X-1 180<br />

300 WM-21-NMS-30X-1 240<br />

500 WM-21-NMS-50X-1 350<br />

WM-21-NMS-SET-1<br />

set of above 6 x 100 mL<br />

$ 1050<br />

Wt. / Wt. %<br />

n-Hexadecane 75<br />

Naphthalene 2.0<br />

Wt. / Wt. %<br />

Tetralin 3.0<br />

Toluene 20<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Aluminum Standard Solution<br />

D-5184-91-AL-1 $ 34 / 1 x 100 mL<br />

D-5184-91-AL-5 $ 67 / 1 x 500 mL<br />

Al @ 1000 µg/mL in 5 % HCl<br />

Technical Note<br />

Contact the our Technical department for Ready-to-<br />

Aspirate working level calibration curves designed for<br />

your laboratories' specific calibration ranges.<br />

Each Wear Metal Standard contains<br />

the below list of 21 elements in<br />

hydrocarbon oil at the stated<br />

concentration<br />

Ag (Silver)<br />

Al (Aluminum)<br />

B (Boron)<br />

Ba (Barium)<br />

Ca (Calcium)<br />

Cd (Cadmium)<br />

Cr (Chromium)<br />

Cu (Copper)<br />

Fe (Iron)<br />

Mg (Magnesium)<br />

Mn (Manganese)<br />

Sulfur free Organometallic (IS) Sulfur free Organometallic (IS)<br />

Element @ 1000 µg/g Price @ 5000 µg/g Price<br />

Cat. No. 50 mL Cat. No. 50 mL<br />

Cobalt WM-NMS-14 $ 75 WM-NMS-14-5X $ 110<br />

Detector Linearity Check Solution Set<br />

D-5186-96-DLC-SET $ 30 / 2 x 1 mL<br />

Set includes the below two Cat. No.'s<br />

D-5186-96-DLC-25X 25% w/w #2 Diesel Fuel in n-Hexadecane<br />

D-5186-96-DLC-50X 50% w/w #2 Diesel Fuel in n-Hexadecane<br />

ISO 9001:2000<br />

Certificate Number: 31692<br />

Mo (Molybdenum)<br />

Na (Sodium)<br />

Ni (Nickel)<br />

P (Phosphorus)<br />

Pb (Lead)<br />

Si (Silicon)<br />

Sn (Tin)<br />

Ti (Titanium)<br />

V (Vanadium)<br />

Zn (Zinc)<br />

Originally designed for<br />

D-5184-91<br />

Originally designed for<br />

D-5185-97<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

<strong>Standards</strong> of Interests<br />

See Table of Contents for the<br />

Wear Metals Group pages<br />

Technical Notes<br />

This calibration curve has been<br />

formulated with starting<br />

materials containing no metal<br />

sulfonates. So a sulfur<br />

calibration curve can easily be<br />

developed using a high<br />

concentration sulfur standard.<br />

Originally designed for<br />

D-5186-99


<strong>ASTM</strong> D-5188 Vapor - Liquid Ratio Temperature <strong>Standards</strong><br />

<strong>ASTM</strong> D-5191 & D-5482 Vapor Pressure <strong>Standards</strong><br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Performance Check Samples for daily monitoring of instrument performance<br />

Cat. No. V/L Temp Price / Set<br />

<strong>ASTM</strong>-P-125-01-VAP 36.1˚C (96.9˚F) $ 45 / 5 x 20 mL<br />

<strong>ASTM</strong>-P-125-02-VAP 68.0˚C (155.7˚F) 45 / 5 x 20 mL<br />

Vapor Pressure Quality Control Samples<br />

Cat. No. Vapor Pressure Price / Set<br />

<strong>ASTM</strong>-P-124-01-VAP 68.3kPa (9.91 psi) $ 65 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-02-VAP 68.0kPa (9.86 psi) 75 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-03-VAP 51.1kPa (7.41 psi) 70 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-04-VAP 46.7kPa (6.77 psi) 115 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-05-VAP 22.5kPa (3.26 psi) 50 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-06-VAP 7.1kPa (1.03 psi) 50 / 10 x 10 mL<br />

<strong>ASTM</strong> D-5307-97 Boiling Range Distribution of Crude Petroleum by GC<br />

Quantitative Paraffins Standard<br />

D-5307-QUANT $ 60 / 1 x 2 mL<br />

D-5307-QUANT-PAK SAVE 20% $ 240 / 5 x 2 mL<br />

Equal Wt. % 16 comps.<br />

n-Decane<br />

n-Undecane<br />

n-Dodecane<br />

n-Tridecane<br />

n-Tetradecane<br />

n-Pentadecane<br />

n-Hexadecane<br />

n-Heptadecane<br />

Wt./Wt. %<br />

n-Hexadecane 1.0<br />

n-Octadecane 1.0<br />

n-Octadecane<br />

n-Eicosane<br />

n-Tetracosane<br />

n-Octacosane<br />

n-Dotriacontane<br />

n-Hexatriacontane<br />

n-Tetracontane<br />

n-Tetratetracontane<br />

Column Resolution Mixture<br />

D-5307-CR $ 15 / 1 x 1 mL<br />

D-5307-CR-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

At stated approx. Wt. % 3 comps.<br />

Wt./Wt. %<br />

n-Octane 98.0<br />

Member<br />

Wt./Wt. %<br />

Propane 10<br />

Butane 15<br />

n-Pentane 15<br />

n-Hexane 15<br />

Wt./Wt. %<br />

n-Tetradecane 25<br />

n-Pentadecane 25<br />

Originally designed for<br />

D-5188-99<br />

Originally designed for<br />

D-5191-99 & D-5482-99<br />

Technical Note<br />

Consists of pure<br />

solvents with<br />

known vapor<br />

pressure<br />

Qualitative Paraffins Standard<br />

D-5307-QUAL $ 40 / 1 x 1 mL<br />

D-5307-QUAL-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

At stated approx. Wt. % 7 comps.<br />

Wt./Wt. %<br />

n-Heptane 15<br />

n-Octane 15<br />

n-Nonane 15<br />

Internal Standard<br />

D-5307-IS-10ML $ 30 / 1 x 10 mL<br />

D-5307-IS-10ML-PAK SAVE 20% $ 120 / 5 x 10 mL<br />

4 comps.<br />

Wt./Wt. %<br />

n-Hexadecane 25<br />

n-Heptadecane 25<br />

AccuStandard is an active member in <strong>ASTM</strong> and<br />

strives to keep abreast of <strong>ASTM</strong> method revisions.<br />

If our listed formulation does not meet the most<br />

recent method revision, please contact Technical<br />

Support, ext. 117 for an updated product.<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 29<br />

Method 5188<br />

5191 &<br />

5482<br />

5307<br />

Member<br />

Value Added Paks (Cat. No.’s<br />

ending in -VAP) provide multiple<br />

single units packaged together<br />

for both greater stability and<br />

cost savings.<br />

<strong>ASTM</strong>


Method 5441<br />

Member<br />

<strong>ASTM</strong><br />

<strong>ASTM</strong> D-5441 Analysis of Methyl tert-butyl ether (MtBE) by GC<br />

trans-2-Pentene<br />

tert-Butanol<br />

30<br />

tert-Amyl methyl ether<br />

tert-Butanol<br />

tert-Butyl ethyl ether<br />

4,4-Dimethyl-2-neopentyl-1-pentene<br />

Methanol<br />

2-Methylbutane<br />

2-Methyl-2-butene<br />

2,2',4,6,6'-Pentamethyl-3-heptene<br />

Pentane<br />

cis-2-Pentene<br />

trans-2-Pentene<br />

2,4,4-Trimethyl-1-pentene<br />

Methanol<br />

Isobutylene<br />

n-Butane<br />

trans-2-butene<br />

cis-2-butene<br />

3-Methyl-1-butene<br />

Acetone<br />

Isopentane<br />

2-Propanol<br />

1-Pentene<br />

2-Methyl-1-butene<br />

n-Pentane<br />

trans-2-Pentene<br />

t-Butanol<br />

cis-2-Pentene<br />

2-Methyl-2-butene<br />

Cyclopentene<br />

MtBE<br />

2,3-Dimethyl-1-butene<br />

4-Methyl-cis-2-pentene<br />

2-Methylpentane<br />

Methylethyl ketone<br />

3-Methylpentane<br />

sec-Butyl methyl ether<br />

ETBE<br />

TAME<br />

3,5-Dimethyl-1-hexene<br />

2,4,4-Trimethyl-1-pentene<br />

2,4,4-Trimethyl-2-pentene<br />

3,4,4-Trimethyl-trans-2-pentene<br />

2,3,4-Trimethyl-2-pentene<br />

4,4-Dimethyl-2-neopentyl-1-pentene<br />

2,2’,4,6,6’-Pentamethyl-3-heptene<br />

MtBE Resolution Test Mixture<br />

D-5441-RES $ 20 / 1 x 1 mL<br />

D-5441-RES-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

D-5441-RES-5ML $ 60 / 1 x 5 mL<br />

D-5441-RES-5ML-PAK SAVE 20% $ 240 / 5 x 5 mL<br />

Each comp. at 1% Wt./Wt. in MtBE 3 comps.<br />

cis-Pentene<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

The <strong>ASTM</strong> Committee D-02 on Petroleum Products and Lubricants has issued the Standard Method<br />

D-5441-98 for the determination of the purity of methyl tert-butyl ether (MtBE) by Gas Chromatography.<br />

This method provides a procedure to measure impurities in MtBE such as C 4 to C 12 olefins, methyl,<br />

isopropyl and tert-butyl alcohols, methyl sec-butyl & methyl tert-amyl ethers, acetone, and methyl ethyl<br />

ketones. The presence of these impurities in MtBE can have a direct effect upon the value of the MtBE as<br />

a gasoline additive. AccuStandard has formulated the following reference standards to meet the method<br />

specifications. Different packaging sizes are available to meet various sample testing capacities .<br />

MtBE Contaminant Standard<br />

Low Concentration<br />

D-5441 $ 30 / 1 x 1 mL<br />

D-5441-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

D-5441-5ML $ 100 / 1 x 5 mL<br />

D-5441-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL<br />

Each comp. at 0.1% Wt./Wt. in MtBE 12 comps.<br />

Qualitative Standard<br />

D-5441-QUAL $ 145 / 1 x 1 mL<br />

0.1% Wt./Wt. in n-Dodecane 33 comps.<br />

MtBE Contaminant Standard<br />

High Concentration<br />

D-5441-10X $ 30 / 1 x 1 mL<br />

D-5441-10X-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

D-5441-10X-5ML $ 100 / 1 x 5 mL<br />

D-5441-10X-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL<br />

Each comp.at 1% Wt./Wt. in MtBE 12 comps.<br />

tert-Amyl methyl ether<br />

tert-Butanol<br />

tert-Butyl ethyl ether<br />

4,4-Dimethyl-2-neopentyl-1-pentene<br />

Methanol<br />

2-Methylbutane<br />

2-Methyl-2-butene<br />

2,2',4,6,6'-Pentamethyl-3-heptene<br />

Pentane<br />

cis-2-Pentene<br />

trans-2-Pentene<br />

2,4,4-Trimethyl-1-pentene<br />

Quantitative Standard<br />

D-5441-QUANT $ 130 / 1 x 1 mL<br />

0.1% Wt./Wt. in n-Dodecane 29 comps.<br />

Methanol<br />

2-Methylpentane<br />

3-Methyl-1-butene Methyl ethyl ketone<br />

Acetone<br />

3-Methylpentane<br />

Isopentane sec-Butyl methyl ether<br />

2-Propanol Ethyl tert-butyl ether<br />

1-Pentene<br />

TAME<br />

2-Methyl-1-butene 3,5-Dimethyl-1-hexene<br />

n-Pentane<br />

2,4,4-Trimethyl-1-pentene<br />

trans-2-Pentene 2,4,4-Trimethyl-2-pentene<br />

t-Butanol<br />

3,4,4-Trimethyl-trans-2-pentene<br />

cis-2-Pentene 2,3,4-Trimethyl-2-pentene<br />

2-Methyl-2-butene 4,4-Dimethyl-2-neopentyl-1-pentene<br />

Cyclopentene<br />

MtBE<br />

2,3-Dimethyl-1-butene<br />

2,2’,4,6,6’-Pentamethyl-3-heptene<br />

4-Methyl-cis-2-pentene<br />

Originally designed for<br />

D-5441-98<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

For our complete line of<br />

Organic <strong>Standards</strong> and<br />

Inorganic <strong>Standards</strong>, request<br />

a copy of the Catalog(s).


<strong>ASTM</strong> <strong>Standards</strong><br />

<strong>ASTM</strong> D-5442 (Reapproved 1998) Analysis of Petroleum Waxes by GC<br />

Quantitative Wax Standard<br />

D-5442-PAK $ 95 / 5 x 1 mL<br />

At stated Wt. % in Cyclohexane 16 comps.<br />

Wt./Wt. %<br />

n-Dodecane 0.02<br />

n-Tetradecane 0.03<br />

n-Hexadecane 0.04<br />

n-Octadecane 0.05<br />

n-Eicosane 0.06<br />

n-Docosane 0.08<br />

Retention Time Standard Mix 1<br />

D-5442-RT1 $ 50 / 500 mg<br />

Equal parts by weight 12 comps.<br />

n-Hexadecane (c16)<br />

n-Octadecane (c18)<br />

n-Eicosane (c20)<br />

n-Docosane(c22)<br />

n-Tetracosane (c24)<br />

n-Hexacosane (c26)<br />

<strong>ASTM</strong> D-5443 Paraffin, Naphthene, and Aromatic Hydrocarbon Type Analysis in<br />

(Reapproved 1998) Petroleum Distillates through 200°C by Multi-dimensional GC<br />

Hydrocarbon Test Mixture<br />

D-5443-93-HTM $ 100 / 1 x 1 mL<br />

At stated Wt. % 28 comps.<br />

Wt./Wt. %<br />

Cyclopentane 1.00<br />

n-Pentane 1.00<br />

Cyclohexane 2.00<br />

2,3-Dimethylbutane 2.00<br />

n-Hexane 2.00<br />

n-Hexene 1.50<br />

Methylcyclohexane 4.25<br />

4-Methyl-1-hexene 1.50<br />

n-Heptane 3.50<br />

Wt./Wt. %<br />

n-Tetracosane 0.10<br />

n-Hexacosane 0.12<br />

n-Octacosane 0.12<br />

n-Triacontane 0.10<br />

n-Dotriacontane 0.08<br />

n-Octacosane (c28)<br />

n-Triacontane (c30)<br />

n-Dotriacontane (c32)<br />

n-Hexatriacontane (c36)<br />

n-Tetracontane (c40)<br />

n-Tetratetracontane (c44)<br />

NEW<br />

Wt./Wt. %<br />

1cis,2-Dimethylcyclohexane 5.00<br />

Isooctane 5.00<br />

n-Octane 5.00<br />

1cis,2 cis,4-Trimethylcyclohexane 4.25<br />

n-Nonane 4.50<br />

n-Decane 4.25<br />

n-Undecane 3.50<br />

n-Dodecane 3.25<br />

Benzene 2.25<br />

Toluene 2.25<br />

Retention Time Standard Mix 2<br />

D-5442-RT2 $ 55 / 500 mg<br />

Equal parts by weight 16 comps.<br />

<strong>ASTM</strong> D-5453 Total Sulfur in Light Hydrocarbons,<br />

Motor Fuels and Oils by Ultraviolet Fluorescence<br />

Low Level Sulfur Set<br />

D-5453-LL-SET $ 90 / 5 x 2 mL<br />

The set contains the following 5 standards in Isooctane<br />

Cat. No. Description Unit<br />

D-5453-LL-BL Sulfur Blank 2 mL<br />

D-5453-LL-01 Sulfur @ 0.5 ng/µL 2 mL<br />

D-5453-LL-02 Sulfur @ 2.5 ng/µL 2 mL<br />

D-5453-LL-03 Sulfur @ 5.0 ng/µL 2 mL<br />

D-5453-LL-04 Sulfur @ 10.0 ng/µL 2 mL<br />

Mid Level Sulfur Set<br />

D-5453-ML-SET $ 90 / 6 x 2 mL<br />

The set contains the following 5 standards in Isooctane<br />

Cat. No. Description Unit<br />

D-5453-ML-BL Sulfur Blank 2 mL<br />

D-5453-ML-01 Sulfur @ 5.0 ng/µL 2 mL<br />

D-5453-ML-02 Sulfur @ 25 ng/µL 2 mL<br />

D-5453-ML-03 Sulfur @ 50 ng/µL 2 mL<br />

D-5453-ML-04 Sulfur @ 100 ng/µL 2 mL<br />

D-5453-ML-05 Sulfur @ 200 ng/µL 2 mL<br />

Wt./Wt. %<br />

n-Hexatriacontane 0.06<br />

n-Tetracontane 0.05<br />

n-Tetratetracontane 0.04<br />

n-Pentacontane 0.03<br />

n-Hexacontane 0.02<br />

n-Dodecane (c12)<br />

n-Tetradecane (c14)<br />

n-Hexadecane (c16)<br />

n-Octadecane (c18)<br />

n-Eicosane (c20)<br />

n-Docosane (c22)<br />

n-Tetracosane (c24)<br />

n-Hexacosane (c26)<br />

Column Resolution<br />

Standard<br />

D-5442-CR-PAK $ 40 / 5 x 1 mL<br />

At stated Wt. % in Cyclohexane<br />

2 comps.<br />

Wt./Wt. %<br />

n-Eicosane 0.05<br />

n-Tetracontane 0.05<br />

NEW<br />

n-Octacosane (c28)<br />

n-Triacontane (c30)<br />

n-Dotriacontane (c32)<br />

n-Hexatriacontane (c36)<br />

n-Tetracontane (c40)<br />

n-Tetratetracontane (c44)<br />

n-Pentacontane (c50)<br />

n-Hexacontane (c60)<br />

Wt./Wt. %<br />

trans-Decahydronaphthelene 4.25<br />

n-Tetradecane 4.50<br />

Ethylbenzene 4.50<br />

o-Xylene 4.25<br />

n-Propylbenzene 5.00<br />

1,2,4-Trimethylbenzene 4.50<br />

1,2,3-Trimethylbenzene 5.00<br />

1,2,4,5-Tetramethylbenzene 5.00<br />

Pentamethylbenzene 5.00<br />

Real World Sulfur in Various<br />

Gasoline & Fuels<br />

QC Samples<br />

SBPT-LSGAS $ 25 / 2 x 15 mL<br />

Parameter Method Approx .Range<br />

Sulfur D-5453-00 0 - 50 µg/g<br />

Originally designed for<br />

D-5453-00<br />

High Level Sulfur Set<br />

D-5453-HL-SET $ 90 / 5 x 2 mL<br />

The set contains the following 5 standards in Isooctane<br />

Cat. No. Description Unit<br />

D-5453-HL-BL Sulfur Blank 2 mL<br />

D-5453-HL-01 Sulfur @ 100 ng/µL 2 mL<br />

D-5453-HL-02 Sulfur @ 250 ng/µL 2 mL<br />

D-5453-HL-03 Sulfur @ 500 ng/µL 2 mL<br />

D-5453-HL-04 Sulfur @ 1000 ng/µL 2 mL<br />

Originally designed for<br />

D-5442-93<br />

Technical Note<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 31<br />

Member<br />

<strong>Standards</strong> of Interests<br />

<strong>Standards</strong> of Interests<br />

See pages 6-11 for a<br />

comprehensive line of Certified<br />

Sulfur Calibration <strong>Standards</strong>,<br />

Petrocheck, & Petrotest quality<br />

control products, pages 1-2.<br />

D-5453<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

Method 5442<br />

5443<br />

5453<br />

See <strong>ASTM</strong> Methods D-3710,<br />

D-5307, D-6352 for additional<br />

calibration standards for<br />

hydrocarbon analysis or page 15<br />

for new proposed methods.<br />

Originally designed for<br />

D-5443-93<br />

Due to the wide variety of<br />

recommended solvents and<br />

starting materials mentioned in<br />

the preparation of the sulfur<br />

standards, please review the<br />

current product offering listed<br />

for certified sulfur standards.<br />

Should AccuStandard’s current<br />

sulfur standard line be missing<br />

the necessary standards for<br />

your application, please use our<br />

custom quotation request form<br />

to indicate your required<br />

formulation. For ppb Sulfur<br />

measurements, see page 6-11.<br />

<strong>ASTM</strong>


Method 5480<br />

5482<br />

5501<br />

5580<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-5480 Engine Oil Volatility by GC<br />

Stock Column Resolution Standard<br />

D-5480-CR-PAK $ 40 / 5 x 1 mL<br />

Each comp. at 10 µg/mL in CS2 5 comps.<br />

D-5480-CR-100X-PAK $ 50 / 5 x 1 mL<br />

Each comp. at 1000 µg/mL in CS2 5 comps.<br />

<strong>ASTM</strong> D-5482 & D-5191 Vapor Pressure <strong>Standards</strong><br />

Vapor Pressure Quality Control Samples<br />

<strong>ASTM</strong> D-5501 Ethanol Content of Denatured Fuel Ethanol by GC<br />

Denatured Fuel Ethanol Calibration Set<br />

D-5501-94-SET $ 75 / set of 7 x 1 mL<br />

32<br />

n-Decane<br />

n-Dodecane<br />

n-Hexadecane<br />

n-Octadecane<br />

n-Tetracosane<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Internal Standard Solution<br />

D-5480-IS-5ML $ 30 / 1 x 5 mL<br />

D-5480-IS-5ML-PAK SAVE 20% $ 120 / 5 x 5 mL<br />

Each comp. at equal weights 3 comps.<br />

n-Decane<br />

n-Undecane<br />

n-Dodecane<br />

Tetracosane (Solution A)<br />

D-5480-C40-5ML $ 15 / 1 x 5 mL<br />

D-5480-C40-5ML-PAK SAVE 20% $ 60 / 5 x 5 mL<br />

500 µg/mL in CS 2<br />

n-Tetracosane<br />

Cat. No. Vapor Pressure Price / Set of 10<br />

<strong>ASTM</strong>-P-124-01 68.3kPa (9.91 psi) $ 65 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-02 68.0kPa (9.86 psi) 75 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-03 51.1kPa (7.41 psi) 70 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-04 46.7kPa (6.77 psi) 125 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-05 22.5kPa (3.26 psi) 50 / 10 x 10 mL<br />

<strong>ASTM</strong>-P-124-06 7.1kPa (1.03 psi) 50 / 10 x 10 mL<br />

Technical Note<br />

Consists of pure<br />

solvents with<br />

known vapor<br />

pressure.<br />

Cat. No. Comp.1 Wt./ Wt.% Comp.2 Wt./ Wt.% Comp.3 Wt./ Wt.% Unit<br />

D-5501-94-01 Ethanol 92 Methanol 0.6 Heptane 7.4 1 x 1 mL<br />

D-5501-94-02 Ethanol 93 Methanol 0.5 Heptane 6.5 1 x 1 mL<br />

D-5501-94-03 Ethanol 94 Methanol 0.4 Heptane 5.6 1 x 1 mL<br />

D-5501-94-04 Ethanol 95 Methanol 0.3 Heptane 4.7 1 x 1 mL<br />

D-5501-94-05 Ethanol 96 Methanol 0.2 Heptane 3.8 1 x 1 mL<br />

D-5501-94-06 Ethanol 97 Methanol 0.1 Heptane 2.9 1 x 1 mL<br />

D-5501-94-07 Ethanol 98 Methanol 0.05 Heptane 1.95 1 x 1 mL<br />

<strong>ASTM</strong> D-5580 Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene, C 9 and<br />

Heavier Aromatics, & Total Aromatics in Finished Gasoline by GC<br />

Aromatics Quantitative Calibration Mixes (without Internal Standard)<br />

D-5580-95-CAL-SET-10ML $ 300 / set of 5 x 10 mL of 6 component mix<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

Analyte Calibration range Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Benzene 0.10 - 5.00 0.10 0.50 1.00 2.00 5.00<br />

Toluene 1.00 - 15.00 15.00 10.00 5.00 2.50 1.00<br />

Ethylbenzene 0.50 - 10.00 0.50 1.00 2.50 5.00 10.00<br />

o-Xylene 0.50 - 10.00 1.00 2.50 10.00 5.00 0.50<br />

1,2,4-Trimethylbenzene 0.50 - 10.00 1.00 10.00 0.50 5.00 2.50<br />

Isooctane 82.40 76.00 81.00 80.50 81.00<br />

Aromatics Quantitative Calibration Mixes (with Internal Standard)<br />

D-5580-95-CAL-IS-SET $ 100 / set of 5 x 1 mL of 7 component mix<br />

Originally designed for<br />

D-5501-94<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

Analyte Calibration range Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Benzene 0.09 - 4.50 0.09 0.45 0.90 1.80 4.50<br />

Toluene 0.90 - 13.50 13.50 9.00 4.50 2.25 0.90<br />

Ethylbenzene 0.45 - 9.00 0.45 0.90 2.25 4.50 9.00<br />

o-Xylene 0.45 - 9.00 0.90 2.25 9.00 4.50 0.45<br />

1,2,4-Trimethylbenzene 0.45 - 9.00 0.90 9.00 0.45 4.50 2.25<br />

2-Hexanone (Internal Std.) 10.00 10.00 10.00 10.00 10.00<br />

Isooctane 74.16 68.40 72.90 72.45 72.90<br />

Originally designed for<br />

D-5480-95<br />

Quality System is Certified <strong>ASTM</strong> to D-5580-00 comply with Continued the International on the ISO Next 9001 Page Quality Standard<br />

<strong>Standards</strong> of Interest<br />

Alternative n-Paraffin standards<br />

are available on page 15 for<br />

further method development<br />

work or more Detailed<br />

Hydrocarbon Analysis (DHA).<br />

Originally designed for<br />

D-5482-99 & D-5191-99<br />

Technical Note<br />

Additional Oxygenate calibration,<br />

check standards, and<br />

independent reference standards<br />

can be found in <strong>ASTM</strong> method<br />

D-4815 (page 24) or D-5622-94<br />

(page 37). The required QA/QC<br />

procedures in EPA methods<br />

stipulate a calibration check<br />

standard be used once per<br />

analytical batch or per 10 sample<br />

set. AccuStandard has bulk<br />

packaged check standards to<br />

meet this increased usage.<br />

Originally designed for<br />

D-5580-00


<strong>ASTM</strong> D-5580-00 Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene, C9 &<br />

Continued Heavier Aromatics, and Total Aromatics in Finished Gasoline by GC<br />

Valve Timing Calibration Mix<br />

(with Internal Standard)<br />

M-GRA-VT/IS-AS $ 25 / 1 x 1 mL<br />

M-GRA-VT/IS-AS-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

Each at stated conc. 6 comps.<br />

Wt./Wt. %<br />

Benzene 4.5<br />

Toluene 4.5<br />

Ethylbenzene 9.0<br />

o-Xylene 9.0<br />

2-Hexanone (Internal Std.) 10.0<br />

Isooctane 63.0<br />

Internal Standard<br />

M-GRA-IS-AS-5ML $ 10 / 1 x 5 mL<br />

M-GRA-IS-AS-5ML-PAK SAVE 20% $ 40 / 5 x 5 mL<br />

2-Hexanone (Neat)<br />

Daily Quality Control Standard<br />

without Internal Standard<br />

D-5580-QC-R1 $ 125 / 1 x 10 mL<br />

D-5580-QC-R1-PAK SAVE 20% $ 500 / 5 x 10 mL<br />

14 comps.<br />

Wt./Wt. %<br />

n-Hexane 12<br />

n-Heptane 20<br />

n-Octane 15<br />

n-Decane 10<br />

n-Dodecane 1<br />

Isooctane 20<br />

Benzene 1<br />

Wt./Wt. %<br />

Toluene 9<br />

Ethylbenzene 2<br />

p-Xylene 3<br />

o-Xylene 2<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 1<br />

Naphthalene 1<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Valve Timing Calibration Mix<br />

(without Internal Standard)<br />

M-GRA-VT-AS-10ML $ 100 / 1 x 10 mL<br />

M-GRA-VT-AS-10ML-PAK SAVE 20% $ 400 / 5 x 10 mL<br />

Each at stated conc. 5 comps.<br />

Wt./Wt. %<br />

Benzene 5.0<br />

Toluene 5.0<br />

Ethylbenzene 10.0<br />

o-Xylene 10.0<br />

Isooctane 70.0<br />

Selectivity Check Standard<br />

M-GRA-SCS-AS $ 10 / 1 x 1 mL<br />

M-GRA-SCS-AS-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

Each at stated conc. 2 comps.<br />

Wt./Wt. %<br />

n-Dodecane 1.5<br />

Isooctane 98.5<br />

Daily Quality Control Standard<br />

without Internal Standard<br />

D-5580-QC $ 125 / 1 x 10 mL<br />

D-5580-QC-PAK $ 500 / 5 x 10 mL<br />

14 comps.<br />

Wt./Wt. %<br />

n-Hexane 12<br />

n-Heptane 20<br />

n-Octane 15<br />

n-Decane 10<br />

n-Triadecane 1<br />

Isooctane 20<br />

Benzene 1<br />

Wt./Wt. %<br />

Toluene 9<br />

Ethylbenzene 2<br />

p-Xylene 3<br />

o-Xylene 2<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 1<br />

Naphthalene 1<br />

Originally designed for<br />

D-5580-00<br />

Technical Note<br />

Exclusive Aromatic Chemical Reference Material<br />

Benefits from AccuStandard<br />

Every analyte in each solution is individually weighed<br />

Actual weights and weight percents are available with all<br />

<strong>ASTM</strong>/EPA solutions<br />

Method 5580<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 33<br />

Member<br />

<strong>ASTM</strong> D-5580 Gasoline<br />

Refinery Quality Control<br />

Standard<br />

AccuStandard was requested by<br />

the Petrochemical Industry to<br />

manufacture the following QA/QC<br />

standards for <strong>ASTM</strong> Method<br />

D-5580. The configuration of your<br />

instrument valve time switching and<br />

the pre-column incorporated<br />

determines which QA/QC standard<br />

provides optimum performance<br />

when analyzing gasolines samples<br />

by Method D-5580. Use of the<br />

D-5580 standards in conjunction<br />

with the real world gasoline<br />

AccuPetroTest & AccuPetroCheck<br />

Consensus Value Reference<br />

Material (see pages 1-2) can<br />

provide added assurance that the<br />

analytical results being generated<br />

by the laboratory are reproducible<br />

and the analytical system is<br />

performing to method specifications.<br />

<strong>ASTM</strong>


Method 5599<br />

<strong>ASTM</strong><br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-5599 Oxygenates in Gas by GC & O-FID<br />

Oxygenates Calibration Curve with Internal Standard<br />

M-GRO-CAL/IS-SET $ 250 / set of 8 x 1 mL<br />

M-GRO-CAL/IS-SET-PAK $ 1,000 / 5 x (8 x 1) mL<br />

of 15 Comp. Mix<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Every analyte in each solution<br />

is individually weighed<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7 Std. 8<br />

Calibration range Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Methanol 0.1 - 5.0 --- 0.1 2.5 --- 5 0.5 1 ---<br />

Ethanol 1.0 - 12.0 12 --- 3 --- 8 5 1 ---<br />

Isopropanol 0.1 - 2.0 2 1 --- 0.1 0.3 --- 0.5 --t-Butanol<br />

0.1 - 2.0 0.5 0.1 1 --- 2 0.3 --- ---<br />

Propanol 0.2 - 2.0 2 --- 0.7 0.2 1 --- 0.4 ---<br />

MtBE 1.0 - 17.0 5 17 --- --- 1 2.5 10 --sec-Butanol<br />

0.1 - 2.5 1 --- 0.5 0.1 --- 2.5 0.7 ---<br />

Diisopropyl ether 0.1 - 2.0 --- 0.5 0.3 0.1 2 1 --- --iso-Butanol<br />

0.1 - 2.0 2 0.5 --- 1 0.1 0.3 --- ---<br />

EtBE 1.0 - 18.0 --- 3.5 18 7.5 --- 1 12 --t-Pentanol<br />

0.1 - 2.0 0.3 1 --- 0.5 0.1 2 --- ---<br />

Butanol 0.1 - 2.0 1 --- 0.3 --- 0.5 0.1 2 ---<br />

TAME 1.0 - 18.0 --- 3.5 1 18 7.5 12 --- ---<br />

1,2- Dimethoxyethane (ISTD) 4 4 4 4 4 4 4 ---<br />

RFA Gasoline 70.2 68.8 68.7 68.5 68.5 68.8 68.4 100<br />

Total oxygenates & ISTD 29.8 31.2 31.3 31.5 31.5 31.2 31.6 0<br />

Oxygenates Calibration Curve without Internal Standard<br />

M-GRO-CAL-SET $ 850 / set of 8 x 10 mL<br />

of 14 Comp. Mix<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7 Std. 8<br />

Calibration range Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Methanol 0.1 - 5.0 --- 0.1 2.5 --- 5 0.5 1 ---<br />

Ethanol 1.0 - 12.0 12 --- 3 --- 8 5 1 ---<br />

Isopropanol 0.1 - 2.0 2 1 --- 0.1 0.3 --- 0.5 --t-Butanol<br />

0.1 - 2.0 0.5 0.1 1 --- 2 0.3 --- ---<br />

Propanol 0.2 - 2.0 2 --- 0.7 0.2 1 --- 0.4 ---<br />

MtBE 1.0 - 17.0 5 17 --- --- 1 2.5 10 --sec-Butanol<br />

0.1 - 2.5 1 --- 0.5 0.1 --- 2.5 0.7 ---<br />

Diisopropyl ether 0.1 - 2.0 --- 0.5 0.3 0.1 2 1 --- --iso-Butanol<br />

0.1 - 2.0 2 0.5 --- 1 0.1 0.3 --- ---<br />

EtBE 1.0 - 18.0 --- 3.5 18 7.5 --- 1 12 --t-Pentanol<br />

0.1 - 2.0 0.3 1 --- 0.5 0.1 2 --- ---<br />

Butanol 0.1 - 2.0 1 --- 0.3 --- 0.5 0.1 2 ---<br />

TAME 1.0 - 18.0 --- 3.5 1 18 7.5 12 --- ---<br />

RFA Gasoline 74.2 64.8 64.7 64.5 64.5 64.8 64.4 100<br />

Total oxygenates 25.8 27.2 27.3 27.5 27.5 27.2 27.6 0<br />

34<br />

Features: Benefits:<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Technical Note<br />

Oxygenate Calibration Curves<br />

ISTD-Free and Larger<br />

Packaging Size.<br />

AccuStandard has received<br />

requests from the Petroleum<br />

Industry to formulate our D-5599<br />

Oxygenate product without internal<br />

standard (ISTD) and package it in a<br />

larger volume. We have met those<br />

requests by introducing the<br />

M-GRO-CAL-SET calibration curve.<br />

This curve is manufactured without<br />

incorporating an internal standard<br />

and is packaged in Ready-to-Use<br />

10 mL sample volume.<br />

The certified oxygenate calibration<br />

curve can be used in combination<br />

with other aromatic standards for<br />

combined oxygenate/aromatic<br />

analysis, to change the amount of<br />

internal standard added, or to<br />

incorporate alternative internal<br />

standard analytes.<br />

D-5599<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

Technical Note<br />

AccuStandard’s M-GRO<br />

oxygenate calibration curve has<br />

been successfully used by<br />

Petroleum Refineries and<br />

supporting laboratories for both<br />

<strong>ASTM</strong> Method D-5599 and<br />

<strong>ASTM</strong> Method D-4815. In<br />

addition, AccuStandard’s<br />

certified oxygenate chemical<br />

reference materials provide the<br />

following features and benefits<br />

for superior performance and<br />

value.<br />

Analytes checked for chemical purity & water content The use & validation of the highest purity neats enhance the integrity of the standard.<br />

Analyzed by Independent Laboratories Independent product validation of certified values.<br />

Certified method specific calibration standards Increased confidence in analytical results.<br />

Elimination of standards preparation Time is utilized quantifying samples.<br />

Internal <strong>Standards</strong> incorporated Ready-to-Inject <strong>Standards</strong>.<br />

Originally designed for<br />

D-5599-95<br />

Actual weights and weight percents are<br />

provided with all <strong>ASTM</strong>/EPA Solutions<br />

Benefits from AccuStandard’s Oxygenates<br />

Weights and weight percents provided Ease of use in performing back calculations.<br />

All necessary solutions included Provides single source for sample analysis.<br />

Variations in Packaging size Meet laboratory sample volumes.<br />

Economical Time is spent on analysis rather than preparing stds.<br />

7 stds. used to generate 5 point curve Generate a 5 point curve in 30% less time than competitors' 10 standard set.


<strong>ASTM</strong> <strong>Standards</strong><br />

<strong>ASTM</strong> D-5599 Oxygenates in Gasoline by GC & O-FID<br />

Continued<br />

<strong>ASTM</strong>/EPA Oxygenate Quality Control <strong>Standards</strong><br />

Daily Quality Control Standard<br />

(without Internal Standard)<br />

M-GRO-QC-10ML $ 100 / 1 x 10 mL<br />

M-GRO-QC-10ML-PAK SAVE 20% $ 400 / 5 x 10 mL<br />

Compound Target<br />

Oxygenate Wt. %<br />

Methanol 1<br />

Ethanol 1<br />

Isopropanol 1<br />

t-Butanol 1<br />

Propanol 1<br />

MtBE 3<br />

sec-Butanol 1<br />

Di-isopropyl ether 3<br />

Compound Target<br />

Oxygenate Wt. %<br />

iso-Butanol 1<br />

EtBE 3<br />

t-Pentanol 1<br />

Butanol 1<br />

TAME 3<br />

RFA Gasoline 79<br />

14 comps. 100<br />

Daily Quality Control Standard<br />

(with Internal Standard)<br />

M-GRO-QC/IS-5ML $ 75 / 1 x 5 mL<br />

M-GRO-QC/IS-5ML-PAK SAVE 27% $ 275 / 5 x 5 mL<br />

Compound Target<br />

Oxygenate Wt. %<br />

Methanol 1<br />

Ethanol 1<br />

Isopropanol 1<br />

t-Butanol 1<br />

Propanol 1<br />

MtBE 3<br />

sec-Butanol 1<br />

Compound Target<br />

Oxygenate Wt. %<br />

Di-isopropyl ether 3<br />

iso-Butanol 1<br />

EtBE 3<br />

t-Pentanol 1<br />

Butanol 1<br />

TAME 3<br />

RFA Gasoline 79<br />

1,2-Dimethoxyethane (ISTD) is combined with<br />

the above 14 comps. in a 4 to 100 weight ratio<br />

15 comps.<br />

100<br />

Gasoline Refinery Blank<br />

(with Internal Standard)<br />

M-GRO-BLNK/IS-10ML $ 15 / 1 x 10mL<br />

M-GRO-BLNK/IS-10ML-PAK SAVE 20% $ 60 / 5 x 10mL<br />

2 comps.<br />

Wt. %<br />

1,2- Dimethoxyethane (ISTD) 4<br />

RFA Gasoline 96<br />

O-FID Gasoline Refinery Blank<br />

M-GRO-BLNK-10ML $ 10 / 1 x 10mL<br />

M-GRO-BLNK-10ML-PAK SAVE 20% $ 40 / 5 x 10mL<br />

RFA Gasoline (neat)<br />

Revised Daily Quality Control Standard<br />

(without Internal Standard)<br />

M-GRO-QC-R-10ML $ 100 / 1 x 10 mL<br />

M-GRO-QC-R-10ML-PAK SAVE 20% $ 400 / 5 x 10 mL<br />

Compound Target<br />

Oxygenate Wt. %<br />

Methanol 1<br />

Ethanol 1<br />

Isopropanol 1<br />

t-Butanol 1<br />

Propanol 1<br />

MtBE 3<br />

sec-Butanol 1<br />

Di-isopropyl ether 1<br />

Compound Target<br />

Oxygenate Wt. %<br />

iso-Butanol 1<br />

EtBE 3<br />

t-Pentanol 1<br />

Butanol 1<br />

TAME 3<br />

RFA Gasoline 81<br />

14 comps. 100<br />

Revised Daily Quality Control Standard<br />

(with Internal Standard)<br />

M-GRO-QC-R/IS-5ML $ 75 / 1 x 5 mL<br />

M-GRO-QC-R/IS-5ML-PAK SAVE 27% $ 275 / 5 x 5 mL<br />

Compound Target<br />

Oxygenate Wt. %<br />

Methanol 1<br />

Ethanol 1<br />

Isopropanol 1<br />

t-Butanol 1<br />

Propanol 1<br />

MtBE 3<br />

sec-Butanol 1<br />

Compound Target<br />

Oxygenate Wt. %<br />

Di-isopropyl ether 1<br />

iso-Butanol 1<br />

EtBE 3<br />

t-Pentanol 1<br />

Butanol 1<br />

TAME 3<br />

RFA Gasoline 81<br />

1,2-Dimethoxyethane (ISTD) is combined with<br />

the above 14 comps. in a 4 to 100 weight ratio<br />

15 comps.<br />

D-5599<br />

Meets<br />

EPA Guidelines<br />

for RFG<br />

Analysis<br />

Technical Note<br />

The Daily Quality Control<br />

Standard M-GRO-QC-R was<br />

developed in response to your<br />

requests for a QC mix<br />

bracketed by the Calibration<br />

Curve.<br />

AccuStandard reduced the<br />

diisopropyl ether content from 3<br />

Wt. % to 1 Wt. % to meet the<br />

method specifications.<br />

Technical Note<br />

Additional Oxygenate calibration,<br />

check standards, and<br />

independent reference standards<br />

can be found in <strong>ASTM</strong> method<br />

D-4815 (page 24) or D-5622<br />

(page 37). The required QA/QC<br />

procedures in EPA methods<br />

stipulate a calibration check<br />

standard be used once per<br />

analytical batch or per 10 sample<br />

set. AccuStandard has bulk<br />

packaged check standards to<br />

meet this increased usage.<br />

Fax 203-786-5287 • AccuStandard • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 35<br />

100<br />

O-FID/EPA Gasoline Refinery<br />

Internal Standard<br />

M-GRO-IS-5ML $ 10 / 1 x 5 mL<br />

M-GRO-IS-5ML-PAK SAVE 20% $ 40 / 5 x 5 mL<br />

1,2- Dimethoxyethane (ISTD)<br />

Originally designed for<br />

D-5599-95<br />

Method 5599<br />

Member<br />

<strong>ASTM</strong>


Method 5599<br />

<strong>ASTM</strong><br />

<strong>ASTM</strong><br />

Member<br />

EPA O-FID Oxygenate Petrochemical <strong>Standards</strong><br />

AccuStandard has formulated this second oxygenate version to meet the specific analyte requirements set forth in the EPA methodology.<br />

<strong>ASTM</strong> D-5599 EPA Gasoline Refinery Oxygenates Calibration Curves<br />

EPA O-FID Quantitative Calibration Mixes (without Internal Standard)<br />

M-GRO-CAL-EPA-SET-10ML $ 350 / set of 5 x 10 mL<br />

5 comps.<br />

Wt./Wt. %<br />

Methanol 4.0<br />

Ethanol 8.0<br />

tert-Butanol 5.0<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

Calibr. range Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Methanol 0.30 - 12.00 6.00 12.00 3.00 0.30 9.00<br />

Ethanol 0.30 - 12.00 0.30 3.00 6.00 9.00 12.00<br />

t-Butanol 0.30 - 12.00 0.30 6.00 9.00 12.00 3.00<br />

MtBE 0.30 - 15.00 15.00 7.50 11.25 3.75 0.30<br />

RFA Gasoline 78.40 71.50 70.75 74.95 75.70<br />

EPA O-FID Quantitative Calibration Mixes (with Internal Standard)<br />

M-GRO-CAL-IS/EPA-SET $ 175 / set of 5 x 1 mL<br />

6 comps.<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

Calibr. range Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Methanol 0.29 - 11.40 5.70 11.40 2.85 0.29 8.55<br />

Ethanol 0.29 - 11.40 0.29 2.85 5.70 8.55 11.40<br />

t-Butanol 0.29 - 11.40 0.29 5.70 8.55 11.40 2.85<br />

MtBE 0.29 - 14.29 14.25 7.13 10.69 3.56 0.29<br />

1,2-Dimethoxyethane (ISTD) 5.00 5.00 5.00 5.00 5.00<br />

RFA Gasoline 74.48 67.93 67.31 71.20 71.92<br />

EPA O-FID Quantitative Calibration<br />

Check Standard<br />

(without Internal Standard)<br />

M-GRO-EPA-CC-10ML $ 50 / 1 x 10 mL<br />

M-GRO-EPA-CC-10ML-PAKSAVE 20% $ 200 / 5 x 10 mL<br />

5 comps.<br />

Wt./Wt. %<br />

Methyl tert-butyl ether 12.0<br />

RFA gasoline 71.0<br />

EPA O-FID Spiking Solution<br />

M-GRO-EPA-SP-5ML $ 50 / 1 x 5 mL<br />

M-GRO-EPA-SP-5ML-PAK SAVE 20% $ 200 / 5 x 5 mL<br />

4 comps.<br />

Wt./Wt. %<br />

Methanol 14.3<br />

Ethanol 28.6<br />

Internal Standard<br />

M-GRO-IS-5ML $ 10 / 1 x 10 mL<br />

M-GRO-IS-5ML-PAK SAVE 20% $ 40 / 5 x 10 mL<br />

36<br />

1,2-Dimethoxyethane (ISTD)<br />

Wt./Wt. %<br />

tert-Butanol 14.3<br />

Methyl tert-butyl ether 42.8<br />

Oxygenates Using O-FID<br />

EPA O-FID Quantitative Calibration<br />

Check Standard<br />

(with Internal Standard)<br />

M-GRO-EPA-CC/IS-5ML $ 35 / 1 x 5 mL<br />

M-GRO-EPA-CC/IS-5MLPAK SAVE 20% $ 150 / 5 x 5 mL<br />

6 comps.<br />

Wt./Wt. %<br />

Methanol 3.80<br />

Ethanol 7.60<br />

tert-Butanol 4.75<br />

Cross Reference Table<br />

<strong>ASTM</strong> IP ISO DIN JIS AFNOR sorted by<br />

<strong>ASTM</strong> Method see beginning of Catalog<br />

Wt./Wt. %<br />

Methyl tert-butyl ether 11.40<br />

RFA gasoline 67.45<br />

DME (internal standard) 5.0<br />

Oxygenate Free Gasoline Refinery<br />

Blank<br />

M-GRO-BLNK-10ML $ 10 / 1 x 10 mL<br />

M-GRO-BLNK-10ML-PAK SAVE 20% $ 40 / 5 x 10 mL<br />

RFA Gasoline (neat)<br />

Originally designed for<br />

D-5599-95<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

For our complete line of<br />

Organic <strong>Standards</strong>,<br />

request a copy of our<br />

Catalog.<br />

Technical Note<br />

Additional Oxygenate calibration,<br />

check standards, and independent<br />

reference standards can be found in<br />

<strong>ASTM</strong> method D-4815 (page 24) or<br />

D-5622 (page 37). The required<br />

QA/QC procedures in EPA methods<br />

stipulate a calibration check<br />

standard be used once per<br />

analytical batch or per 10 sample<br />

set. AccuStandard has bulk<br />

packaged check standards to meet<br />

this increased usage.


<strong>Standards</strong> of Interests<br />

See <strong>ASTM</strong> Methods D-4815 (page 24) and D-5599<br />

(pages 34-36) for additional oxygenate calibration<br />

standards.<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

<strong>ASTM</strong> D-5600 Trace Metals in Petroleum Coke by ICP-AES<br />

Multi-Element Calibration Standard<br />

D-5600-01-1 $ 225 / 1 x 100 mL<br />

500 µg/mL each in 2-5% HNO 3 tr. HF 12 comps.<br />

Aluminum<br />

Barium<br />

Calcium<br />

Iron<br />

Magnesium<br />

Manganese<br />

Nickel<br />

Silicon<br />

<strong>Standards</strong> of Interest<br />

Sodium<br />

Titanium<br />

Vanadium<br />

Zinc<br />

Individual ICP <strong>Standards</strong> are on pages 67-72.<br />

Hydrochloric Acid Diluent<br />

D-5600-BLH-5 $ 50 / 1 x 500 mL<br />

D-5600-BLH-L $ 65 / 1 x 1 L<br />

20% HCl in <strong>ASTM</strong> Type II water<br />

Lithium Borate Diluent<br />

D-5600-LIB-1 $ 125 / 1 x 100 mL<br />

D-5600-LIB-5 $ 180 / 1 x 500 mL<br />

2.0% Lithium Borate in 10% HCl<br />

<strong>ASTM</strong> D-5622 Total Oxygen in Gasoline & MeOH Fuels by Reductive Pyrolysis<br />

Oxygenate Unit<br />

Cat. No. Description (2 x 10 mL, plus an RFA gasoline blank) Wt. % Price<br />

<strong>ASTM</strong>-P-0061-SET * Ethanol in Oxygenate free RFA gasoline 5.0 3 x 10 mL $ 50<br />

<strong>ASTM</strong>-P-0062-SET * Ethanol in Oxygenate free RFA gasoline 10.0 3 x 10 mL 50<br />

<strong>ASTM</strong>-P-0063-SET * t-Amyl methyl ether in Oxygenate free RFA gasoline 10.0 3 x 10 mL 50<br />

<strong>ASTM</strong>-P-0064-SET * t-Amyl methyl ether in Oxygenate free RFA gasoline 15.0 3 x 10 mL 50<br />

<strong>ASTM</strong>-P-0065-SET * Ethyl t-butyl ether in Oxygenate free RFA gasoline 10.0 3 x 10 mL 50<br />

<strong>ASTM</strong>-P-0066-SET * Ethyl t-butyl ether in Oxygenate free RFA gasoline 15.0 3 x 10 mL 50<br />

<strong>ASTM</strong>-P-0067-SET * Methyl t-butyl ether in Oxygenate free RFA gasoline 10.0 3 x 10 mL 50<br />

<strong>ASTM</strong>-P-0068-SET * Methyl t-butyl ether in Oxygenate free RFA gasoline 15.0 3 x 10 mL 50<br />

<strong>ASTM</strong>-P-0069-SET * Methanol & t-Butanol in Oxygenate free RFA gasoline 10.0 & 5.0 3 x 10 mL 50<br />

* Each Set includes M-GRO-BLNK-10ML<br />

Oxygenate Free Gasoline Refinery Blank<br />

M-GRO-BLNK-10ML $ 10 / 1 x 10 mL<br />

RFA Gasoline (neat)<br />

Technical Note<br />

Originally designed for<br />

D-5600-98<br />

Use M-GRO-BLNK-10ML as an<br />

oxygenate free RFA gasoline matrix to<br />

make up your own oxygenate standards<br />

or call our Technical Dept. to have a<br />

Standard custom made for you.<br />

Technical Note<br />

For our complete line of<br />

Inorganic <strong>Standards</strong>,<br />

request a copy of our<br />

Inorganics Catalog.<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 37<br />

Method 5600<br />

5622<br />

Member<br />

D-5600 Ready-to-Aspirate<br />

<strong>Standards</strong><br />

AccuStandard has formulated the<br />

following stock standards for<br />

<strong>ASTM</strong> Method D-5600. We have<br />

prepared numerous Ready-to-<br />

Aspirate ICP multi-element<br />

solutions. Should your company<br />

want to eliminate the preparation<br />

process for Inorganic standards<br />

contact our Technical Department<br />

for a quote on a Ready-to-<br />

Aspirate working level Inorganic<br />

standard.<br />

Originally designed for<br />

D-5622-95<br />

Technical Note<br />

AccuStandard’s Oxygenate<br />

reference fuel line was<br />

designed as a cost effective<br />

alternative for Petrochemical<br />

Laboratories. All oxygenate<br />

blends come with a certificate<br />

to maintain traceability links to<br />

NIST SRMs (when available).<br />

By packaging the standard in<br />

10 mL sealed ampules your<br />

laboratory will realize cost<br />

savings. The 10 mL size<br />

avoids having special<br />

packaging and hazardous<br />

material fees billed to your<br />

invoice.<br />

<strong>ASTM</strong>


Method 5623<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-5623 Sulfur Compounds in Light Petroleum Liquids by GC and<br />

Sulfur Selective Detection<br />

<strong>ASTM</strong>-P-0091-10X-SET $ 625 / set of 22 x 1 mL<br />

Approx. 2.0 mg/mL each in Toluene<br />

Custom Ampulling for Bulk Quantity Requirements<br />

• Flammables<br />

• QC Services available<br />

38<br />

Fill Volumes from 0.2 mL to 20 mL<br />

AccuStandard has the resources and equipment to meet your<br />

custom packaging requirements. Our full automated filler-sealer<br />

can accommodate a fill range from 0.2 to 20 mL, and ampule<br />

sizes from 1 mL to 20 mL.<br />

AccuStandard has extensive experience with Round Robin<br />

samples for <strong>ASTM</strong> committees.<br />

Call our Technical Department for a quotation.<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

This set of qualitative Sulfur <strong>Standards</strong> are formulated for research evaluation of the presence of the sulfur<br />

analytes or their breakdown products.<br />

Analyte Cat. No. Unit Price<br />

Hydrogen sulfide <strong>ASTM</strong>-P-0091-01-10X 1 x 1 mL $ 35<br />

Carbonyl sulfide (Carbon oxysulfide) <strong>ASTM</strong>-P-0091-02-10X 1 x 1 mL 35<br />

Methyl mercaptan (Methanethiol) <strong>ASTM</strong>-P-0091-03-10X 1 x 1 mL 35<br />

Ethyl mercaptan (Ethanethiol) <strong>ASTM</strong>-P-0091-04-10X 1 x 1 mL 35<br />

Methyl sulfide (Dimethyl sulfide) <strong>ASTM</strong>-P-0091-05-10X 1 x 1 mL 35<br />

Carbon disulfide <strong>ASTM</strong>-P-0091-06-10X 1 x 1 mL 35<br />

2-Propanethiol (Isopropyl mercaptan <strong>ASTM</strong>-P-0091-07-10X 1 x 1 mL 35<br />

2-Methyl-2-propanethiol (t-butyl mercaptan) <strong>ASTM</strong>-P-0091-08-10X 1 x 1 mL 35<br />

1-Propanethiol (Propyl mercaptan) <strong>ASTM</strong>-P-0091-09-10X 1 x 1 mL 35<br />

Ethyl methyl sulfide <strong>ASTM</strong>-P-0091-10-10X 1 x 1 mL 35<br />

1-Methyl-1-propanethiol (2-butanethiol) <strong>ASTM</strong>-P-0091-11-10X 1 x 1 mL 35<br />

Thiophene <strong>ASTM</strong>-P-0091-12-10X 1 x 1 mL 35<br />

2-Methyl-1-propanethiol (Isobutyl mercaptan) <strong>ASTM</strong>-P-0091-13-10X 1 x 1 mL 35<br />

Diethyl sulfide <strong>ASTM</strong>-P-0091-14-10X 1 x 1 mL 35<br />

1-Butanethiol (Butyl mercaptan) <strong>ASTM</strong>-P-0091-15-10X 1 x 1 mL 35<br />

Methyl disulfide (Dimethyl disulfide) <strong>ASTM</strong>-P-0091-16-10X 1 x 1 mL 35<br />

2-Methylthiophene <strong>ASTM</strong>-P-0091-17-10X 1 x 1 mL 35<br />

3-Methylthiophene <strong>ASTM</strong>-P-0091-18-10X 1 x 1 mL 35<br />

Diethyl disulfide (Ethyl disulfide) <strong>ASTM</strong>-P-0091-19-10X 1 x 1 mL 35<br />

3-Methylbenzo[b]thiophene <strong>ASTM</strong>-P-0091-20-10X 1 x 1 mL 35<br />

5-Methylbenzo[b]thiophene <strong>ASTM</strong>-P-0091-21-10X 1 x 1 mL 75<br />

Diphenyl sulfide <strong>ASTM</strong>-P-0091-22-10X 1 x 1 mL 35<br />

Originally designed for<br />

D-5623-94<br />

We can reduce your costs by using the Cozzoli Auto Filling/Sealing Machine to<br />

package just the right size product for your application.<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


<strong>ASTM</strong> D-5708 Nickel, Vanadium, & Iron in Crude Oils & Residual Fuels by ICP-AES<br />

Sulfur and Metals in Mineral Oil<br />

<strong>ASTM</strong>-P-0102-SET $ 1850 / 100 mL<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Sulfur Iron Nickel Vanadium<br />

Cat. No. Conc. Conc. Conc. Conc. Price<br />

(Wt. %) (µg/g) (µg/g) (µg/g) 100 mL<br />

<strong>ASTM</strong>-P-0102-01 0.00 0 0 0 $ 200<br />

<strong>ASTM</strong>-P-0102-02 0.50 300 10 500 200<br />

<strong>ASTM</strong>-P-0102-03 1.00 500 100 25 200<br />

<strong>ASTM</strong>-P-0102-04 - 100 80 250 200<br />

<strong>ASTM</strong>-P-0102-05 2.00 200 40 100 200<br />

<strong>ASTM</strong>-P-0102-06 2.50 400 5 400 200<br />

<strong>ASTM</strong>-P-0102-07 3.00 0 60 300 200<br />

<strong>ASTM</strong>-P-0102-08 3.50 500 0 200 200<br />

<strong>ASTM</strong>-P-0102-09 - 100 100 0 200<br />

<strong>ASTM</strong>-P-0102-10 4.50 300 50 250 200<br />

<strong>ASTM</strong>-P-0102-11 5.00 200 20 500 200<br />

<strong>ASTM</strong>-P-0102-12 5.50 50 100 50 200<br />

Sulfur and Metals in Residual Fuel Oil<br />

<strong>ASTM</strong>-P-0103-SET $ 2100 / 100 mL<br />

Sulfur Iron Nickel Vanadium<br />

Cat. No. Conc. Conc. Conc. Conc. Price<br />

(Wt. %) (µg/g) (µg/g) (µg/g) 100 mL<br />

<strong>ASTM</strong>-P-0103-01 0.00 0 0 0 $ 200<br />

<strong>ASTM</strong>-P-0103-02 0.50 300 10 500 200<br />

<strong>ASTM</strong>-P-0103-03 1.00 500 100 25 200<br />

<strong>ASTM</strong>-P-0103-04 - 100 80 250 200<br />

<strong>ASTM</strong>-P-0103-05 2.00 200 40 100 200<br />

<strong>ASTM</strong>-P-0103-06 2.50 400 5 400 200<br />

<strong>ASTM</strong>-P-0103-07 3.00 0 60 300 200<br />

<strong>ASTM</strong>-P-0103-08 3.50 500 0 200 200<br />

<strong>ASTM</strong>-P-0103-09 - 100 100 0 200<br />

<strong>ASTM</strong>-P-0103-10 4.50 300 50 250 200<br />

<strong>ASTM</strong>-P-0103-11 5.00 200 20 500 200<br />

<strong>ASTM</strong>-P-0103-12 5.50 50 100 50 200<br />

Iron<br />

Nickel<br />

Test Method A - ICP with an Organic Solvent Specimen Solution<br />

Vanadium<br />

Iron<br />

Nickel<br />

Iron<br />

Nickel<br />

Vanadium<br />

<strong>Standards</strong> of Interests<br />

See Table of Contents for<br />

the Wear Metals Group<br />

pages.<br />

Test Method B - ICP after Acid Decomposition of Sample<br />

Stock Multi-Element<br />

Aqueous Standard<br />

D-5708-B-10X-1 $ 60 / 100 mL<br />

D-5708-B-10X-5 $ 115 / 500 mL<br />

Each at 100 µg/mL in 2-5% HNO3 3 comps.<br />

Nitric Acid Blank<br />

CLP-BLN-5 $ 30 / 500 mL<br />

CLP-BLN-L $ 45 / L (2 x 500 mL)<br />

5% HNO 3 in <strong>ASTM</strong> Type I Water<br />

Member<br />

Stock Multi-Element in<br />

Mineral Oil<br />

D-5708-A-10X $ 150 / 4 oz.<br />

100 µg/g in 20 cSt mineral oil<br />

3 comps.<br />

Working Level Multi-Element<br />

Aqueous Standard<br />

D-5708-B-5 $ 105 / 500 mL<br />

Each at 10 µg/mL in 2-5% HNO3 3 comps.<br />

Vanadium<br />

AccuStandard is an active member in <strong>ASTM</strong> and<br />

strives to keep abreast of <strong>ASTM</strong> method revisions.<br />

If our listed formulation does not meet the most<br />

recent method revision, please contact Technical<br />

Support, ext. 117 for an updated product.<br />

Originally designed for<br />

D-5708-95a<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 39<br />

Method 5599<br />

Member<br />

For our complete line of<br />

Inorganic <strong>Standards</strong>,<br />

request a copy of our<br />

Inorganics Catalog<br />

<strong>ASTM</strong><br />

WEAR METALS


Method 5762<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-5762 Nitrogen in Petroleum & Petroleum Products by Boat-Inlet Chemiluminescence<br />

Stock Nitrogen Standard<br />

D-5762-95-500X-PAK $ 45 / 5 x 1 mL<br />

Nitrogen @ 500 µg/mL in Xylene (Acridine @ 6397 µg/mL)<br />

Nitrogen Calibration Set<br />

D-5762-95-CAL-SET $ 75 / 6 x 1 mL<br />

Cat. No. Description Unit<br />

D-5762-95-BL Xylene Blank 1 x 1 mL<br />

D-5762-95-1X Nitrogen @ 1.0 µg/mL in Xylene 1 x 1 mL<br />

D-5762-95-5X Nitrogen @ 5.0 µg/mL in Xylene 1 x 1 mL<br />

D-5762-95-10X Nitrogen @ 10 µg/mL in Xylene 1 x 1 mL<br />

D-5762-95-50X Nitrogen @ 50 µg/mL in Xylene 1 x 1 mL<br />

D-5762-95-100X Nitrogen @ 100 µg/mL in Xylene 1 x 1 mL<br />

Low level Nitrogen Calibration Set<br />

<strong>ASTM</strong>-P-0070-SET $ 75 / 6 x 1 mL<br />

Cat. No. Description Unit<br />

<strong>ASTM</strong>-P-0070-BL Isooctane Blank 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-1X Nitrogen @ 0.5 µg/g in Isooctane 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-2X Nitrogen @ 1.0 µg/g in Isooctane 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-4X Nitrogen @ 2.0 µg/g in Isooctane 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-10X Nitrogen @ 5.0 µg/g in Isooctane 1 x 1 mL<br />

<strong>ASTM</strong>-P-0070-20X Nitrogen @ 10.0 µg/g in Isooctane 1 x 1 mL<br />

AccuPetroCheck and AccuPetroTest Real World Gasoline QC <strong>Standards</strong><br />

In cooperation with <strong>ASTM</strong> D-02 subcommittee 3 and 4, AccuStandard ampulled 21 Real World gasoline reference fuels. Consensus Values have<br />

been determined for these reference fuels by various <strong>ASTM</strong> Round Robins to provide Petrochemical Laboratories with a source of well<br />

characterized gasoline standards for use in QA/QC applications and as Single Blind test samples over an extended period of time. As new <strong>ASTM</strong><br />

D-02.03 and D-02.04 Test methods are promulgated they require mandatory Quality Control testing of real world samples. AccuStandard’s<br />

AccuPetroTest & AccuPetroCheck standards are being successfully used to achieve these new Quality Control requirements.<br />

QC <strong>Standards</strong><br />

CARB Low Sulfur RFG QC<br />

Standard<br />

<strong>ASTM</strong>-FUEL-QCS-01-PAK $ 60 / 5 x 15 mL<br />

Parameter Method Value Conc.<br />

Total Aromatics D-1319 24.5 Vol.%<br />

Total Olefins D-1319 5.3 Vol.%<br />

Total Saturates D-1319 58.3 Vol.%<br />

Sulfur D-2622 0.0057 Wt.%<br />

Sulfur D-4294 0.0078 Wt.%<br />

Sulfur D-5453 55.76 µg/g<br />

Sulfur D-6344 59.31 µg/g<br />

Benzene D-5769 0.80 Vol.%<br />

Toluene D-5769 4.92 Vol.%<br />

Total Aromatics D-5769 23.42 Vol.%<br />

Benzene D-6227 0.78 Vol.%<br />

Total Olefins D-6550 5.3 Vol.%<br />

40<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Low level Nitrogen & Sulfur Calibration Set<br />

<strong>ASTM</strong>-P-0071-SET $ 50 / 4 x 1 mL<br />

Cat. No. Description Unit<br />

<strong>ASTM</strong>-P-0071-BL Benzene Blank 1 x 1 mL<br />

<strong>ASTM</strong>-P-0071-01 Nitrogen @ 0.25 µg/g & Sulfur @ 0.25 µg/g in Benzene 1 x 1 mL<br />

<strong>ASTM</strong>-P-0071-02 Nitrogen @ 0.50 µg/g & Sulfur @ 0.50 µg/g in Benzene 1 x 1 mL<br />

<strong>ASTM</strong>-P-0071-03 Nitrogen @ 1.00 µg/g & Sulfur @ 1.00 µg/g in Benzene 1 x 1 mL<br />

Conventional Gasoline QC<br />

Standard<br />

<strong>ASTM</strong>-FUEL-QCS-02-PAK $ 60 / 5 x 15 mL<br />

Technical Note<br />

Nitrogen introduced using<br />

Acridine.<br />

Technical Note<br />

Nitrogen introduced using<br />

Acridine.<br />

Parameter Method Value Conc.<br />

Total Aromatics D-1319 34.6 Vol.%<br />

Total Olefins D-1319 12.4 Vol.%<br />

Total Saturates D-1319 62.8 Vol.%<br />

Sulfur D-2622 0.0338 Wt.%<br />

Sulfur D-4294 0.0368 Wt.%<br />

Sulfur D-5453 317.36 µg/g<br />

Sulfur D-6344 338.78 µg/g<br />

Benzene D-5769 0.55 Vol.%<br />

Toluene D-5769 5.53 Vol.%<br />

Total Aromatics D-5769 32.51 Vol.%<br />

Benzene D-6227 0.52 Vol.%<br />

Total Olefins D-6550 12.4 Vol.%<br />

Technical Note<br />

The Nitrogen is<br />

introduced using<br />

Aniline and the Sulfur<br />

is introduced using<br />

n-Butyl sulfide.<br />

AccuPetroCheck QC <strong>Standards</strong><br />

Two of the fuels are available as AccuPetroCheck<br />

Consensus Value QC <strong>Standards</strong>. The<br />

AccuPetroCheck CARB and Conventional<br />

gasoline reference materials have all parameters<br />

listed on the certificate with the Consensus Values<br />

and the regression equations for reproducability.<br />

Use of these Reference Materials improve the<br />

quality of laboratory results. The Consensus<br />

Values listed reflect initial statistical treatment of<br />

the data at the time the catalog was published.<br />

The actual certificate provided with the<br />

AccuPetroCheck QC standard will have the<br />

accepted Consensus Value based on statistical<br />

treatment of the data.<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Originally designed for<br />

D-5762-98


AccuPetroTest<br />

Sulfur in Diesel Fuel QC Standard<br />

SBPT-SDF $ 25 / 2 x 15 mL<br />

Parameter Approx. Range<br />

Sulfur 20 - 11000 mg/kg<br />

See <strong>ASTM</strong> Methods D-2622, D-3120, D-3246-92,<br />

D-4294, D-5453, for Sulfur Calibration <strong>Standards</strong><br />

AccuPetroTest Gasoline<br />

Low Sulfur QC Sample<br />

SBPT-LSGAS $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Sulfur 5453 0 - 50 µg/g<br />

AccuPetroTest Gasoline QC<br />

Olefins QC Sample<br />

SBPT-OLEFIN $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Total Aromatics D-1319 8-60 Vol.%<br />

Total Olefins D-1319 1 - 40 Vol.%<br />

Total Saturates D-1319 30-80 Vol. %<br />

See <strong>ASTM</strong> Method D-1319 for Sulfur Calibration<br />

<strong>Standards</strong><br />

Aromatics QC Sample<br />

SBPT-AROM $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Total Aromatics D-5769 8 - 60 Vol.%<br />

See <strong>ASTM</strong> Methods D-3606, D-5580-95, D-5769-95<br />

for Benzene Calibration <strong>Standards</strong><br />

AccuPetroTest Gasoline<br />

Comprehensive Single Blind Gasoline QC<br />

Sample<br />

SBPT-COMP $ 50 / 2 x 15 mL<br />

Parameter Method Approx. Range Conc.<br />

Total Aromatics D-1319 8 - 60 Vol.%<br />

Total Olefins D-1319 1 - 40 Vol.%<br />

Total Saturates D-1319 30 - 80 Vol.%<br />

Sulfur D-2622 0.0001 - 0.0930 Wt.%<br />

Sulfur D-4294 0.0016 - 0.0930 Wt.%<br />

Sulfur D-5453 0.5 -500 µg/g<br />

Sulfur D-6344 1.0 - 1000 µg/g<br />

Benzene D-5769 0.1 - 2.0 Vol.%<br />

Toluene D-5769 1.0 - 15 Vol.%<br />

Total Aromatics D-5769 8 - 60 Vol.%<br />

Benzene D-6277 0.1 - 2.0 Vol.%<br />

Total Olefins D-6550 1 - 40 Vol.%<br />

Petrochemical <strong>Standards</strong><br />

Sulfur in White Mineral Oil QC<br />

Standard<br />

SBPT-SWMO $ 25 / 2 x 15 mL<br />

Parameter Approx. Range<br />

Sulfur 20 - 11000 mg/kg<br />

See <strong>ASTM</strong> Methods D-2622, D-3120,<br />

D-3246-92, D-4294, D-5453 for Sulfur<br />

Calibration <strong>Standards</strong><br />

Olefin QC Sample<br />

SBPT-OLEFINSFC $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Olefins 6550 1 - 40 Vol.%<br />

Sulfur QC Sample<br />

SBPT-SGAS $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Sulfur D-2622 0.0001 - 0.0930 Wt.%<br />

Sulfur D-4294 0.0016 - 0.0930 Wt.%<br />

Sulfur D-5453 4.0 - 500 µg/g<br />

Sulfur D-XXXX 1.0 - 1000 µg/g<br />

See <strong>ASTM</strong> Methods D-2622, D-3120, D-3246-92,<br />

D-4294, D-5453 for Sulfur Calibration <strong>Standards</strong><br />

Benzene/Toluene QC Sample<br />

SBPT-BENZ $ 25 / 2 x 15 mL<br />

Parameter Method Approx. Range<br />

Benzene D-5769 0.1 - 2.0 Vol.%<br />

Toluene D-5769 1.0 - 15 Vol.%<br />

See <strong>ASTM</strong> Methods D-3606, D-5580-95, D-5769-95<br />

for Benzene Calibration <strong>Standards</strong><br />

Technical Note<br />

Our new comprehensive single blind<br />

gasoline QC sample tests for more<br />

parameters from a single sample.<br />

The actual gasoline sample will<br />

have consensus values listed on the<br />

datasheet that fall within the range<br />

listed for each parameter.<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 41<br />

Member<br />

Sulfur Single Blind AccuPetroTest<br />

Alternative Matrices <strong>Standards</strong><br />

AccuStandard has manufactured a number of<br />

Diesel and White Mineral Oil quality control<br />

products containing a gravimetrically prepared<br />

amount of Sulfur. Use of these alternative<br />

matrix materials can provide further evaluation<br />

of the QA/QC process in the laboratory. Two<br />

samples will be sent for the test parameter and<br />

a separate sealed envelope containing the<br />

gravimetrically prepared sulfur values is also<br />

provided. The second sample is for<br />

repeatability testing or for use as a future<br />

QA/QC reference.<br />

AccuPetroTest Single Blind<br />

<strong>Standards</strong><br />

Petrochemical Laboratories looking to<br />

test the performance of the laboratory for<br />

a specific parameter can order the Single<br />

Blind AccuPetroTest sample for the<br />

parameter of interest. Two real world<br />

gasoline samples will be sent for the test<br />

parameter requested and a separate sealed<br />

envelope containing the determined<br />

Consensus Value is also provided. The<br />

second sample is for repeatability testing<br />

or as a future QA/QC reference.<br />

Test to<br />

Low ppb<br />

Sulfur<br />

See Pages 6-11<br />

Conducting a Petrochemical Round Robin for a new <strong>ASTM</strong> method?<br />

Select AccuStandard to prepare the necessary samples for the Round Robin<br />

study.<br />

<strong>ASTM</strong>


Method 5769<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> Method D-5769-98<br />

Benzene, Toluene, and Total Aromatics in Finished Gasoline by GC/MS<br />

<strong>ASTM</strong> D-5769 Benzene, Toluene & Total Aromatics in Finished Gasoline by GC/MS<br />

Features: Benefits:<br />

Purity and Identity of all analytes verified .......... Impurity interferences in analyte retention time<br />

under identical operating conditions window are compensated.<br />

Certified method specific calibration standards . Increased confidence in analytical results.<br />

Eliminates preparation of calibration standards ..Time is utilized quantifying actual samples.<br />

Internal <strong>Standards</strong> Incorporated .........................Saves time.<br />

Weights and weight percents provided .............. Ease of use in performing back calculations.<br />

Includes all necessary solutions .........................Complete single source for reference materials.<br />

Variations in packaging size .............................. Meet laboratory sample volumes and demands.<br />

Low Cost ............................................................ More economical to purchase than to prepare standards.<br />

Flexibility ............................................................ Meet your lab requirements/method changes.<br />

Only 5 standards needed for a 5 Point Curve ... Generate a full calibration curve in 1/2 the time of the<br />

two set version composed of 10 standards.<br />

No charge disk deliverable calibration curve .... Direct computer uploading eliminates the input of 135<br />

weights (CALAMTS) separate data points.<br />

42<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

All of your standards requirements for <strong>ASTM</strong> Method D-5769 have been put together in the<br />

following 10 pages. These standards and methods are used in the monitoring of Total<br />

Aromatics according to the latest methods and amendments to the US Clean Air Act.<br />

A set of Amendments, containing more stringent specifications became effective January 1,<br />

1995 limiting the volatility and composition of reformulated gasoline.<br />

The D-02 Committee of the American Society of Testing Materials, developed a standard test<br />

method D-5769 for the determination of the analyte composition by GC/MS of reformulated<br />

gasoline.<br />

Aromatic Product Line yields the following important benefits<br />

Originally designed for<br />

D-5769-98<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


<strong>ASTM</strong> <strong>Standards</strong><br />

<strong>ASTM</strong> D-5769 Benzene, Toluene & Total Aromatics in Finished Gasoline by GC/MS<br />

<strong>Standards</strong> Designed for <strong>ASTM</strong> D-5769 as published in the 1997 Annual Book of <strong>ASTM</strong> <strong>Standards</strong>,<br />

Vol. 05.03 Petroleum Products and Lubricants (III): D-4636-latest; Catalysts<br />

The following M-GRA catalog numbers contain the necessary calibration curves, daily quality control, and<br />

internal standards designed to meet the promulgated GC/MS Aromatic method listed in the 1997 <strong>ASTM</strong><br />

Book of <strong>Standards</strong>.<br />

AccuStandard offers two different versions of the M-GRA catalog numbers: M-GRA three component<br />

internal standard version, and the M-GRA four component internal standard version.<br />

The three component internal standard version contains the necessary deuterated analytes for full<br />

qualitative and quantitative analysis of the 25 components listed in the published version.<br />

The four component internal standard version was designed at the request of the petroleum refinery<br />

laboratories. This four internal standard version incorporates not only the Benzene-d 6, Ethyl benzene-d 10,<br />

Naphthalene-d 8, but also Toluene-d 8. Incorporating the Toluene-d 8 as the internal standard for the<br />

quantification of gasolines with higher Toluene levels has improved analytical results for this analyte.<br />

Incorporation of a 6th Calibration Standard<br />

A6th calibration standard has been formulated for the M-GRA product line to improve the linearity at the<br />

high end of the calibration curve see page 44. This sixth standard can be especially important in the<br />

quantification of gasoline samples containing high toluene levels. The formulation contains an analyte<br />

concentration between the high level standard and the next level, which is standard two. Use of the sixth<br />

standard provides an additional calibration point that is desirable when the calibration curve is developed<br />

using a quadratic fit.<br />

M-GRA-K1 $ 600<br />

(Original Formulations)<br />

Kit includes: Units Function<br />

M-GRA-CAL/IS-SET 5 x 1 mL 5 Pt. Curve w/ 3 ISTD's<br />

M-GRA-QC/IS-5ML 1 x 5 mL Daily QC w/ 3 ISTD's<br />

M-GRA-IS-5ML 1 x 5 mL Internal Std. 3 comps.<br />

M-GRA-ST 1 x 1 mL Sensitivity Test Solution<br />

See page 44 for product description with<br />

analytes & conc.<br />

M-GRA-K2 $ 700<br />

(Developed for improved high concentration linearity)<br />

Kit includes: Units Function<br />

M-GRA-CAL/IS-SET 5 x 1 mL 5 Pt. Curve w/ 3 ISTD's<br />

M-GRA-ADD/IS 1 x 1 mL 6th Std. for revison 5 F<br />

M-GRA-QC/IS-5ML 1 x 5 mL Daily QC w/ 3 ISTD's<br />

M-GRA-IS-5ML 1 x 5 mL Internal Std. 3 comps.<br />

M-GRA-ST 1 x 1 mL Sensitivity Test Solution<br />

See page 44 for product description with<br />

analytes & conc.<br />

Aromatics Kits for analysis by GC/MS<br />

For your added convenience we have<br />

provided the following Aromatics Kits<br />

to meet the analytical requirements for<br />

this method.<br />

M-GRA-K4 $ 850<br />

(Used to meet the Toluene-d 8 internal standard version<br />

recommended by a network of major petroleum refineries)<br />

Kit includes: Units Function<br />

M-GRA-CAL-R/IS-R-SET 5 x 1 mL 5 Pt. Curve w/ 4 ISTD's<br />

M-GRA-ADD/IS-R 1 x 1 mL 6th Standard for rev. 5 F<br />

M-GRA-QC-R/IS-R-5ML 1 x 5 mL Daily QC w/ 4 ISTD's<br />

M-GRA-IS-R-10ML 1 x 10 mL Internal Std. 4 comps.<br />

M-GRA-ST 1 x 1 mL Sensitivity Test Solution<br />

See page 45 for product description with<br />

analytes & conc.<br />

Cross Reference Table<br />

<strong>ASTM</strong> IP ISO DIN JIS AFNOR sorted by<br />

<strong>ASTM</strong> Method see beginning of Catalog<br />

Originally designed for<br />

D-5769-95<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 43<br />

Method 5769<br />

Member<br />

<strong>ASTM</strong>


Method 5769<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-5769 Calibration Curve with 3 Component Deuterated Internal Standard Added<br />

Aromatics Calibration <strong>Standards</strong> Kit<br />

(3 Internal Standard Version)<br />

M-GRA-CAL/IS-SET $ 375 / set of 5 x 1 mL<br />

Core Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

24 Comps. Target Vol. % Vol. % Vol. % Vol. % Vol. %<br />

Benzene 3 1.50 0.75 0.375 0.1875<br />

Toluene 19 9.50 4.75 2.375 1.1875<br />

Ethylbenzene 5 2.50 1.25 0.625 0.3125<br />

m-Xylene 6 3.00 1.50 0.750 0.3750<br />

p-Xylene 6 3.00 1.50 0.750 0.3750<br />

o-Xylene 6 3.00 1.50 0.750 0.3750<br />

Isopropylbenzene 3 1.50 0.75 0.375 0.1875<br />

n-Propylbenzene 3 1.50 0.75 0.375 0.1875<br />

1-Methyl-3-ethylbenzene 3 1.50 0.75 0.375 0.1875<br />

1-Methyl-4-ethylbenzene 3 1.50 0.75 0.375 0.1875<br />

1,3,5-Trimethylbenzene 3 1.50 0.75 0.375 0.1875<br />

1-Methyl-2-ethylbenzene 3 1.50 0.75 0.375 0.1875<br />

1,2,4-Trimethylbenzene 5 2.50 1.25 0.625 0.3125<br />

1,2,3-Trimethylbenzene 3 1.50 0.75 0.375 0.1875<br />

Indan 3 1.50 0.75 0.375 0.1875<br />

1,4-Diethylbenzene 3 1.50 0.75 0.375 0.1875<br />

n-Butylbenzene 3 1.50 0.75 0.375 0.1875<br />

1,2-Diethylbenzene 3 1.50 0.75 0.375 0.1875<br />

1,2,4,5-Tetramethylbenzene 2 1.00 0.50 0.250 0.1250<br />

1,2,3,5-Tetramethylbenzene 2 1.00 0.50 0.250 0.1250<br />

Naphthalene 2 1.00 0.50 0.250 0.1250<br />

Pentamethylbenzene 2 1.00 0.50 0.250 0.1250<br />

1-Methylnaphthalene 2 1.00 0.50 0.250 0.1250<br />

2-Methylnaphthalene 2 1.00 0.50 0.250 0.1250<br />

Isooctane -- Bal Bal Bal Bal<br />

Internal Standard (M-GRA-IS)<br />

Benzene-d 6 2 2 2 2 2<br />

Ethylbenzene-d 10 2 2 2 2 2<br />

Naphthalene-d 8 1 1 1 1 1<br />

Daily Quality Control Standard<br />

(without Internal Standard)<br />

M-GRA-QC-10ML $ 125 / 1 x 10 mL<br />

M-GRA-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

44<br />

Wt.<br />

Compound Ratio<br />

Toluene 9<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 3<br />

13 Comp. Core Mix 100<br />

Technical Note<br />

Use with any M-GRA Calibration Curve.<br />

<strong>ASTM</strong>/EPA Sensitivity Test Solution<br />

M-GRA-ST $ 10 / 1 x 1 mL<br />

M-GRA-ST-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

100 µg/mL in Isooctane<br />

1,4-Diethyl benzene<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Daily Quality Control Standard<br />

(with Internal Standard)<br />

M-GRA-QC/IS-5ML $ 100 / 1 x 5 mL<br />

M-GRA-QC/IS-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

3 Comp. Deuterated Internal Std. Mix<br />

M-GRA-IS-5ML $ 150 / 1 x 5 mL<br />

M-GRA-IS-5ML-PAK SAVE 20% $ 600 / 5 x 5 mL<br />

3 comps.<br />

Compound Mix Ratio Compound Mix Ratio<br />

Benzene-d6 2 mL<br />

2 mL<br />

Naphthalene-d8 1 gm<br />

Ethylbenzene-d 10<br />

Optional Sixth Standard<br />

with 3 Comp. Deuterated<br />

Internal Standard Added<br />

M-GRA-ADD/IS $ 100 / 1 x 1 mL<br />

Core Calibr. Mix Optional Std. 6<br />

24 Comps. Target Vol. %<br />

Benzene 2.25<br />

Toluene 15<br />

Ethylbenzene 3.75<br />

m-Xylene 4.50<br />

p-Xylene 4.50<br />

o-Xylene 4.50<br />

Isopropylbenzene 2.25<br />

n-Proplylbenzene 2.25<br />

3-Ethyltoluene 2.25<br />

4-Ethyltoluene 2.25<br />

1,3,5-Trimethylbenzene 2.25<br />

2-Ethyltoluene 2.25<br />

1,2,4-Trimethylbenzene 3.75<br />

1,2,3-Trimethylbenzene 2.25<br />

Indan 2.25<br />

1,4-Diethylbenzene 2.25<br />

n-Butylbenzene 2.25<br />

1,2-Diethylbenzene 2.25<br />

1,2,4,5-Tetramethylbenzene 4.0<br />

1,2,3,5-Tetramethylbenzene 1.5<br />

Naphthalene 1.5<br />

Pentamethylbenzene 1.5<br />

1-Methylnaphthalene 1.5<br />

2-Methylnaphthalene 1.5<br />

Isooctane Bal<br />

Internal Standard (M-GRA-IS)<br />

Benzene-d6 Ethylbenzene-d10 Naphthalene-d8 Wt.<br />

Compound Ratio<br />

Toluene 9<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 3<br />

13 Comp. Core Mix 100<br />

Includes M-GRA-IS (3 Comp. Internal <strong>Standards</strong> mix)<br />

combined with the above 13 Comp. Core QC Mix:<br />

M-GRA-QC in a 5 to 100 weight ratio. 16 comps.<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

2<br />

2<br />

1<br />

Originally designed for<br />

D-5769-95<br />

Disk Deliverable<br />

(At no additional charge)<br />

Eliminates hand keyed-in<br />

data.<br />

CALAMTS<br />

(Disk containing “Calibration<br />

Amounts”)<br />

Each analyte in each<br />

standard is individually<br />

weighed. Actual weights<br />

and weight percents are<br />

provided.


<strong>ASTM</strong> <strong>Standards</strong><br />

<strong>ASTM</strong> D-5769 Calibration Curve with 4 Component Deuterated Internal Standard Added<br />

Aromatics Calibration <strong>Standards</strong> Kit<br />

(4 Internal Standard Version)<br />

M-GRA-CAL-R/IS-R-SET $ 425 / set of 5 x 1 mL<br />

Core Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

24 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Benzene 3.13 1.78 0.95 0.490 0.2490<br />

Toluene 19.65 11.11 5.90 3.058 1.5547<br />

Ethylbenzene 5.12 2.92 1.55 0.805 0.4090<br />

m-Xylene 6.27 3.50 1.86 0.962 0.4891<br />

p-Xylene 6.33 3.50 1.86 0.962 0.4891<br />

o-Xylene 6.51 3.56 1.89 0.980 0.4981<br />

Isopropylbenzene 3.06 1.74 0.93 0.480 0.2439<br />

n-Propylbenzene 3.04 1.74 0.93 0.480 0.2440<br />

3-Ethyltoluene 3.08 1.75 0.93 0.481 0.2446<br />

4-Ethyltoluene 3.05 1.74 0.93 0.479 0.2437<br />

1,3,5-Trimethylbenzene 3.07 1.75 0.93 0.481 0.2448<br />

2-Ethyltoluene 3.14 1.78 0.95 0.490 0.2492<br />

1,2,4-Trimethylbenzene 5.18 2.95 1.57 0.812 0.4130<br />

1,2,3-Trimethylbenzene 3.19 1.81 0.96 0.498 0.2530<br />

Indan 3.46 1.95 1.04 0.536 0.2726<br />

1,4-Diethylbenzene 3.04 1.74 0.93 0.480 0.2439<br />

n-Butylbenzene 3.05 1.74 0.92 0.479 0.2434<br />

1,2-Diethylbenzene 3.22 1.78 0.95 0.490 0.2489<br />

1,2,4,5-Tetramethylbenzene 2.10 1.20 0.64 0.329 0.1674<br />

1,2,3,5-Tetramethylbenzene 2.09 1.20 0.64 0.330 0.1679<br />

Naphthalene 2.35 1.34 0.71 0.369 0.1877<br />

Pentamethylbenzene 2.16 1.23 0.66 0.340 0.1727<br />

1-Methylnaphthalene 2.32 1.34 0.71 0.369 0.1877<br />

2-Methylnaphthalene 2.41 1.37 0.73 0.378 0.1922<br />

Isooctane ----- 43.47 69.96 84.441 92.0905<br />

Internal Standard<br />

(M-GRA-IS-R) Mix Ratio<br />

Benzene-d 6 (2 mL) 16.57 16.57 16.57 16.57 16.57<br />

Ethylbenzene-d 10 (2 mL) 16.76 16.76 16.76 16.76 16.76<br />

Naphthalene-d 8 (1 gm) 8.78 8.78 8.78 8.78 8.78<br />

Toluene-d 8 (7 mL) 57.88 57.88 57.88 57.88 57.88<br />

The 4 component internal standard mix (M-GRA-IS-R) is combined with the 25 component core calibration<br />

curve mixtures in a 12 to 100 weight ratio to formulate a complete calibration solution containing 29 comps.<br />

Daily Quality Control Standard<br />

(without Internal Standard)<br />

M-GRA-QC-10ML $ 125 / 1 x 10 mL<br />

M-GRA-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Compound Mix Ratio<br />

Benzene-d6 2 mL<br />

2 mL<br />

Ethylbenzene-d 10<br />

Wt.<br />

Compound Ratio<br />

Toluene 9<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 3<br />

13 Comp. Core Mix 100<br />

4 Comp. Deuterated Internal Std. Mix<br />

M-GRA-IS-R-10ML $ 225 / 1 x 10 mL<br />

M-GRA-IS-R-10ML-PAK SAVE 20% $ 900 / 5 x 10 mL<br />

4 comps.<br />

Technical Note<br />

Compound Mix Ratio<br />

Naphthalene-d8 1 gm<br />

7 mL<br />

Toluene-d 8<br />

Use with any M-GRA Calibration Curve.<br />

Daily Quality Control Standard<br />

(with Internal Standard M-GRA-IS-R)<br />

M-GRA-QC/IS-R-5ML $ 125 / 1 x 5 mL<br />

M-GRA-QC/IS-R-5ML-PAKSAVE 20% $ 500 / 5 x 5mL<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Wt.<br />

Compound Ratio<br />

Toluene 9<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 3<br />

13 Comp. Core Mix 100<br />

Includes M-GRA-IS-R (4 Comp. Internal <strong>Standards</strong><br />

Mix) combined with the above 13 Comp. Core QC Mix:<br />

M-GRA-QC in a 12 to 100 weight ratio. 17 comps.<br />

<strong>ASTM</strong>/EPA Sensitivity Test Solution<br />

M-GRA-ST $ 10 / 1 x 1 mL<br />

M-GRA-ST-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

100 µg/mL in Isooctane<br />

1,4-Diethyl benzene<br />

Optional Sixth Standard<br />

with 4 Comp. Deuterated<br />

Internal Standard Added<br />

M-GRA-ADD/IS-R $ 100 / 1 x 1 mL<br />

Core Calibr. Mix Optional Std. 6<br />

24 Comps. Target Wt. %<br />

Benzene 2.48<br />

Toluene 16.29<br />

Ethylbenzene 4.07<br />

m-Xylene 4.87<br />

p-Xylene 4.87<br />

o-Xylene 4.96<br />

Isopropylbenzene 2.43<br />

n-Propylbenzene 2.43<br />

3-Ethyltoluene 2.44<br />

4-Ethyltoluene 2.43<br />

1,3,5-Trimethylbenzene 2.44<br />

2-Ethyltoluene 2.48<br />

1,2,4-Trimethylbenzene 4.11<br />

1,2,3-Trimethylbenzene 2.52<br />

Indan 2.71<br />

1,4-Diethylbenzene 2.43<br />

n-Butylbenzene 2.42<br />

1,2-Diethylbenzene 2.48<br />

1,2,4,5-Tetramethylbenzene 4.44<br />

1,2,3,5-Tetramethylbenzene 1.67<br />

Naphthalene 1.87<br />

Pentamethylbenzene 1.72<br />

1-Methylnaphthalene 1.87<br />

2-Methylnaphthalene 1.91<br />

Isooctane 17.67<br />

Internal Standard<br />

(M-GRA-IS-R) Mix Ratio<br />

Benzene-d 6 (2 mL) 16.57<br />

Ethylbenzene-d 10 (2 mL) 16.76<br />

Naphthalene-d 8 (1 mL) 8.78<br />

Toluene-d 8 (7 mL) 57.88<br />

Originally designed for<br />

D-5769-95<br />

Technical Note<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 45<br />

Member<br />

This set of calibration solutions<br />

was formulated to improve<br />

quantification for Toluene by<br />

using Toluene-d 8 as an<br />

additional Internal Standard.<br />

<strong>Standards</strong> of Interest<br />

For the mandatory real world<br />

QC samples stipulated in the<br />

Method, see pages 1-2<br />

Method 5769<br />

<strong>ASTM</strong>


Method 5769<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-5769 Version with No Internal Standard<br />

Calibration Curve with No Internal Std. Added<br />

D-5769-CAL-SET-5ML $ 1500 / Set of 5 x 5 mL<br />

D-5769-CAL-SET-10ML $ 2750 / Set of 5 x 10 mL<br />

Core Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

23 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Benzene 5.25 2.95 1.575 0.8144 0.4143<br />

Toluene 19.67 11.06 5.898 3.0505 1.5519<br />

Ethylbenzene 5.18 2.91 1.552 0.8026 0.4083<br />

m-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />

p-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />

o-Xylene 6.30 3.54 1.890 0.9776 0.4973<br />

Isopropylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />

n-Propylbenzene 3.09 1.74 0.926 0.4787 0.2435<br />

3-Ethyltoluene 3.10 1.74 0.928 0.4801 0.2442<br />

4-Ethyltoluene 3.08 1.73 0.925 0.4782 0.2433<br />

1,3,5-Trimethylbenzene 3.10 1.74 0.929 0.4804 0.2444<br />

2-Ethyltoluene 3.15 1.77 0.945 0.4890 0.2488<br />

1,2,4-Trimethylbenzene 5.23 2.94 1.567 0.8104 0.4123<br />

1,2,3-Trimethylbenzene 3.20 1.80 0.960 0.4965 0.2526<br />

Indan 3.45 1.94 1.034 0.5350 0.2722<br />

1,4-Diethylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />

n-Butylbenzene 3.08 1.73 0.923 0.4776 0.2430<br />

1,2-Diethylbenzene 3.15 1.77 0.945 0.4885 0.2485<br />

1,2,4,5-Tetramethylbenzene 2.12 1.19 0.635 0.3284 0.1671<br />

1,2,3,5-Tetramethylbenzene 2.12 1.19 0.637 0.3295 0.1676<br />

Naphthalene 2.37 1.34 0.712 0.3683 0.1874<br />

1-Methylnaphthalene 2.37 1.34 0.712 0.3683 0.1874<br />

2-Methylnaphthalene 2.43 1.37 0.730 0.3773 0.1919<br />

Isooctane ----- 43.77 70.015 84.4922 92.1105<br />

4 Comp. Deuterated Internal Std. Mix<br />

M-GRA-IS-R-10ML $ 225 / 1 x 10 mL<br />

M-GRA-IS-R-10ML-PAK SAVE 20% $ 900 / 5 x 10 mL<br />

4 comps.<br />

Mix<br />

Mix<br />

Compound Ratio Compound Ratio<br />

Benzene-d6 2 mL Naphthalene-d8 1 gm<br />

Ethylbenzene-d10 2 mL<br />

7 mL<br />

Naphthalene-d 8<br />

46<br />

Toluene-d 8<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

The following D-5769 and M-GRA <strong>Standards</strong> were formulated to address proposed and promulgated<br />

changes to <strong>ASTM</strong> Method D-5769-98 Aromatics by GC/MS. Many of these changes were evaluated and/<br />

or adopted due to the results generated from the 1997 Round Robin, which used a select group of 21<br />

gasolines ampulized by AccuStandard.<br />

AccuStandard is committed to staying abreast of <strong>ASTM</strong> committee D-02 method developments. We ask<br />

that you contact us when your analytical group finds a beneficial procedure or modification.<br />

Modifications<br />

A Sixth Standard was added to meet the latest D-5769 method requirements and provide improved<br />

linearity at the high end of the Calibration curve<br />

The Calibration Curve was packaged in two convenient sizes without the internal standard. This<br />

packaging scheme allows for the addition of any ISTD formulation or oxygenate components.<br />

The Quality Control Standard was reformulated in the latest D-5769 revision. The formulation<br />

changes include reducing the 1,2,4,5-Tetramethylbenzene weight ratio and adding Naphthalene.<br />

The Benzene Target Weight % has been increased to meet the latest D-5769 method requirements.<br />

Pentamethylbenzene has now been removed from the analyte list.<br />

3 Comp. Deuterated Internal Std. Mix<br />

M-GRA-IS-5ML $ 150 / 1 x 5 mL<br />

M-GRA-IS-5ML-PAK SAVE 20% $ 600 / 5 x 5 mL<br />

3 comps.<br />

Compound Mix Ratio<br />

Benzene-d6 2 mL<br />

Ethylbenzene-d10 2 mL<br />

1 gm<br />

Daily Quality Control Standard<br />

(without Internal Standard)<br />

D-5769-QC-10ML $ 125 / 1 x 10 mL<br />

D-5769-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Optional Sixth Standard<br />

D-5769-ADD-5ML $ 150 / 1 x 5 mL<br />

D-5769-ADD-10ML $ 300 / 1 x 10 mL<br />

Core Calibration Mix Target<br />

23 Comps. Wt. %<br />

Benzene 4.16<br />

Toluene 16.41<br />

Ethylbenzene 4.10<br />

m-Xylene 4.91<br />

p-Xylene 4.91<br />

o-Xylene 5.00<br />

Isopropylbenzene 2.45<br />

n-Propylbenzene 2.45<br />

3-Ethyltoluene 2.45<br />

4-Ethyltoluene 2.44<br />

1,3,5-Trimethylbenzene 2.46<br />

2-Ethyltoluene 2.50<br />

1,2,4-Trimethylbenzene 4.14<br />

1,2,3-Trimethylbenzene 2.54<br />

Indan 2.73<br />

1,4-Diethylbenzene 2.45<br />

n-Butylbenzene 2.44<br />

1,2-Diethylbenzene 2.50<br />

1,2,4,5-Tetramethylbenzene 1.68<br />

1,2,3,5-Tetramethylbenzene 1.68<br />

Naphthalene 1.88<br />

1-Methylnaphthalene 1.88<br />

2-Methylnaphthalene 1.93<br />

Isooctane 19.92<br />

Wt.<br />

Compound Ratio<br />

Toluene 9<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 2<br />

Naphthalene 1<br />

14 Comp. Core Mix 100<br />

Originally designed for<br />

D-5769-98<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Disk Deliverable<br />

(At no additional charge)<br />

Eliminates hand keyed-in<br />

data.<br />

CALAMTS ®<br />

(Disk containing “Calibration<br />

Amounts”)<br />

Each analyte in each<br />

standard is individually<br />

weighed. Actual weights<br />

and weight percents are<br />

provided.


<strong>ASTM</strong> D-5769 Version with 3 Internal <strong>Standards</strong><br />

Core Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

24 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Compound<br />

17 comps.<br />

Wt.<br />

Ratio<br />

Toluene 9<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 2<br />

Naphthalene 1<br />

Includes M-GRA-IS (3 component mix)<br />

added in 5 to 100 weight ratio<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Benzene 5.25 2.95 1.575 0.8144 0.4143<br />

Toluene 19.67 11.06 5.898 3.0505 1.5519<br />

Ethylbenzene 5.18 2.91 1.552 0.8026 0.4083<br />

m-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />

p-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />

o-Xylene 6.30 3.54 1.890 0.9776 0.4973<br />

Isopropylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />

n-Propylbenzene 3.09 1.74 0.926 0.4787 0.2435<br />

3-Ethyltoluene 3.10 1.74 0.928 0.4801 0.2442<br />

4-Ethyltoluene 3.08 1.73 0.925 0.4782 0.2433<br />

1,3,5-Trimethylbenzene 3.10 1.74 0.929 0.4804 0.2444<br />

2-Ethyltoluene 3.15 1.77 0.945 0.4890 0.2488<br />

1,2,4-Trimethylbenzene 5.23 2.94 1.567 0.8104 0.4123<br />

1,2,3-Trimethylbenzene 3.20 1.80 0.960 0.4965 0.2526<br />

Indan 3.45 1.94 1.034 0.5350 0.2722<br />

1,4-Diethylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />

n-Butylbenzene 3.08 1.73 0.923 0.4776 0.2430<br />

1,2-Diethylbenzene 3.15 1.77 0.945 0.4885 0.2485<br />

1,2,4,5-Tetramethylbenzene 2.12 1.19 0.635 0.3284 0.1671<br />

1,2,3,5-Tetramethylbenzene 2.12 1.19 0.637 0.3295 0.1676<br />

Naphthalene 2.37 1.34 0.712 0.3683 0.1874<br />

1-Methylnaphthalene 2.37 1.34 0.712 0.3683 0.1874<br />

2-Methylnaphthalene 2.43 1.37 0.730 0.3773 0.1919<br />

Isooctane ----- 43.77 70.015 84.4922 92.1105<br />

Internal Standard<br />

M-GRA-IS<br />

Compound Mix ratio<br />

Benzene-d6 2 mL<br />

Ethylbenzene-d10 2 mL<br />

1 gm<br />

Naphthalene-d 8<br />

Daily Quality Control Standard<br />

(with Internal Standard)<br />

D-5769-QC/IS-5ML $ 100 / 1 x 5 mL<br />

D-5769-QC/IS-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL<br />

100<br />

Resolution Standard<br />

M-GRA-RES $ 30 / 1 x 1 mL<br />

M-GRA-RES-PAK $ 120 / 5 x 1 mL<br />

Wt. % 3 comps.<br />

1,3,5-Trimethylbenzene 3.0<br />

1-Methyl-2-ethylbenzene 3.0<br />

Isooctane 94<br />

Naphthalene-d 8<br />

Core Calibration Mix Target<br />

24 Comps. Wt. %<br />

Benzene 4.16<br />

Toluene 16.41<br />

Ethylbenzene 4.10<br />

m-Xylene 4.91<br />

p-Xylene 4.91<br />

o-Xylene 5.00<br />

Isopropylbenzene 2.45<br />

n-Propylbenzene 2.45<br />

3-Ethyltoluene 2.45<br />

4-Ethyltoluene 2.44<br />

1,3,5-Trimethylbenzene 2.46<br />

2-Ethyltoluene 2.50<br />

1,2,4-Trimethylbenzene 4.14<br />

1,2,3-Trimethylbenzene 2.54<br />

Indan 2.73<br />

1,4-Diethylbenzene 2.45<br />

n-Butylbenzene 2.44<br />

1,2-Diethylbenzene 2.50<br />

1,2,4,5-Tetramethylbenzene 1.68<br />

1,2,3,5-Tetramethylbenzene 1.68<br />

Naphthalene 1.88<br />

1-Methylnaphthalene 1.88<br />

2-Methylnaphthalene 1.93<br />

Isooctane 19.92<br />

The 3 Comp. Internal Standard Mix (M-GRA-IS) is<br />

combined with the 24 Comp. Core Calibration Curve Mixes<br />

above in a 5 to 100 weight ratio to formulate these<br />

27 Comp. calibration solutions.<br />

3 Comp. Deuterated Internal Std. Mix<br />

M-GRA-IS-5ML $ 150 / 1 x 5 mL<br />

M-GRA-IS-5ML-PAK SAVE 20% $ 600 / 5 x 5 mL<br />

3 comps.<br />

Compound Mix Ratio<br />

Benzene-d6 2 mL<br />

Ethylbenzene-d10 2 mL<br />

1 gm<br />

Sensitivity Test Solution<br />

M-GRA-ST $ 10 / 1 x 1 mL<br />

M-GRA-ST-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

100 µg/mL in Isooctane<br />

1,4-Diethyl benzene<br />

Fragmentation Pattern Standard<br />

M-GRA-FP $ 20 / 1 x 1 mL<br />

M-GRA-FP-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

3.0% w/w in Isooctane<br />

1,2,3-Trimethylbenzene<br />

Mass Scan Range Standard<br />

M-GRA-MSR $ 20 / 1 x 1 mL<br />

M-GRA-MSR-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

3.0% w/w in Isooctane<br />

Toluene<br />

Originally designed for<br />

D-5769-98<br />

Calibration Curve with a 3 Comp.<br />

Optional Sixth Standard<br />

Deuterated<br />

with a 3 Comp. Deuterated<br />

Internal Standard added<br />

Internal Standard added<br />

D-5769-CAL/IS-SET $ 375 / 5 x 1 mL D-5769-ADD/IS $ 100 / 1 x 1 mL<br />

Test to<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 47<br />

Method 5769<br />

Member<br />

Low ppb<br />

Sulfur<br />

See Pages 6-11<br />

<strong>ASTM</strong>


Method 5769<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-5769 4 Internal Standard Version (includes Toluene-d 8)<br />

Calibration Curve with a 4 Comp. Deuterated<br />

Internal Standard added<br />

D-5769-CAL/IS-R-SET $ 425 / 5 x 1 mL<br />

Core Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

24 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %<br />

Benzene 5.25 2.95 1.575 0.8144 0.4143<br />

Toluene 19.67 11.06 5.898 3.0505 1.5519<br />

Ethylbenzene 5.18 2.91 1.552 0.8026 0.4083<br />

m-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />

p-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />

o-Xylene 6.30 3.54 1.890 0.9776 0.4973<br />

Isopropylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />

n-Propylbenzene 3.09 1.74 0.926 0.4787 0.2435<br />

3-Ethyltoluene 3.10 1.74 0.928 0.4801 0.2442<br />

4-Ethyltoluene 3.08 1.73 0.925 0.4782 0.2433<br />

1,3,5-Trimethylbenzene 3.10 1.74 0.929 0.4804 0.2444<br />

2-Ethyltoluene 3.15 1.77 0.945 0.4890 0.2488<br />

1,2,4-Trimethylbenzene 5.23 2.94 1.567 0.8104 0.4123<br />

1,2,3-Trimethylbenzene 3.20 1.80 0.960 0.4965 0.2526<br />

Indan 3.45 1.94 1.034 0.5350 0.2722<br />

1,4-Diethylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />

n-Butylbenzene 3.08 1.73 0.923 0.4776 0.2430<br />

1,2-Diethylbenzene 3.15 1.77 0.945 0.4885 0.2485<br />

1,2,4,5-Tetramethylbenzene 2.12 1.19 0.635 0.3284 0.1671<br />

1,2,3,5-Tetramethylbenzene 2.12 1.19 0.637 0.3295 0.1676<br />

Naphthalene 2.37 1.34 0.712 0.3683 0.1874<br />

1-Methylnaphthalene 2.37 1.34 0.712 0.3683 0.1874<br />

2-Methylnaphthalene 2.43 1.37 0.730 0.3773 0.1919<br />

Isooctane ----- 43.77 70.015 84.4922 92.1105<br />

Internal Standard<br />

M-GRA-IS-R<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Compound Mix Ratio<br />

Benzene-d6 2 mL<br />

2 mL<br />

Ethylbenzene-d 10<br />

48<br />

Compound Mix ratio<br />

Benzene-d6 2 mL<br />

Ethylbenzene-d10 2 mL<br />

Naphthalene-d8 1 gm<br />

7 mL<br />

Toluene-d 8<br />

Daily Quality Control Standard<br />

(with Internal Standard)<br />

D-5769-QC/IS-R-5ML $ 100 / 1 x 5 mL<br />

D-5769-QC/IS-R-5ML-PAK SAVE 20% $ 400/5 x 5 mL<br />

18 comps.<br />

Wt.<br />

Compound Ratio<br />

Toluene 9<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 2<br />

Naphthalene 1<br />

Includes M-GRA-IS-R (4 component mix)<br />

added in 12 to 100 weight ratio<br />

Compound Mix Ratio<br />

Naphthalene-d8 1 gm<br />

7 mL<br />

Toluene-d 8<br />

100<br />

4 Comp. Deuterated Internal Std. Mix<br />

M-GRA-IS-R-10ML $ 225 / 1 x 10 mL<br />

M-GRA-IS-R-10ML-PAK SAVE 20% $ 900/ 5 x 10 mL<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Optional Sixth Standard<br />

with a 4 Comp. Deuterated<br />

Internal Standard added<br />

D-5769-ADD/IS-R $ 100 / 1 x 1 mL<br />

Core Calibration Mix Target<br />

24 Comp. Wt. %<br />

Benzene 4.16<br />

Toluene 16.41<br />

Ethylbenzene 4.10<br />

m-Xylene 4.91<br />

p-Xylene 4.91<br />

o-Xylene 5.00<br />

Isopropylbenzene 2.45<br />

n-Propylbenzene 2.45<br />

3-Ethyltoluene 2.45<br />

4-Ethyltoluene 2.44<br />

1,3,5-Trimethylbenzene 2.46<br />

2-Ethyltoluene 2.50<br />

1,2,4-Trimethylbenzene 4.14<br />

1,2,3-Trimethylbenzene 2.54<br />

Indan 2.73<br />

1,4-Diethylbenzene 2.45<br />

n-Butylbenzene 2.44<br />

1,2-Diethylbenzene 2.50<br />

1,2,4,5-Tetramethylbenzene 1.68<br />

1,2,3,5-Tetramethylbenzene 1.68<br />

Naphthalene 1.88<br />

1-Methylnaphthalene 1.88<br />

2-Methylnaphthalene 1.93<br />

Isooctane 19.92<br />

The 4 Comp. Internal Standard Mix (M-GRA-IS-R) is<br />

combined with the 24 component core calibration<br />

curve mixtures above in a 12 to 100 weight ratio to<br />

formulate these 28 component calibration solutions.<br />

Sensitivity Test Solution<br />

M-GRA-ST $ 10 / 1 x 1 mL<br />

M-GRA-ST-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

100 µg/mL in Isooctane<br />

1,4-Diethyl benzene<br />

Resolution Standard<br />

M-GRA-RES $ 30 / 1 x 1 mL<br />

M-GRA-RES-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

Compound Wt. %<br />

1,3,5-Trimethylbenzene 3.0<br />

1-Methyl-2-ethylbenzene 3.0<br />

Isooctane 94<br />

3 comps.<br />

Fragmentation Pattern Standard<br />

M-GRA-FP $ 20 / 1 x 1 mL<br />

M-GRA-FP-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

3.0 w/w in Isooctane<br />

1,2,3-Trimethylbenzene<br />

Originally designed for<br />

D-5769-98<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


<strong>ASTM</strong> D-5769 New Proposed / Promulgated Method Modifications<br />

Calibration Curve with a 3 Comp. Chlorinated<br />

Internal Standard added<br />

D-5769-CAL/IS-R2-SET $ 375 / 5 x 1 mL<br />

Core Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />

24 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Benzene 5.25 2.95 1.575 0.8144 0.4143<br />

Toluene 19.67 11.06 5.898 3.0505 1.5519<br />

Ethylbenzene 5.18 2.91 1.552 0.8026 0.4083<br />

m-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />

p-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />

o-Xylene 6.30 3.54 1.890 0.9776 0.4973<br />

Isopropylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />

n-Propylbenzene 3.09 1.74 0.926 0.4787 0.2435<br />

3-Ethyltoluene 3.10 1.74 0.928 0.4801 0.2442<br />

4-Ethyltoluene 3.08 1.73 0.925 0.4782 0.2433<br />

1,3,5-Trimethylbenzene 3.10 1.74 0.929 0.4804 0.2444<br />

2-Ethyltoluene 3.15 1.77 0.945 0.4890 0.2488<br />

1,2,4-Trimethylbenzene 5.23 2.94 1.567 0.8104 0.4123<br />

1,2,3-Trimethylbenzene 3.20 1.80 0.960 0.4965 0.2526<br />

Indan 3.45 1.94 1.034 0.5350 0.2722<br />

1,4-Diethylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />

n-Butylbenzene 3.08 1.73 0.923 0.4776 0.2430<br />

1,2-Diethylbenzene 3.15 1.77 0.945 0.4885 0.2485<br />

1,2,4,5-Tetramethylbenzene 2.12 1.19 0.635 0.3284 0.1671<br />

1,2,3,5-Tetramethylbenzene 2.12 1.19 0.637 0.3295 0.1676<br />

Naphthalene 2.37 1.34 0.712 0.3683 0.1874<br />

1-Methylnaphthalene 2.37 1.34 0.712 0.3683 0.1874<br />

2-Methylnaphthalene 2.43 1.37 0.730 0.3773 0.1919<br />

Isooctane ----- 43.77 70.015 84.4922 92.1105<br />

Internal Standard<br />

M-GRA-IS-R2<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Compound Mix Ratio<br />

Chlorobenzene 2 mL<br />

1,2-Dichlorobenzene 2 mL<br />

1,2,4-Trichlorobenzene 1 mL<br />

Compound<br />

17 comps.<br />

Wt.<br />

Ratio<br />

Toluene 9<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 2<br />

Naphthalene 1<br />

Includes M-GRA-IS-R2 (3 component mix)<br />

added in 5 to 100 weight ratio<br />

Compound Mix ratio<br />

Chlorobenzene 2 mL<br />

1,2-Dichlorobenzene 2 mL<br />

1,2,4-Trichlorobenzene 1 mL<br />

Daily Quality Control Standard<br />

(with Internal Standard)<br />

D-5769-QC/IS-R2-5ML $ 100 / 1 x 5 mL<br />

D-5769-QC/IS-R2-5ML-PAKSAVE 20% $400/5 x 5 mL<br />

100<br />

3 Comp. Chlorinated Internal Std. Mix<br />

M-GRA-IS-R2-SET $125 / set of 25 x 1 mL<br />

M-GRA-IS-R2-25ML $ 100 / 1 x 25 mL<br />

3 comps.<br />

Optional Sixth Standard<br />

with a 3 Comp. Chlorinated<br />

Internal Standard added<br />

D-5769-ADD/IS-R2 $ 100 / 1 x 1 mL<br />

Core Calibration Mix Target<br />

24 Component Wt.%<br />

Benzene 4.16<br />

Toluene 16.41<br />

Ethylbenzene 4.10<br />

m-Xylene 4.91<br />

p-Xylene 4.91<br />

o-Xylene 5.00<br />

Isopropylbenzene 2.45<br />

n-Propylbenzene 2.45<br />

3-Ethyltoluene 2.45<br />

4-Ethyltoluene 2.44<br />

1,3,5-Trimethylbenzene 2.46<br />

2-Ethyltoluene 2.50<br />

1,2,4-Trimethylbenzene 4.14<br />

1,2,3-Trimethylbenzene 2.54<br />

Indan 2.73<br />

1,4-Diethylbenzene 2.45<br />

n-Butylbenzene 2.44<br />

1,2-Diethylbenzene 2.50<br />

1,2,4,5-Tetramethylbenzene 1.68<br />

1,2,3,5-Tetramethylbenzene 1.68<br />

Naphthalene 1.88<br />

1-Methylnaphthalene 1.88<br />

2-Methylnaphthalene 1.93<br />

Isooctane 19.92<br />

The 3 Comp. Internal Standard Mix (M-GRA-IS-R2)<br />

is combined with the 24 Comp. Core Calibration<br />

Curve mixtures above in a 5 to 100 weight ratio to<br />

formulate these 27 Comp. calibration solutions.<br />

Sensitivity Test Solution<br />

M-GRA-ST $ 10 / 1 x 1 mL<br />

M-GRA-ST-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

100 µg/mL in Isooctane<br />

1,4-Diethyl benzene<br />

Fragmentation Pattern Standard<br />

M-GRA-FP $ 20 / 1 x 1 mL<br />

M-GRA-FP-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

3.0 w/w in Isooctane<br />

1,2,3-Trimethylbenzene<br />

Resolution Standard<br />

M-GRA-RES $ 30 / 1 x 1 mL<br />

M-GRA-RES-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

Compound Wt. %<br />

1,3,5-Trimethylbenzene 3.0<br />

1-Methyl-2-ethylbenzene 3.0<br />

Isooctane 94<br />

3 comps.<br />

Originally designed for<br />

D-5769-98<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 49<br />

Member<br />

Disk Deliverable<br />

(At no additional charge)<br />

Eliminates hand keyed-in<br />

data.<br />

CALAMTS ®<br />

(Disk containing “Calibration<br />

Amounts”)<br />

Each analyte in each<br />

standard is individually<br />

weighed. Actual weights<br />

and weight percents are<br />

provided.<br />

<strong>Standards</strong> of Interest<br />

For the mandatory real world<br />

QC samples stipulated in the<br />

Method, see pages 1-2.<br />

Method 5769<br />

<strong>ASTM</strong>


Method 5769<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-5769 Special QA/QC Formulations<br />

Daily Quality Control Standard<br />

(without Internal Standard)<br />

M-GRA-QC-R-10ML $ 125 / 1 x 10 mL<br />

M-GRA-QC-R-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Toluene 9<br />

Includes M-GRA-IS (3 Comp. Internal <strong>Standards</strong><br />

Mix) combined with the above 15 Comp. Core<br />

QC Mix: M-GRA-QC-R in a 5 to 100 weight ratio<br />

50<br />

Wt.<br />

Compound Ratio<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 1<br />

Pentamethylbenzene 1<br />

1-Methylnaphthalene 1<br />

15 Comp. Core Mix 100<br />

For use with any M-GRA<br />

Calibration Curve<br />

Daily Quality Control Standard<br />

(with Internal Standard M-GRA-IS)<br />

M-GRA-QC-R/IS-5ML $ 100 / 1 x 5 mL<br />

M-GRA-QC-R/IS-5ML-PAKSAVE 20% $ 400 / 5 x 5 mL<br />

18 comps.<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Toluene 9<br />

Wt.<br />

Compound Ratio<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 1<br />

Pentamethylbenzene 1<br />

1-Methylnaphthalene 1<br />

100<br />

3 Comp. Deuterated Internal Std. Mix<br />

M-GRA-IS-5ML $ 150 / 1 x 5 mL<br />

M-GRA-IS-5ML-PAK SAVE 20% $ 600 / 5 x 5 mL<br />

3 comps.<br />

Compound Mix Ratio<br />

Benzene-d6 2 mL<br />

Ethylbenzene-d10 2 mL<br />

1 gm<br />

Naphthalene-d 8<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Specially formulated Daily Quality Control<br />

<strong>Standards</strong> originally designed in response to<br />

client requests for QC mixes that bracket the<br />

curve and contain more C9+ analytes to verify<br />

the instrument and QC solution integrity.<br />

Daily Quality Control Standard<br />

(with Internal Std. M-GRA-IS-R)<br />

M-GRA-QC-R/IS-R-5ML $ 125 / 1 x 5 mL<br />

M-GRA-QC-R/IS-R-5ML-PAK SAVE $ 500 / 5 x 5 mL<br />

19 comps.<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Toluene 9<br />

Wt.<br />

Compound Ratio<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 1<br />

Pentamethylbenzene 1<br />

1-Methylnaphthalene 1<br />

100<br />

Includes M-GRA-IS-R (4 Comp. Internal<br />

<strong>Standards</strong> mix) combined with the above 15 Comp.<br />

Core QC Mix: M-GRA-QC-R in a 12 to 100 Wt. ratio<br />

4 Comp. Deuterated Internal Std. Mix<br />

M-GRA-IS-R-10ML $ 225 / 1 x 10 mL<br />

M-GRA-IS-R-10ML-PAK SAVE 20% $ 900 / 5 x 10 mL<br />

4 comps.<br />

Compound Mix Ratio<br />

Benzene-d6 2 mL<br />

Ethylbenzene-d10 2 mL<br />

Naphthalene-d8 1 gm<br />

7 mL<br />

Toluene-d 8<br />

Custom Ampulling for Bulk Quantity Requirements<br />

•<br />

•<br />

Technical Note<br />

Fill Volumes from 0.2 mL to 20 mL<br />

• Flammables<br />

QC Services available<br />

AccuStandard has the resources and equipment to meet your custom packaging<br />

requirements. Our full automated filler-sealer can accommodate a fill range from<br />

0.5 to 20 mL, and ampule sizes from 1 mL to 20 mL.<br />

AccuStandard has extensive experience with Round Robin samples for <strong>ASTM</strong><br />

committees.<br />

Call our Technical Department for a quotation.<br />

Originally designed for<br />

D-5769-98<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Save 20-40%<br />

Buy AccuPAKs<br />

AccuPAK ®<br />

Reduce reordering frequency<br />

Reduce data entry time for<br />

Calibration tables due to<br />

Lot No. consistency<br />

Economical


<strong>ASTM</strong> <strong>Standards</strong><br />

Through a collaborative effort involving the instrument manufactures, Petrochemical end users, and Chemical Reference Standard manufacturers,<br />

the following proposed D-5769 method is under consideration. A number of end users would like to evaluate this proposed D-5769 method and<br />

have asked AccuStandard to make the standards. We have formulated the following certified standards to meet those requests.<br />

Summary Proposed Modifications for D-5769<br />

• Calibration standards when combined with internal standards are diluted into significantly more isooctane.<br />

• The analytes in the Performance Standard have been expanded to better tune the GC/MS system for optimum performance.<br />

• The number of components in the QA/QC mix has been reduced with new QA/QC tolerances.<br />

• The number of analytes in the calibration mix has been reduced.<br />

• Samples that exceed the linear range are to be diluted, reducing the number of extra calibration points required.<br />

<strong>ASTM</strong> D-5769-XX Calibration Curve with No Internal Standard Added<br />

<strong>ASTM</strong>-P-0140-SET $ 1500 / Set of 5 x 5 mL<br />

<strong>ASTM</strong>-P-0140-01<br />

<strong>ASTM</strong>-P-0140-02<br />

<strong>ASTM</strong>-P-0140-03<br />

<strong>ASTM</strong>-P-0140-04<br />

Performance Evalutation Standard<br />

<strong>ASTM</strong>-P-0140-PES $ 55 / 1 x 1 mL<br />

<strong>ASTM</strong>-P-0140-PES-PAK $ 220 / 5 x 1 mL<br />

11 comps.<br />

<strong>ASTM</strong>-P-0140-05<br />

Core Calibr. Mix Level 1 Level 2 Level 3 Level 4 Level 5<br />

Compound Target Mass % Mass % Mass % Mass % Mass %<br />

Benzene 5 3 1 0.5 0.1<br />

Toluene 12 9 6 3 0.5<br />

Ethylbenzene 5 3.75 2.5 1.25 0.2<br />

1,3-Dimethylbenzene 10 7.5 5 2.5 0.2<br />

1,4-Dimethylbenezene 5 3.75 2.5 1.25 0.2<br />

1,2-Dimethylbenezene 5 3.75 2.5 1.25 0.2<br />

(1-Methylethyl)-benzene 3 2.25 1.5 0.75 0.2<br />

1-Methyl-3-ethylbenzene 3 2.25 1.5 0.75 0.2<br />

1-Methyl-4-ethylbenzene 3 2.25 1.5 0.75 0.2<br />

1,3,5-Trimethylbenzene 3 2.25 1.5 0.75 0.2<br />

1-Methyl-2-ethylbenzene 3 2.25 1.5 0.75 0.2<br />

1,2,4-Trimethylbenzene 6 4.5 3 1.5 0.2<br />

1,2,3-Trimethylbenzene 3 2.25 1.5 0.75 0.2<br />

Indan 3 2.25 1.5 0.75 0.2<br />

1,2-Diethylbenzene 2 1.5 1 0.5 0.2<br />

Naphthalene A 2 1.5 1 0.5 0.1<br />

2-Methylnaphthalene A 2 1.5 1 0.5 0.1<br />

1-Methylnaphthalene A 2 1.5 1 0.5 0.1<br />

Isooctane (solvent) * balance balance balance balance balance<br />

4 Comp. Deuterated Internal Std. Mix<br />

<strong>ASTM</strong>-P-0140-IS $ 75 / 1 x 10 mL<br />

<strong>ASTM</strong>-P-0140-IS-PAK $ 300 / 5 x 10 mL<br />

4 comps.<br />

Compound Mass %<br />

Benzene-d6 2<br />

2<br />

Ethylbenzene-d 10<br />

Target<br />

Compound Mass %<br />

Benzene 1<br />

1,2-Diethylbenzene 0.005<br />

1,3,5-Trimethylbenzene 1<br />

1-Methyl-2-ethylbenzene 1<br />

Styrene 0.1<br />

Indene 0.1<br />

Biphenyl 0.1<br />

1,2,4,5-Tetramethylbenzene 1<br />

1,2,3,5-Tetramethylbenzene 1<br />

Hexadecane 1<br />

Isooctane:Toluene(1:1) * balance<br />

Compound Mass %<br />

Naphthalene-d8 1<br />

Isooctane * balance<br />

A= This component is a solid at room<br />

temperature<br />

4 Comp. Deuterated Internal Std. Mix<br />

<strong>ASTM</strong>-P-0140-IS2 $ 95 / 1 x 10 mL<br />

<strong>ASTM</strong>-P-0140-IS2-PAK $ 380 / 5 x 10 mL<br />

5 comps.<br />

Compound Mass % Compound Mass %<br />

Benzene-d6 2 Naphthalene-d8 1<br />

Ethylbenzene-d10 2 Toluene-d8 7<br />

Isooctane * balance<br />

Composition of Daily QC Standard<br />

<strong>ASTM</strong>-P-0140-QC $ 125 / 1 x 10 mL<br />

<strong>ASTM</strong>-P-0140-QC-PAK $ 500 / 5 x 10 mL<br />

9 comps.<br />

Target<br />

Compound Mass %<br />

Benzene 1<br />

Toluene 10<br />

Ethylbenzene 3<br />

1,3-Dimethylbenzene 6<br />

1,2-Dimethylbenzene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2-Diethylbenzene 0.02<br />

Naphthalene 1<br />

Isooctane (solvent) * balance<br />

Technical Note<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 51<br />

Member<br />

* The isooctane balance is the<br />

amount of material to make up<br />

a 100 mL calibration standard.<br />

Certificate will reflect actual<br />

weight of each component in<br />

the 100 mL batch including the<br />

isooctane.<br />

Method 5769<br />

<strong>ASTM</strong>


Method 5771<br />

5772<br />

5773<br />

5863<br />

<strong>ASTM</strong><br />

WEAR METALS<br />

Member<br />

<strong>ASTM</strong> D-5771 Cloud Point of Petroleum Products<br />

See page 5 for AccuStandard’s comprehensive line of certified Cloud Point <strong>Standards</strong>.<br />

<strong>ASTM</strong> D-5772 Cloud Point of Petroleum Products (Linear Cooling Rate Method)<br />

See page 5 for AccuStandard’s comprehensive line of certified Cloud Point <strong>Standards</strong>.<br />

<strong>ASTM</strong> D-5773 Cloud Point of Petroleum Products (Constant Cooling Rate Method)<br />

See page 5 for AccuStandard’s comprehensive line of certified Cloud Point <strong>Standards</strong>.<br />

<strong>ASTM</strong> D-5863 Nickel, Vanadium, Iron, & Sodium in Crude Oils & Residual Fuels by<br />

Flame AA Spectrometry<br />

Test Method A - Sample Decomposition with Acid for Total Ni, V and Fe<br />

Determination<br />

Stock Multi-Element<br />

Aqueous Standard<br />

D-5863-95A-10X-1 $ 75 / 1 x 100 mL<br />

2-5% HNO3 3 comps.<br />

µg/mL<br />

Iron 100<br />

Nickel 200<br />

µg/g<br />

Sodium 50<br />

Nickel 200<br />

52<br />

µg/mL<br />

Vanadium 200<br />

µg/g<br />

Vanadium 150<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Individual High Concentration Elements in Aqueous Matrix<br />

1,000 µg/mL Conc.<br />

Element Matrix Unit Cat. No. Price<br />

Iron Fe<br />

in HNO3 500 mL ICP-27N-5 $ 67<br />

Nickel Ni<br />

in HNO3 500 mL ICP-37N-5 67<br />

Vanadium V2O5 in HNO3 500 mL ICP-67N-5 67<br />

Stock Multi-Element Standard in<br />

Mineral Oil<br />

D-5863-95B-10X $ 160 / 1 x 4 oz<br />

At stated conc. in 20 cst Mineral Oil 3 comps.<br />

Matrix Blank<br />

Nitric Acid Blank<br />

CLP-BLN-5 $ 30 / 500 mL<br />

CLP-BLN-L SAVE 33% $ 45 / L (2 x 500 mL)<br />

5% HNO 3 in <strong>ASTM</strong> Type I Water<br />

Test Method B - Sample Dilution with Organic Solvent for the Determination of<br />

Ni, V and Na using Oil-Soluble Metals as Calibrants.<br />

<strong>Standards</strong> of Interest<br />

See pages 59-65 for AccuStandard’s<br />

comprehensive line of Certified Oil Dissolved<br />

Wear Metal calibration standards designed for<br />

flame AA Applications.<br />

Originally designed for<br />

D-5863-00<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

<strong>Standards</strong> of Interest<br />

See page 73-75 for additional<br />

Trace Metal <strong>Standards</strong> by AA.


<strong>ASTM</strong> <strong>Standards</strong><br />

<strong>ASTM</strong> D-5901 Freezing Point Aviation Fuels (Automated Optical Method)<br />

See page 5 for AccuStandard’s comprehensive line of Certified Freezing Point <strong>Standards</strong>.<br />

<strong>ASTM</strong> D-5972 Freezing Point Aviation Fuels (Automated Phase Transition Method)<br />

See page 5 for AccuStandard’s comprehensive line of Certified Freezing Point <strong>Standards</strong>.<br />

<strong>ASTM</strong> D-5986 Oxygenates, Benzene, Toluene, C 8-C 12, Aromatics & Total Aromatics in Finished Gasolines by GC/FTIR<br />

Daily Quality Control Standard<br />

(without Internal Standard)<br />

M-GRA-QC-10ML $ 125 / 1 x 10 mL<br />

M-GRA-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL<br />

Wt.<br />

Compound Ratio<br />

n-Hexane 12<br />

n-Heptane 17<br />

n-Octane 17<br />

n-Decane 12<br />

n-Dodecane 5<br />

Isooctane 12<br />

Benzene 1<br />

Wt.<br />

Compound Ratio<br />

Toluene 9<br />

Ethylbenzene 3<br />

m-Xylene 3<br />

o-Xylene 3<br />

1,2,4-Trimethylbenzene 3<br />

1,2,4,5-Tetramethylbenzene 3<br />

13 Comp. Core Mix 100<br />

Technical Note<br />

AccuStandard formulated this quality control<br />

standard to meet Section 11 of <strong>ASTM</strong><br />

D-5986-96 specifications stipulating to<br />

“analyze the quality control reference material<br />

before every batch of samples. Bracket the<br />

samples with the reference materials”.<br />

Oxygenate QC samples are available on<br />

pages 1- 2 or can be custom formulated.<br />

Cross Reference Table<br />

<strong>ASTM</strong> IP ISO DIN JIS AFNOR sorted by<br />

<strong>ASTM</strong> Method see beginning of Catalog<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 53<br />

Member<br />

<strong>Standards</strong> of Interest<br />

Also see Cloud Point standards<br />

used for <strong>ASTM</strong> Method D-2500<br />

on page 5.<br />

Originally designed for<br />

D-5986-96<br />

<strong>Standards</strong> of Interest<br />

Method 5901 -<br />

5986<br />

See page 34 for AccuStandard’s<br />

Oxygenate Calibration Curve<br />

(Cat. No. M-GRO-CAL-SET)<br />

and page 46 for AccuStandard’s<br />

Aromatic Calibration Curve (Cat.<br />

No. D-5769-CAL-SET-5ML).<br />

<strong>ASTM</strong>


Method 6160<br />

6258<br />

6277<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-6160 Polychlorinated Biphenyls (PCBs in Waste Materials by GC)<br />

Aroclor Solutions (Individual and Kit)<br />

<strong>ASTM</strong> D-6258 Solvent Red 164 Dye Concentration in Diesel Fuels<br />

Stock Solvent Red 26 Standard<br />

D-6258-CONC-5ML $ 45 / 1 x 5 mL<br />

Solvent Red 26 @ 300 µg/mL in Xylene<br />

<strong>ASTM</strong> D-6277 Benzene in Spark - Ignition Engine Fuels using Mid Infrared Spectroscopy<br />

54<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

D-6258 Calibration Curve<br />

D-6258-CAL-SET-5ML $ 125 / set of 6 x 5 mL<br />

Cat. No.<br />

Set includes the following Cat. No.’s<br />

Description Unit<br />

D-6258-BL Xylene Blank 1 x 5 mL<br />

D-6258-01 Solvent Red 26 Dye @ 3 µg/mL in Xylene 1 x 5 mL<br />

D-6258-02 Solvent Red 26 Dye @ 6 µg/mL in Xylene 1 x 5 mL<br />

D-6258-03 Solvent Red 26 Dye @ 9 µg/mL in Xylene 1 x 5 mL<br />

D-6258-04 Solvent Red 26 Dye @ 12 µg/mL in Xylene 1 x 5 mL<br />

D-6258-05 Solvent Red 26 Dye @ 15 µg/mL in Xylene 1 x 5 mL<br />

See page 1 for AccuStandard’s QA/QC material reference in the method.<br />

SAVE 20%<br />

in PAK<br />

(35 µg/mL in (35 µg/mL in (35 µg/mL in<br />

Isooctane) MeOH) Hexane) 1 x 1 mL 5 x 1 mL<br />

Aroclor # Cat. No. Cat. No. Cat. No. Price Cat. No. Price<br />

Aroclor 1016 C-216S C-216S-M C-216S-H-10X $ 15 Cat. #-PAK $ 60<br />

Aroclor 1221 C-221S C-221S-M C-221S-H-10X 15 Cat. #-PAK 60<br />

Aroclor 1232 C-232S C-232S-M C-232S-H-10X 15 Cat. #-PAK 60<br />

Aroclor 1242 C-242S C-242S-M C-242S-H-10X 15 Cat. #-PAK 60<br />

Aroclor 1248 C-248S C-248S-M C-248S-H-10X 15 Cat. #-PAK 60<br />

Aroclor 1254 C-254S C-254S-M C-254S-H-10X 15 Cat. #-PAK 60<br />

Aroclor 1260 C-260S C-260S-M C-260S-H-10X 15 Cat. #-PAK 60<br />

Aroclor 1262 C-262S C-262S-M C-262S-H-10X 15 Cat. #-PAK 60<br />

Aroclor 1268 C-268S C-268S-M C-268S-H-10X 15 Cat. #-PAK 60<br />

Kit of all 9 above Z-008S Z-008S-M Z-008S-H-10X $ 78 / 9 x 1 mL<br />

Member<br />

Originally designed for<br />

D-6258-98<br />

AccuStandard is an active member in <strong>ASTM</strong> and<br />

strives to keep abreast of <strong>ASTM</strong> method revisions.<br />

If our listed formulation does not meet the most<br />

recent method revision, please contact Technical<br />

Support, ext. 117 for an updated product.<br />

Originally designed for<br />

D-6160-98<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Additional Ready-to-Inject<br />

PCB Aroclor Calibration<br />

Curves available in our<br />

Organic Catalog<br />

Technical Note<br />

Solvent Red 26 is the azo dye<br />

standard against which the<br />

concentration of Solvent Red<br />

164 is measured. The visible<br />

spectrum of Solvent Red 164 is<br />

virtually identical to the<br />

spectrum of Solvent Red 26.


<strong>ASTM</strong> D-6293 Oxygenates & Paraffin, Olefin, Naphthene, Aromatics (O-PONA) Hydrocarbon<br />

types in Low-Olefin Spark-Ignition Engine Fuels by GC<br />

O-PONA System Validation Mixture<br />

<strong>ASTM</strong>-P-0080 $ 135 / 1 x 1 mL<br />

<strong>ASTM</strong>-P-0080-PAK SAVE 26% $ 500 / 5 x 1 mL<br />

33 comps.<br />

Wt./Wt. %<br />

Cyclopentane 1.5<br />

n-Pentane 1.5<br />

Cyclohexane 2.0<br />

2,3-Dimethylbutane 2.0<br />

n-Hexane 2.0<br />

1-Hexene 1.5<br />

Methylcyclohexane 3.5<br />

4-Methyl-1-hexene 1.5<br />

n-Heptane 3.0<br />

cis-1,2-Dimethylcyclohexane 4.5<br />

Isooctane 4.0<br />

n-Octane 4.0<br />

1,2,4-Trimethylcyclohexane 3.5<br />

n-Nonane 3.0<br />

n-Decane 3.5<br />

n-Undecane 2.0<br />

n-Dodecane 2.0<br />

For the mandatory real world QC samples<br />

stipulated in QA/QC section 8.6 of the method<br />

see pages 1-2.<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

O-PONA Paraffin Mix<br />

<strong>ASTM</strong>-P-0082-R1 $ 25 / 1 x 1 mL<br />

<strong>ASTM</strong>-P-0082-R1-PAK $ 100 / 5 x 1 mL<br />

At stated conc. in Hexane : Heptane (1:1)<br />

2 comps.<br />

Wt./Wt. %<br />

n-Nonane 3.0<br />

n-Decane 3.0<br />

<strong>ASTM</strong> D-6296 Total Olefins in Spark-Ignition Engine Fuels by Multidimensional GC<br />

Wt. %<br />

Pentene 1.0<br />

Hexene 1.0<br />

Heptene 1.0<br />

Octene 1.0<br />

Nonene 1.0<br />

<strong>Standards</strong> of Interest<br />

Wt./Wt. %<br />

Benzene 2.5<br />

Toluene 2.5<br />

trans-Decahydronaphthelene 3.5<br />

n-Tetradecane 2.0<br />

Ethylbenzene 3.5<br />

o-Xylene 3.0<br />

n-Propylbenzene 3.5<br />

1,2,4-Trimethylbenzene 3.0<br />

1,2,3-Trimethylbenzene 2.0<br />

1,2,4,5-Tetramethylbenzene 2.0<br />

Pentamethylbenzene 2.5<br />

Ethanol 5.0<br />

t-Butanol 4.0<br />

MtBE 8.0<br />

ETBE 3.0<br />

TAME 5.0<br />

Isooctane Blank Compensation Standard<br />

D-6296-BL $ 15 / 1 x 5 mL<br />

Isooctane (Neat)<br />

O-PONA Olefin Mix<br />

<strong>ASTM</strong>-P-0081 $ 45 / 1 x 1 mL<br />

<strong>ASTM</strong>-P-0081-PAK $ 180 / 5 x 1 mL<br />

At stated conc. in Hexane : Heptane (1:1)<br />

Wt./Wt. %<br />

1-Pentene 5.0<br />

1-Hexene 2.0<br />

1-Heptene 2.0<br />

1-Octene 2.0<br />

1-Nonene 3.0<br />

O-PONA Paraffin Mix<br />

<strong>ASTM</strong>-P-0082 $ 25 / 1 x 1 mL<br />

<strong>ASTM</strong>-P-0082-PAK $ 100 / 5 x 1 mL<br />

At stated conc. in Hexane : Heptane (1:1)<br />

Wt./Wt. %<br />

n-Nonane 5.0<br />

n-Decane 2.0<br />

System Setup & Verification <strong>Standards</strong><br />

D-6296-VER-SET $ 40 / 2 x 1 mL<br />

Set contains 1 ampule of each Cat. No. listed below<br />

D-6296-VER-SET-PAK SAVE 23% $ 150 / 5 x (2 x 1 mL)<br />

5 sets containing 1 ampule of each Cat. No. listed below<br />

System Setup & Verification <strong>Standards</strong><br />

D-6296-VER1 1 x 1 mL<br />

Wt. %<br />

MTBE 5%<br />

Isooctane 95%<br />

2 comps.<br />

Calibration Standard with MTBE<br />

D-6296-CAL1 $ 65 / 1 x 1 mL<br />

D-6296-CAL1-PAK SAVE 23% $ 250 / 5 x 1 mL<br />

10 comps.<br />

Wt. %<br />

Decene 1.0<br />

Undecane 1.0<br />

Dodecane 1.0<br />

Isooctane 87.0<br />

MTBE 5.0<br />

Wt. %<br />

ETBE 5%<br />

Isooctane 95%<br />

5 comps.<br />

2 comps.<br />

System Setup & Verification <strong>Standards</strong><br />

D-6296-VER2 1 x 1 mL<br />

2 comps.<br />

Calibration Standard with ETBE<br />

D-6296-CAL2 $ 65 / 1 x 1 mL<br />

D-6296-CAL2-PAK SAVE 23% $ 250 / 5 x 1 mL<br />

11 comps.<br />

Wt. %<br />

Pentene 1.0<br />

Hexene 1.0<br />

Heptene 1.0<br />

Octene 1.0<br />

Nonene 1.0<br />

Decene 1.0<br />

Wt. %<br />

Decane 1.0<br />

Undecane 1.0<br />

Dodecane 1.0<br />

Isooctane 86.0<br />

ETBE 5.0<br />

Originally designed for<br />

D-6293-98<br />

Originally designed for<br />

D-6296-98<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 55<br />

Method 6293<br />

6296<br />

Member<br />

<strong>ASTM</strong>


Method 6304<br />

6334<br />

6352<br />

<strong>ASTM</strong><br />

Member<br />

<strong>ASTM</strong> D-6304 Determination of Water in Petroleum Products Lubricating oil, and<br />

additives by Coulometric Karl Fischer Titration<br />

<strong>ASTM</strong> D-6334 Sulfur in Gasoline by Wavelength Dispersive X-Ray Fluorescence<br />

<strong>ASTM</strong> D-6352 Boiling Range Distribution of Petroleum Distillates from 174 to 700ºC by GC<br />

<strong>ASTM</strong> D-6378 Vapor Pressure (VPx) of Petroleum Products, Hydrocarbons, &<br />

Hydrocarbon-Oxygenate Mixtures (Triple Expansion Method)<br />

56<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

See page 5 for AccuStandard’s comprehensive line of Certified Water <strong>Standards</strong>, for<br />

Karl Fischer Analysis.<br />

See Sulfur <strong>Standards</strong> Group listing in the Table of Contents for AccuStandard’s comprehensive<br />

line of Certified Sulfur Calibration <strong>Standards</strong>.<br />

Polywax 500 ®<br />

<strong>ASTM</strong>-P-0051N-2G $ 20 / 2 grams<br />

Polywax 850 ®<br />

<strong>ASTM</strong>-P-0137N-2G $ 20 / 2 grams<br />

Polywax 500 Polywax 850<br />

Contact AccuStandard’s<br />

Polywax 655 ®<br />

<strong>ASTM</strong>-P-0053N-2G $ 20 / 2 grams<br />

Polywax 655<br />

Hydrocarbon Window<br />

Defining Standard*<br />

DRH-008S-R2 $ 65 / 1 x 1 mL<br />

DRH-008S-R2-PAK SAVE 20% $ 260 / 5 x 1 mL<br />

500 µg/mL each in Chloroform 35 comps.<br />

Octane<br />

Nonane<br />

Decane<br />

Undecane<br />

Dodecane<br />

Tridecane<br />

Tetradecane<br />

Pentadecane<br />

Hexadecane<br />

Heptadecane<br />

Octadecane<br />

Pristane<br />

Nonadecane<br />

Phytane<br />

Eicosane<br />

Heneicosane<br />

Docosane<br />

Tricosane<br />

Tetracosane<br />

Pentacosane<br />

Hexacosane<br />

Heptacosane<br />

Octacosane<br />

Nonacosane<br />

Triacontane<br />

n-Hentriacontane<br />

Dotriacontane<br />

Tritriacontane<br />

Tetratriacontane<br />

Pentatriacontane<br />

Hexatriacontane<br />

Heptatriacontane<br />

Octatriacontane<br />

Nonatriacontane<br />

Tetracontane<br />

* Can be shipped by Air and Sea<br />

Polywax 1000 ®<br />

<strong>ASTM</strong>-P-0138N-2G $ 20 / 2 grams<br />

Polywax 1000<br />

Calibration Mix<br />

DRH-002N $ 10 / 100 mg<br />

DRH-002N-10X $ 40 / 1 gm<br />

Wt. %<br />

n-Hexane 6<br />

n-Heptane 6<br />

n-Octane 8<br />

n-Nonane 8<br />

n-Decane 12<br />

n-Undecane 12<br />

n-Dodecane 12<br />

n-Tetradecane 12<br />

n-Hexadecane 10<br />

n-Octadecane<br />

17 comps.<br />

Wt. %<br />

5<br />

n-Eicosane 2<br />

n-Tetracosane 2<br />

n-Octacosane 1<br />

n-Dotriacontane 1<br />

n-Hexatriacontane 1<br />

n-Tetracontane 1<br />

n-Tetratetracontane 1<br />

Column Test Mixture<br />

<strong>ASTM</strong>-D2887 $ 10 / 1 x 1 mL<br />

1% v/v in n-Octane 2 comps.<br />

n-Hexadecane n-Octadecane<br />

See pages 29 & 32 for AccuStandard’s comprehensive line of Vapor Pressure <strong>Standards</strong> &<br />

Instrument Quality Control Samples.<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Originally designed for<br />

D-6352-98<br />

<strong>Standards</strong> of Interest<br />

Technical Department<br />

regarding the availability of a<br />

QA/QC Reference Oil Sample<br />

under development in <strong>ASTM</strong>.


<strong>ASTM</strong> D-6379 Aromatic Hydrocarbon Types in Aviation Fuels & Petroleum Distillates -<br />

HPLC method with Refractive Index<br />

System Resolution Standard<br />

D-6379-SRS $ 40 / 1 x 1 mL<br />

D-6379-SRS-PAK SAVE 30% $ 140 / 5 x 1 mL<br />

At stated Conc. in n-Heptane 3 comps.<br />

Cyclohexane 10 mg/mL<br />

o-Xylene 0.5 mg/mL<br />

1-Methyl naphthalene 0.05 mg/mL<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

D-6591 Aromatic Hydrocarbon Types in Middle Distillates -<br />

IP 391 HPLC method with Refractive Index Detection<br />

System Performance Standard<br />

<strong>ASTM</strong>-P-0135 $ 75 / 1 x 5 mL<br />

<strong>ASTM</strong>-P-0135-PAK SAVE 20% $ 300 / 5 x 5 mL<br />

At stated Conc. in n-Heptane 4 comps.<br />

Cyclohexane 10 mg/mL<br />

o-Xylene 5.0 mg/mL<br />

Dibenzothiophene 0.5 mg/mL<br />

9-Methylanthracene 0.5 mg/mL<br />

D-6379 Calibration Curve<br />

D-6379-SET $ 100 / 4 x 1 mL<br />

D-6379-SET-PAK SAVE 30% $ 350 / 5 x (4 x 1 mL)<br />

At stated Conc. in n-Heptane<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4<br />

(mg/mL) (mg/mL) (mg/mL) (mg/mL)<br />

Cyclohexane 5 2 0.5 0.1<br />

o-Xylene 15 5 1.0 0.1<br />

1-Methyl naphthalene 5 1.0 0.2 0.05<br />

IP 391-95 Calibration Curve<br />

<strong>ASTM</strong>-P-0136-SET $ 145 / 4 x 1 mL<br />

At stated Conc. in n-Heptane<br />

Analyte Std. 1 Std. 2 Std. 3 Std. 4<br />

(mg/mL) (mg/mL) (mg/mL) (mg/mL)<br />

Cyclohexane 50 20 5 1<br />

o-Xylene 40 10 2.5 0.5<br />

1-Methyl naphthalene 40 10 2.5 0.2<br />

Phenanthrene 4 2 0.5 0.1<br />

<strong>ASTM</strong> D-6417 Estimation of Engine Oil Volatility by Capillary GC<br />

See page 15 for Alkane and Polywax standards suitable for D-6417.<br />

<strong>ASTM</strong> D-6428 Sulfur by Combustion and Electrochemical Detection<br />

D-6428-R1-4-SET $ 300 / 7 x 4 oz<br />

D-6428-R1-SET $ 65 / 7 x 1 mL<br />

Sulfur as Dibenzothiophene<br />

D-6428-R1-4-SET D-6428-R1-SET<br />

Description Cat. No. Unit Cat. No. Unit<br />

Sulfur Blank D-6428-BL-4 4 oz D-6428-BL 1 mL<br />

Sulfur @ 0.1 µg/g D-6428-0.1X-4 4 oz D-6428-0.1X 1 mL<br />

Sulfur @ 0.5 µg/g D-6428-0.5X-4 4 oz D-6428-0.5X 1 mL<br />

Sulfur @ 1.0 µg/g D-6428-1X-4 4 oz D-6428-1X 1 mL<br />

Sulfur @ 2.5 µg/g D-6428-2.5X-4 4 oz D-6428-2.5X 1 mL<br />

Sulfur @ 5.0 µg/g D-6428-5X-4 4 oz D-6428-5X 1 mL<br />

Sulfur @ 10 µg/g D-6428-10X-4 4 oz D-6428-10X 1 mL<br />

D-6428-R2-4-SET $ 275 / 6 x 4 oz<br />

D-6428-R2-SET $ 65 / 6 x 1 mL<br />

Sulfur as Dibenzothiophene<br />

D-6428-R2-4-SET D-6428-R2-SET<br />

Description Cat. No. Unit Cat. No. Unit<br />

Sulfur Blank D-6428-BL-4 4 oz D-6428-BL 1 mL<br />

Sulfur @ 10 µg/g D-6428-10X-4 4 oz D-6428-10X 1 mL<br />

Sulfur @ 25 µg/g D-6428-25X-4 4 oz D-6428-25X 1 mL<br />

Sulfur @ 50 µg/g D-6428-50X-4 4 oz D-6428-50X 1 mL<br />

Sulfur @ 75 µg/g D-6428-75X-4 4 oz D-6428-75X 1 mL<br />

Sulfur @ 100 µg/g D-6428-100X-4 4 oz D-6428-100X 1 mL<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 57<br />

NEW<br />

Originally designed for<br />

D-6379-99<br />

Member<br />

<strong>Standards</strong> of Interest<br />

See <strong>ASTM</strong> Methods D-3710,<br />

D-5307, D-5442, D-6352 for<br />

additional calibration<br />

standards for hydrocarbon<br />

analysis.<br />

Method 6379<br />

IP 391<br />

6417<br />

6428<br />

<strong>ASTM</strong>


Method 6443<br />

6481<br />

6550<br />

<strong>ASTM</strong><br />

WEAR METALS<br />

Member<br />

<strong>ASTM</strong> D-6443 Ca, Cl, Cu, Mg, P, S, Zn in Unused Lubricating Oils & Additives by<br />

Wavelength Dispersive X-ray Fluorescence & Spectrometry<br />

<strong>ASTM</strong> D-6445 Sulfur in Gasoline by ED - XRF<br />

<strong>ASTM</strong> D-6481 P, S, Ca and Zn in Lube Oils by ED-XRF<br />

Lubricating Oil, Elements, EDXRF <strong>ASTM</strong> Method<br />

(Nominal Value) Wt.% listed below<br />

<strong>ASTM</strong>-P-0114-SET $ 1900 / 17 x 100 mL<br />

Ca P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0114-01 0.005 0.005 0.050 0.050<br />

<strong>ASTM</strong>-P-0114-02 0.600 0.000 0.000 0.000<br />

<strong>ASTM</strong>-P-0114-03 0.000 0.300 0.000 0.000<br />

<strong>ASTM</strong>-P-0114-04 1.000 0.000 1.000 0.000<br />

<strong>ASTM</strong>-P-0114-05 0.000 0.000 0.000 0.300<br />

<strong>ASTM</strong>-P-0114-06 0.005 0.250 0.800 0.300<br />

<strong>ASTM</strong>-P-0114-07 0.500 0.150 0.500 0.150<br />

<strong>ASTM</strong>-P-0114-08 0.010 0.200 0.100 0.250<br />

<strong>ASTM</strong>-P-0114-09 0.050 0.010 0.400 0.075<br />

<strong>ASTM</strong>-P-0114-10 0.100 0.150 0.200 0.200<br />

<strong>ASTM</strong>-P-0114-11 0.200 0.200 0.800 0.100<br />

<strong>ASTM</strong>-P-0114-12 0.400 0.005 0.800 0.300<br />

<strong>ASTM</strong>-P-0114-13 0.600 0.100 0.500 0.050<br />

<strong>ASTM</strong>-P-0114-14 0.800 0.010 0.050 0.100<br />

<strong>ASTM</strong>-P-0114-15 1.000 0.300 1.000 0.150<br />

<strong>ASTM</strong>-P-0114-16 0.400 0.050 0.600 0.250<br />

<strong>ASTM</strong>-P-0114-17 0.000 0.000 0.000 0.000<br />

<strong>ASTM</strong> D-6550 Olefin Content of Gasolines by SFC<br />

Stock Olefin Calibration Standard<br />

D-6550-CONC $ 80 / 1 x 1 mL<br />

D-6550-CONC-5ML $ 350 / 1 x 5 mL<br />

At stated Conc. by Wt. % 15 comps.<br />

Wt. %<br />

1-Nonene 2.5<br />

Cyclohexene 5<br />

1-Hexene 5<br />

1-Octene 5<br />

1-Decene 5<br />

2-Methyl-1,3-butadiene 5<br />

4-Methyl-1-pentene 5<br />

1,5-Hexadiene 3<br />

58<br />

Wt. %<br />

3-Methyl-1,3-pentadiene 2<br />

2-Methyl-1-butene 25<br />

2-Methyl-2-pentene 10<br />

1-Heptene 10<br />

2-Methyl-1-octene 2.5<br />

2-Methyl-1-heptene 5<br />

5-Methyl-1-hexene 10<br />

<strong>ASTM</strong> <strong>Standards</strong><br />

Lubricating Oil, Elements, WLXRF <strong>ASTM</strong> Method (Nominal Value) Wt.% listed below<br />

<strong>ASTM</strong>-P-0117-SET $ 2100 / 10 x 100 mL<br />

Ca Cl Cu Mg P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0117-01 0.020 0.030 0.010 0.200 0.250 1.000 0.020<br />

<strong>ASTM</strong>-P-0117-02 0.020 0.020 0.050 0.200 0.020 0.020 0.250<br />

<strong>ASTM</strong>-P-0117-03 0.020 0.200 0.010 0.040 0.250 0.150 0.250<br />

<strong>ASTM</strong>-P-0117-04 0.020 0.200 0.050 0.040 0.020 1.000 0.020<br />

<strong>ASTM</strong>-P-0117-05 0.400 0.020 0.010 0.040 0.020 1.000 0.250<br />

<strong>ASTM</strong>-P-0117-06 0.400 0.020 0.050 0.040 0.250 0.020 0.020<br />

<strong>ASTM</strong>-P-0117-07 0.400 0.200 0.010 0.200 0.020 0.020 0.050<br />

<strong>ASTM</strong>-P-0117-08 0.400 0.200 0.050 0.200 0.250 1.000 0.250<br />

<strong>ASTM</strong>-P-0117-09 0.200 0.100 0.025 0.080 0.150 0.500 0.100<br />

<strong>ASTM</strong>-P-0117-10 0.000 0.000 0.000 0.000 0.000 0.000 0.000<br />

See the Sulfur <strong>Standards</strong> Group listing in the Table of Contents for AccuStandard’s<br />

comprehensive line of Certified Sulfur Calibration <strong>Standards</strong>.<br />

Originally designed for<br />

D-6481-99<br />

Originally designed for<br />

D-6550-00<br />

Technical Note<br />

AccuStandard worked in<br />

conjunction with the D-02<br />

technical committee and Shell<br />

Oil to develop this stock Olefin<br />

Standard proven useful in<br />

creating the required calibration<br />

curve.<br />

Originally designed for<br />

D-6443-99<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

<strong>Standards</strong> of Interest<br />

See the Wear Metal Group<br />

listing in the Table of Contents<br />

for AccuStandard’s<br />

comprehensive line of Certified<br />

Oil Dissolved Wear Metal<br />

Calibration <strong>Standards</strong>.<br />

<strong>Standards</strong> of Interest<br />

See page 2 for consensus value<br />

QA/QC material available for<br />

this method.


Organometallic Wear Metals<br />

Organometallic <strong>Standards</strong><br />

for AA, ICP, DCP & XRF Analysis<br />

These <strong>Standards</strong> were formulated for the analysis of metals in oils and other organic matrices. These <strong>Standards</strong><br />

and curves provide a convenient way to analyze for metals (wear metals, additives and contaminants) in<br />

lubricating oils, gasolines, residual oils, crude oils, turbine fuels and environmental samples.<br />

All standards undergo rigorous quality assurance checks. Major constituents in the final Standard are typically<br />

analyzed by both plasma emission and rotrode techniques.<br />

Organometallic <strong>Standards</strong> listed on this page may contain sulfur which can be introduced by possible sulfonate<br />

starting materials used to formulate the actual organometallic standard.<br />

AccuStandard has developed a New Premium Organometallic line for those clients preferring to have<br />

organometallic standards with


Wear Metals<br />

ORGANOMETALLIC<br />

C<br />

These highly concentrated stabilized solutions can be used for customer specific formulations of additive elements in lubricating oils, iron, nickel and vanadium<br />

in residual oil, and wear metals in oils. These organometallic solutions can also be used to prepare single element or multi-element standards for plasma<br />

emission (ICP or DCP), rotating disk (rotrode), or atomic absorption spectroscopy (AA). The starting materials for the standards are PURE REAGENTS and<br />

have been certified against NIST SRM’s whenever available. THEY DO NOT CONTAIN PHOSPHORUS OR SULFUR. TRACE IMPURITIES ARE<br />

DOCUMENTED ON THE CERTIFICATE OF ANALYSIS.<br />

60<br />

Highly Concentrated Liquid Organo-Metallic <strong>Standards</strong><br />

Stabilized<br />

Organometallic Single-Element Concentrates<br />

Organometallic Single-Element Stock <strong>Standards</strong><br />

Sulfur free Organometallic Sulfur free Organometallic<br />

Element @ 1000 µg/g Price @ 5000 µg/g Price<br />

Cat. No. 50 mL Cat. No. 50 mL<br />

Aluminum WM-NMS-01 $ 50 WM-NMS-01-5X $ 90<br />

Antimony WM-NMS-02 50 WM-NMS-02-5X 90<br />

Barium WM-NMS-04 50 WM-NMS-04-5X 90<br />

Cadmium WM-NMS-08 50 WM-NMS-08-5X 90<br />

Calcium WM-NMS-09 50 WM-NMS-09-5X 90<br />

Chromium WM-NMS-13 50 WM-NMS-13-5X 90<br />

Cobalt WM-NMS-14 75 WM-NMS-14-5X 110<br />

Copper WM-NMS-15 75 WM-NMS-15-5X 110<br />

Iron WM-NMS-27 50 WM-NMS-27-5X 90<br />

Lead WM-NMS-29 50 WM-NMS-29-5X 90<br />

Magnesium WM-NMS-32 50 WM-NMS-32-5X 90<br />

Manganese WM-NMS-33 50 WM-NMS-33-5X 90<br />

Molybdenum WM-NMS-35 50 WM-NMS-35-5X 90<br />

Nickel WM-NMS-37 50 WM-NMS-37-5X 90<br />

Phosphorous WM-NMS-41 50 WM-NMS-41-5X 90<br />

Potassium WM-NMS-43 50 WM-NMS-43-5X 90<br />

Selenium WM-NMS-51 60 WM-NMS-51-5X 100<br />

Silicon WM-NMS-52 75 WM-NMS-52-5X 110<br />

Sodium WM-NMS-54 50 WM-NMS-54-5X 90<br />

Strontium WM-NMS-55 50 WM-NMS-55-5X 90<br />

Thallium WM-NMS-60 60 WM-NMS-60-5X 100<br />

Tin WM-NMS-63 50 WM-NMS-63-5X 90<br />

Titanium WM-NMS-64 50 WM-NMS-64-5X 90<br />

Vanadium WM-NMS-67 50 WM-NMS-67-5X 90<br />

Yttrium WM-NMS-68 60 WM-NMS-68-5X 100<br />

Zinc WM-NMS-70 50 WM-NMS-70-5X 90<br />

Zirconium WM-NMS-71 50 WM-NMS-71-5X 90<br />

Organometallic <strong>Standards</strong><br />

Premium Sulfur-Free<br />

Element Conc. (Wt. %) Cat. No. Price Cat. No. Price<br />

25 grams 50 grams<br />

Aluminum 3 WM-NMS-01-30X-25G $ 150 WM-NMS-01-30X-50G $ 210<br />

Barium 12.5 WM-NMS-04-125X-25G 540 WM-NMS-04-125X-50G 780<br />

Boron 2.5 WM-NMS-07-25X-25G 130 WM-NMS-07-25X-50G 180<br />

Cadmium 10 WM-NMS-08-100X-25G 510 WM-NMS-08-100X-50G 710<br />

Calcium 5 WM-NMS-09-50X-25G 250 WM-NMS-09-50X-50G 355<br />

Chromium 2.5 WM-NMS-13-25X-25G 145 WM-NMS-13-25X-50G 200<br />

Cobalt 7.5 WM-NMS-14-75X-25G 330 WM-NMS-14-75X-50G 450<br />

Copper 6 WM-NMS-15-60X-25G 250 WM-NMS-15-60X-50G 355<br />

Iron 4 WM-NMS-27-40X-25G 220 WM-NMS-27-40X-50G 300<br />

Lead 20 WM-NMS-29-200X-25G 900 WM-NMS-29-200X-50G 1260<br />

Magnesium 3 WM-NMS-32-30X-25G 180 WM-NMS-32-30X-50G 252<br />

Manganese 7.5 WM-NMS-33-75X-25G 330 WM-NMS-33-75X-50G 450<br />

Molybdenum 5 WM-NMS-35-50X-25G 215 WM-NMS-35-50X-50G 294<br />

Nickel 5 WM-NMS-37-50X-25G 250 WM-NMS-37-50X-50G 350<br />

Phosphorus 5 WM-NMS-41-50X-25G 250 WM-NMS-41-50X-50G 350<br />

Praseodymium 3 WM-NMS-44-30X-25G 175 WM-NMS-44-30X-50G 240<br />

Selenium 3.5 WM-NMS-51-35X-25G 200 WM-NMS-51-35X-50G 270<br />

Strontium 10 WM-NMS-55-100X-25G 510 WM-NMS-55-100X-50G 710<br />

Thallium 5 WM-NMS-60-50X-25G 265 WM-NMS-60-50X-50G 360<br />

Titanium 5 WM-NMS-64-50X-25G 215 WM-NMS-64-50X-50G 295<br />

Vanadium 2 WM-NMS-67-20X-25G 115 WM-NMS-67-20X-50G 150<br />

Zinc 6 WM-NMS-70-60X-25G 270 WM-NMS-70-60X-50G 380<br />

Zirconium 5 WM-NMS-71-50X-25G 250 WM-NMS-71-50X-50G 355<br />

Sulfur/Phosphorous free (< 1 ppm)<br />

Ready for Use<br />

Technical Note<br />

Premium<br />

Sulfur-Free<br />

Sulfur below<br />

detection limits<br />

These standards are sulfur free (below<br />

detection limits) organometallic standards<br />

for X-ray Fluorescence (XRF), plasma<br />

emission (ICP or DCP), rotating disk<br />

(rotrode), or atomic absorption (AA). They<br />

are stabilized for blending together with<br />

other Analytes to prepare multi-element<br />

standards.<br />

Stabilization Solutions<br />

The solutions were specifically<br />

designed for chelating and solubilizing<br />

the organometallic line of solids and<br />

solutions for single and multi-element<br />

standards.<br />

Stabilizer Solutions A<br />

<strong>ASTM</strong>-P-0122-0.5 $ 80 / 50 mL<br />

<strong>ASTM</strong>-P-0122-1 $ 120 / 100 mL<br />

Stabilizer Solutions B<br />

<strong>ASTM</strong>-P-0123-0.5 $ 80 / 50 mL<br />

<strong>ASTM</strong>-P-0123-1 $ 120 / 100 mL<br />

(use in conjunction with stabilizer solution A)<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


Wear Metals Multi-Element<br />

11 Wear Metal Multi-Element Standard<br />

Containing No Metallic Sulfonates<br />

Conc.<br />

(µg/g)<br />

Cat. No. Price<br />

10 WM-11-NMS-1X-1 $ 130<br />

30 WM-11-NMS-3X-1 130<br />

50 WM-11-NMS-5X-1 130<br />

100 WM-11-NMS-10X-1 140<br />

300 WM-11-NMS-30X-1 165<br />

500 WM-11-NMS-50X-1 245<br />

900 WM-11-NMS-90X-1 325<br />

WM-11-NMS-SET-1 $ 1100<br />

set of above 7 x 100 mL<br />

Each Wear Metal Standard contains<br />

11 elements in hydrocarbon oil at<br />

the stated concentration<br />

Al (Aluminum)<br />

Cr (Chromium)<br />

Cu (Copper)<br />

Fe (Iron)<br />

Mg (Magnesium)<br />

Na (Sodium)<br />

Ni (Nickel)<br />

Pb (Lead)<br />

Si (Silicon)<br />

Sn (Tin)<br />

Ti (Titanium)<br />

20 Wear Metal Multi-Element Standard<br />

Containing No Metallic Sulfonates<br />

Conc.<br />

(µg/g)<br />

Cat. No. Price<br />

10 WM-20-NMS-1X-1 $ 150<br />

30 WM-20-NMS-3X-1 150<br />

50 WM-20-NMS-5X-1 150<br />

100 WM-20-NMS-10X-1 170<br />

300 WM-20-NMS-30X-1 230<br />

500 WM-20-NMS-50X-1 350<br />

900 WM-20-NMS-90X-1 500<br />

Al (Aluminum)<br />

B (Boron)<br />

Ba (Barium)<br />

Ca (Calcium)<br />

Cd (Cadmium)<br />

Cr (Chromium)<br />

Cu (Copper)<br />

Fe (Iron)<br />

Mg (Magnesium)<br />

Mn (Manganese)<br />

WM-20-NMS-SET-1 $ 1450<br />

set of above 7 x 100 mL<br />

Each Wear Metal Standard contains<br />

20 elements in hydrocarbon oil at<br />

the stated concentration<br />

Organometallic <strong>Standards</strong><br />

Premium Sulfur-Free<br />

Mo (Molybdenum)<br />

Na (Sodium)<br />

Ni (Nickel)<br />

P (Phosphorus)<br />

Pb (Lead)<br />

Si (Silicon)<br />

Sn (Tin)<br />

Ti (Titanium)<br />

V (Vanadium)<br />

Zn (Zinc)<br />

12 Wear Metal Multi-Element Standard<br />

Containing No Metallic Sulfonates<br />

Conc.<br />

(µg/g)<br />

Cat. No. Price<br />

10 WM-12-NMS-1X-1 $ 135<br />

30 WM-12-NMS-3X-1 135<br />

50 WM-12-NMS-5X-1 135<br />

100 WM-12-NMS-10X-1 145<br />

300 WM-12-NMS-30X-1 170<br />

500 WM-12-NMS-50X-1 250<br />

WM-12-NMS-SET-1<br />

set of above 6 x 100 mL<br />

$ 850<br />

Ag (Silver)<br />

Al (Aluminum)<br />

Cr (Chromium)<br />

Cu (Copper)<br />

Fe (Iron)<br />

Mg (Magnesium)<br />

21 Wear Metal Multi-Element Standard<br />

Containing No Metallic Sulfonates<br />

Ag (Silver)<br />

Al (Aluminum)<br />

B (Boron)<br />

Ba (Barium)<br />

Ca (Calcium)<br />

Cd (Cadmium)<br />

Cr (Chromium)<br />

Cu (Copper)<br />

Fe (Iron)<br />

Mg (Magnesium)<br />

Mn (Manganese)<br />

Test to<br />

Low ppb<br />

Sulfur<br />

See Pages 6-11<br />

Each Wear Metal Standard contains<br />

12 elements in hydrocarbon oil at<br />

the stated concentration<br />

Na (Sodium)<br />

Ni (Nickel)<br />

Pb (Lead)<br />

Si (Silicon)<br />

Sn (Tin)<br />

Ti (Titanium)<br />

Conc.<br />

(µg/g)<br />

Cat. No. Price<br />

10 WM-21-NMS-1X-1 $ 160<br />

30 WM-21-NMS-3X-1 160<br />

50 WM-21-NMS-5X-1 160<br />

100 WM-21-NMS-10X-1 180<br />

300 WM-21-NMS-30X-1 240<br />

500 WM-21-NMS-50X-1 350<br />

WM-21-NMS-SET-1<br />

set of above 6 x 100 mL<br />

$ 1050<br />

Each Wear Metal Standard contains<br />

21 elements in hydrocarbon oil at<br />

the stated concentration<br />

Mo (Molybdenum)<br />

Na (Sodium)<br />

Ni (Nickel)<br />

P (Phosphorus)<br />

Pb (Lead)<br />

Si (Silicon)<br />

Sn (Tin)<br />

Ti (Titanium)<br />

V (Vanadium)<br />

Zn (Zinc)<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

Premium<br />

Sulfur-Free<br />

Wear Metals<br />

Sulfur below<br />

detection limits<br />

61<br />

ORGANOMETALLIC<br />

C


Wear Metals<br />

ORGANOMETALLIC<br />

C<br />

Sulfur & Metals in Oil<br />

Sulfur and Metals in Mineral Oil<br />

<strong>ASTM</strong>-P-0100-SET $ 1650 / 12 x 100 mL<br />

Sulfur Nickel Vanadium<br />

Cat. No. Conc. Conc. Conc. Price<br />

(Wt. %) (µg/g) (µg/g) 100 mL<br />

<strong>ASTM</strong>-P-0100-01<br />

<strong>ASTM</strong>-P-0100-02<br />

<strong>ASTM</strong>-P-0100-03<br />

<strong>ASTM</strong>-P-0100-04<br />

<strong>ASTM</strong>-P-0100-05<br />

<strong>ASTM</strong>-P-0100-06<br />

<strong>ASTM</strong>-P-0100-07<br />

<strong>ASTM</strong>-P-0100-08<br />

<strong>ASTM</strong>-P-0100-09<br />

<strong>ASTM</strong>-P-0100-10<br />

<strong>ASTM</strong>-P-0100-11<br />

<strong>ASTM</strong>-P-0100-12<br />

0.00<br />

0.50<br />

1.00<br />

1.50<br />

2.00<br />

2.50<br />

3.00<br />

3.50<br />

4.00<br />

4.50<br />

5.00<br />

5.50<br />

0<br />

10<br />

100<br />

80<br />

40<br />

5<br />

60<br />

0<br />

100<br />

50<br />

20<br />

100<br />

0<br />

500<br />

25<br />

250<br />

100<br />

400<br />

300<br />

200<br />

0<br />

250<br />

500<br />

50<br />

$ 200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

Sulfur and Metals in Mineral Oil<br />

<strong>ASTM</strong>-P-0102-SET $ 1850 / 12 x 100 mL<br />

Sulfur Iron Nickel Vanadium<br />

Cat. No. Conc. Conc. Conc. Conc. Price<br />

(Wt. %) (µg/g) (µg/g) (µg/g) 100 mL<br />

<strong>ASTM</strong>-P-0102-01 0.00 0 0 0 $ 200<br />

<strong>ASTM</strong>-P-0102-02 0.50 300 10 500 200<br />

<strong>ASTM</strong>-P-0102-03 1.00 500 100 25 200<br />

<strong>ASTM</strong>-P-0102-04 ----- 100 80 250 200<br />

<strong>ASTM</strong>-P-0102-05 2.00 200 40 100 200<br />

<strong>ASTM</strong>-P-0102-06 2.50 400 5 400 200<br />

<strong>ASTM</strong>-P-0102-07 3.00 0 60 300 200<br />

<strong>ASTM</strong>-P-0102-08 3.50 500 0 200 200<br />

<strong>ASTM</strong>-P-0102-09 ----- 100 100 0 200<br />

<strong>ASTM</strong>-P-0102-10 4.50 300 50 250 200<br />

<strong>ASTM</strong>-P-0102-11 5.00 200 20 500 200<br />

<strong>ASTM</strong>-P-0102-12 5.50 50 100 50 200<br />

ISO/CD 14597<br />

Vanadium and Nickel <strong>Standards</strong> with Manganese Internal Standard for ISO/CD 14597<br />

Vanadium <strong>Standards</strong> - Low Range for ISO/CD<br />

14597 with 0.05% Manganese Internal Standard<br />

in Xylene-Mineral Oil<br />

<strong>ASTM</strong>-P-0104-SET $ 1050 / 9 x 100 mL<br />

Vanadium Price<br />

Cat. No. Conc. (Wt.%) 100 mL<br />

<strong>ASTM</strong>-P-0104-01 0.0005 $ 150<br />

<strong>ASTM</strong>-P-0104-02 0.0025 150<br />

<strong>ASTM</strong>-P-0104-03 0.0050 150<br />

<strong>ASTM</strong>-P-0104-04 0.0075 150<br />

<strong>ASTM</strong>-P-0104-05 0.0100 150<br />

<strong>ASTM</strong>-P-0104-06 0.0125 150<br />

<strong>ASTM</strong>-P-0104-07 0.0150 150<br />

<strong>ASTM</strong>-P-0104-08 0.0175 150<br />

<strong>ASTM</strong>-P-0104-09 0.0200 150<br />

62<br />

Organometallic <strong>Standards</strong><br />

for AA, ICP, DCP & XRF Analysis<br />

Designed for<br />

<strong>ASTM</strong> D-5708-95a<br />

Vanadium <strong>Standards</strong> - High Range for ISO/CD<br />

14597 with 0.05% Manganese Internal Standard<br />

in Xylene-Mineral Oil<br />

<strong>ASTM</strong>-P-0105-SET $ 780 / 7 x 100 mL<br />

Vanadium Price<br />

Cat. No. Conc. (Wt.%) 100 mL<br />

<strong>ASTM</strong>-P-0105-01 0.0000 $ 135<br />

<strong>ASTM</strong>-P-0105-02 0.0300 135<br />

<strong>ASTM</strong>-P-0105-03 0.0400 135<br />

<strong>ASTM</strong>-P-0105-04 0.0500 135<br />

<strong>ASTM</strong>-P-0105-05 0.0600 135<br />

<strong>ASTM</strong>-P-0105-06 0.0800 135<br />

<strong>ASTM</strong>-P-0105-07 0.1000 135<br />

Internal Standard<br />

<strong>ASTM</strong>-P-0107-5 $ 235 / 500 mL<br />

Manganese @ 0.05 Wt. % in Xylene-Mineral Oil<br />

Technical Note<br />

Concentration for the sets on pages 62-65 are targets. Actual production lots may vary.<br />

Sulfur and Metals in Residual Fuel Oil<br />

<strong>ASTM</strong>-P-0101-SET $ 1800 / 12 x 100 mL<br />

Sulfur Nickel Vanadium<br />

Cat. No. Conc. Conc. Conc. Price<br />

(Wt. %) (µg/g) (µg/g) 100 mL<br />

<strong>ASTM</strong>-P-0101-01<br />

<strong>ASTM</strong>-P-0101-02<br />

<strong>ASTM</strong>-P-0101-03<br />

<strong>ASTM</strong>-P-0101-04<br />

<strong>ASTM</strong>-P-0101-05<br />

<strong>ASTM</strong>-P-0101-06<br />

<strong>ASTM</strong>-P-0101-07<br />

<strong>ASTM</strong>-P-0101-08<br />

<strong>ASTM</strong>-P-0101-09<br />

<strong>ASTM</strong>-P-0101-10<br />

<strong>ASTM</strong>-P-0101-11<br />

<strong>ASTM</strong>-P-0101-12<br />

0.00<br />

0.50<br />

1.00<br />

1.50<br />

2.00<br />

2.50<br />

3.00<br />

3.50<br />

4.00<br />

4.50<br />

5.00<br />

5.50<br />

0<br />

10<br />

100<br />

80<br />

40<br />

5<br />

60<br />

0<br />

100<br />

50<br />

20<br />

100<br />

0<br />

500<br />

25<br />

250<br />

100<br />

400<br />

300<br />

200<br />

0<br />

250<br />

500<br />

50<br />

$ 200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

200<br />

Sulfur and Metals in Residual Fuel Oil<br />

<strong>ASTM</strong>-P-0103-SET $ 2100 / 12 x 100 mL<br />

Sulfur Iron Nickel Vanadium<br />

Cat. No. Conc. Conc. Conc. Conc. Price<br />

(Wt. %) (µg/g) (µg/g) (µg/g) 100 mL<br />

<strong>ASTM</strong>-P-0103-01 0.00 0 0 0 $ 200<br />

<strong>ASTM</strong>-P-0103-02 0.50 300 10 500 200<br />

<strong>ASTM</strong>-P-0103-03 1.00 500 100 25 200<br />

<strong>ASTM</strong>-P-0103-04 ----- 100 80 250 200<br />

<strong>ASTM</strong>-P-0103-05 2.00 200 40 100 200<br />

<strong>ASTM</strong>-P-0103-06 2.50 400 5 400 200<br />

<strong>ASTM</strong>-P-0103-07 3.00 0 60 300 200<br />

<strong>ASTM</strong>-P-0103-08 3.50 500 0 200 200<br />

<strong>ASTM</strong>-P-0103-09 ----- 100 100 0 200<br />

<strong>ASTM</strong>-P-0103-10 4.50 300 50 250 200<br />

<strong>ASTM</strong>-P-0103-11 5.00 200 20 500 200<br />

<strong>ASTM</strong>-P-0103-12 5.50 50 100 50 200<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Designed for<br />

<strong>ASTM</strong> D-5708-95a<br />

Nickel <strong>Standards</strong> for ISO/CD 14597 with 0.05%<br />

Manganese Internal Standard in Xylene-Mineral Oil<br />

<strong>ASTM</strong>-P-0106-SET $ 780 / 7 x 100 mL<br />

Nickel Price<br />

Cat. No. Conc. (Wt.%) 100 mL<br />

<strong>ASTM</strong>-P-0106-01 0.0000 $ 135<br />

<strong>ASTM</strong>-P-0106-02 0.0005 135<br />

<strong>ASTM</strong>-P-0106-03 0.0010 135<br />

<strong>ASTM</strong>-P-0106-04 0.0025 135<br />

<strong>ASTM</strong>-P-0106-05 0.0050 135<br />

<strong>ASTM</strong>-P-0106-06 0.0075 135<br />

<strong>ASTM</strong>-P-0106-07 0.0100 135


Lubricating Oil <strong>Standards</strong><br />

Designed for<br />

<strong>ASTM</strong> D-6481-99<br />

Lubricating Oil, Elements Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0108-SET $ 1900 / 17 x 100 mL<br />

Ca P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0108-01 0.600 0.005 0.175 0.060<br />

<strong>ASTM</strong>-P-0108-02 0.500 0.200 0.050 0.080<br />

<strong>ASTM</strong>-P-0108-03 0.400 0.150 0.300 0.180<br />

<strong>ASTM</strong>-P-0108-04 0.260 0.250 0.150 0.120<br />

<strong>ASTM</strong>-P-0108-05 0.005 0.005 0.450 0.070<br />

<strong>ASTM</strong>-P-0108-06 0.400 0.025 0.350 0.100<br />

<strong>ASTM</strong>-P-0108-07 0.300 0.060 0.250 0.120<br />

<strong>ASTM</strong>-P-0108-08 0.200 0.100 0.450 0.100<br />

<strong>ASTM</strong>-P-0108-09 0.060 0.080 0.300 0.130<br />

<strong>ASTM</strong>-P-0108-10 0.060 0.050 0.200 0.050<br />

<strong>ASTM</strong>-P-0108-11 0.050 0.120 0.100 0.075<br />

<strong>ASTM</strong>-P-0108-12 0.025 0.150 0.200 0.130<br />

<strong>ASTM</strong>-P-0108-13 0.005 0.200 0.400 0.150<br />

<strong>ASTM</strong>-P-0108-14 0.170 0.250 0.550 0.110<br />

<strong>ASTM</strong>-P-0108-15 0.100 0.100 0.200 0.200<br />

<strong>ASTM</strong>-P-0108-16 0.010 0.010 0.600 0.250<br />

<strong>ASTM</strong>-P-0108-17 0.000 0.000 0.000 0.000<br />

Organometallic <strong>Standards</strong><br />

for AA, ICP, DCP & XRF Analysis<br />

Designed for<br />

<strong>ASTM</strong> D-4927-96<br />

Lubricating Oil, Elements Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0110-SET $ 2300 / 17 x 100 mL<br />

Ba Ca P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0110-01 0.100 0.600 0.005 0.175 0.060<br />

<strong>ASTM</strong>-P-0110-02 0.175 0.500 0.200 0.050 0.080<br />

<strong>ASTM</strong>-P-0110-03 0.000 0.400 0.150 0.300 0.180<br />

<strong>ASTM</strong>-P-0110-04 0.025 0.260 0.250 0.150 0.120<br />

<strong>ASTM</strong>-P-0110-05 0.150 0.005 0.005 0.450 0.070<br />

<strong>ASTM</strong>-P-0110-06 0.000 0.400 0.025 0.350 0.100<br />

<strong>ASTM</strong>-P-0110-07 0.200 0.300 0.060 0.250 0.120<br />

<strong>ASTM</strong>-P-0110-08 0.000 0.200 0.100 0.450 0.100<br />

<strong>ASTM</strong>-P-0110-09 0.100 0.060 0.080 0.300 0.130<br />

<strong>ASTM</strong>-P-0110-10 0.050 0.060 0.050 0.200 0.050<br />

<strong>ASTM</strong>-P-0110-11 0.075 0.050 0.120 0.100 0.075<br />

<strong>ASTM</strong>-P-0110-12 0.010 0.025 0.150 0.200 0.130<br />

<strong>ASTM</strong>-P-0110-13 0.005 0.005 0.200 0.400 0.150<br />

<strong>ASTM</strong>-P-0110-14 0.000 0.170 0.250 0.550 0.110<br />

<strong>ASTM</strong>-P-0110-15 0.000 0.100 0.100 0.200 0.200<br />

<strong>ASTM</strong>-P-0110-16 0.005 0.010 0.010 0.600 0.250<br />

<strong>ASTM</strong>-P-0110-17 0.000 0.000 0.000 0.000 0.000<br />

Lubricating Oil, Elements Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0112-SET $ 2300 / 16 x 100 mL<br />

Ca Mg P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0112-01 0.600 0.100 0.005 0.175 0.060<br />

<strong>ASTM</strong>-P-0112-02 0.500 0.150 0.200 0.050 0.080<br />

<strong>ASTM</strong>-P-0112-03 0.400 0.350 0.150 0.300 0.180<br />

<strong>ASTM</strong>-P-0112-04 0.260 0.225 0.250 0.150 0.120<br />

<strong>ASTM</strong>-P-0112-05 0.005 0.450 0.005 0.450 0.070<br />

<strong>ASTM</strong>-P-0112-06 0.400 0.500 0.025 0.350 0.100<br />

<strong>ASTM</strong>-P-0112-07 0.300 0.325 0.060 0.250 0.120<br />

<strong>ASTM</strong>-P-0112-08 0.200 0.250 0.100 0.450 0.100<br />

<strong>ASTM</strong>-P-0112-09 0.060 0.100 0.080 0.300 0.130<br />

<strong>ASTM</strong>-P-0112-10 0.060 0.400 0.050 0.200 0.050<br />

<strong>ASTM</strong>-P-0112-11 0.050 0.300 0.120 0.100 0.075<br />

<strong>ASTM</strong>-P-0112-12 0.025 0.200 0.150 0.200 0.130<br />

<strong>ASTM</strong>-P-0112-13 0.005 0.375 0.200 0.400 0.150<br />

<strong>ASTM</strong>-P-0112-14 0.170 0.175 0.250 0.550 0.110<br />

<strong>ASTM</strong>-P-0112-15 0.100 0.425 0.100 0.200 0.200<br />

<strong>ASTM</strong>-P-0112-16 0.010 0.275 0.010 0.600 0.250<br />

<strong>ASTM</strong>-P-0112-17 0.000 0.000 0.000 0.000 0.000<br />

Lubricating Oil, Elements Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0109-SET $ 1600 / 17 x 100 mL<br />

Standard Ca Cl P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0109-01 0.600 0.100 0.005 0.175 0.060<br />

<strong>ASTM</strong>-P-0109-02 0.500 0.000 0.200 0.050 0.080<br />

<strong>ASTM</strong>-P-0109-03 0.400 0.010 0.150 0.300 0.180<br />

<strong>ASTM</strong>-P-0109-04 0.260 0.500 0.250 0.150 0.120<br />

<strong>ASTM</strong>-P-0109-05 0.005 1.000 0.005 0.450 0.070<br />

<strong>ASTM</strong>-P-0109-06 0.400 0.400 0.025 0.350 0.100<br />

<strong>ASTM</strong>-P-0109-07 0.300 0.100 0.060 0.250 0.120<br />

<strong>ASTM</strong>-P-0109-08 0.200 0.010 0.100 0.450 0.100<br />

<strong>ASTM</strong>-P-0109-09 0.060 0.050 0.080 0.300 0.130<br />

<strong>ASTM</strong>-P-0109-10 0.060 0.200 0.050 0.200 0.050<br />

<strong>ASTM</strong>-P-0109-11 0.050 0.500 0.120 0.100 0.075<br />

<strong>ASTM</strong>-P-0109-12 0.025 0.800 0.150 0.200 0.130<br />

<strong>ASTM</strong>-P-0109-13 0.005 1.000 0.200 0.400 0.150<br />

<strong>ASTM</strong>-P-0109-14 0.170 0.600 0.250 0.550 0.110<br />

<strong>ASTM</strong>-P-0109-15 0.100 0.200 0.100 0.200 0.200<br />

<strong>ASTM</strong>-P-0109-16 0.010 0.400 0.010 0.600 0.250<br />

<strong>ASTM</strong>-P-0109-17 0.000 0.000 0.000 0.000 0.000<br />

Lubricating Oil, Elements Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0111-SET $ 2800 / 17 x 100 mL<br />

Ba Ca Cl P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0111-01 0.100 0.600 0.100 0.005 0.175 0.060<br />

<strong>ASTM</strong>-P-0111-02 0.175 0.500 0.000 0.200 0.050 0.080<br />

<strong>ASTM</strong>-P-0111-03 0.000 0.400 0.010 0.150 0.300 0.180<br />

<strong>ASTM</strong>-P-0111-04 0.025 0.260 0.500 0.250 0.150 0.120<br />

<strong>ASTM</strong>-P-0111-05 0.150 0.005 1.000 0.005 0.450 0.070<br />

<strong>ASTM</strong>-P-0111-06 0.000 0.400 0.400 0.025 0.350 0.100<br />

<strong>ASTM</strong>-P-0111-07 0.200 0.300 0.100 0.060 0.250 0.120<br />

<strong>ASTM</strong>-P-0111-08 0.000 0.200 0.010 0.100 0.450 0.100<br />

<strong>ASTM</strong>-P-0111-09 0.100 0.060 0.050 0.080 0.300 0.130<br />

<strong>ASTM</strong>-P-0111-10 0.050 0.060 0.200 0.050 0.200 0.050<br />

<strong>ASTM</strong>-P-0111-11 0.075 0.050 0.500 0.120 0.100 0.075<br />

<strong>ASTM</strong>-P-0111-12 0.010 0.025 0.800 0.150 0.200 0.130<br />

<strong>ASTM</strong>-P-0111-13 0.005 0.005 1.000 0.200 0.400 0.150<br />

<strong>ASTM</strong>-P-0111-14 0.000 0.170 0.600 0.250 0.550 0.110<br />

<strong>ASTM</strong>-P-0111-15 0.000 0.100 0.200 0.100 0.200 0.200<br />

<strong>ASTM</strong>-P-0111-16 0.005 0.010 0.400 0.010 0.600 0.250<br />

<strong>ASTM</strong>-P-0111-17 0.000 0.000 0.000 0.000 0.000 0.000<br />

Lubricating Oil, Elements Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0113-SET $ 2850 / 17 x 100 mL<br />

Ba Ca Mg P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0113-01 0.025 0.600 0.100 0.005 0.175 0.060<br />

<strong>ASTM</strong>-P-0113-02 0.000 0.500 0.150 0.200 0.050 0.080<br />

<strong>ASTM</strong>-P-0113-03 0.100 0.400 0.350 0.150 0.300 0.180<br />

<strong>ASTM</strong>-P-0113-04 0.175 0.260 0.225 0.250 0.150 0.120<br />

<strong>ASTM</strong>-P-0113-05 0.150 0.005 0.450 0.005 0.450 0.070<br />

<strong>ASTM</strong>-P-0113-06 0.000 0.400 0.500 0.025 0.350 0.100<br />

<strong>ASTM</strong>-P-0113-07 0.100 0.300 0.325 0.060 0.250 0.120<br />

<strong>ASTM</strong>-P-0113-08 0.200 0.200 0.250 0.100 0.450 0.100<br />

<strong>ASTM</strong>-P-0113-09 0.050 0.060 0.100 0.080 0.300 0.130<br />

<strong>ASTM</strong>-P-0113-10 0.075 0.060 0.400 0.050 0.200 0.050<br />

<strong>ASTM</strong>-P-0113-11 0.010 0.050 0.300 0.120 0.100 0.075<br />

<strong>ASTM</strong>-P-0113-12 0.000 0.025 0.200 0.150 0.200 0.130<br />

<strong>ASTM</strong>-P-0113-13 0.175 0.005 0.375 0.200 0.400 0.150<br />

<strong>ASTM</strong>-P-0113-14 0.005 0.170 0.175 0.250 0.550 0.110<br />

<strong>ASTM</strong>-P-0113-15 0.000 0.100 0.425 0.100 0.200 0.200<br />

<strong>ASTM</strong>-P-0113-16 0.005 0.010 0.275 0.010 0.600 0.250<br />

<strong>ASTM</strong>-P-0113-17 0.000 0.000 0.000 0.000 0.000 0.000<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

Wear Metals<br />

Designed for<br />

<strong>ASTM</strong> D-4927-96<br />

Designed for <strong>ASTM</strong><br />

D-4628-97 & D-4927-96<br />

63<br />

WEAR METALS<br />

ORGANOMETALLIC<br />

C


Wear Metals<br />

WEAR METALS<br />

ORGANOMETALLIC<br />

C<br />

Lubricating Oil <strong>Standards</strong> Continued<br />

Lubricating Oil, Elements, EDXRF <strong>ASTM</strong> Method<br />

Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0114-SET $ 1900 / 17 x 100 mL<br />

Ca P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0114-01 0.005 0.005 0.050 0.050<br />

<strong>ASTM</strong>-P-0114-02 0.600 0.000 0.000 0.000<br />

<strong>ASTM</strong>-P-0114-03 0.000 0.300 0.000 0.000<br />

<strong>ASTM</strong>-P-0114-04 1.000 0.000 1.000 0.000<br />

<strong>ASTM</strong>-P-0114-05 0.000 0.000 0.000 0.300<br />

<strong>ASTM</strong>-P-0114-06 0.005 0.250 0.800 0.300<br />

<strong>ASTM</strong>-P-0114-07 0.500 0.150 0.500 0.150<br />

<strong>ASTM</strong>-P-0114-08 0.010 0.200 0.100 0.250<br />

<strong>ASTM</strong>-P-0114-09 0.050 0.010 0.400 0.075<br />

<strong>ASTM</strong>-P-0114-10 0.100 0.150 0.200 0.200<br />

<strong>ASTM</strong>-P-0114-11 0.200 0.200 0.800 0.100<br />

<strong>ASTM</strong>-P-0114-12 0.400 0.005 0.800 0.300<br />

<strong>ASTM</strong>-P-0114-13 0.600 0.100 0.500 0.050<br />

<strong>ASTM</strong>-P-0114-14 0.800 0.010 0.050 0.100<br />

<strong>ASTM</strong>-P-0114-15 1.000 0.300 1.000 0.150<br />

<strong>ASTM</strong>-P-0114-16 0.400 0.050 0.600 0.250<br />

<strong>ASTM</strong>-P-0114-17 0.000 0.000 0.000 0.000<br />

Lubricating Oil, Additives Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0116-SET $ 2450 / 11 x 100 mL<br />

Ca P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0116-01 0.500 1.000 0.500 0.500<br />

<strong>ASTM</strong>-P-0116-02 3.000 1.000 3.000 2.000<br />

<strong>ASTM</strong>-P-0116-03 2.000 1.250 1.000 1.500<br />

<strong>ASTM</strong>-P-0116-04 5.000 1.500 0.500 1.200<br />

<strong>ASTM</strong>-P-0116-05 4.000 0.500 1.500 0.750<br />

<strong>ASTM</strong>-P-0116-06 2.500 0.750 4.000 1.000<br />

<strong>ASTM</strong>-P-0116-07 4.000 0.500 2.000 1.250<br />

<strong>ASTM</strong>-P-0116-08 0.500 2.000 5.000 1.000<br />

<strong>ASTM</strong>-P-0116-09 1.000 0.750 2.000 1.500<br />

<strong>ASTM</strong>-P-0116-10 2.500 1.200 3.000 0.500<br />

<strong>ASTM</strong>-P-0116-11 0.000 0.000 0.000 0.000<br />

Organometallic <strong>Standards</strong> for<br />

AA, ICP, DCP & XRF Analysis<br />

Lubricating Oil, Elements, WLXRF <strong>ASTM</strong> Method Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0117-SET $ 2100 / 10 x 100 mL<br />

Ca Cl Cu Mg P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0117-01 0.020 0.030 0.010 0.200 0.250 1.000 0.020<br />

<strong>ASTM</strong>-P-0117-02 0.020 0.020 0.050 0.200 0.020 0.020 0.250<br />

<strong>ASTM</strong>-P-0117-03 0.020 0.200 0.010 0.040 0.250 0.150 0.250<br />

<strong>ASTM</strong>-P-0117-04 0.020 0.200 0.050 0.040 0.020 1.000 0.020<br />

<strong>ASTM</strong>-P-0117-05 0.400 0.020 0.010 0.040 0.020 1.000 0.250<br />

<strong>ASTM</strong>-P-0117-06 0.400 0.020 0.050 0.040 0.250 0.020 0.020<br />

<strong>ASTM</strong>-P-0117-07 0.400 0.200 0.010 0.200 0.020 0.020 0.050<br />

<strong>ASTM</strong>-P-0117-08 0.400 0.200 0.050 0.200 0.250 1.000 0.250<br />

<strong>ASTM</strong>-P-0117-09 0.200 0.100 0.025 0.080 0.150 0.500 0.100<br />

<strong>ASTM</strong>-P-0117-10 0.000 0.000 0.000 0.000 0.000 0.000 0.000<br />

Lubricating Oil, Elements Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0115-SET $ 2300 / 17 x 100 mL<br />

Ca P S Zn Mg<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0115-01 0.005 0.005 0.050 0.050 0.100<br />

<strong>ASTM</strong>-P-0115-02 0.600 0.000 0.000 0.000 0.150<br />

<strong>ASTM</strong>-P-0115-03 0.000 0.300 0.000 0.000 0.350<br />

<strong>ASTM</strong>-P-0115-04 1.000 0.000 1.000 0.000 .0225<br />

<strong>ASTM</strong>-P-0115-05 0.000 0.000 0.000 0.300 0.450<br />

<strong>ASTM</strong>-P-0115-06 0.005 0.250 0.800 0.300 0.500<br />

<strong>ASTM</strong>-P-0115-07 0.500 0.150 0.500 0.150 0.325<br />

<strong>ASTM</strong>-P-0115-08 0.010 0.200 0.100 0.250 0.250<br />

<strong>ASTM</strong>-P-0115-09 0.050 0.010 0.400 0.075 0.050<br />

<strong>ASTM</strong>-P-0115-10 0.100 0.150 0.200 0.200 0.400<br />

<strong>ASTM</strong>-P-0115-11 0.200 0.200 0.800 0.100 0.300<br />

<strong>ASTM</strong>-P-0115-12 0.400 0.005 0.800 0.300 0.200<br />

<strong>ASTM</strong>-P-0115-13 0.600 0.100 0.500 0.050 0.375<br />

<strong>ASTM</strong>-P-0115-14 0.800 0.010 0.050 0.100 0.175<br />

<strong>ASTM</strong>-P-0115-15 1.000 0.300 1.000 .0150 0.425<br />

<strong>ASTM</strong>-P-0115-16 0.400 0.050 0.600 0.250 0.275<br />

<strong>ASTM</strong>-P-0115-17 0.000 0.000 0.000 0.000 0.000<br />

Lubricating Oil, Elements, WLXRF <strong>ASTM</strong> Method Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0118-SET $ 2400 / 10 x 100 mL<br />

Ba Ca Cl Cu Mg P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0118-01 0.020 0.020 0.030 0.010 0.200 0.250 1.000 0.020<br />

<strong>ASTM</strong>-P-0118-02 0.250 0.020 0.020 0.050 0.200 0.020 0.020 0.250<br />

<strong>ASTM</strong>-P-0118-03 0.020 0.020 0.200 0.010 0.040 0.250 0.150 0.250<br />

<strong>ASTM</strong>-P-0118-04 0.250 0.020 0.200 0.050 0.040 0.020 1.000 0.020<br />

<strong>ASTM</strong>-P-0118-05 0.020 0.400 0.020 0.010 0.040 0.020 1.000 0.250<br />

<strong>ASTM</strong>-P-0118-06 0.250 0.400 0.020 0.050 0.040 0.250 0.020 0.020<br />

<strong>ASTM</strong>-P-0118-07 0.020 0.400 0.200 0.010 0.200 0.020 0.020 0.050<br />

<strong>ASTM</strong>-P-0118-08 0.250 0.400 0.200 0.050 0.200 0.250 1.000 0.250<br />

<strong>ASTM</strong>-P-0118-09 0.130 0.200 0.100 0.025 0.080 0.150 0.500 0.100<br />

<strong>ASTM</strong>-P-0118-10 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000<br />

64<br />

Designed for<br />

<strong>ASTM</strong> D-6481-99<br />

Designed for<br />

<strong>ASTM</strong> D-6443-99<br />

Designed for <strong>ASTM</strong><br />

D-4628-97, D-4927-96<br />

D-4951-96, D-6443-99<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


Organometallic <strong>Standards</strong> for<br />

AA, ICP, DCP & XRF Analysis<br />

Lubricating Oil <strong>Standards</strong> Continued<br />

Lubricating Oil, Elements Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0119-SET $ 2900 / 22 x 100 mL<br />

Ca Cl Cu Mg P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0119-01 0.300 0.080 0.030 0.060 0.060 0.275 0.060<br />

<strong>ASTM</strong>-P-0119-02 0.250 0.100 0.000 0.010 0.150 0.000 0.150<br />

<strong>ASTM</strong>-P-0119-03 0.500 0.000 0.035 0.160 0.150 0.000 0.020<br />

<strong>ASTM</strong>-P-0119-04 0.350 0.010 0.000 0.120 0.080 0.200 0.000<br />

<strong>ASTM</strong>-P-0119-05 0.110 0.000 0.015 0.100 0.100 0.300 0.050<br />

<strong>ASTM</strong>-P-0119-06 0.200 0.100 0.000 0.200 0.050 0.250 0.150<br />

<strong>ASTM</strong>-P-0119-07 0.000 0.050 0.025 0.000 0.000 0.450 0.020<br />

<strong>ASTM</strong>-P-0119-08 0.150 0.030 0.000 0.100 0.030 0.400 0.040<br />

<strong>ASTM</strong>-P-0119-09 0.250 0.150 0.010 0.160 0.000 0.350 0.080<br />

<strong>ASTM</strong>-P-0119-10 0.110 0.150 0.040 0.005 0.030 0.750 0.150<br />

<strong>ASTM</strong>-P-0119-11 0.260 0.050 0.000 0.000 0.000 0.750 0.000<br />

<strong>ASTM</strong>-P-0119-12 0.200 0.000 0.005 0.140 0.080 0.500 0.080<br />

<strong>ASTM</strong>-P-0119-13 0.000 0.000 0.005 0.020 0.020 0.200 0.020<br />

<strong>ASTM</strong>-P-0119-14 0.070 0.150 0.020 0.080 0.140 0.650 0.150<br />

<strong>ASTM</strong>-P-0119-15 0.050 0.000 0.000 0.000 0.150 0.000 0.000<br />

<strong>ASTM</strong>-P-0119-16 0.400 0.000 0.001 0.080 0.000 0.500 0.020<br />

<strong>ASTM</strong>-P-0119-17 0.180 0.020 0.020 0.000 0.020 0.600 0.060<br />

<strong>ASTM</strong>-P-0119-18 0.400 0.010 0.001 0.010 0.020 0.000 0.000<br />

<strong>ASTM</strong>-P-0119-19 0.010 0.020 0.040 0.010 0.020 0.200 0.100<br />

<strong>ASTM</strong>-P-0119-20 0.050 0.005 0.050 0.000 0.008 0.000 0.120<br />

<strong>ASTM</strong>-P-0119-21 0.200 0.050 0.020 0.080 0.050 0.275 0.050<br />

<strong>ASTM</strong>-P-0119-22 0.000 0.000 0.000 0.000 0.000 0.000 0.000<br />

Lubricating Oil, Elements Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0120-SET $ 3100 / 23 x 100 mL<br />

Ba Ca Cl Cu Mg P S Zn<br />

Cat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0120-01 0.100 0.300 0.080 0.030 0.060 0.060 0.275 0.060<br />

<strong>ASTM</strong>-P-0120-02 0.175 0.250 0.100 0.000 0.010 0.150 0.000 0.150<br />

<strong>ASTM</strong>-P-0120-03 0.040 0.500 0.000 0.035 0.160 0.150 0.000 0.020<br />

<strong>ASTM</strong>-P-0120-04 0.020 0.350 0.010 0.000 0.120 0.080 0.200 0.000<br />

<strong>ASTM</strong>-P-0120-05 0.150 0.110 0.000 0.015 0.100 0.100 0.300 0.050<br />

<strong>ASTM</strong>-P-0120-06 0.000 0.200 0.100 0.000 0.200 0.050 0.250 0.150<br />

<strong>ASTM</strong>-P-0120-07 0.200 0.000 0.050 0.025 0.000 0.000 0.450 0.020<br />

<strong>ASTM</strong>-P-0120-08 0.000 0.150 0.030 0.000 0.100 0.030 0.400 0.040<br />

<strong>ASTM</strong>-P-0120-09 0.000 0.250 0.150 0.010 0.160 0.000 0.350 0.080<br />

<strong>ASTM</strong>-P-0120-10 0.000 0.110 0.150 0.040 0.005 0.030 0.750 0.150<br />

<strong>ASTM</strong>-P-0120-11 0.100 0.260 0.050 0.000 0.000 0.000 0.750 0.000<br />

<strong>ASTM</strong>-P-0120-12 0.050 0.200 0.000 0.005 0.140 0.080 0.500 0.080<br />

<strong>ASTM</strong>-P-0120-13 0.000 0.000 0.000 0.005 0.020 0.020 0.200 0.020<br />

<strong>ASTM</strong>-P-0120-14 0.080 0.070 0.150 0.020 0.080 0.140 0.650 0.150<br />

<strong>ASTM</strong>-P-0120-15 0.010 0.050 0.000 0.000 0.000 0.150 0.000 0.000<br />

<strong>ASTM</strong>-P-0120-16 0.000 0.400 0.000 0.001 0.080 0.000 0.500 0.020<br />

<strong>ASTM</strong>-P-0120-17 0.000 0.180 0.020 0.020 0.000 0.020 0.600 0.060<br />

<strong>ASTM</strong>-P-0120-18 0.000 0.400 0.010 0.001 0.010 0.020 0.000 0.000<br />

<strong>ASTM</strong>-P-0120-19 0.150 0.010 0.020 0.040 0.010 0.020 0.200 0.100<br />

<strong>ASTM</strong>-P-0120-20 0.005 0.050 0.005 0.050 0.000 0.008 0.000 0.120<br />

<strong>ASTM</strong>-P-0120-21 0.100 0.200 0.050 0.020 0.080 0.050 0.275 0.050<br />

<strong>ASTM</strong>-P-0120-22 0.120 0.200 0.000 0.000 0.000 0.000 0.750 0.000<br />

<strong>ASTM</strong>-P-0120-23 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000<br />

Metal Working Fluids<br />

Metal Working Fluid Wt.% (Nominal Value) listed below<br />

<strong>ASTM</strong>-P-0121-SET $ 1300 / 13 x 100 mL<br />

Standard Cl P S<br />

No. (Wt.%) (Wt.%) (Wt.%)<br />

<strong>ASTM</strong>-P-0121-01 0.000 0.000 0.000<br />

<strong>ASTM</strong>-P-0121-02 0.750 0.025 0.500<br />

<strong>ASTM</strong>-P-0121-03 0.050 0.100 3.000<br />

<strong>ASTM</strong>-P-0121-04 1.000 0.500 2.500<br />

<strong>ASTM</strong>-P-0121-05 0.100 0.005 2.000<br />

<strong>ASTM</strong>-P-0121-06 1.500 0.200 1.000<br />

<strong>ASTM</strong>-P-0121-07 2.000 0.005 3.000<br />

<strong>ASTM</strong>-P-0121-08 1.000 0.050 0.100<br />

<strong>ASTM</strong>-P-0121-09 0.500 0.400 0.000<br />

<strong>ASTM</strong>-P-0121-10 2.000 0.200 1.500<br />

<strong>ASTM</strong>-P-0121-11 0.000 0.500 1.500<br />

<strong>ASTM</strong>-P-0121-12 1.250 0.010 0.050<br />

<strong>ASTM</strong>-P-0121-13 0.050 0.300 0.050<br />

Stabilization Solutions<br />

The solutions were specifically<br />

designed for chelating and<br />

solubilizing the organometallic line<br />

of solids and solutions for single<br />

and multi-element standards.<br />

Stabilizer Solutions A<br />

<strong>ASTM</strong>-P-0122-0.5 $ 80 / 50 mL<br />

<strong>ASTM</strong>-P-0122-1 $ 120 / 100 mL<br />

Stabilizer Solutions B<br />

<strong>ASTM</strong>-P-0123-0.5 $ 80 / 50 mL<br />

<strong>ASTM</strong>-P-0123-1 $ 120 / 100 mL<br />

(use in conjunction with stabilizer solution A)<br />

Designed for <strong>ASTM</strong><br />

D-4628-97, D-4927-96<br />

D-4951-96, D-6443-99<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

Technical Note<br />

Concentration for the sets on pages<br />

62-65 are targets. Actual production<br />

lots may vary.<br />

Wear Metals<br />

65<br />

ORGANOMETALLIC<br />

C


Wear Metals<br />

ORGANOMETALLIC<br />

C<br />

Proposed <strong>ASTM</strong> Method Trace Metals Phosphorous, Sulfur, Calcium, & Zinc in Lubrication Oils by XRF<br />

<strong>ASTM</strong>-P-0090-SET $ 1600 / 16 x 4 oz.<br />

The Organo Tin standards shown below were developed in response to concerns about Organo Tin as an endocrine disrupter. Organo Tin<br />

compounds such as Tributyl Tin were used as marine antifouling agents and Triphenyl Tin as a crop pesticide.<br />

Organo Tin Analysis Sample Extraction, Derivatization & Cleanup with Analysis by Flame-Photometric Detector<br />

Butyltin Chloride Standard<br />

OMT-001 $ 40 / 1 x 1 mL<br />

OMT-001-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

2000 µg/mL each in CH2Cl2 4 comps.<br />

66<br />

Butyltin trichloride<br />

Dibutyltin dichloride<br />

Diphenyltin dichloride<br />

Phenyltin trichloride<br />

Tetrabutyltin<br />

Tributyltin chloride<br />

Phenyltin Chloride Standard<br />

OMT-002 $ 40 / 1 x 1 mL<br />

OMT-002-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

2000 µg/mL each in CH2Cl2 4 comps.<br />

Tetraphenyltin<br />

Triphenyltin chloride<br />

Petrochemical <strong>Standards</strong><br />

Cat. No. Calcium Phosphorus Sulfur Zinc Unit Price<br />

Wt.% Wt.% Wt.% Wt.%<br />

<strong>ASTM</strong>-P-0090-01 0 0 0 0 4 oz. $ 200<br />

<strong>ASTM</strong>-P-0090-02 0 0.02 0.3 0.175 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-03 0.005 0 0.55 0.14 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-04 0.025 0.175 0.35 0.1 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-05 0.05 0.15 0.2 0.2 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-06 0.075 0.225 0.5 0.15 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-07 0.1 0.01 0.45 0.25 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-08 0.1 0.125 0.6 0.06 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-09 0.15 0.1 0.25 0.089 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-10 0.2 0.008 0.075 0.12 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-11 0.25 0.05 0.125 0 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-12 0.3 0.06 0.1 0.13 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-13 0.35 0.004 0.4 0.11 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-14 0.4 0.2 0.175 0.05 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-15 0.5 0.03 0.15 0.07 4 oz. 200<br />

<strong>ASTM</strong>-P-0090-16 0.6 0.005 0.05 0.08 4 oz. 200<br />

Proposed <strong>ASTM</strong> Method for Chlorine in Lube Oils Chlorine in Lube Oils<br />

<strong>ASTM</strong>-P-0092-SET $ 400 / 7 x 4 oz.<br />

Cat. No. Chlorine Chlorine Unit Price<br />

Wt. % µg/g<br />

<strong>ASTM</strong>-P-0092-BL Blank Blank 4 oz. $ 10<br />

<strong>ASTM</strong>-P-0092-0.1X 0.001 10 4 oz. 75<br />

<strong>ASTM</strong>-P-0092-1X 0.01 100 4 oz. 75<br />

<strong>ASTM</strong>-P-0092-5X 0.05 500 4 oz. 75<br />

<strong>ASTM</strong>-P-0092-10X 0.1 1,000 4 oz. 75<br />

<strong>ASTM</strong>-P-0092-100X 1 10,000 4 oz. 75<br />

<strong>ASTM</strong>-P-0092-500X 5 50,000 4 oz. 75<br />

Tri-n-propyltin Chloride<br />

Surrogate Standard<br />

OMT-003 $ 30 / 1 x 1 mL<br />

OMT-003-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

2000 µg/mL in CH 2Cl 2<br />

Tri-n-propyltin chloride<br />

Tripentyltin Chloride<br />

Surrogate Standard<br />

OMT-004 $ 30 / 1 x 1 mL<br />

OMT-004-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

2000 µg/mL in CH 2Cl 2<br />

Tripentyltin chloride<br />

Tetra-n-propyltin chloride<br />

Internal Standard<br />

OMT-005 $ 40 / 1 x 1 mL<br />

OMT-005-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

2000 µg/mL in CH 2Cl 2<br />

Tetra-n-propyl tin chloride<br />

Tetrapentyltin Chloride<br />

Internal Standard<br />

OMT-006 $ 30 / 1 x 1 mL<br />

OMT-006-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

2000 µg/mL in CH 2Cl 2<br />

Tetrapentyltin chloride<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


Inorganic <strong>Standards</strong><br />

Used for influent and effluent monitoring in aqueous matrices by <strong>ASTM</strong> and other EPA Methods in<br />

the Petrochemical Industry.<br />

•Formulated from High Purity Starting Materials, Water & Acids<br />

• Concentration verified by Wet Chemical & Instrumental Analysis<br />

• Certificate of Analysis provided with each Standard<br />

• Actual Lot Analysis provided on label & Certificate of Analysis<br />

• Packaged in specially prepared pre-cleaned bottles<br />

• 18 Month Stability Dating<br />

All NoHaz products come as kits including<br />

20 mL of concentrate, pre-cleaned and prelabeled<br />

dilution bottle, instructions and<br />

Certificate of Analysis<br />

Empty<br />

Pre-Washed<br />

500 mL<br />

Bottle<br />

ICP, ICP/MS, AA, Ion Chrom<br />

Traceable to NIST Reference Materials<br />

Stop Paying Hazardous Shipping Fees!<br />

AccuNoHaz<br />

20 mL<br />

Concentrate<br />

HAZ<br />

FEE<br />

Inorganic Petrochemical<br />

Reference <strong>Standards</strong><br />

page<br />

ICP 68-71<br />

IPC/MS 72<br />

AA 73-75<br />

Ion Chrom 76-79<br />

ICP<br />

69 elements at 10K µg/mL &<br />

59 elements at 25K µg/mL<br />

see pages 68-71<br />

AA<br />

69 elements at 10K µg/mL &<br />

59 elements at 25K µg/mL<br />

see pages 73-75<br />

20 mL meets the Excepted Quantity rule under DOT & IATA regulations which<br />

do not require hazardous shipping fees.<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

INO<br />

67<br />

INORGANIC


ICP<br />

68<br />

ICP Single Element <strong>Standards</strong><br />

Plasma Emission Spectroscopy<br />

Element<br />

Starting Mat'l 1000 µg/mL 10,000 µg/mL<br />

Matrix Unit Cat. No. Price Cat. No. Price<br />

NoHaz Package (No Hazardous Charges) *<br />

10,000 µg/mL 25,000 µg/mL<br />

Cat. No. Price Cat. No. Price<br />

Aluminum 20 mL ------ -- ------ -- ICP-01N-10X-20ML $ 37 ICP-01N-25X-20ML $ 70<br />

Al(NO 3) 3 • 9H 2O 50 mL ------ -- ICP-01N-0.5-10X $ 34 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-01N-1 $ 34 ICP-01N-1-10X 59 ------ -- ------ --<br />

500 mL ICP-01N-5 67 ICP-01N-5-10X 175 ------ -- ------ --<br />

Antimony 20 mL ------ -- ------ -- ICP-02N-10X-20ML 37 ------ --<br />

Sb 50 mL ------ -- ICP-02N-0.5-10X 36 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-02N-1 34 ICP-02N-1-10X 65 ------ -- ------ --<br />

500 mL ICP-02N-5 67 ICP-02N-5-10X 135 ------ -- ------ --<br />

Arsenic 20 mL ------ -- ------ -- ICP-03N-10X-20ML 37 ICP-03N-25X-20ML 70<br />

As 50 mL ------ -- ICP-03N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-03N-1 34 ICP-03N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-03N-5 67 ICP-03N-5-10X 120 ------ -- ------ --<br />

Barium 20 mL ------ -- ------ -- ICP-04N-10X-20ML 37 ICP-04N-25X-20ML 70<br />

Ba(NO 3) 2 50 mL ------ -- ICP-04N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-04N-1 34 ICP-04N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-04N-5 67 ICP-04N-5-10X 120 ------ -- ------ --<br />

Beryllium 20 mL ------ -- ------ -- ICP-05N-10X-20ML 37 ------ --<br />

BeO(C 2H 3O 2) 6 50 mL ------ -- ICP-05N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-05N-1 34 ICP-05N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-05N-5 67 ICP-05N-5-10X 240 ------ -- ------ --<br />

Bismuth 20 mL ------ -- ------ -- ICP-06N-10X-20ML 37 ICP-06N-25X-20ML 70<br />

Bi 50 mL ------ -- ICP-06N-0.5-10X 36 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-06N-1 34 ICP-06N-1-10X 65 ------ -- ------ --<br />

500 mL ICP-06N-5 67 ICP-06N-5-10X 135 ------ -- ------ --<br />

Boron 20 mL ------ -- ------ -- ICP-07W-10X-20ML 37 ------ --<br />

H 3BO 3 50 mL ------ -- ICP-07W-0.5-10X 32 ------ -- ------ --<br />

Water tr. NH4OH 100 mL ICP-07W-1 34 ICP-07W-1-10X 54 ------ -- ------ --<br />

500 mL ICP-07W-5 67 ICP-07W-5-10X 120 ------ -- ------ --<br />

Cadmium 20 mL ------ -- ------ -- ICP-08N-10X-20ML 37 ICP-08N-25X-20ML 70<br />

Cd 50 mL ------ -- ICP-08N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-08N-1 34 ICP-08N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-08N-5 67 ICP-08N-5-10X 120 ------ -- ------ --<br />

Calcium 20 mL ------ -- ------ -- ICP-09N-10X-20ML 37 ICP-09N-25X-20ML 70<br />

CaCO 3 50 mL ------ -- ICP-09N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-09N-1 34 ICP-09N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-09N-5 67 ICP-09N-5-10X 120 ------ -- ------ --<br />

Cerium 20 mL ------ -- ------ -- ICP-11N-10X-20ML 37 ICP-11N-25X-20ML 80<br />

Ce(NO 3) 3 50 mL ------ -- ICP-11N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-11N-1 34 ICP-11N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-11N-5 67 ICP-11N-5-10X 168 ------ -- ------ --<br />

Cesium 20 mL ------ -- ------ -- ICP-12N-10X-20ML 55 ICP-12N-25X-20ML 100<br />

CsNO 3 50 mL ------ -- ICP-12N-0.5-10X 45 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-12N-1 42 ICP-12N-1-10X 75 ------ -- ------ --<br />

500 mL ICP-12N-5 82 ICP-12N-5-10X 231 ------ -- ------ --<br />

Chromium 20 mL ------ -- ------ -- ICP-13N-10X-20ML 37 ICP-13N-25X-20ML 70<br />

reduced to (+3) state 50 mL ------ -- ICP-13N-0.5-10X 34 ------ -- ------ --<br />

(NH 4) 2Cr 2O 7 100 mL ICP-13N-1 34 ICP-13N-1-10X 59 ------ -- ------ --<br />

2-5% Nitric acid 500 mL ICP-13N-5 67 ICP-13N-5-10X 125 ------ -- ------ --<br />

Chromium 50 mL -------------- ICP-13H-0.5-10X 34 ICP-13H-0.5-10X 34 ------ -reduced<br />

to (+3) state 100 mL ICP-13H-1 34 ICP-13H-1-10X 59 ------ -- ------ --<br />

Cr 500 mL ICP-13H-5 67 ICP-13H-5-10X 125 ------ -- ------ --<br />

2-5% Nitric acid<br />

Cobalt 20 mL ------ -- ------ -- ICP-14N-10X-20ML 37 ICP-14N-25X-20ML 70<br />

Co 50 mL ------ -- ICP-14N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-14N-1 34 ICP-14N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-14N-5 67 ICP-14N-5-10X 168 ------ -- ------ --<br />

Copper 20 mL ------ -- ------ -- ICP-15N-10X-20ML 37 ICP-15N-25X-20ML 70<br />

Cu 50 mL ------ -- ICP-15N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-15N-1 34 ICP-15N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-15N-5 67 ICP-15N-5-10X 120 ------ -- ------ --<br />

Dysprosium 20 mL ------ -- ------ -- ICP-16N-10X-20ML 55 ICP-16N-25X-20ML 100<br />

Dy 2O 3 50 mL ------ -- ICP-16N-0.5-10X 45 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-16N-1 42 ICP-16N-1-10X 75 ------ -- ------ --<br />

500 mL ICP-16N-5 82 ICP-16N-5-10X 231 ------ -- ------ --<br />

Erbium 20 mL ------ -- ------ -- ICP-17N-10X-20ML 55 ICP-17N-25X-20ML 100<br />

Er 2O 3 50 mL ------ -- ICP-17N-0.5-10X 52 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-17N-1 42 ICP-17N-1-10X 85 ------ -- ------ --<br />

500 mL ICP-17N-5 82 ICP-17N-5-10X 259 ------ -- ------ --<br />

Europium 20 mL ------ -- ------ -- ICP-18N-10X-20ML 55 ICP-18N-25X-20ML 100<br />

Eu 2O 3 50 mL ------ -- ICP-18N-0.5-10X 52 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-18N-1 42 ICP-18N-1-10X 85 ------ -- ------ --<br />

500 mL ICP-18N-5 82 ICP-18N-5-10X 185 ------ -- ------ --<br />

Gadolinium 20 mL ------ -- ------ -- ICP-19N-10X-20ML 55 ICP-19N-25X-20ML 100<br />

Gd 2O 3 50 mL ------ -- ICP-19N-0.5-10X 69 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-19N-1 42 ICP-19N-1-10X 115 ------ -- ------ --<br />

500 mL ICP-19N-5 82 ICP-19N-5-10X 315 ------ -- ------ --<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


ICP Single Element <strong>Standards</strong><br />

Plasma Emission Spectroscopy<br />

Element<br />

Starting Mat'l 1000 µg/mL 10,000 µg/mL<br />

Matrix Unit Cat. No. Price Cat. No. Price<br />

* see page 67 for details<br />

NoHaz Package (No Hazardous Charges) *<br />

10,000 µg/mL 25,000 µg/mL<br />

Cat. No. Price Cat. No. Price<br />

Gallium 20 mL ------ -- ------ -- ICP-20N-10X-20ML $ 55 ------ --<br />

Ga 50 mL ------ -- ICP-20N-0.5-10X $ 45 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-20N-1 $ 42 ICP-20N-1-10X 75 ------ -- ------ --<br />

500 mL ICP-20N-5 82 ICP-20N-5-10X 165 ------ -- ------ --<br />

Germanium 20 mL ------ -- ------ -- ICP-21W-10X-20ML 55 ------ --<br />

(NH 4) 2GeF 6 50 mL ------ -- ICP-21W-0.5-10X 52 ------ -- ------ --<br />

Water tr. HF 100 mL ICP-21W-1 42 ICP-21W-1-10X 85 ------ -- ------ --<br />

500 mL ICP-21W-5 82 ICP-21W-5-10X 231 ------ -- ------ --<br />

Gold 20 mL ------ -- ------ -- ICP-22H-10X-20ML 95 ICP-22H-25X-20ML $ 165<br />

Au 50 mL ------ -- ICP-22H-0.5-10X 175 ------ -- ------ --<br />

10% HCl (min.) 100 mL ICP-22H-1 78 ICP-22H-1-10X 295 ------ -- ------ --<br />

500 mL ICP-22H-5 152 ICP-22H-5-10X 695 ------ -- ------ --<br />

Hafnium 20 mL ------ -- ------ -- ICP-23N-10X-20ML 75 ICP-23N-25X-20ML 135<br />

HfO 2 50 mL ------ -- ICP-23N-0.5-10X 80 ------ -- ------ --<br />

2-5% Nitric acid tr. HF 100 mL ICP-23N-1 60 ICP-23N-1-10X 135 ------ -- ------ --<br />

500 mL ICP-23N-5 118 ICP-23N-5-10X 364 ------ -- ------ --<br />

Holmium 20 mL ------ -- ------ -- ICP-24N-10X-20ML 55 ICP-24N-25X-20ML 100<br />

Ho 2O 3 50 mL ------ -- ICP-24N-0.5-10X 52 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-24N-1 42 ICP-24N-1-10X 85 ------ -- ------ --<br />

500 mL ICP-24N-5 82 ICP-24N-5-10X 259 ------ -- ------ --<br />

Indium 20 mL ------ -- ------ -- ICP-25N-10X-20ML 55 ICP-25N-25X-20ML 100<br />

In 50 mL ------ -- ICP-25N-0.5-10X 52 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-25N-1 42 ICP-25N-1-10X 85 ------ -- ------ --<br />

500 mL ICP-25N-5 82 ICP-25N-5-10X 185 ------ -- ------ --<br />

Iridium 20 mL ------ -- ------ -- ICP-26H-10X-20ML 95 ICP-26H-25X-20ML 175<br />

IrCl 3 • 3H 20 50 mL ------ -- ICP-26H-0.5-10X 175 ------ -- ------ --<br />

10% HCl (min.) 100 mL ICP-26H-1 78 ICP-26H-1-10X 295 ------ -- ------ --<br />

500 mL ICP-26H-5 152 ICP-26H-5-10X 695 ------ -- ------ --<br />

Iron 20 mL ------ -- ------ -- ICP-27N-10X-20ML 37 ICP-27N-25X-20ML 70<br />

Fe 50 mL ------ -- ICP-27N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-27N-1 34 ICP-27N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-27N-5 67 ICP-27N-5-10X 120 ------ -- ------ --<br />

Lanthanum 20 mL ------ -- ------ -- ICP-28N-10X-20ML 37 ICP-28N-25X-20ML 80<br />

La 2O 3 50 mL ------ -- ICP-28N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-28N-1 34 ICP-28N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-28N-5 67 ICP-28N-5-10X 168 ------ -- ------ --<br />

Lead 20 mL ------ -- ------ -- ICP-29N-10X-20ML 37 ICP-29N-25X-20ML 70<br />

Pb(NO 3) 2 50 mL ------ -- ICP-29N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-29N-1 34 ICP-29N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-29N-5 67 ICP-29N-5-10X 168 ------ -- ------ --<br />

Lithium 20 mL ------ -- ------ -- ICP-30N-10X-20ML 37 ICP-30N-25X-20ML 70<br />

Li 2CO 3 50 mL ------ -- ICP-30N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-30N-1 34 ICP-30N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-30N-5 67 ICP-30N-5-10X 120 ------ -- ------ --<br />

Lutetium 20 mL ------ -- ------ -- ICP-31N-10X-20ML 90 ICP-31N-25X-20ML 300<br />

Lu 2O 3 50 mL ------ -- ICP-31N-0.5-10X 175 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-31N-1 75 ICP-31N-1-10X 295 ------ -- ------ --<br />

500 mL ICP-31N-5 285 ICP-31N-5-10X 1393 ------ -- ------ --<br />

Magnesium 20 mL ------ -- ------ -- ICP-32N-10X-20ML 37 ICP-32N-25X-20ML 70<br />

MgO 50 mL ------ -- ICP-32N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-32N-1 34 ICP-32N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-32N-5 67 ICP-32N-5-10X 120 ------ -- ------ --<br />

Manganese 20 mL ------ -- ------ -- ICP-33N-10X-20ML 37 ICP-33N-25X-20ML 70<br />

Mn(C 2H 3O 2) 2 50 mL ------ -- ICP-33N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-33N-1 34 ICP-33N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-33N-5 67 ICP-33N-5-10X 168 ------ -- ------ --<br />

Mercury 20 mL ------ -- ------ -- ICP-34N-10X-20ML 37 ICP-34N-25X-20ML 70<br />

Hg 50 mL ------ -- ICP-34N-0.5-10X 32 ------ -- ------ --<br />

10% Nitric acid 100 mL ICP-34N-1 34 ICP-34N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-34N-5 67 ICP-34N-5-10X 120 ------ -- ------ --<br />

Molybdenum 20 mL ------ -- ------ -- ICP-35W-10X-20ML 37 ICP-35W-25X-20ML 70<br />

(NH 4) 2MoO 4 50 mL ------ -- ICP-35W-0.5-10X 32 ------ -- ------ --<br />

Water tr. NH 4OH 100 mL ICP-35W-1 34 ICP-35W-1-10X 54 ------ -- ------ --<br />

500 mL ICP-35W-5 67 ICP-35W-5-10 120 ------ -- ------ --<br />

Neodymium 20 mL ------ -- ------ -- ICP-36N-10X-20ML 37 ICP-36N-25X-20ML 80<br />

Nd 2O 3 50 mL ------ -- ICP-36N-0.5-10X 45 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-36N-1 34 ICP-36N-1-10X 75 ------ -- ------ --<br />

500 mL ICP-36N-5 67 ICP-36N-5-10X 203 ------ -- ------ --<br />

Nickel 20 mL ------ -- ------ -- ICP-37N-10X-20ML 37 ICP-37N-25X-20ML 70<br />

Ni 50 mL ------ -- ICP-37N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-37N-1 34 ICP-37N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-37N-5 67 ICP-37N-5-10X 120 ------ -- ------ --<br />

Single Element <strong>Standards</strong> for Plasma Emission Spectroscopy Continued on Next Page<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

69<br />

ICP


ICP<br />

70<br />

ICP Single Element <strong>Standards</strong><br />

Plasma Emission Spectoscopy<br />

Element<br />

Starting Mat'l 1000 µg/mL 10,000 µg/mL<br />

Matrix Unit Cat. No. Price Cat. No. Price<br />

NoHaz Package (No Hazardous Charges) *<br />

10,000 µg/mL 25,000 µg/mL<br />

Cat. No. Price Cat. No. Price<br />

Niobium 20 mL ------ -- ------ -- ICP-38W-10X-20ML $ 37 ICP-38W-25X-20ML $ 80<br />

Nb 2O 5 50 mL ------ -- ICP-38W-0.5-10X $ 38 ------ -- ------ --<br />

Water tr. HF 100 mL ICP-38W-1 $ 34 ICP-38W-1-10X 64 ------ -- ------ --<br />

500 mL ICP-38W-5 67 ICP-38W-5-10X 175 ------ -- ------ --<br />

Palladium 20 mL ------ -- ------ -- ICP-40H-10X-20ML 95 ICP-40H-25X-20ML 165<br />

Pd 50 mL ------ -- ICP-40H-0.5-10X 175 ------ -- ------ --<br />

10% HCl (min.) 100 mL ICP-40H-1 78 ICP-40H-1-10X 295 ------ -- ------ --<br />

500 mL ICP-40H-5 152 ICP-40H-5-10X 973 ------ -- ------ --<br />

Phosphorus 20 mL ------ -- ------ -- ICP-41W-10X-20ML 37 ------ --<br />

NH 4H 2PO 4 50 mL ------ -- ICP-41W-0.5-10X 32 ------ -- ------ --<br />

Water 100 mL ICP-41W-1 34 ICP-41W-1-10X 54 ------ -- ------ --<br />

500 mL ICP-41W-5 67 ICP-41W-5-10X 120 ------ -- ------ --<br />

Platinum 20 mL ------ -- ------ -- ICP-42H-10X-20ML 95 ICP-42H-25X-20ML 165<br />

Pt 50 mL ------ -- ICP-42H-0.5-10X 175 ------ -- ------ --<br />

10% HCl (min.) 100 mL ICP-42H-1 78 ICP-42H-1-10X 295 ------ -- ------ --<br />

500 mL ICP-42H-5 152 ICP-42H-5-10X 695 ------ -- ------ --<br />

Potassium 20 mL ------ -- ------ -- ICP-43N-10X-20ML 37 ICP-43N-25X-20ML 70<br />

KNO 3 50 mL ------ -- ICP-43N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-43N-1 34 ICP-43N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-43N-5 67 ICP-43N-5-10X 120 ------ -- ------ --<br />

Praseodymium 20 mL ------ -- ------ -- ICP-44N-10X-20ML 55 ICP-44N-25X-20ML 100<br />

Pr 6O 11 50 mL ------ -- ICP-44N-0.5-10X 72 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-44N-1 42 ICP-44N-1-10X 120 ------ -- ------ --<br />

500 mL ICP-44N-5 82 ICP-44N-5-10X 329 ------ -- ------ --<br />

Rhenium 20 mL ------ -- ------ -- ICP-45W-10X-20ML 95 ICP-45W-25X-20ML 175<br />

Re 50 mL ------ -- ICP-45W-0.5-10X 175 ------ -- ------ --<br />

Water 100 mL ICP-45W-1 78 ICP-45W-1-10X 295 ------ -- ------ --<br />

500 mL ICP-45W-5 152 ICP-45W-5-10X 695 ------ -- ------ --<br />

Rhodium 20 mL ------ -- ------ -- ICP-46H-10X-20ML 250 ICP-46H-25X-20ML 475<br />

RhCl 3 • 3H 2O 50 mL ------ -- ICP-46H-0.5-10X 315 ------ -- ------ --<br />

10% HCl (min.) 100 mL ICP-46H-1 190 ICP-46H-1-10X 525 ------ -- ------ --<br />

500 mL ICP-46H-5 425 ICP-46H-5-10X 2050 ------ -- ------ --<br />

Rubidium 20 mL ------ -- ------ -- ICP-47N-10X-20ML 37 ICP-47N-25X-20ML 80<br />

RbNO 3 50 mL ------ -- ICP-47N-0.5-10X 52 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-47N-1 36 ICP-47N-1-10X 85 ------ -- ------ --<br />

500 mL ICP-47N-5 70 ICP-47N-5-10X 175 ------ -- ------ --<br />

Ruthenium 20 mL ------ -- ------ -- ICP-48H-10X-20ML 95 ICP-48H-25X-20ML 185<br />

RuCl 3 • 3H 2O 50 mL ------ -- ICP-48H-0.5-10X 175 ------ -- ------ --<br />

10% HCl 100 mL ICP-48H-1 78 ICP-48H-1-10X 295 ------ -- ------ --<br />

500 mL ICP-48H-5 152 ICP-48H-5-10X 695 ------ -- ------ --<br />

Samarium 20 mL ------ -- ------ -- ICP-49N-10X-20ML 55 ICP-49N-25X-20ML 100<br />

Sm 2O 3 50 mL ------ -- ICP-49N-0.5-10X 45 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-49N-1 42 ICP-49N-1-10X 75 ------ -- ------ --<br />

500 mL ICP-49N-5 82 ICP-49N-5-10X 231 ------ -- ------ --<br />

Scandium 20 mL ------ -- ------ -- ICP-50N-10X-20ML 95 ICP-50N-25X-20ML 175<br />

Sc 2O 3 50 mL ------ -- ICP-50N-0.5-10X 175 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-50N-1 78 ICP-50N-1-10X 295 ------ -- ------ --<br />

500 mL ICP-50N-5 152 ICP-50N-5-10X 973 ------ -- ------ --<br />

Selenium 20 mL ------ -- ------ -- ICP-51N-10X-20ML 37 ICP-51N-25X-20ML 70<br />

Se 50 mL ------ -- ICP-51N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-51N-1 34 ICP-51N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-51N-5 67 ICP-51N-5-10X 120 ------ -- ------ --<br />

Silicon 20 mL ------ -- ------ -- ICP-52W-10X-20ML 37 ------ --<br />

(NH 4)2SiF 6 50 mL ------ -- ICP-52W-0.5-10X 32 ------ -- ------ --<br />

Water tr. HF 100 mL ICP-52W-1 34 ICP-52W-1-10X 54 ------ -- ------ --<br />

500 mL ICP-52W-5 67 ICP-52W-5-10X 168 ------ -- ------ --<br />

Silver 20 mL ------ -- ------ -- ICP-53N-10X-20ML 37 ICP-53N-25X-20ML 70<br />

AgNO 3 50 mL ------ -- ICP-53N-0.5-10X 42 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-53N-1 34 ICP-53N-1-10X 70 ------ -- ------ --<br />

500 mL ICP-53N-5 67 ICP-53N-5-10X 145 ------ -- ------ --<br />

Sodium 20 mL ------ -- ------ -- ICP-54N-10X-20ML 37 ICP-54N-25X-20ML 70<br />

NaNO 3 50 mL ------ -- ICP-54N-0.5-10X 34 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-54N-1 34 ICP-54N-1-10X 59 ------ -- ------ --<br />

500 mL ICP-54N-5 67 ICP-54N-5-10X 175 ------ -- ------ --<br />

Strontium 20 mL ------ -- ------ -- ICP-55N-10X-20ML 37 ICP-55N-25X-20ML 70<br />

Sr(NO 3) 2 50 mL ------ -- ICP-55N-0.5-10X 42 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-55N-1 34 ICP-55N-1-10X 70 ------ -- ------ --<br />

500 mL ICP-55N-5 67 ICP-55N-5-10X 203 ------ -- ------ --<br />

Sulfur 20 mL ------ -- ------ -- ICP-56W-10X-20ML 37 ICP-56W-25X-20ML 70<br />

(NH 4) 2SO4 50 mL ------ -- ICP-56W-0.5-10X 32 ------ -- ------ --<br />

Water 100 mL ICP-56W-1 34 ICP-56W-1-10X 54 ------ -- ------ --<br />

500 mL ICP-56W-5 67 ICP-56W-5-10X 120 ------ -- ------ --<br />

Tantalum 20 mL ------ -- ------ -- ICP-57W-10X-20ML 55 ICP-57W-25X-20ML 100<br />

Ta 50 mL ------ -- ICP-57W-0.5-10X 52 ------ -- ------ --<br />

Water tr. HF 100 mL ICP-57W-1 42 ICP-57W-1-10X 85 ------ -- ------ --<br />

500 mL ICP-57W-5 82 ICP-57W-5-10X 224 ------ -- ------ --<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


ICP Single Element <strong>Standards</strong><br />

Plasma Emission Spectroscopy<br />

Element<br />

Starting Mat'l 1000 µg/mL 10,000 µg/mL<br />

Matrix Unit Cat. No. Price Cat. No. Price<br />

NoHaz Package (No Hazardous Charges) *<br />

10,000 µg/mL 25,000 µg/mL<br />

Cat. No. Price Cat. No. Price<br />

Tellurium 20 mL ------ -- ------ -- ICP-58H-10X-20ML $ 37 ------ --<br />

Te 50 mL ------ -- ICP-58H-0.5-10X $ 46 ------ -- ------ --<br />

10% HCl (min.) 100 mL ICP-58H-1 $ 34 ICP-58H-1-10X 78 ------ -- ------ --<br />

500 mL ICP-58H-5 67 ICP-58H-5-10X 210 ------ -- ------ --<br />

Terbium 20 mL ------ -- ------ -- ICP-59N-10X-20ML 55 ICP-59N-25X-20ML $ 100<br />

Tb 4O 7 50 mL ------ -- ICP-59N-0.5-10X 69 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-59N-1 42 ICP-59N-1-10X 115 ------ -- ------ --<br />

500 mL ICP-59N-5 82 ICP-59N-5-10X 315 ------ -- ------ --<br />

Thallium 20 mL ------ -- ------ -- ICP-60N-10X-20ML 37 ICP-60N-25X-20ML 70<br />

Tl 50 mL ------ -- ICP-60N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-60N-1 34 ICP-60N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-60N-5 67 ICP-60N-5-10X 125 ------ -- ------ --<br />

Thorium 100 mL ICP-61N-1 34 ------ -- ------ -- ------ --<br />

Th(NO 3)4 • 4H 2O 500 mL ICP-61N-5 67 ------ -- ------ -- ------ --<br />

2-5% Nitric acid<br />

Thulium 20 mL ------ -- ------ -- ICP-62N-10X-20ML 75 ICP-62N-25X-20ML 135<br />

Tm 2O 3 50 mL ------ -- ICP-62N-0.5-10X 78 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-62N-1 58 ICP-62N-1-10X 130 ------ -- ------ --<br />

500 mL ICP-62N-5 120 ICP-62N-5-10X 250 ------ -- ------ --<br />

Tin ------ -- ICP-63N-10X-20ML 37 ICP-63N-25X-20ML 70<br />

Sn 50 mL -------------- ICP-63N-0.5-10X 42 ------ -- ------ --<br />

2-5% Nitric acid tr. HF 100 mL ICP-63N-1 34 ICP-63N-1-10X 70 ------ -- ------ --<br />

500 mL ICP-63N-5 67 ICP-63N-5-10X 135 ------ -- ------ --<br />

Tin 50 mL -------------- ------ -- ICP-63H-0.5-10X 42 ------ --<br />

Sn 100 mL ICP-63H-1 34 ICP-63H-1-10X 70 ------ -- ------ --<br />

HCl 500 mL ICP-63H-5 67 ICP-63H-5-10X 135 ------ -- ------ --<br />

Titanium 20 mL ------ -- ------ -- ICP-64W-10X-20ML 37 ------ --<br />

(NH 4) 2TiF 6 50 mL ------ -- ICP-64W-0.5-10X 32 ------ -- ------ --<br />

Water tr. HF 100 mL ICP-64W-1 34 ICP-64W-1-10X 54 ------ -- ------ --<br />

500 mL ICP-64W-5 67 ICP-64W-5-10X 120 ------ -- ------ --<br />

Tungsten 20 mL ------ -- ------ -- ICP-65W-10X-20ML 37 ------ --<br />

(NH 4) 2WO 4 50 mL ------ -- ICP-65W-0.5-10X 32 ------ -- ------ --<br />

Water tr. NH 4OH 100 mL ICP-65W-1 34 ICP-65W-1-10X 54 ------ -- ------ --<br />

500 mL ICP-65W-5 67 ICP-65W-5-10X 168 ------ -- ------ --<br />

Uranium 50 mL ------ -- ------ -- ------ -- ------ --<br />

U 3O 8 100 mL ICP-66N-1 42 ------ -- ------ -- ------ --<br />

500 mL ICP-66N-5 82 ------ -- ------ -- ------ --<br />

Vanadium 20 mL ------ -- ------ -- ICP-67N-10X-20ML 37 ICP-67N-25X-20ML 70<br />

NH 4VO 3 50 mL ------ -- ICP-67N-0.5-10X 36 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-67N-1 34 ICP-67N-1-10X 65 ------ -- ------ --<br />

500 mL ICP-67N-5 67 ICP-67N-5-10X 135 ------ -- ------ --<br />

Ytterbium 20 mL ------ -- ------ -- ICP-68N-10X-20ML 55 ICP-68N-25X-20ML 100<br />

Yb 2O 3 50 mL ------ -- ICP-68N-0.5-10X 60 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-68N-1 42 ICP-68N-1-10X 100 ------ -- ------ --<br />

500 mL ICP-68N-5 82 ICP-68N-5-10X 273 ------ -- ------ --<br />

Yttrium 20 mL ------ -- ------ -- ICP-69N-10X-20ML 37 ICP-69N-25X-20ML 70<br />

Y 2O 3 50 mL ------ -- ICP-69N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-69N-1 34 ICP-69N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-69N-5 67 ICP-69N-5-10X 120 ------ -- ------ --<br />

Zinc 20 mL ------ -- ------ -- ICP-70N-10X-20ML 37 ICP-70N-25X-20ML 70<br />

Zn 50 mL ------ -- ICP-70N-0.5-10X 32 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-70N-1 34 ICP-70N-1-10X 54 ------ -- ------ --<br />

500 mL ICP-70N-5 67 ICP-70N-5-10X 120 ------ -- ------ --<br />

Zirconium 20 mL ------ -- ------ -- ICP-71N-10X-20ML 37 ICP-71N-25X-20ML 70<br />

ZrO(NO 3) 2 50 mL ------ -- ICP-71N-0.5-10X 42 ------ -- ------ --<br />

2-5% Nitric acid 100 mL ICP-71N-1 34 ICP-71N-1-10X 70 ------ -- ------ --<br />

500 mL ICP-71N-5 67 ICP-71N-5-10X 203 ------ -- ------ --<br />

Calibration and Matrix Blanks<br />

Nitric Acid Blank<br />

CLP-BLN-5 $ 30 / 500 mL<br />

CLP-BLN-L $ 45 / L (2 x 500 mL)<br />

5% HNO 3 in <strong>ASTM</strong> Type I Water<br />

Hydrochloric Acid Blank<br />

CLP-BLH-5 $ 30 / 500 mL<br />

CLP-BLH-L $ 45 / L (2 x 500 mL)<br />

5% HCl in <strong>ASTM</strong> Type I Water<br />

Mixed Acid Blank<br />

CLP-BLMA-5 $ 30 / 500 mL<br />

CLP-BLMA-L $ 45 / L (2 x 500 mL)<br />

5% HCl + 1% HNO 3 in<br />

<strong>ASTM</strong> Type I Water<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

* see page 67 for details<br />

Water Blank<br />

CLP-BLW-5 $ 30 / 500 mL<br />

$ 40 / L (2 x 500 mL)<br />

<strong>ASTM</strong> Type I Water<br />

71<br />

ICP


ICP/MS<br />

72<br />

ICP/MS Single Element <strong>Standards</strong><br />

Plasma Emission / Mass Spectroscopy<br />

Pure Matrix Special Packaging Traceability to NIST Reference Materials<br />

AccuStandard’s ICP/MS <strong>Standards</strong> are formulated to meet the needs of this very special instrument. As matrix effect is of utmost concern, each<br />

standard is formulated in specially purified de-ionized 18 megohm water and Parts per Trillion acids; after both wet chemical and instrumental<br />

analysis, the standards are packaged in acid leached FLPE containers to provide required protection and, of course, all standards are traceable to<br />

the National Institute of <strong>Standards</strong> and Technology (NIST) weights and Reference Materials.<br />

100 µg/mL Conc. 1,000 µg/mL Conc. 10,000 µg/mL Conc.<br />

Element Matrix Unit Cat. No. Price Cat. No. Price Cat. No. Price<br />

Al (Aluminum) 2% HNO3 100 mL ICP-MS-01N-0.01X-1 $ 34 ICP-MS-01N-0.1X-1 $ 45 ICP-MS-01N-1 $ 76<br />

Sb (Antimony) 2% HNO3 100 mL ICP-MS-02N-0.01X-1 34 ICP-MS-02N-0.1X-1 45 ICP-MS-02N-1 76<br />

As (Arsenic) 2% HNO3 100 mL ICP-MS-03N-0.01X-1 34 ICP-MS-03N-0.1X-1 45 ICP-MS-03N-1 76<br />

Ba (Barium) 2% HNO3 100 mL ICP-MS-04N-0.01X-1 34 ICP-MS-04N-0.1X-1 45 ICP-MS-04N-1 76<br />

Be (Beryllium) 2% HNO3 100 mL ICP-MS-05N-0.01X-1 34 ICP-MS-05N-0.1X-1 45 ICP-MS-05N-1 76<br />

Bi (Bismuth) 2% HNO3 100 mL ICP-MS-06N-0.01X-1 34 ICP-MS-06N-0.1X-1 45 ICP-MS-06N-1 76<br />

Cd (Cadmium) 2% HNO3 100 mL ICP-MS-08N-0.01X-1 34 ICP-MS-08N-0.1X-1 45 ICP-MS-08N-1 76<br />

Ca (Calcium) 2% HNO3 100 mL ICP-MS-09N-0.01X-1 34 ICP-MS-09N-0.1X-1 45 ICP-MS-09N-1 76<br />

Cr (Chromium) 2% HNO3 100 mL ICP-MS-13N-0.01X-1 34 ICP-MS-13N-0.1X-1 45 ICP-MS-13N-1 76<br />

Co (Cobalt) 2% HNO3 100 mL ICP-MS-14N-0.01X-1 34 ICP-MS-14N-0.1X-1 45 ICP-MS-14N-1 76<br />

Cu (Copper) 2% HNO3 100 mL ICP-MS-15N-0.01X-1 34 ICP-MS-15N-0.1X-1 45 ICP-MS-15N-1 76<br />

Ge (Germanium) H2O tr. HF 100 mL ICP-MS-21W-0.01X-1 42 ICP-MS-21W-0.1X-1 53 ICP-MS-21W-1 84<br />

Au (Gold) 10% HCl 100 mL ICP-MS-22H-0.01X-1 78 ICP-MS-22H-0.1X-1 89 ICP-MS-22H-1 120<br />

In (Indium) 2% HNO3 100 mL ICP-MS-25N-0.01X-1 42 ICP-MS-25N-0.1X-1 53 ICP-MS-25N-1 84<br />

Fe (Iron) 5% HNO3 100 mL ICP-MS-27N-0.01X-1 34 ICP-MS-27N-0.1X-1 45 ICP-MS-27N-1 76<br />

Pb (Lead) 2% HNO3 100 mL ICP-MS-29N-0.01X-1 34 ICP-MS-29N-0.1X-1 45 ICP-MS-29N-1 76<br />

Li (Lithium) 2% HNO3 100 mL ICP-MS-30N-0.01X-1 34 ICP-MS-30N-0.1X-1 45 ICP-MS-30N-1 76<br />

Mg (Magnesium) 2% HNO3 100 mL ICP-MS-32N-0.01X-1 34 ICP-MS-32N-0.1X-1 45 ICP-MS-32N-1 76<br />

Mn (Manganese) 2% HNO3 100 mL ICP-MS-33N-0.01X-1 34 ICP-MS-33N-0.1X-1 45 ICP-MS-33N-1 76<br />

Hg (Mercury) 10% HNO3 100 mL ICP-MS-34N-0.01X-1 34 ICP-MS-34N-0.1X-1 45 ICP-MS-34N-1 76<br />

Mo (Molybdenum) H2O tr. NH4OH 100 mL ICP-MS-35W-0.01X-1 34 ICP-MS-35W-0.1X-1 45 ICP-MS-35W-1 76<br />

Ni (Nickel) 2% HNO3 100 mL ICP-MS-37N-0.01X-1 34 ICP-MS-37N-0.1X-1 45 ICP-MS-37N-1 76<br />

P (Phosphorous) H2O 100 mL ICP-MS-41W-0.01X-1 34 ICP-MS-41W-0.1X-1 45 ICP-MS-41W-1 76<br />

K (Potassium) 2% HNO3 100 mL ICP-MS-43N-0.01X-1 34 ICP-MS-43N-0.1X-1 45 ICP-MS-43N-1 76<br />

Rh (Rhodium) 10% HCl 100 mL ICP-MS-46H-0.01X-1 190 ICP-MS-46H-0.1X-1 201 ICP-MS-46H-1 232<br />

Sc (Scandium) 2% HNO3 100 mL ICP-MS-50N-0.01X-1 78 ICP-MS-50N-0.1X-1 89 ICP-MS-50N-1 120<br />

Se (Selenium) 2% HNO3 100 mL ICP-MS-51N-0.01X-1 34 ICP-MS-51N-0.1X-1 45 ICP-MS-51N-1 76<br />

Ag (Silver) 2% HNO3 100 mL ICP-MS-53N-0.01X-1 34 ICP-MS-53N-0.1X-1 45 ICP-MS-53N-1 76<br />

Na (Sodium) 2% HNO3 100 mL ICP-MS-54N-0.01X-1 34 ICP-MS-54N-0.1X-1 45 ICP-MS-54N-1 76<br />

Sr (Strontium) 2% HNO3 100 mL ICP-MS-55N-0.01X-1 34 ICP-MS-55N-0.1X-1 45 ICP-MS-55N-1 76<br />

S (Sulphur) H2O 100 mL ICP-MS-56W-0.01X-1 34 ICP-MS-56W-0.1X-1 45 ICP-MS-56W-1 76<br />

Tb (Terbium) 2% HNO3 100 mL ICP-MS-59N-0.01X-1 42 ICP-MS-59N-0.1X-1 53 ICP-MS-59N-1 84<br />

Tl (Thallium) 2% HNO3 100 mL ICP-MS-60N-0.01X-1 34 ICP-MS-60N-0.1X-1 45 ICP-MS-60N-1 76<br />

Th (Thorium) 2% HNO3 100 mL ICP-MS-61N-0.01X-1 34 ICP-MS-61N-0.1X-1 45 ----------------- ---<br />

Sn (Tin) 2% HNO3 tr HF 100 mL ICP-MS-63N-0.01X-1 34 ICP-MS-63N-0.1X-1 45 ICP-MS-63N-1 76<br />

Ti (Titanium) H2O tr. HF 100 mL ICP-MS-64W-0.01X-1 34 ICP-MS-64W-0.1X-1 45 ICP-MS-64W-1 76<br />

U (Uranium) 2% HNO3 100 mL ICP-MS-66N-0.01X-1 42 ICP-MS-66N-0.1X-1 53 ----------------- ---<br />

V (Vanadium) 2% HNO3 100 mL ICP-MS-67N-0.01X-1 34 ICP-MS-67N-0.1X-1 45 ICP-MS-67N-1 76<br />

Y (Yttrium) 2% HNO3 100 mL ICP-MS-69N-0.01X-1 34 ICP-MS-69N-0.1X-1 45 ICP-MS-69N-1 76<br />

Zn (Zinc) 2% HNO3 100 mL ICP-MS-70N-0.01X-1 34 ICP-MS-70N-0.1X-1 45 ICP-MS-70N-1 76<br />

If you need an element that is not listed above or you require a different matrix, size or<br />

concentration, our experienced chemists will provide you with a custom quotation.<br />

Get exactly what you need.<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


AA Single Element <strong>Standards</strong><br />

Atomic Absorption Spectroscopy<br />

Traceable to NIST Reference Materials<br />

Certificate of Analysis included at No Charge with each Standard<br />

Actual Concentration Analysis<br />

Most available in either Nitric or Hydrochloric acid matrix<br />

ISO 9001 Quality System<br />

Each standard is prepared from high purity starting material, de-ionized water and high purity acids. Every standard is instrumentally assayed<br />

to verify concentration of specified element. Actual Lot Analysis is provided on the label and a Certificate of Analysis is included for ease of<br />

record keeping and availability at audits.<br />

Element<br />

Starting Mat'l 1000 µg/mL<br />

Matrix Unit Cat. No. Price<br />

NoHaz Package (No Hazardous Charges) *<br />

10,000 µg/mL 25,000 µg/mL<br />

Cat. No. Price Cat. No. Price<br />

Aluminum 20 mL ------ -- AA01N-10X-20ML $ 20 AA01N-25X-20ML $ 37<br />

2-5% Nitric acid 100 mL AA01N-1 $ 13 ------ -- ------ --<br />

500 mL AA01N-5 33 ------ -- ------ --<br />

Antimony 20 mL ------ -- AA02W-10X-20ML 20 ------ --<br />

H 2O tr. HNO 3 tr. 100 mL AA02N-1 13 ------ -- ------ --<br />

Tartaric acid 500 mL AA02N-5 33 ------ -- ------ --<br />

Arsenic 20 mL ------ -- AA03N-10X-20ML 20 AA03N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA03N-1 13 ------ -- ------ --<br />

500 mL AA03N-5 33 ------ -- ------ --<br />

Barium 20 mL ------ -- AA04N-10X-20ML 20 AA04N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA04N-1 12 ------ -- ------ --<br />

500 mL AA04N-5 30 ------ -- ------ --<br />

Beryllium 20 mL ------ -- AA05N-10X-20ML 20 ------ --<br />

2-5% Nitric acid 100 mL AA05N-1 19 ------ -- ------ --<br />

500 mL AA05N-5 48 ------ -- ------ --<br />

Bismuth 20 mL ------ -- AA06N-10X-20ML 20 AA06N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA06N-1 13 ------ -- ------ --<br />

500 mL AA06N-5 33 ------ -- ------ --<br />

Boron 20 mL ------ -- AA07W-10X-20ML 20 ------ --<br />

Water tr. NH 4OH 100 mL AA07W-1 13 ------ -- ------ --<br />

500 mL AA07W-5 33 ------ -- ------ --<br />

Cadmium 20 mL ------ -- AA08N-10X-20ML 20 AA08N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA08N-1 13 ------ -- ------ --<br />

500 mL AA08N-5 33 ------ -- ------ --<br />

Calcium 20 mL ------ -- AA09N-10X-20ML 20 AA09N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA09N-1 12 ------ -- ------ --<br />

500 mL AA09N-5 30 ------ -- ------ --<br />

Cerium 20 mL ------ -- AA11N-10X-20ML 20 AA11N-25X-20ML 45<br />

2-5% Nitric acid 100 mL AA11N-1 18 ------ -- ------ --<br />

500 mL AA11N-5 40 ------ -- ------ --<br />

Cesium 20 mL ------ -- AA12N-10X-20ML 35 AA12N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA12N-1 15 ------ -- ------ --<br />

500 mL AA12N-5 36 ------ -- ------ --<br />

Chromium 20 mL ------ -- AA13N-10X-20ML 20 AA13N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA13N-1 12 ------ -- ------ --<br />

500 mL AA13N-5 30 ------ -- ------ --<br />

Cobalt 20 mL ------ -- AA14N-10X-20ML 20 AA14N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA14N-1 12 ------ -- ------ --<br />

500 mL AA14N-5 30 ------ -- ------ --<br />

Copper 20 mL ------ -- AA15N-10X-20ML 20 AA15N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA15N-1 12 ------ -- ------ --<br />

500 mL AA15N-5 30 ------ -- ------ --<br />

Dysprosium 20 mL ------ -- AA16N-10X-20ML 35 AA16N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA16N-1 20 ------ -- ------ --<br />

500 mL AA16N-5 45 ------ -- ------ --<br />

Erbium 20 mL ------ -- AA17N-10X-20ML 35 AA17N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA17N-1 20 ------ -- ------ --<br />

500 mL AA17N-5 45 ------ -- ------ --<br />

Europium 20 mL ------ -- AA18N-10X-20ML 35 AA18N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA18N-1 20 ------ -- ------ --<br />

500 mL AA18N-5 45 ------ -- ------ --<br />

Gadolinium 20 mL ------ -- AA19N-10X-20ML 35 AA19N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA19N-1 20 ------ -- ------ --<br />

500 mL AA19N-5 45 ------ -- ------ --<br />

Gallium 20 mL ------ -- AA20N-10X-20ML 45 ------ --<br />

2-5% Nitric acid 100 mL AA20N-1 15 ------ -- ------ --<br />

500 mL AA20N-5 36 ------ -- ------ --<br />

Germanium 20 mL ------ -- AA21W-10X-20ML 35 ------ --<br />

Water tr. HF 100 mL AA21W-1 18 ------ -- ------ --<br />

500 mL AA21W-5 40 ------ -- ------ --<br />

Gold 20 mL ------ -- AA22H-10X-20ML 80 AA22H-25X-20ML 200<br />

10% HCl (min.) 100 mL AA22H-1 66 ------ -- ------ --<br />

500 mL AA22H-5 179 ------ -- ------ --<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

* see page 67<br />

for details<br />

For your convenience<br />

these elements are also<br />

available in Other<br />

Matrices.<br />

Contact Technical<br />

Service for more info<br />

73<br />

AA


AA<br />

Element<br />

Starting Mat'l 1000 µg/mL<br />

Matrix Unit Cat. No. Price<br />

Hafnium 20 mL ------ -- AA23N-10X-20ML $ 60 AA23N-25X-20ML $ 125<br />

2-5% Nitric acid tr. HF 100 mL AA23N-1 $ 45 ------ -- ------ --<br />

500 mL AA23N-5 110 ------ -- ------ --<br />

Holmium 20 mL ------ -- AA24N-10X-20ML 35 AA24N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA24N-1 20 ------ -- ------ --<br />

500 mL AA24N-5 45 ------ -- ------ --<br />

Indium 20 mL ------ -- AA25N-10X-20ML 35 AA25N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA25N-1 18 ------ -- ------ --<br />

500 mL AA25N-5 40 ------ -- ------ --<br />

Iridium 20 mL ------ -- AA26H-10X-20ML 70 AA26H-25X-20ML 165<br />

10% HCl (min.) 100 mL AA26H-1 65 ------ -- ------ --<br />

500 mL AA26H-5 150 ------ -- ------ --<br />

Iron 20 mL ------ -- AA27N-10X-20ML 20 AA27N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA27N-1 12 ------ -- ------ --<br />

500 mL AA27N-5 30 ------ -- ------ --<br />

Lanthanum 20 mL ------ -- AA28N-10X-20ML 20 AA28N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA28N-1 15 ------ -- ------ --<br />

500 mL AA28N-5 36 ------ -- ------ --<br />

Lead 20 mL ------ -- AA29N-10X-20ML 20 AA29N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA29N-1 12 ------ -- ------ --<br />

500 mL AA29N-5 30 ------ -- ------ --<br />

Lithium 20 mL ------ -- AA30N-10X-20ML 20 AA30N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA30N-1 12 ------ -- ------ --<br />

500 mL AA30N-5 30 ------ -- ------ --<br />

Lutetium 20 mL ------ -- AA31N-10X-20ML 80 AA31N-25X-20ML 275<br />

2-5% Nitric acid 100 mL AA31N-1 65 ------ -- ------ --<br />

500 mL AA31N-5 250 ------ -- ------ --<br />

Magnesium 20 mL ------ -- AA32N-10X-20ML 20 AA32N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA32N-1 12 ------ -- ------ --<br />

500 mL AA32N-5 30 ------ -- ------ --<br />

Manganese 20 mL ------ -- AA33N-10X-20ML 20 AA33N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA33N-1 11 ------ -- ------ --<br />

500 mL AA33N-5 28 ------ -- ------ --<br />

Mercury 20 mL ------ -- AA34N-10X-20ML 20 AA34N-25X-20ML 37<br />

10% Nitric acid 100 mL AA34N-1 13 ------ -- ------ --<br />

500 mL AA34N-5 33 ------ -- ------ --<br />

Molybdenum 20 mL ------ -- AA35W-10X-20ML 20 AA35W-25X-20ML 37<br />

Water tr. NH4OH 100 mL AA35W-1 13 ------ -- ------ --<br />

500 mL AA35W-5 33 ------ -- ------ --<br />

Neodymium 20 mL ------ -- AA36N-10X-20ML 25 AA36N-25X-20ML 50<br />

2-5% Nitric acid 100 mL AA36N-1 20 ------ -- ------ --<br />

500 mL AA36N-5 45 ------ -- ------ --<br />

Nickel 20 mL ------ -- AA37N-10X-20ML 20 AA37N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA37N-1 12 ------ -- ------ --<br />

500 mL AA37N-5 30 ------ -- ------ --<br />

Niobium 20 mL ------ -- AA38W-10X-20ML 20 AA38W-25X-20ML 37<br />

Water tr. HF 100 mL AA38W-1 15 ------ -- ------ --<br />

500 mL AA38W-5 36 ------ -- ------ --<br />

Palladium 20 mL ------ -- AA40H-10X-20ML 80 AA40H-25X-20ML 175<br />

10% HCl (min.) 100 mL AA40H-1 62 ------ -- ------ --<br />

500 mL AA40H-5 145 ------ -- ------ --<br />

Phosphorus 20 mL ------ -- AA41W-10X-20ML 20 ------ --<br />

Water 100 mL AA41W-1 13 ------ -- ------ --<br />

500 mL AA41W-5 33 ------ -- ------ --<br />

Platinum 20 mL ------ -- AA42H-10X-20ML 80 AA42H-25X-20ML 175<br />

10% HCl (min.) 100 mL AA42H-1 62 ------ -- ------ --<br />

500 mL AA42H-5 145 ------ -- ------ --<br />

Potassium 20 mL ------ -- AA43N-10X-20ML 20 AA43N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA43N-1 12 ------ -- ------ --<br />

500 mL AA43N-5 30 ------ -- ------ --<br />

Praseodymium 20 mL ------ -- AA44N-10X-20ML 35 AA44N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA44N-1 20 ------ -- ------ --<br />

500 mL AA44N-5 45 ------ -- ------ --<br />

Rhenium 20 mL ------ -- AA45W-10X-20ML 80 AA45W-25X-20ML 175<br />

Water 100 mL AA45W-1 65 ------ -- ------ --<br />

500 mL AA45W-5 150 ------ -- ------ --<br />

Rhodium 20 mL ------ -- AA46H-10X-20ML 210 AA46H-25X-20ML 425<br />

10% HCl (min.) 100 mL AA46H-1 80 ------ -- ------ --<br />

500 mL AA46H-5 385 ------ -- ------ --<br />

Rubidium 20 mL ------ -- AA47N-10X-20ML 20 AA47N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA47N-1 15 ------ -- ------ --<br />

500 mL AA47N-5 36 ------ -- ------ --<br />

Ruthenium 20 mL ------ -- AA48H-10X-20ML 80 AA48H-25X-20ML 165<br />

10% HCl 100 mL AA48H-1 65 ------ -- ------ --<br />

500 mL AA48H-5 150 ------ -- ------ --<br />

74<br />

AA Single Element <strong>Standards</strong><br />

Atomic Absorption Spectroscopy<br />

NoHaz Package (No Hazardous Charges) *<br />

10,000 µg/mL 25,000 µg/mL<br />

Cat. No. Price Cat. No. Price<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

* see page 67<br />

for details


AA Single Element <strong>Standards</strong><br />

Atomic Absorption Spectroscopy<br />

Element<br />

Starting Mat'l 1000 µg/mL<br />

Matrix Unit Cat. No. Price<br />

NoHaz Package (No Hazardous Charges) *<br />

10,000 µg/mL 25,000 µg/mL<br />

Cat. No. Price Cat. No. Price<br />

Samarium 20 mL ------ -- AA49N-10X-20ML $ 35 AA49N-25X-20ML $ 60<br />

2-5% Nitric acid 100 mL AA49N-1 $ 20 ------ -- ------ --<br />

500 mL AA49N-5 45 ------ -- ------ --<br />

Scandium 20 mL ------ -- AA50N-10X-20ML 75 AA50N-25X-20ML 160<br />

2-5% Nitric acid 100 mL AA50N-1 62 ------ -- ------ --<br />

500 mL AA50N-5 145 ------ -- ------ --<br />

Selenium 20 mL ------ -- AA51N-10X-20ML 20 AA51N-25X-20ML 50<br />

2-5% Nitric acid 100 mL AA51N-1 19 ------ -- ------ --<br />

500 mL AA51N-5 46 ------ -- ------ --<br />

Silicon 20 mL ------ -- AA-52W-10X-20ML 20 ------ --<br />

Water tr. HF 100 mL AA52W-1 13 ------ -- ------ --<br />

500 mL AA52W-5 33 ------ -- ------ --<br />

Silver 20 mL ------ -- AA53N-10X-20ML 20 AA53N-25X-20ML 45<br />

2-5% Nitric acid 100 mL AA53N-1 16 ------ -- ------ --<br />

500 mL AA53N-5 40 ------ -- ------ --<br />

Sodium 20 mL ------ -- AA54N-10X-20ML 20 AA54N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA54N-1 13 ------ -- ------ --<br />

500 mL AA54N-5 33 ------ -- ------ --<br />

Strontium 20 mL ------ -- AA55N-10X-20ML 20 AA55N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA55N-1 12 ------ -- ------ --<br />

500 mL AA55N-5 30 ------ -- ------ --<br />

Sulfur 20 mL ------ -- AA56W-10X-20ML 20 AA56W-25X-20ML 37<br />

Water 100 mL AA56W-1 15 ------ -- ------ --<br />

500 mL AA56W-5 35 ------ -- ------ --<br />

Tantalum 20 mL ------ -- AA57W-10X-20ML 35 AA57W-25X-20ML 60<br />

Water tr. HF 100 mL AA57W-1 15 ------ -- ------ --<br />

500 mL AA57W-5 35 ------ -- ------ --<br />

Tellurium 20 mL ------ -- AA58H-10X-20ML 20<br />

10% HCl (min.) 100 mL AA58H-1 15 ------ -- ------ --<br />

500 mL AA58H-5 35 ------ -- ------ --<br />

Terbium 20 mL ------ -- AA59N-10X-20ML 35 AA59N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA59N-1 20 ------ -- ------ --<br />

500 mL AA59N-5 45 ------ -- ------ --<br />

Thallium 20 mL ------ -- AA60N-10X-20ML 20 AA60N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA60N-1 15 ------ -- ------ --<br />

500 mL AA60N-5 35 ------ -- ------ --<br />

Thorium 20 mL ------ -- ------ -- ------ --<br />

100 mL AA61N-1 20 ------ -- ------ --<br />

2-5% Nitric acid 500 mL AA61N-5 45 ------ -- ------ --<br />

Thulium 20 mL ------ -- AA62N-10X-20ML 65 AA62N-25X-20ML 150<br />

2-5% Nitric acid 100 mL AA62N-1 60 ------ -- ------ --<br />

500 mL AA62N-5 135 ------ -- ------ --<br />

Tin 20 mL ------ -- AA63N-10X-20ML 20 AA63N-25X-20ML 50<br />

2-5% Nitric acid tr. HF 100 mL AA63N-1 19 ------ -- ------ --<br />

500 mL AA63N-5 46 ------ -- ------ --<br />

Titanium 20 mL ------ -- AA64W-10X-20ML 20 ------ --<br />

Water tr. HF 100 mL AA64W-1 13 ------ -- ------ --<br />

500 mL AA64W-5 33 ------ -- ------ --<br />

Tungsten 20 mL ------ -- AA65W-10X-20ML 20<br />

Water tr. NH4OH 100 mL AA65W-1 15 ------ -- ------ --<br />

500 mL AA65W-5 35 ------ -- ------ --<br />

Uranium 20 mL ------ -- ------ -- ------ --<br />

2-5% Nitric acid 100 mL AA66N-1 15 ------ -- ------ --<br />

500 mL AA66N-5 35 ------ -- ------ --<br />

Vanadium 20 mL ------ -- AA67N-10X-20ML 20 AA67N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA67N-1 13 ------ -- ------ --<br />

500 mL AA67N-5 33 ------ -- ------ --<br />

Ytterbium 20 mL ------ -- AA68N-10X-20ML 35 AA68N-25X-20ML 60<br />

2-5% Nitric acid 100 mL AA68N-1 20 ------ -- ------ --<br />

500 mL AA68N-5 45 ------ -- ------ --<br />

Yttrium 20 mL ------ -- AA69N-10X-20ML 20 AA69N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA69N-1 15 ------ -- ------ --<br />

500 mL AA69N-5 35 ------ -- ------ --<br />

Zinc 20 mL ------ -- AA70N-10X-20ML 20 AA70N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA70N-1 13 ------ -- ------ --<br />

500 mL AA70N-5 33 ------ -- ------ --<br />

Zirconium 20 mL ------ -- AA71N-10X-20ML 20 AA71N-25X-20ML 37<br />

2-5% Nitric acid 100 mL AA71N-1 15 ------ -- ------ --<br />

500 mL AA71N-5 35 ------ -- ------ --<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

* see page 67<br />

for details<br />

75<br />

AA


IC<br />

IC<br />

•<br />

•<br />

•<br />

Ion Chrom - Anion Singles (Water Matrix)<br />

76<br />

99.999% High Purity Starting Materials<br />

18 Megohm, <strong>ASTM</strong> type 1 Water<br />

Packaged in pre-cleaned high quality HDPE bottles<br />

Ion Chromatography<br />

Anion Singles<br />

Each Standard is Supplied with a Certificate of Analysis,<br />

stating traceability to NIST, certified value and expiration date<br />

Final Solution is filtered through a 0.2 µm filter to<br />

eliminate contaminants (such as suspended solids and<br />

microbes). This extends shelf life and protects your column.<br />

Ready-To-Use Mixes and Calibration Sets<br />

<strong>Standards</strong> may be used for other “Classical or Wet” methods<br />

Most Complete Product Line<br />

"The Right Size” allows you to purchase as much or as little as you need -<br />

minimizing waste, and assuring Fresh Solution when you need it most<br />

Next Day Delivery on request<br />

Used for Influent & Effluent monitoring in aqueous matrices by<br />

<strong>ASTM</strong> & other EPA Methods in the Petrochemical Industry<br />

Anion Conc. Price Anion Conc. Price Anion Conc. Price<br />

Symbol (Element) Unit 100 µg/mL 200 µg/mL 1000 µg/mL<br />

F (Fluoride) 100 mL IC-F-1X-1 $ 15 IC-F-2X-1 $ 25 IC-F-10X-1 $ 45<br />

500 mL IC-F-1X-5 55 IC-F-2X-5 60 IC-F-10X-5 70<br />

Cl (Chloride) 100 mL IC-Cl-1X-1 $ 15 IC-Cl-2X-1 $ 25 IC-Cl-10X-1 $ 45<br />

500 mL IC-Cl-1X-5 55 IC-Cl-2X-5 60 IC-Cl-10X-5 70<br />

NO2 (Nitrite) 100 mL IC-NO2-1X-1 $ 15 IC-NO2-2X-1 $ 25 IC-NO2-10X-1 $ 45<br />

500 mL IC-NO2-1X-5 55 IC-NO2-2X-5 60 IC-NO2-10X-5 70<br />

NO3 (Nitrate) 100 mL IC-NO3-1X-1 $ 15 IC-NO3-2X-1 $ 25 IC-NO3-10X-1 $ 45<br />

500 mL IC-NO3-1X-5 55 IC-NO3-2X-5 60 IC-NO3-10X-5 70<br />

Br (Bromide) 100 mL IC-BR-1X-1 $ 15 IC-BR-2X-1 $ 25 IC-BR-10X-1 $ 45<br />

500 mL IC-BR-1X-5 55 IC-BR-2X-5 60 IC-BR-10X-5 70<br />

PO4 (Phosphate) 100 mL IC-PO4-1X-1 $ 15 IC-PO4-2X-1 $ 25 IC-PO4-10X-1 $ 45<br />

500 mL IC-PO4-1X-5 55 IC-PO4-2X-5 60 IC-PO4-10X-5 70<br />

SO4 (Sulfate) 100 mL IC-SO4-1X-1 $ 15 IC-SO4-2X-1 $ 25 IC-SO4-10X-1 $ 45<br />

500 mL IC-SO4-1X-5 55 IC-SO4-2X-5 60 IC-SO4-10X-5 70<br />

Ion Chrom - Anion Kits (Water Matrix)<br />

Unit Anion Conc. Kit Anion Conc. Kit Anion Conc. Kit<br />

100 µg/mL Price 200 µg/mL Price 1000 µg/mL Price<br />

Kit Price SAVE 25% 100 mL IC-AN-KIT-1X-1 $ 75 IC-AN-KIT-2X-1 $ 130 IC-AN-KIT-10X-1$ 235<br />

Kit = one bottle of each analyte 7 x 100 mL 7 x 100 mL 7 x 100 mL<br />

IC-F-1X-1 IC-Cl-1X-1 IC-F-2X-1 IC-Cl-2X-1 IC-F-10X-1 IC-Cl-10X-1<br />

IC-NO2-1X-1 IC-NO3-1X-1 IC-NO2-2X-1 IC-NO3-2X-1 IC-NO2-10X-1 IC-NO3-10X-1<br />

IC-BR-1X-1 IC-PO4-1X-1 IC-BR-2X-1 IC-PO4-2X-1 IC-BR-10X-1 IC-PO4-10X-1<br />

IC-SO4-1X-1 IC-SO4-2X-1 IC-SO4-10X-1<br />

Kit Price SAVE 25% 500 mL IC-AN-KIT-1X-5 $ 285 IC-AN-KIT-2X-5 $ 315 IC-AN-KIT-10X-5$ 365<br />

Kit = one bottle of each analyte 7 x 500 mL 7 x 500 mL 7 x 500 mL<br />

IC-F-1X-5 IC-Cl-1X-5 IC-F-2X-5 IC-Cl-2X-5 IC-F-10X-5 IC-Cl-10X-5<br />

IC-NO2-1X-5 IC-NO3-1X-5 IC-NO2-2X-5 IC-NO3-2X-5 IC-NO2-10X-5 IC-NO3-10X-5<br />

IC-BR-1X-5 IC-PO4-1X-5 IC-BR-2X-5 IC-PO4-2X-5 IC-BR-10X-5 IC-PO4-10X-5<br />

IC-SO4-1X-5 IC-SO4-2X-5 IC-SO4-10X-5<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


Anion Mixes Ion Chrom <strong>Standards</strong><br />

Anion Mix #1<br />

IC-MAN-01-1 $ 100 / 100 mL<br />

Water Matrix 5 comps.<br />

F (Fluoride) 20 µg/mL<br />

Cl (Chloride) 30 µg/mL<br />

NO3 (Nitrate) 100 µg/mL<br />

PO4 (Phosphate) 150 µg/mL<br />

SO4 (Sulfate) 150 µg/mL<br />

Anion Mix #2<br />

IC-MAN-02-1 $ 115 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 100 µg/mL<br />

Cl (Chloride) 200 µg/mL<br />

Br (Bromide) 400 µg/mL<br />

NO3 (Nitrate) 400 µg/mL<br />

PO4 (Phosphate) 600 µg/mL<br />

SO4 (Sulfate) 400 µg/mL<br />

Anion Mix #3<br />

IC-MAN-03-1 $ 75 / 100 mL<br />

Water Matrix 3 comps.<br />

F (Fluoride) 100 µg/mL<br />

Cl (Chloride) 100 µg/mL<br />

SO4 (Sulfate) 100 µg/mL<br />

Anion Mix #4<br />

IC-MAN-04-1 $ 115 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 100 µg/mL<br />

Cl (Chloride) 100 µg/mL<br />

Br (Bromide) 100 µg/mL<br />

NO3 (Nitrate) 100 µg/mL<br />

PO4 (Phosphate) 100 µg/mL<br />

SO4 (Sulfate) 100 µg/mL<br />

Anion Mix #5<br />

IC-MAN-05-SET $ 100 / 2 x 100 mL<br />

IC-MAN-05-R1-1 $ 85 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 10 µg/mL<br />

Cl (Chloride) 20 µg/mL<br />

Br (Bromide) 20 µg/mL<br />

NO3 (Nitrate) 20 µg/mL<br />

PO4 (Phosphate) 5 µg/mL<br />

SO4 (Sulfate) 30 µg/mL<br />

IC-NO2-0.2X-1 100 mL<br />

NO2 (Nitrite) 20 µg/mL<br />

Anion Mix #6<br />

IC-MAN-06-SET $ 100 / 2 x 100 mL<br />

IC-MAN-06-R1-1 $ 85 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 1 µg/mL<br />

Cl (Chloride) 5 µg/mL<br />

Br (Bromide) 5 µg/mL<br />

NO3 (Nitrate) 5 µg/mL<br />

PO4 (Phosphate) 5 µg/mL<br />

SO4 (Sulfate) 10 µg/mL<br />

IC-NO2-0.05X-1 100 mL<br />

NO2 (Nitrite) 5 µg/mL<br />

Technical Note<br />

In order to enhance the shelf life and<br />

long term stability of our IC products.<br />

AccuStandard has split the Nitrite out<br />

of mixes that contain Nitrate.<br />

Ion Chromatography<br />

Anion Mixtures<br />

Anion Mix #7<br />

IC-MAN-07-SET $ 100 / 2 x 100 mL<br />

IC-MAN-07-R1-1 $ 85 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 1 µg/mL<br />

Cl (Chloride) 10 µg/mL<br />

Br (Bromide) 10 µg/mL<br />

NO3 (Nitrate) 10 µg/mL<br />

PO4 (Phosphate) 10 µg/mL<br />

SO4 (Sulfate) 10 µg/mL<br />

IC-NO2-0.1X-1 100 mL<br />

NO2 (Nitrite) 10 µg/mL<br />

Anion Mix #8<br />

IC-MAN-08-SET $ 100 / 2 x 100 mL<br />

IC-MAN-08-R1-1 $ 85 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 10 µg/mL<br />

Cl (Chloride) 20 µg/mL<br />

Br (Bromide) 20 µg/mL<br />

NO3 (Nitrate) 20 µg/mL<br />

PO4 (Phosphate) 20 µg/mL<br />

SO4 (Sulfate) 20 µg/mL<br />

IC-NO2-0.2X-1 100 mL<br />

NO2 (Nitrite) 20 µg/mL<br />

Anion Mix #9<br />

IC-MAN-09-SET $ 100 / 2 x 100 mL<br />

IC-MAN-09-R1-1 $ 85 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 20 µg/mL<br />

Cl (Chloride) 40 µg/mL<br />

Br (Bromide) 40 µg/mL<br />

NO3 (Nitrate) 40 µg/mL<br />

PO4 (Phosphate) 40 µg/mL<br />

SO4 (Sulfate) 40 µg/mL<br />

IC-NO2-0.4X-1 100 mL<br />

NO2 (Nitrite) 40 µg/mL<br />

Anion Mix #10<br />

IC-MAN-10-SET $ 100 / 2 x 100 mL<br />

IC-MAN-10-R1-1 $ 85 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 25 µg/mL<br />

Cl (Chloride) 50 µg/mL<br />

Br (Bromide) 50 µg/mL<br />

NO3 (Nitrate) 50 µg/mL<br />

PO4 (Phosphate) 50 µg/mL<br />

SO4 (Sulfate) 50 µg/mL<br />

IC-NO2-0.5X-1 100 mL<br />

NO2 (Nitrite) 50 µg/mL<br />

IC-MAN-CAL-SET $ 395 / 9 x 100 mL<br />

Contains one each of:<br />

CLP-BLW-5 (500 mL)<br />

IC-MAN-07-SET IC-MAN-09-SET<br />

IC-MAN-08-SET IC-MAN-10-SET<br />

Technical Note<br />

This Ready-to-Use set of<br />

standards can be used to<br />

generate a 5 point calibration<br />

curve (including blank).<br />

Anion Mix #11<br />

IC-MAN-11-1 $ 175 / 100 mL<br />

Water Matrix 5 comps.<br />

Cl (Chloride) 1000 µg/mL<br />

Br (Bromide) 1000 µg/mL<br />

NO3 (Nitrate) 1000 µg/mL<br />

PO4 (Phosphate) 1000 µg/mL<br />

SO4 (Sulfate) 1000 µg/mL<br />

Anion Mix #12<br />

IC-MAN-12-1 $ 100 / 100 mL<br />

Water Matrix 5 comps.<br />

Cl (Chloride) 15 µg/mL<br />

Br (Bromide) 15 µg/mL<br />

NO3 (Nitrate) 15 µg/mL<br />

PO4 (Phosphate) 15 µg/mL<br />

SO4 (Sulfate) 15 µg/mL<br />

Anion Mix #13<br />

IC-MAN-13-1 $ 75 / 100 mL<br />

Water Matrix 3 comps.<br />

F (Fluoride) 25 µg/mL<br />

Cl (Chloride) 50 µg/mL<br />

SO4 (Sulfate) 100 µg/mL<br />

Anion Mix #14<br />

IC-MAN-14-SET $ 115 / 2 x 100 mL<br />

IC-MAN-14-R3-1 $ 85 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 20 µg/mL<br />

Cl (Chloride) 30 µg/mL<br />

NO3 (Nitrate) 100 µg/mL<br />

Br (Bromide) 100 µg/mL<br />

PO4 (Phosphate) 150 µg/mL<br />

SO4 (Sulfate) 150 µg/mL<br />

IC-NO2-1X-1<br />

NO2 (Nitrite)<br />

$ 15 / 100 mL<br />

100 µg/mL<br />

IC-MAN-14-R2-SET is perfect for<br />

US EPA Method 300.0<br />

Anion Mix #14 Revised<br />

IC-MAN-14-R2-SET$ 115 / 2 x 100 mL<br />

IC-MAN-14-R2-1 $ 85 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 20 µg/mL<br />

Cl (Chloride) 30 µg/mL<br />

Br (Bromide) 100 µg/mL<br />

N-NO 3 (Nitrogen-Nitrate) 100 µg/mL<br />

P-PO 4 (Phosphorus-Phosphate) 150 µg/mL<br />

SO 4 (Sulfate) 150 µg/mL<br />

IC-NO2-N-1X-1 $ 15 / 100 mL<br />

N-NO 2 (Nitrogen-Nitrite) 100 µg/mL<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

IC<br />

Anion Mix #15<br />

IC-MAN-15R-SET $ 80 / 2 x 100 mL<br />

IC-MAN-15-R2-1 $ 70 / 100 mL<br />

Water Matrix 3 comps.<br />

F (Fluoride) 100 µg/mL<br />

NO3 (Nitrate) 100 µg/mL<br />

PO4 (Phosphate) 100 µg/mL<br />

IC-NO2-1X-1 $ 15 / 100 mL<br />

NO2 (Nitrite) 100 µg/mL<br />

Anion Mix #16<br />

IC-MAN-16-SET $ 115 / 2 x 100 mL<br />

IC-MAN-16-R1-1 $ 100 / 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 100 µg/mL<br />

Cl (Chloride) 200 µg/mL<br />

Br (Bromide) 100 µg/mL<br />

NO3 (Nitrate) 20 µg/mL<br />

PO4 (Phosphate) 30 µg/mL<br />

SO4 (Sulfate) 20 µg/mL<br />

IC-NO2-0.4X-1 $ 15 / 100 mL<br />

NO2 (Nitrite) 40 µg/mL<br />

Anion Mix #17<br />

IC-MAN-17-SET $ 100 / 2 x 100 mL<br />

IC-MAN-17-R1-1 $ 85 / 100 mL<br />

Water Matrix 5 comps.<br />

Cl (Chloride) 20 µg/mL<br />

Br (Bromide) 12 µg/mL<br />

NO3 (Nitrate) 12 µg/mL<br />

PO4 (Phosphate) 12 µg/mL<br />

SO4 (Sulfate) 80 µg/mL<br />

IC-NO2-0.12X-1 100 mL<br />

NO2 (Nitrite) 12 µg/mL<br />

Anion Mix #18<br />

IC-MAN-18-SET $ 115 / 2 x 100 mL<br />

IC-MAN-18-R1-1 $ 85 / 100 mL<br />

Water Matrix 5 comps.<br />

F (Fluoride) 100 µg/mL<br />

Cl (Chloride) 100 µg/mL<br />

NO3 (Nitrate) 100 µg/mL<br />

PO4 (Phosphate) 100 µg/mL<br />

SO4 (Sulfate) 100 µg/mL<br />

IC-NO2-1X-1 $ 15 / 100 mL<br />

NO2 (Nitrite) 100 µg/mL<br />

Don't see the solution you need ?<br />

Use our Custom Quotation FAX Form in the<br />

back of the catalog and take advantage of<br />

our technical experience to help you<br />

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77<br />

IC


IC<br />

IC<br />

Ion Chrom - Cation Singles (Dilute HNO 3 Matrix)<br />

Cation Mixes Ion Chrom <strong>Standards</strong><br />

78<br />

Ion Chromatography<br />

Used for Influent & Effluent monitoring in aqueous matrices by<br />

<strong>ASTM</strong> & other EPA Methods in the Petrochemical Industry<br />

Symbol (Element) Unit 100 µg/mL Price 200 µg/mL Price 1000 µg/mL Price<br />

Ca (Calcium) 100 mL IC-CA-1X-1 $ 15 IC-CA-2X-1 $ 25 IC-CA-10X-1 $ 45<br />

500 mL IC-CA-1X-5 55 IC-CA-2X-5 60 IC-CA-10X-5 70<br />

NH4 (Ammonium) 100 mL IC-NH4-1X-1 $ 15 IC-NH4-2X-1 $ 25 IC-NH4-10X-1 * $ 45<br />

500 mL IC-NH4-1X-5 55 IC-NH4-2X-5 60 IC-NH4-10X-5 * 70<br />

Mg (Magnesium) 100 mL IC-MG-1X-1 $ 15 IC-MG-2X-1 $ 25 IC-MG-10X-1 $ 45<br />

500 mL IC-MG-1X-5 55 IC-MG-2X-5 60 IC-MG-10X-5 70<br />

K (Potassium) 100 mL IC-K-1X-1 $ 15 IC-K-2X-1 $ 25 IC-K-10X-1 $ 45<br />

500 mL IC-K-1X-5 55 IC-K-2X-5 60 IC-K-10X-5 70<br />

Na (Sodium) 100 mL IC-NA-1X-1 $ 15 IC-NA-2X-1 $ 25 IC-NA-10X-1 $ 45<br />

500 mL IC-NA-1X-5 55 IC-NA-2X-5 60 IC-NA-10X-5 70<br />

Li (Lithium) 100 mL IC-LI-1X-1 $ 15 IC-LI-2X-1 $ 25 IC-LI-10X-1 $ 45<br />

500 mL IC-LI-1X-5 55 IC-LI-2X-5 60 IC-LI-10X-5 70<br />

Ba (Barium) 100 mL IC-BA-1X-1 $ 15 IC-BA-2X-1 $ 25 IC-BA-10X-1 $ 45<br />

500 mL IC-BA-1X-5 55 IC-BA-2X-5 60 IC-BA-10X-5 70<br />

Sr (Strontium) 100 mL IC-SR-1X-1 $ 15 IC-SR-2X-1 $ 25 IC-SR-10X-1 $ 45<br />

500 mL IC-SR-1X-5 55 IC-SR-2X-5 60 IC-SR-10X-5 70<br />

* These <strong>Standards</strong> are 1,000 µg/mL as Ammonium (NH 4)<br />

Other Nitrogen species equivalents are: NH 3 (Ammonia) = 944 µg/mL N (Nitrogen) = 776 µg/mL<br />

Ion Chrom - Cation Kits (Dilute HNO 3 Matrix)<br />

Unit 100 µg/mL Price 200 µg/mL Price 1000 µg/mL Price<br />

Kit Price SAVE 25% 100 mL IC-CAT-KIT-1X-1 $ 75 IC-CAT-KIT-2X-1 $ 130 IC-CAT-KIT-10X-1 $ 235<br />

Kit = one bottle of each analyte 8 x 100 mL 8 x 100 mL 8 x 100 mL<br />

IC-CA-1X-1 IC-NH4-1X-1 IC-CA-2X-1 IC-NH4-2X-1 IC-CA-10X-1 IC-NH4-10X-1<br />

IC-MG-1X-1 IC-K-1X-1 IC-MG-2X-1 IC-K-2X-1 IC-MG-10X-1 IC-K-10X-1<br />

IC-NA-1X-1 IC-LI-1X-1 IC-NA-2X-1 IC-LI-2X-1 IC-NA-10X-1 IC-LI-10X-1<br />

IC-BA-1X-1 IC-SR-1X-1 IC-BA-2X-1 IC-SR-2X-1 IC-BA-10X-1 IC-SR-10X-1<br />

Kit Price SAVE 25% 500 mL IC-CAT-KIT-1X-5 $ 285 IC-CAT-KIT-2X-5 $ 315 IC-CAT-KIT-10X-5 $ 365<br />

Kit = one bottle of each analyte 8 x 500 mL 8 x 500 mL 8 x 500 mL<br />

IC-CA-1X-5 IC-NH4-1X-5 IC-CA-2X-5 IC-NH4-2X-5 IC-CA-10X-5 IC-NH4-10X-5<br />

IC-MG-1X-5 IC-K-1X-5 IC-MG-2X-5 IC-K-2X-5 IC-MG-10X-5 IC-K-10X-5<br />

IC-NA-1X-5 IC-LI-1X-5 IC-NA-2X-5 IC-LI-2X-5 IC-NA-10X-5 IC-LI-10X-5<br />

IC-BA-1X-5 IC-SR-1X-5 IC-BA-2X-5 IC-SR-2X-5 IC-BA-10X-5 IC-SR-10X-5<br />

Cation Mix #1<br />

IC-MCA-01-1 $ 150 / 100 mL<br />

Dilute HNO3 6 comps.<br />

Ca (Calcium) 1000 µg/mL<br />

NH 4 (Ammonium) 400 µg/mL<br />

Mg (Magnesium) 200 µg/mL<br />

Cation Mix #2<br />

IC-MCA-02-1 $ 125 / 100 mL<br />

Dilute HNO3 6 comps.<br />

Ca (Calcium) 100 µg/mL<br />

NH 4 (Ammonium) 100 µg/mL<br />

Mg (Magnesium) 100 µg/mL<br />

K (Potassium) 200 µg/mL<br />

Na (Sodium) 200 µg/mL<br />

Li (Lithium) 50 µg/mL<br />

K (Potassium) 100 µg/mL<br />

Na (Sodium) 100 µg/mL<br />

Li (Lithium) 100 µg/mL<br />

Cation Mix #3<br />

IC-MCA-03-1 $ 100 / 100 mL<br />

Dilute HNO3 4 comps.<br />

Ca (Calcium) 100 µg/mL<br />

NH4 (Ammonium) 100 µg/mL<br />

Na (Sodium) 50 µg/mL<br />

Li (Lithium) 10 µg/mL<br />

Cation Mix #4<br />

IC-MCA-04-1 $ 125 / 100 mL<br />

Dilute HNO3 4 comps.<br />

Ca (Calcium) 400 µg/mL<br />

Mg (Magnesium) 200 µg/mL<br />

Ba (Barium) 1600 µg/mL<br />

Sr (Strontium) 600 µg/mL<br />

Cation Mix #5<br />

IC-MCA-05-1 $ 125 / 100 mL<br />

Dilute HNO3 4 comps.<br />

NH4 (Ammonium) 3 µg/mL<br />

K (Potassium) 6 µg/mL<br />

Na (Sodium) 3 µg/mL<br />

Li (Lithium) 0.5 µg/mL<br />

Cation Mix #6<br />

IC-MCA-06-1 $ 125 / 100 mL<br />

Dilute HNO3 6 comps.<br />

Ca (Calcium) 2 µg/mL<br />

NH 4 (Ammonium) 1.5 µg/mL<br />

Mg (Magnesium) 2 µg/mL<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

K (Potassium) 2.5 µg/mL<br />

Na (Sodium) 1.5 µg/mL<br />

Li (Lithium) 0.2 µg/mL


Ion Chrom Eluents<br />

Ion Chromatography<br />

0.5 M Sodium bicarbonate 50 mL $ 45 100 mL $ 60 5 x 50 mL $ 135 5 x 100 mL $ 250<br />

(100X concentrate) IC-ELU-01-0.5 IC-ELU-01-1 IC-ELU-01-0.5-PAK IC-ELU-01-1-PAK<br />

0.5 M Sodium carbonate 50 mL $ 45 100 mL $ 60 5 x 50 mL $ 135 5 x 100 mL $ 250<br />

(100X concentrate) IC-ELU-02-0.5 IC-ELU-02-1 IC-ELU-02-0.5-PAK IC-ELU-02-1-PAK<br />

0.18 M Sodium carbonate/ 50 mL $ 25 100 mL $ 30 5 x 50 mL $ 60 5 x 100 mL $ 115<br />

0.17 M Sodium bicarbonate<br />

(100X concentrate)<br />

IC-ELU-03-0.5 IC-ELU-03-1 IC-ELU-03-0.5-PAK IC-ELU-03-1-PAK<br />

Ion Chrom - Ion Singles as the Element<br />

EPA 300.0, <strong>ASTM</strong> Method D-4327<br />

Unit 100 µg/mL Price 1000 µg/mL Price<br />

NO2-N (Nitrite-Nitrogen) 100 mL IC-NO2-N-1X-1 $ 15 IC-NO2-N-10X-1 $ 45<br />

Water Matrix 500 mL IC-NO2-N-1X-5 55 IC-NO2-N-10X-5 70<br />

NO3-N (Nitrate-Nitrogen) 100 mL IC-NO3-N-1X-1 $ 15 IC-NO3-N-10X-1 $ 45<br />

Water Matrix 500 mL IC-NO3-N-1X-5 55 IC-NO3-N-10X-5 70<br />

PO4-P (Phosphate-Phosphorous) 100 mL IC-PO4-P-1X-1 $ 15 IC-PO4-P-10X-1 $ 45<br />

Water Matrix 500 mL IC-PO4-P-1X-5 55 IC-PO4-P-10X-5 70<br />

SO4-S (Sulfate-Sulfur) 100 mL IC-SO4-S-1X-1 $ 15 IC-SO4-S-10X-1 $ 45<br />

Water Matrix 500 mL IC-SO4-S-1X-5 55 IC-SO4-S-10X-5 70<br />

NH4-N (Ammonium-Nitrogen) 100 mL IC-NH4-N-1X-1 $ 15 IC-NH4-N-10X-1 $ 45<br />

Water Matrix 500 mL IC-NH4-N-1X-5 55 IC-NH4-N-10X-5 70<br />

Anion Singles Kits<br />

IC-AN-KIT-R-10X-1 $ 235 / 7 x 100 mL<br />

Each at 1000 µg/mL<br />

IC-F-10X-1 Fluoride<br />

IC-Cl-10X-1 Chloride<br />

IC-NO2-N-10X-1 Nitrite-Nitrogen<br />

IC-NO3-N-10X-1 Nitrate-Nitrogen<br />

IC-BR-10X-1 Bromide<br />

IC-PO4-P-10X-1 Phosphate-Phosphorous<br />

IC-SO4-S-10X-1 Sulfate-Sulfur<br />

Organic Acid Salt <strong>Standards</strong><br />

IC-AN-KIT-R-10X-5<br />

Each at 1000 µg/mL<br />

$ 365 / 7 x 500 mL<br />

IC-F-10X-5 Fluoride<br />

IC-Cl-10X-5 Chloride<br />

IC-NO2-N-10X-5 Nitrite-Nitrogen<br />

IC-NO3-N-10X-5 Nitrate-Nitrogen<br />

IC-BR-10X-5 Bromide<br />

IC-PO4-P-10X-5 Phosphate-Phosphorous<br />

IC-SO4-S-10X-5 Sulfate-Sulfur<br />

Unit 100 µg/mL Price 1000 µg/mL Price<br />

Formate 100 mL IC-FORM-1X-1 $ 15 IC-FORM-10X-1 $ 45<br />

Water Matrix 500 mL IC-FORM-1X-5 55 IC-FORM-10X-5 70<br />

Acetate 100 mL IC-ACET-1X-1 $ 15 IC-ACET-10X-1 $ 45<br />

Water Matrix 500 mL IC-ACET-1X-5 55 IC-ACET-10X-5 70<br />

Oxalate 100 mL IC-OXAL-1X-1 $ 15 IC-OXAL-10X-1 $ 45<br />

Water Matrix 500 mL IC-OXAL-1X-5 55 IC-OXAL-10X-5 70<br />

Chlorate 100 mL IC-CHLR-1X-1 $ 15 IC-CHLR-10X-1 $ 45<br />

Water Matrix 500 mL IC-CHLR-1X-5 55 IC-CHLR-10X-5 70<br />

Chromate 100 mL IC-CHRM-1X-1 $ 15 IC-CHRM-10X-1 $ 45<br />

Water Matrix 500 mL IC-CHRM-1X-5 55 IC-CHRM-10X-5 70<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

IC<br />

Easy to use, ready to dilute<br />

concentrates. Open a fresh<br />

bottle and dilute the volume<br />

(50 mL to 5 L or 100 mL to 10 L)<br />

and be assured of a fresh<br />

uncontaminated mobile phase.<br />

Recommended product for EPA Method 300.0<br />

“Determination of Inorganic Anions by Ion<br />

Chromatography” and <strong>ASTM</strong> D-4327-91, “Test<br />

Method for Anions in Water by Chemically<br />

Suppressed Ion Chromatography.”<br />

Anion Mix #14 Revised<br />

IC-MAN-14-R2-SET $ 115 / 2 x 100 mL<br />

IC-MAN-14-R2-1 100 mL<br />

Water Matrix 6 comps.<br />

F (Fluoride) 20 µg/mL<br />

Cl (Chloride) 30 µg/mL<br />

Br (Bromide) 100 µg/mL<br />

N-NO3 (Nitrogen-Nitrate) 100 µg/mL<br />

P-PO4 (Phosphorus-Phosphate) 150 µg/mL<br />

SO4 (Sulfate) 150 µg/mL<br />

IC-NO2-N-1X-1 100 mL<br />

N-NO2 (Nitrogen-Nitrite) 100 µg/mL<br />

79<br />

IC


IC<br />

80<br />

On-Line Ordering<br />

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make an inquiry for Custom Quotes visit our website.<br />

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information: List of analytes and concentrations, Solvent or matrix, Quantity required (milliliters), Packaging unit size (milliliters<br />

per ampule, bottle, or vial).<br />

Quality Control Options<br />

1. Gravimetric/Volumetric Certification: Each standard is measured gravimetrically and then QC’ed instrumentally (where<br />

available). Every component in the standard is guaranteed to be within ±0.5% of the requested value unless otherwise stated. The<br />

solutions are made up to volume using class A glassware. A certificate comes with each standard and documents the gravimetric<br />

values used.<br />

2. Quantitative Validation: Full QA/QC method includes extended GC analysis using both internal and calibration standards plus<br />

statistical analysis. A data package is provided containing analytical and gravimetric data (Organic customs only).<br />

Also available: OEM <strong>Standards</strong> - Privately labeled standards manufactured and tested to your specifications.


LUFT/LUST <strong>Standards</strong><br />

Alaska 82-84<br />

GRO Hydrocarbons<br />

DRO Hydrocarbons<br />

RRO Hydrocarbons<br />

Arizona 85<br />

Diesel Range<br />

California 85<br />

Gasoline<br />

Connecticut 85<br />

Extractable TPH<br />

Florida 86<br />

FTRPH<br />

State Methods<br />

TPH Pattern Recognition <strong>Standards</strong> 92-93<br />

Weathered LUFT/LUST Fuel <strong>Standards</strong> 93<br />

Gasoline Range HC Analysis (CA, PA, WI) 94<br />

Diesel Range HC Analysis 95<br />

<strong>ASTM</strong> Method D-2887 95<br />

Complete Hydrocarbon Analysis 95<br />

Proficiency Test Samples 96<br />

Method 1664, Oil, Grease & TPH Analysis 97<br />

Methods 413.2, 418.1 & TPH Analysis 97<br />

Method 8440 TPH Analysis 97<br />

Method 1004 Alcohol Oxidation Products in Engine Exhaust 98<br />

<strong>ASTM</strong> E-1387 and E-1618 for Fire Debris Analysis 98<br />

Skinner List Refinery Waste (<strong>ASTM</strong>#E1387) 98<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

Massachusetts 87-88<br />

EPH<br />

VPH<br />

Mississippi 86<br />

DRO<br />

Multi-State 86<br />

Hydrocarbon Window Defining<br />

Pensylvania 89<br />

Storage Tank Monitoring <strong>Standards</strong><br />

Tennessee 86<br />

DRO<br />

Texas 89<br />

Method 1005 (PST)<br />

Washington 90-91<br />

VPH<br />

EPH<br />

Wisconsin 91<br />

Gasoline Range Hydrocarbons<br />

LUFT/LUST<br />

81<br />

LUFT/LUST


LUFT/LUST<br />

Alaska<br />

LUFT/LUST<br />

Alaska Method Determination of Gasoline Range Organic (GRO) Hydrocarbons<br />

Normal Alkane Standard - GRO Defining Mixture<br />

AK-101.0-NAS-10X $ 20 / 1 x 1 mL<br />

AK-101.0-NAS-10X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

2.0 mg/mL each in MeOH 5 comps.<br />

n-Hexane<br />

n-Heptane<br />

n-Octane<br />

Certified BTEX in Gasoline Composite Mix<br />

(Multi Source) see Technical Note<br />

AK-101.0-GCS-BTEX $ 55 / 1 x 1 mL<br />

5 mg/mL total in MeOH 3 comps.<br />

Gasoline - Premium (1.66 mg/mL)<br />

Gasoline - Regular, leaded (1.67 mg/mL)<br />

Gasoline - Regular, unleaded (1.67 mg/mL)<br />

Technical Notes<br />

Laboratory Control Standard<br />

The Gasoline Laboratory Control Standard was taken from an <strong>ASTM</strong><br />

selected fuel set and a source independent of what is being used in<br />

the Gasoline Composite Mix.<br />

Simultaneous BTEX / Gasoline QA/QC<br />

AccuStandard's QA/QC Department has certified the benzene,<br />

toluene, ethyl benzene and xylene concentrations in our unleaded<br />

gasoline standard (GA-001-20X-BTEX & in AK-101.0-GCS-BTEX).<br />

Use of either standard allows the analytical chemist in a single<br />

injection to verify that the QA/QC requirements are being met for the<br />

BTEX analytes as well as for the gasoline.<br />

Since formulating the standards for the Alaskan method, and<br />

because of numerous laboratory requests, we have added a new<br />

multi source certified BTEX in gasoline composite mix (AK-101.0-<br />

GCS-BTEX). The BTEX values for this multi-source calibration<br />

standard have been determined through in-house analysis against a<br />

BTEX multi level calibration curve, and are listed in the Certificate.<br />

AccuStandard continues to look for innovative approaches to save<br />

the analytical laboratory time and money.<br />

Alaska Method Determination of Aromatic & Aliphatic Hydrocarbons in Gasoline Range Organics<br />

AK101AA Aromatics Mix<br />

AK-101AA-ARO $ 30 / 1 x 1 mL<br />

AK-101AA-ARO-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

2000 µg/mL each in MeOH 14 comps.<br />

Benzene<br />

Toluene<br />

Ethylbenzene<br />

m-Xylene<br />

n-Nonane<br />

n-Decane<br />

Laboratory Control Standard<br />

AK-101.0-LCS $ 20 / 1 x 1 mL<br />

AK-101.0-LCS-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

5.0 mg/mL in MeOH<br />

Gasoline - Regular, unleaded<br />

Certified BTEX in Unleaded Gasoline<br />

(Single Source)<br />

GA-001-20X-BTEX $ 55 / 1 x 1 mL<br />

10.0 mg/mL in MeOH<br />

Gasoline - Regular, unleaded<br />

Surrogate Control Standard<br />

AK-101.0-SS $ 10 / 1 x 1 mL<br />

AK-101.0-SS-PAK<br />

50 µg/mL each in MeOH<br />

SAVE 20% $ 40 / 5 x 1 mL<br />

AK-101.0-SS-10X $ 20 / 1 x 1 mL<br />

AK-101.0-SS-10X-PAK<br />

500 µg/mL each in MeOH<br />

SAVE 20% $ 80 / 5 x 1 mL<br />

AK-101.0-SS-100X $ 20 / 1 x 1 mL<br />

AK-101.0-SS-100X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

5,000 µg/mL each in MeOH 2 comps.<br />

p-Bromofluorobenzene a,a,a-Trifluorotoluene<br />

p-Xylene<br />

o-Xylene<br />

1,2,3-Trimethylbenzene<br />

1,2,4-Trimethylbenzene<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods<br />

1,3,5-Trimethylbenzene<br />

Isopropylbenzene<br />

m-Ethyltoluene<br />

Gasoline Calibration Composite Mixture<br />

AK-101.0-GCS $ 25 / 1 x 1 mL<br />

AK-101.0-GCS-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

Total 5.0 mg/mL in MeOH 3 comps.<br />

Gasoline - Premium (1.66 mg/mL)<br />

Gasoline - Regular, leaded (1.67 mg/mL)<br />

Gasoline - Regular, unleaded (1.67 mg/mL)<br />

Gasoline Calibration Mix Version 4/02<br />

AK-101-GSC-R1 $ 25 / 1 x 1 mL<br />

AK-101-GSC-R1-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

Equal parts by weight of each<br />

Gasoline - Regular, unleaded<br />

Gasoline - Plus, unleaded<br />

Gasoline - Premium, unleaded<br />

Internal Standard<br />

AK-101.0-IS-10X $ 20 / 1 x 1 mL<br />

AK-101.0-IS-10X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

2.0 mg/mL in MeOH<br />

1-Chloro-4-fluorobenzene<br />

p-Ethyltoluene<br />

o-Ethyltoluene<br />

n-Propylbenzene<br />

82 Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

NEW


Alaska Method Determination of Diesel Range Organic (DRO) Hydrocarbons<br />

Diesel Fuel, Arctic (1.66 mg/mL)<br />

#1 Diesel - Low Sulfur (1.67 mg/mL)<br />

Diesel Fuel, Arctic (16.6 mg/mL)<br />

#1 Diesel - Low Sulfur (16.7 mg/mL)<br />

n-Decane<br />

n-Undecane<br />

n-Dodecane<br />

n-Tridecane<br />

n-Tetradecane<br />

n-Pentadecane<br />

n-Hexadecane<br />

n-Heptadecane<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods<br />

Diesel Calibration Composite Mixture (low sulfur)<br />

AK-102.0-DCS $ 25 / 1 x 1 mL<br />

AK-102.0-DCS-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

Total 5.0 mg/mL in CH2Cl2 3 comps.<br />

#2 Diesel - extra Low Sulfur (1.67 mg/mL)<br />

AK-102.0-DCS-10X $ 40 / 1 x 1 mL<br />

AK-102.0-DCS-10X-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

Total 50.0 mg/mL in CH2Cl2 3 comps.<br />

#2 Diesel - extra Low Sulfur (16.7 mg/mL)<br />

Laboratory Control Standard (low sulfur)<br />

AK-102.0-LCS $ 10 / 1 x 1 mL<br />

AK-102.0-LCS-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

5.0 mg/mL in Acetone<br />

AK102.0-LCS-10X $ 20 / 1 x 1 mL<br />

AK-102.0-LCS-10X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

50.0 mg/mL in Acetone<br />

#2 Diesel - extra Low Sulfur<br />

Normal Alkane Standard - DRO Defining Mixture<br />

AK-102.0-NAS-10X $ 40 / 1 x 1 mL<br />

AK-102.0-NAS-10X-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

2.0 mg/mL each in CH2Cl2 16 comps.<br />

n-Octadecane<br />

n-Nonadecane<br />

n-Eicosane<br />

n-Heneicosane<br />

n-Docosane<br />

n-Tricosane<br />

n-Tetracosane<br />

n-Pentacosane<br />

Technical Note<br />

Stock Concentrate Diesel Calibration<br />

Composite Mixture<br />

AK-102.0-DCS-R1-10X $ 40 / 1 x 1 mL<br />

AK-102.0-DCS-R1-10X-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

Total 50.0 mg/mL in CH2Cl2 3 comps.<br />

Diesel Fuel, Arctic (16.6 mg/mL)<br />

#1 Diesel - Low Sulfur (16.7 mg/mL)<br />

#2 Diesel - Conventional (16.7 mg/mL)<br />

Laboratory Control Standard<br />

AK-102.0-LCS-R1-10X $ 20 / 1 x 1 mL<br />

AK-102.0-LCS-R1-10X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

50.0 mg/mL in Acetone<br />

#2 Diesel - Conventional<br />

Technical Note<br />

The Laboratory Control Standard was prepared from an<br />

independent source of material than what was used in the Diesel<br />

Calibration Composite mix.<br />

AccuStandard originally formulated the Diesel Calibration Composite Mix and Laboratory Control Standard using two independent sources<br />

of #2 Diesel as required by the Alaskan method. Unfortunately, the chromatographic patterns for the #2 diesel sources (conventional &<br />

extra low sulfur) are different.<br />

We have actively sought out and obtained independent sources of each type of #2 diesel to insure similar chromatographic patterns . We<br />

recommend that when a customer is analyzing the Diesel Calibration Composite and Laboratory Control standard that the client orders<br />

AK-102.0-DCS & AK-102.0-LCS products together to obtain similar chromatographic patterns for #2 diesel extra low sulfur patterns and<br />

AK-102.0-DCS-R1-10X & AK-102.0-LCS-R1-10X products to obtain similar chromatographic patterns for #2 Diesel conventional patterns.<br />

We believe most laboratories performing the Alaskan DRO analysis will find the #2 Diesel conventional chromatographic pattern more<br />

closely resembles typical Diesel samples drawn from environmental sites.<br />

Surrogate <strong>Standards</strong><br />

AK-102.0-SS $ 10 / 1 x 1 mL<br />

AK-102.0-SS-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

200 µg/mL in Acetone<br />

AK102.0-SS-10X $ 15 / 1 x 1 mL<br />

AK102.0-SS-10X-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

2.0 mg/mL in Acetone<br />

o-Terphenyl<br />

Internal Standard<br />

AK-102.0-IS $ 15 / 1 x 1 mL<br />

AK-102.0-IS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

1.0 mg/mL in CH2Cl2 5-alpha Androstane<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

LUFT/LUST<br />

Alaska<br />

83<br />

LUFT/LUST


LUFT/LUST<br />

Alaska<br />

LUFT/LUST<br />

Alaska Method Determination of Aromatic & Aliphatic Hydrocarbons in Diesel Range Organics<br />

AK102AA DRO Standard<br />

AK-102AA-DRO $ 40 / 1 x 1 mL<br />

AK-102AA-DRO-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

2000 µg/mL each in CH2Cl2 10 comps.<br />

n-Undecane<br />

n-Pentadecane<br />

n-Heptadecane<br />

n-Octadecane<br />

n-Tetracosane<br />

Naphthalene<br />

Acenaphthene<br />

Fluorene<br />

Pyrene<br />

Anthracene<br />

AK102/103AA Retention Time<br />

Marker Standard<br />

AK-102/103AA-RT $ 25 / 1 x 1 mL<br />

AK-102/103AA-RT-PAK $ 100 / 5 x 1 mL<br />

50 µg/mL each in CH2Cl2 3 comps.<br />

n-Decane<br />

n-Pentacosane<br />

n-Hexatriacontane<br />

Alaska Method Determination of Residual Range Organics (RRO) Hydrocarbon<br />

Residual Composite Mixtures<br />

AK-103.0-RCS $ 25 / 1 x 1 mL<br />

AK-103.0-RCS-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

Total 5.0 mg/mL in CH2Cl2 3 comps.<br />

SAE 30W Motor Oil (1.66 mg)<br />

SAE 40W Motor Oil (1.67 mg)<br />

SAE 50W Motor Oil (1.67 mg)<br />

AK-103.0-RCS-10X $ 40 / 1 x 1 mL<br />

AK-103.0-RCS-10X-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

Total 50.0 mg/mL in CH2Cl2 3 comps.<br />

SAE 30W Motor Oil (16.6 mg)<br />

SAE 40W Motor Oil (16.7 mg)<br />

SAE 50W Motor Oil (16.7 mg)<br />

AK102/103AA Surrogate Standard<br />

AK-102/103AA-SS $ 35 / 1 x 1 mL<br />

AK-102/103AA-SS-PAK SAVE 20% $ 140 / 5 x 1 mL<br />

1000 µg/mL each in CH2Cl2 3 comps.<br />

Squalane<br />

o-Terphenyl<br />

5,6,7,8-Tetrahydro-1-naphthol<br />

Alaska Method Determination of Aromatic and Aliphatic Hydrocarbons in Residual Range Organics<br />

AK103AA RRO Standard<br />

AK-103AA-RRO $ 35 / 1 x 1 mL<br />

AK-103AA-RRO-PAKSAVE 20% $ 140 / 5 x 1 mL<br />

50 µg/mL each in CH2Cl2 9 comps.<br />

84<br />

n-Hexacosane<br />

n-Octacosane<br />

n-Triacontane<br />

n-Dotriacontane<br />

n-Tetratriacontane<br />

Benzo[b]fluoranthene<br />

Benzo[a]pyrene<br />

Benzo[g,h,i]perylene<br />

Dibenz[a,h]anthracene<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods<br />

n-Decane<br />

n-Pentacosane<br />

n-Hexatriacontane<br />

Laboratory Control Standard<br />

AK-103.0-LCS $ 10 / 1 x 1 mL<br />

AK-103.0-LCS-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

5.0 mg/mL in Acetone<br />

AK-103.0-LCS-5X $ 20 / 1 x 1 mL<br />

AK-103.0-LCS-5X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

25.0 mg/mL in Acetone: CH2Cl2 (1:1)<br />

SAE 40W Motor Oil<br />

Surrogate Control Standard<br />

AK-103.0-SS $ 20 / 1 x 1 mL<br />

AK-103.0-SS-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

500 µg/mL in Acetone<br />

AK-103.0-SS-10X $ 30 / 1 x 1 mL<br />

AK-103.0-SS-10X-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

5.0 mg/mL in THF : Acetone (1:3)<br />

n-Triacontane-d 62<br />

AK102/103AA Retention Time<br />

Marker Standard<br />

AK-102/103AA-RT $ 25 / 1 x 1 mL<br />

AK-102/103AA-RT-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

50 µg/mL each in CH2Cl2 3 comps.<br />

AK102/103AA Surrogate Standard<br />

AK-102/103AA-SS $ 35 / 1 x 1 mL<br />

AK-102/103AA-SS-PAK SAVE 20% $ 140 / 5 x 1 mL<br />

1000 µg/mL each in CH2Cl2 3 comps.<br />

Squalane<br />

o-Terphenyl<br />

5,6,7,8-Tetrahydro-1-naphthol<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


Arizona Method Determination of Diesel Range and Oil Range Organic Hydrocarbons<br />

California Method<br />

Connecticut Method Extractable Total Petroleum Hydrocarbon<br />

CT ETPH Alkane Standard<br />

DRH-009S $ 35 / 1 x 1 mL<br />

DRH-009S-PAK SAVE 20% $ 140 / 5 x 1 mL<br />

1000 µg/mL in CH2Cl2 15 comps.<br />

n-Nonane<br />

n-Decane<br />

n-Dodecane<br />

n-Tetradecane<br />

n-Hexadecane<br />

n-Octadecane<br />

n-Eicosane<br />

n-Docosane<br />

n-Tetracosane<br />

n-Hexacosane<br />

Technical Note<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods<br />

Diesel & Oil Range Standard<br />

AZ-8015-DRO/ORO $ 40 / 1 x 1 mL<br />

AZ-8015-DRO/ORO-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

2000 µg/mL each in CH2Cl2 12 comps.<br />

n-Decane<br />

n-Dodecane<br />

n-Docosane<br />

n-Dotriacontane<br />

n-Eicosane<br />

n-Hexacosane<br />

n-Hexadecane<br />

n-Octacosane<br />

n-Octadecane<br />

n-Tetracosane<br />

n-Tetradecane<br />

n-Triacontane<br />

Surrogate <strong>Standards</strong><br />

AK-102.0-SS-10X $ 15 / 1 x 1 mL<br />

AK-102.0-SS-10X-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

2.0 mg/mL in Acetone<br />

o-Terphenyl<br />

California - Gasoline Range Hydrocarbons<br />

S-603A-10X $ 25 / 1 x 1 mL<br />

S-603A-10X-PAK SAVE 25% $ 90 / 5 x 1 mL<br />

2.0 mg/mL each in MeOH 7 comps.<br />

Benzene<br />

Ethylbenzene<br />

Methyl t-butyl ether<br />

Benzene<br />

Chlorobenzene<br />

1,2-Dichlorobenzene<br />

1,3-Dichlorobenzene<br />

Toluene<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene<br />

LA County Well Investigation & Monitoring Program<br />

Purgeable Aromatics - Gasoline ID<br />

M-602-GAS-10X $ 30 / 1 x 1 mL<br />

2.0 mg/mL each in MeOH 11 comps.<br />

1,4-Dichlorobenzene<br />

Ethylbenzene<br />

Toluene<br />

o-Xylene<br />

p-Xylene<br />

m-Xylene<br />

MtBE<br />

n-Octacosane<br />

n-Triacontane<br />

n-Dotriacontane<br />

n-Tetratriacontane<br />

n-Hexatriacontane<br />

Proficiency Test Samples required for the ETPH method and<br />

individual fuels are available as standard products. Custom<br />

formulations can be quoted and manufactured to meet your<br />

specific application.<br />

Retention Time Verification Standard<br />

AZ-8015-RTV $ 25 / 1 x 1 mL<br />

AZ-8015-RTV-PAK SAVE 20% $ 100 / 1 x 1 mL<br />

2000 µg/mL each in CH2Cl2 3 comps.<br />

n-Decane<br />

n-Docosane<br />

n-Dotriacontane<br />

Stock Calibration Standard<br />

AZ-8015-SCS $ 40 / 1 x 1 mL<br />

AZ-8015-SCS-PAK SAVE 20% $ 160 / 1 x 1 mL<br />

10000 µg/mL each in CH2Cl2 2 comps.<br />

#2 Diesel 10W 30 Motor Oil<br />

Oxygenate Gasoline Additive Standard<br />

OGAD-001 $ 30 / 1 x 1 mL<br />

OGAD-001-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

At stated conc. in MeOH 5 comps.<br />

MtBE (2000 µg/mL)<br />

ETBE (2000 µg/mL)<br />

Isopropyl ether (2000 µg/mL)<br />

TAME (2000 µg/mL)<br />

t-Butanol (10000 µg/mL)<br />

Ethanol<br />

M-8015B/5031-11 $ 25 / 1 x 1 mL<br />

10 mg/mL in Water<br />

Methanol<br />

M-8015B/5031-17 $ 20 / 1 x 1 mL<br />

10 mg/mL in Water<br />

Surrogate Standard<br />

GRH-SS $ 15 / 1 x 1 mL<br />

GRH-SS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

2.0 mg/mL in Acetone<br />

o-Terphenyl (OTP)<br />

Internal Standard<br />

GRH-IS $ 15 / 1 x 1 mL<br />

GRH-IS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

1.0 mg/mL in CH2Cl2 5-alpha Androstane<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

LUFT/LUST<br />

Arizona<br />

California<br />

Connecticut<br />

85<br />

LUFT/LUST


LUFT/LUST<br />

Florida<br />

Miss/Tenn<br />

Mult-State<br />

LUFT/LUST<br />

Florida Method Total Recoverable Petroleum Hydrocarbon (FTRPH) Standard & Surrogates<br />

Calibration/Window Defining Hydrocarbon Standard<br />

DRH-004S-5X $ 50 / 1 x 1 mL<br />

DRH-004S-5X-PAK SAVE 20% $ 200 / 5 x 1 mL<br />

1.0 mg/mL each in CH 2Cl 2 : CS 2 (1:1) 17 comps.<br />

FTRPH Calibration / Window Defining Standard<br />

DRH-FTRPH $ 35 / 1 x 1 mL<br />

DRH-FTRPH-PAK SAVE $ 150 / 5 x 1 mL<br />

500 µg/mL each in Hexane 17 comps.<br />

n-Octane<br />

n-Decane<br />

n-Dodecane<br />

n-Tetradecane<br />

n-Hexadecane<br />

n-Octadecane<br />

Internal Standard<br />

GRH-IS $ 15 / 1 x 1 mL<br />

GRH-IS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

1.0 mg/mL in CH 2Cl 2<br />

5-alpha Androstane<br />

n-Eicosane<br />

n-Docosane<br />

n-Tetracosane<br />

n-Hexacosane<br />

n-Octacosane<br />

n-Triacontane<br />

Mississippi / Tennessee Method<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods<br />

n-Dotriacontane<br />

n-Tetratriacontane<br />

n-Hexatriacontane<br />

n-Octatriacontane<br />

n-Tetracontane<br />

Surrogate <strong>Standards</strong><br />

DRH-SS $ 30 / 1 x 1 mL<br />

DRH-SS-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

5.0 mg/mL in THF<br />

n-Triacontane-d 62<br />

DRO Defining Mix<br />

AK-102.0-NAS-10X $ 40 / 1 x 1 mL<br />

AK-102.0-NAS-10X-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

2.0 mg/mL each in CH2Cl2 16 comps.<br />

86<br />

Octane C 8<br />

Decane C 10<br />

Dodecane C 12<br />

Tetradecane C 14<br />

Hexadecane C 16<br />

Octadecane C 18<br />

n-Decane<br />

n-Undecane<br />

n-Dodecane<br />

n-Tridecane<br />

n-Tetradecane<br />

n-Pentadecane<br />

Eicosane C 20<br />

Docosane C 22<br />

Tetracosane C 24<br />

Hexacosane C 26<br />

Octacosane C 28<br />

Triacontane C 30<br />

Technical Note<br />

n-Hexadecane<br />

n-Heptadecane<br />

n-Octadecane<br />

n-Nonadecane<br />

n-Eicosane<br />

Dotriacontane C 32<br />

Tetratriacontane C 34<br />

Hexatricontane C 36<br />

Octatriacontane C 38<br />

Tetracontane C 40<br />

The above FTRPH Calibration/Window Defining Standard was<br />

formulated at a lower concentration to insure solubility of the<br />

analytes & eliminate the odor caused by the introduction of Carbon<br />

disulfide as a cosolvent.<br />

n-Heneicosane<br />

n-Docosane<br />

n-Tricosane<br />

n-Tetracosane<br />

n-Pentacosane<br />

FTRPH Surrogate Standard<br />

DRH-FL-SS-3X $ 25 / 1 x 1 mL<br />

DRH-FL-SS-3X-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

3.0 mg/mL in Carbon disulfide<br />

DRH-FL-SS $ 20 / 1 x 1 mL<br />

DRH-FL-SS-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

1.0 mg/mL in Carbon disulfide<br />

Nonatriacontane<br />

FTRPH Combined Surrogate Standard<br />

DRH/GRH-FL-SS $ 50 / 1 x 1 mL<br />

DRH/GRH-FL-SS-PAK SAVE 20% $ 200 / 5 x 1 mL<br />

5.0 mg/mL in Carbon disulfide 2 comps.<br />

Nonatriacontane o-Terphenyl (OTP)<br />

The above FTRPH Surrogate Standard was formulated at a<br />

higher concentration for combined DRH & GRH analysis. This<br />

standard has proven useful for those laboratories performing<br />

gasoline & diesel analysis simultaneously.<br />

GRH-SS $ 30 / 1 x 1 mL<br />

GRH-SS-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

2.0 mg/mL in Acetone<br />

o-Terphenyl (OTP)<br />

Multi-State Method Hydrocarbon Window Defining<br />

DRH-008S-R2 $ 65 / 1 x 1 mL<br />

DRH-008S-R2-PAK SAVE 20% $ 260 / 5 x 1 mL<br />

500 µg/mL each in Chloroform 35 comps.<br />

Octane<br />

Nonane<br />

Decane<br />

Undecane<br />

Dodecane<br />

Tridecane<br />

Tetradecane<br />

Pentadecane<br />

Hexadecane<br />

Heptadecane<br />

Pristane<br />

Octadecane<br />

Phytane<br />

Nonadecane<br />

Eicosane<br />

Heneicosane<br />

Docosane<br />

Tricosane<br />

Technical Note<br />

NEW<br />

DRH/GRH-FL-SS-R2 $ 50 / 1 x 1 mL<br />

DRH/GRH-FL-SS-R2-PAK SAVE 20% $ 200 / 5 x 1 mL<br />

At stated conc. in Carbon disulfide 2 comps.<br />

Nonatriacontane (6000 µg/mL) o-Terphenyl (OTP) (1500 µg/mL)<br />

Technical Note<br />

Items in Carbon disulfide cannot ship by Air. Whenever possible<br />

we try to find an alternate solvent, however some long chain<br />

hydrocarbon will not go in solution or any other solvent.<br />

Tetracosane<br />

Pentacosane<br />

Hexacosane<br />

Heptacosane<br />

Octacosane<br />

Nonacosane<br />

Triacontane<br />

n-Hentriacontane<br />

Dotriacontane<br />

Technical Note<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

Tritriacontane<br />

Tetratriacontane<br />

Pentatriacontane<br />

Hexatriacontane<br />

Heptatriacontane<br />

Octatriacontane<br />

Nonatriacontane<br />

Tetracontane<br />

AccuStandard offers a hydrocarbon window defining standard with<br />

the C 8 to C 40 odd and even alkanes. Use of this one standard should<br />

meet the numerous state-to-state variations for hydrocarbon<br />

validation and reporting. As an added benefit, AccuStandard has<br />

included Pristane and Phytane in the formulation. Again, use of this<br />

one standard can meet numerous LUFT/LUST programs requiring<br />

that the C 17 (Pristane) and C 18 (Phytane) ratio be used to estimate<br />

subsurface degradation of fuel oil spills.


Massachusetts Method Determination of Extractable Petroleum Hydrocarbons (EPH)<br />

Aliphatic Surrogate<br />

DRH-007-SS $ 15 / 1 x 1 mL<br />

DRH-007-SS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

1.0 mg/mL in Hexane<br />

1-Chlorooctadecane<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods - Ready-to-Inject Working Level EPH <strong>Standards</strong><br />

Aromatic Hydrocarbons Calibration Set<br />

DRH-006-CAL-SET $ 125 / 5 x 1 mL<br />

At stated conc. in CH2Cl2 18 comps.<br />

Cat. No.<br />

DRH-006-CAL-1X<br />

DRH-006-CAL-4X<br />

DRH-006-CAL-10X<br />

DRH-006-CAL-20X<br />

Aliphatic Hydrocarbons Calibration Set<br />

DRH-006-CAL-40X<br />

Components Level 1 Level 2 Level 3 Level 4 Level 5<br />

(units in µg/mL) ( 1X ) ( 4X ) ( 10X ) ( 20X ) ( 40X )<br />

Acenaphthene 5 20 50 100 200<br />

Acenaphthylene 5 20 50 100 200<br />

Anthracene 5 20 50 100 200<br />

Benz[a]anthracene 5 20 50 100 200<br />

Benzo[a]pyrene 5 20 50 100 200<br />

Benzo[b]fluoranthene 5 20 50 100 200<br />

Benzo[g,h,i]perylene 5 20 50 100 200<br />

Benzo[k]fluoranthene 5 20 50 100 200<br />

Chrysene 5 20 50 100 200<br />

Dibenz[a,h]anthracene 5 20 50 100 200<br />

Fluoranthene 5 20 50 100 200<br />

Fluorene 5 20 50 100 200<br />

Indeno[1,2,3-cd]pyrene 5 20 50 100 200<br />

2-Methylnaphthalene 5 20 50 100 200<br />

Naphthalene 5 20 50 100 200<br />

Phenanthrene 5 20 50 100 200<br />

Pyrene 5 20 50 100 200<br />

o-Terphenyl (Surrogate) 5 20 50 100 200<br />

DRH-007-CAL-SET $ 125 / 5 x 1 mL<br />

At stated conc. in CH2Cl2 15 comps.<br />

Cat. No.<br />

DRH-007-CAL-1X<br />

DRH-007-CAL-4X<br />

DRH-007-CAL-10X<br />

DRH-007-CAL-40X<br />

DRH-007-CAL-20X<br />

Components Level 1 Level 2 Level 3 Level 4 Level 5<br />

(units in µg/mL) ( 1X ) ( 4X ) ( 10X ) ( 20X ) ( 40X )<br />

n-Nonane 5 20 50 100 200<br />

n-Decane 5 20 50 100 200<br />

n-Dodecane 5 20 50 100 200<br />

n-Tetradecane 5 20 50 100 200<br />

n-Hexadecane 5 20 50 100 200<br />

n-Octadecane 5 20 50 100 200<br />

n-Nonadecane 5 20 50 100 200<br />

n-Eicosane 5 20 50 100 200<br />

n-Docosane 5 20 50 100 200<br />

n-Tetracosane 5 20 50 100 200<br />

n-Hexacosane 5 20 50 100 200<br />

n-Octacosane 5 20 50 100 200<br />

n-Triacontane 5 20 50 100 200<br />

n-Hexatriacontane 5 20 50 100 200<br />

1-Chlorooctadecane (Surrogate) 5 20 50 100 200<br />

EPH Surrogate Spike<br />

DRH-MA-SS 20 µg/mL each in Acetone $ 10 / 1 x 1 mL<br />

DRH-MA-SS-10X 200 µg/mL each in Acetone $ 20 / 1 x 1 mL<br />

DRH-MA-SS-100X 2,000 µg/mL each in Acetone $ 20 / 1 x 1 mL<br />

DRH-MA-SS-100X-PAK 2,000 µg/mL each in Acetone $ 100 / 5 x 1 mL<br />

2 comps.<br />

1-Chlorooctadecane o-Terphenyl<br />

EPH Matrix Spike<br />

DRH-MA-MS 25 µg/mL in Acetone $ 20 / 1 x 1 mL<br />

DRH-MA-MS-PAK 25 µg/mL in Acetone SAVE 20% $ 80 / 5 x 1 mL<br />

DRH-MA-MS-10X 250 µg/mL in Acetone $ 30 / 1 x 1 mL<br />

DRH-MA-MS-10X-PAK 250 µg/mL in AcetoneSAVE 20% $ 120 / 5 x 1 mL<br />

DRH-MA-MS-40X 1,000 µg/mL in Acetone $ 30 / 1 x 1 mL<br />

DRH-MA-MS-40X-PAK 1,000 µg/mL in AcetoneSAVE 20% $ 120 / 5 x 1 mL<br />

10 comps.<br />

Acenaphthene<br />

Anthracene<br />

Chrysene<br />

n-Eicosane<br />

DEP (MA) - Aromatic Hydrocarbons<br />

DRH-006S $ 65 / 1 x 1 mL<br />

DRH-006S-PAK SAVE 20% $ 260 / 5 x 1 mL<br />

1.0 mg/mL each in CH2Cl2 17 comps.<br />

Acenaphthene<br />

Acenaphthylene<br />

Anthracene<br />

Benz[a]anthracene<br />

Benzo[a]pyrene<br />

Benzo[b]fluoranthene<br />

Benzo[g,h,i]perylene<br />

Benzo[k]fluoranthene<br />

Chrysene<br />

DEP (MA) - Aliphatic Hydrocarbons<br />

DRH-007S $ 40 / 1 x 1 mL<br />

DRH-007S-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

1.0 mg/mL each in CH 2Cl 2 : Hexane (1:1) 14 comps.<br />

n-Nonane<br />

n-Decane<br />

n-Dodecane<br />

n-Tetradecane<br />

n-Hexadecane<br />

n-Octadecane<br />

n-Nonadecane<br />

Technical Notes<br />

Naphthalene<br />

n-Nonadecane<br />

n-Nonane<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

Dibenz[a,h]anthracene<br />

Fluoranthene<br />

Fluorene<br />

Indeno[1,2,3-cd]pyrene<br />

2-Methylnaphthalene<br />

Naphthalene<br />

Phenanthrene<br />

Pyrene<br />

High Concentrates<br />

AccuStandard formulated two high concentration EPH<br />

stocks for laboratories that prepare in-house working level<br />

solutions.<br />

CCC Working Level<br />

In addition, AccuStandard received numerous requests to<br />

formulate Ready-to-Use working level aromatic and<br />

aliphatic calibration sets. AccuStandard's Product<br />

Development Team designed the two listed Calibration<br />

sets to meet those requests.<br />

Custom/Bulk Packaging<br />

Larger volumes of Daily Continuing Calibration solution<br />

can be purchased by contacting our Technical Service<br />

Department.<br />

n-Eicosane<br />

n-Docosane<br />

n-Tetracosane<br />

n-Hexacosane<br />

n-Octacosane<br />

n-Triacontane<br />

n-Hexatriacontane<br />

n-Octacosane<br />

Pyrene<br />

n-Tetradecane<br />

LUFT/LUST<br />

Massachusetts<br />

87<br />

LUFT/LUST


LUFT/LUST<br />

Massachusetts<br />

LUFT/LUST<br />

Massachusetts Method Determination of Extractable Petroleum Hydrocarbons (EPH) (Continued)<br />

DEP (MA) - Fractionation Surrogate Spike<br />

DRH-MA-FSS-10ML 40 µg/mL in Hexane $ 25 / 1 x 10 mL<br />

DRH-MA-FSS-50X 2.0 mg/mL in Hexane $ 25 / 1 x 1 mL<br />

DRH-MA-FSS-50X-PAK 2.0 mg/mL in HexaneSAVE 20% $ 100 / 5 x 1 mL<br />

2 comps.<br />

2-Fluorobiphenyl 2-Bromonaphthalene<br />

Aromatic Surrogate<br />

DRH-006-SS $ 15 / 1 x 1 mL<br />

DRH-006-SS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

1.0 mg/mL in CH 2Cl 2<br />

Internal Standard<br />

GRH-IS 1,000 µg/mL in CH2Cl2 $ 15 / 1 x 1 mL<br />

GRH-IS-PAK 1,000 µg/mL in CH2Cl2 SAVE 20% $ 60 / 5 x 1 mL<br />

GRH-IS-10X 10.0 mg/mL in CH2Cl2 $ 30 / 1 x 1 mL<br />

Massachusetts Method Determination of Volatile Petroleum Hydrocarbons (VPH)<br />

Stock Concentrate<br />

Volatile Petroleum Hydrocarbon Mix<br />

GRH-004S-10X $ 40 / 1 x 1 mL<br />

GRH-004S-10X-PAK SAVE 20% $ 160 / 5 x 1 mL<br />

At stated conc. in MeOH 13 comps.<br />

Benzene (5.0 mg/mL)<br />

Ethylbenzene (5.0 mg/mL)<br />

Isooctane (15.0 mg/mL)<br />

2-Methylpentane (15.0 mg/mL)<br />

MtBE (15.0 mg/mL)<br />

Naphthalene (10.0 mg/mL)<br />

n-Nonane (10.0 mg/mL)<br />

VPH Matrix Spike<br />

GRH-004-MS $ 15 / 1 x 1 mL<br />

GRH-004-MS-PAK $ 60 / 5 x 1 mL<br />

50 µg/mL each in MeOH 8 comps.<br />

GRH-004-MS-10X $ 25 / 1 x 1 mL<br />

GRH-004-MS-10X-PAK $ 100 / 5 x 1 mL<br />

500 µg/mL each in MeOH 8 comps.<br />

GRH-004-MS-100X $ 25 / 1 x 1 mL<br />

GRH-004-MS-100X-PAK $ 100 / 5 x 1 mL<br />

5,000 µg/mL each in MeOH 8 comps.<br />

Benzene<br />

Ethylbenzene<br />

MtBE<br />

Naphthalene<br />

Toluene<br />

o-Xylene<br />

n-Pentane (10.0 mg/mL)<br />

Toluene (15.0 mg/mL)<br />

1,2,4-Trimethylbenzene (10.0 mg/mL)<br />

o-Xylene (10.0 mg/mL)<br />

m-Xylene (10.0 mg/mL)<br />

p-Xylene (10.0 mg/mL)<br />

DEP (MA)-VPH Surrogate Standard<br />

GRH-004-SS $ 10 / 1 x 1 mL<br />

GRH-004-SS-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

50 µg/mL in MeOH<br />

GRH-004-SS-10X $ 20 / 1 x 1 mL<br />

GRH-004-SS-10X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

500 µg/mL in MeOH<br />

GRH-004-SS-100X $ 20 / 1 x 1 mL<br />

GRH-004-SS-100X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

5,000 µg/mL in MeOH<br />

88<br />

o-Terphenyl<br />

5-alpha Androstane<br />

2,5-Dibromotoluene<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods<br />

m-Xylene<br />

p-Xylene<br />

Combined Aromatic/Aliphatic<br />

Matrix Spike Standard<br />

DRH-MS-ASL $ 45 / 1 x 1 mL<br />

DRH-MS-ASL-PAK SAVE 20% $ 180 / 5 x 1 mL<br />

25 µg/mL each in Hexane 31 comps.<br />

Acenaphthene<br />

Acenaphthylene<br />

Anthracene<br />

Benz[a]anthracene<br />

Benzo[a]pyrene<br />

Benzo[b]fluoranthene<br />

Benzo[g,h,i]perylene<br />

Benzo[k]fluoranthene<br />

Chrysene<br />

n-Decane<br />

Dibenz[a,h]anthracene<br />

n-Docosane<br />

n-Dodecane<br />

n-Eicosane<br />

Fluoranthene<br />

Fluorene<br />

Volatile Petroleum Hydrocarbons<br />

with Surrogate Standard<br />

GRH-004S/SS $ 30 / 1 x 1 mL<br />

GRH-004S/SS-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

At stated conc. in MeOH 14 comps.<br />

Benzene (500 µg/mL)<br />

2,5-Dibromotoluene(Surrogate) (1,000 µg/mL)<br />

Ethylbenzene (500 µg/mL)<br />

Isooctane (1,500 µg/mL)<br />

2-Methylpentane (1,500 µg/mL)<br />

MtBE (1,500 µg/mL)<br />

Naphthalene (1,000 µg/mL)<br />

Certified BTEX in Unleaded Gasoline<br />

GA-001-20X-BTEX $ 55 / 1 x 1 mL<br />

10.0 mg/mL in MeOH<br />

Gasoline - Regular, unleaded<br />

n-Hexacosane<br />

n-Hexadecane<br />

n-Hexatriacontane<br />

Indeno[1,2,3-cd]pyrene<br />

2-Methylnaphthalene<br />

Naphthalene<br />

n-Nonadecane<br />

n-Nonane<br />

n-Octacosane<br />

n-Octadecane<br />

Phenanthrene<br />

Pyrene<br />

n-Tetracosane<br />

n-Tetradecane<br />

n-Triacontane<br />

Technical Notes<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

n-Nonane (1,000 µg/mL)<br />

n-Pentane (1,000 µg/mL)<br />

Toluene (1,500 µg/mL)<br />

1,2,4-Trimethylbenzene (1,000 µg/mL)<br />

o-Xylene (1,000 µg/mL)<br />

m-Xylene (1,000 µg/mL)<br />

p-Xylene (1,000 µg/mL)<br />

Calibration Curve<br />

Analytical chemists can easily develop the VPH Calibration Curve<br />

using one AccuStandard primary dilution standard that includes the<br />

surrogate.<br />

Simultaneous BTEX / Gasoline QA/QC<br />

AccuStandard's QA/QC department has certified the benzene,<br />

toluene, ethyl benzene and xylene concentrations in our unleaded<br />

gasoline standard (GA-001-20X-BTEX). Use of this standard allows<br />

the analytical chemist in a single injection to verify that the QA/QC<br />

requirements are being met for the BTEX analytes as well as the<br />

gasoline.<br />

AccuStandard's Product Development Team continues to look for<br />

innovative approaches to save the analytical laboratory time and<br />

money.


Pennsylvania Method Storage Tank Site Closure & Monitoring Petroleum <strong>Standards</strong><br />

Texas Method Storage Tank (PST) Division - TX Method 1005 <strong>Standards</strong><br />

Gasoline & Diesel Calibration Curve<br />

DRH-TX-003-SET<br />

Each mix contains:<br />

Regular, Unleaded Gasoline & #2 Diesel Fuel<br />

$ 125 / 8 x 1 mL<br />

Cat. No. Conc. Solvent<br />

DRH-TX-003-0.04X 20 µg/mL Pentane<br />

DRH-TX-003-0.2X 100 µg/mL Pentane<br />

DRH-TX-003-0.5X 250 µg/mL Pentane<br />

DRH-TX-003-1X 500 µg/mL Pentane<br />

DRH-TX-003-1.5X 750 µg/mL Pentane<br />

DRH-TX-003-2X 1000 µg/mL Pentane<br />

DRH-TX-003-10X 5000 µg/mL Pentane<br />

DRH-TX-003-20X 10000 µg/mL Pentane<br />

Surrogate Standard<br />

DRH-TX-003-SS1 $ 35 / 1 x 5 mL<br />

DRH-TX-003-SS1-PAK SAVE 20% $ 175 / 5 x 5 mL<br />

10 mg/mL each in Pentane 2 comps.<br />

1-Chlorooctadecane 1-Chlorooctane<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods<br />

PA Extractable PAH Standard<br />

DRH-PA-001 $ 25 / 1 x 1 mL<br />

DRH-PA-001-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

2000 µg/mL each in CH2Cl2 5 comps.<br />

Benz[a]anthracene<br />

Benzo[a]pyrene<br />

Fluorene<br />

Naphthalene<br />

Phenanthrene<br />

Gasoline & Diesel Calibration Set<br />

DRH-TX-002-D-SET $ 75 / 8 x 1 mL<br />

Each mix contains: Regular, Unleaded Gasoline & #2 Diesel Fuel<br />

Cat. No. Conc. Solvent<br />

DRH-TX-002-D-0.01X 5 µg/mL CH2Cl2 DRH-TX-002-D-0.04X 20 µg/mL CH2Cl2 DRH-TX-002-D-0.1X 50 µg/mL CH2Cl2 DRH-TX-002-D-0.2X 100 µg/mL CH2Cl2 DRH-TX-002-D-0.4X 200 µg/mL CH2Cl2 DRH-TX-002-D-1X 500 µg/mL CH2Cl2 DRH-TX-002-D-2X 1000 µg/mL CH2Cl2 DRH-TX-002-D-10X 5000 µg/mL CH2Cl2 Gasoline/Diesel Continuing Calibration Solution<br />

DRH-TX-002-D-0.4X-10ML $ 50 / 1 x 10 mL<br />

200 µg/mL each in CH2Cl2 2 comps.<br />

Gasoline - Regular, unleaded #2 Diesel Fuel<br />

Technical Notes<br />

PA Volatile Petroleum Standard<br />

GRH-PA-001 $ 25 / 1 x 1 mL<br />

GRH-PA-001-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

At stated conc. in MeOH 9 comps.<br />

Benzene (1000 µg/mL)<br />

Ethylbenzene (1000 µg/mL)<br />

MtBE (2000 µg/mL)<br />

Naphthalene (1000 µg/mL)<br />

Toluene (1000 µg/mL)<br />

n-Hexane<br />

n-Octane<br />

n-Decane<br />

n-Dodecane<br />

Aromatic Fractionation Check Standard<br />

DRH-TX-003-FCS $ 55 / 1 x 10 mL<br />

DRH-TX-003-FCS-PAK SAVE 20% $ 220 / 5 x 10 mL<br />

20 µg/mL each in Pentane 24 comps.<br />

Acenaphthene<br />

Acenaphthylene<br />

Anthracene<br />

Benzene<br />

Benz[a]anthracene<br />

Benzo[b]fluoranthene<br />

Benzo[k]fluoranthene<br />

Benzo[a]pyrene<br />

Carbon Number Distribution Maker<br />

DRH-TX-003-CNM $ 30 / 1 x 1 mL<br />

DRH-TX-003-CNM-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

2000 µg/mL each in Pentane 9 comps.<br />

n-Decane<br />

n-Dodecane<br />

n-Heneicosane<br />

n-Tetradecane<br />

n-Hexadecane<br />

n-Octadecane<br />

n-Eicosane<br />

Benzo[e]pyrene<br />

Benzo[g,h,i]perylene<br />

Chrysene<br />

Dibenz[a,h]anthracene<br />

Ethylbenzene<br />

Fluoranthene<br />

Fluorene<br />

Indeno[1,2,3-cd]pyrene<br />

n-Heptane<br />

n-Hexadecane<br />

n-Hexane<br />

o-Xylene (1000 µg/mL)<br />

m-Xylene (1000 µg/mL)<br />

p-Xylene (1000 µg/mL)<br />

Isopropylbenzene (1000 µg/mL)<br />

Stock Hydrocarbon Calibration Standard<br />

DRH-TX-001-10X $ 25 / 1 x 1 mL<br />

DRH-TX-001-10X-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

2000 µg/mL each in n-Pentane 12 comps.<br />

n-Docosane<br />

n-Tetracosane<br />

n-Hexacosane<br />

n-Octacosane<br />

Gasoline/Diesel Calibration/Matrix Spike Solution<br />

DRH-TX-002-10X $ 25 / 1 x 1 mL<br />

DRH-TX-002-10X-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

5000 µg/mL each in MeOH 2 comps.<br />

Gasoline - Regular, unleaded #2 Diesel Fuel<br />

Stock Gasoline/Diesel Calibration Solution<br />

DRH-TX-002-D-40X $ 25 / 1 x 1 mL<br />

DRH-TX-002-D-40X-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

20,000 µg/mL each in CH2Cl2 2 comps.<br />

Gasoline - Regular, unleaded #2 Diesel Fuel<br />

Texas Method 1005 Rev. 03 and 1006<br />

Over 22,000 notifications of leaking petroleum storage tanks have been received by the Texas Natural Resource Conservation Commission. At least 8000 of these leaks have<br />

affected groundwater resulting in the testing and monitoring of the site. The capability to test for TPH concentration and identify the petrochemical product offers analytical<br />

laboratories additional sources of revenue.<br />

New State specific methods have been proposed and promulgated to determine the Total concentration of Petroleum Hydrocarbons (TPH). AccuStandard continues to support<br />

the analytical community by developing these new formulations to meet both TNRCC method 1005 Rev. 3.0 and 1006. Additionally, QA/QC and Proficiency Testing samples are<br />

now available to monitor sample handling/testing procedures or to receive certification to perform TPH analysis.<br />

These new standards are in ready to use calibration curves, cost effective bulk quantities, and convenient concentrations to simplify the instrument calibration procedures.<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

Naphthalene<br />

Phenanthrene<br />

Pyrene<br />

Toluene<br />

1,2,3-Trimethylbenzene<br />

m-Xylene<br />

p-Xylene<br />

o-Xylene<br />

n-Octacosane<br />

n-Octane<br />

n-Pentatriacontane<br />

LUFT/LUST<br />

89<br />

Penn<br />

Texas<br />

LUFT/LUST


LUFT/LUST<br />

Washington<br />

LUFT/LUST<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods<br />

Washington Method Determination of Volatile Petroleum Hydrocarbons (VPH)<br />

VPH Solution<br />

WA-VPH $ 30 / 1 x 1 mL<br />

WA-VPH-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

200 µg/mL each in MeOH 15 comps.<br />

Benzene<br />

Ethylbenzene<br />

Toluene<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene<br />

MtBE<br />

n-Pentane<br />

n-Hexane<br />

n-Octane<br />

n-Decane<br />

n-Dodecane<br />

1-Methylnaphthalene<br />

Naphthalene<br />

1,2,3-Trimethylbenzene<br />

VPH Matrix Spike<br />

WA-VPH-MS $ 25 / 1 x 1 mL<br />

WA-VPH-MS-PAK SAVE 20% $ 100 / 5 x 1 mL<br />

Varied conc. in MeOH 11 comps.<br />

Benzene (60 µg/mL)<br />

Ethylbenzene (60 µg/mL)<br />

MTBE (180 µg/mL)<br />

Naphthalene (360 µg/mL)<br />

n-Nonane (200 µg/mL)<br />

n-Pentane (600 µg/mL)<br />

Toluene (60 µg/mL)<br />

1,2,3-Trimethylbenzene (60 µg/mL)<br />

m-Xylene (60 µg/mL)<br />

p-Xylene (60 µg/mL)<br />

o-Xylene (60 µg/mL)<br />

Certified BTEX in Unleaded Gasoline<br />

(Single Source)<br />

GA-001-20X-BTEX $ 55 / 1 x 1 mL<br />

10.0 mg/mL in MeOH<br />

Certified BTEX in Gasoline<br />

Composite Mix (Multi Source)<br />

AK-101.0-GCS-BTEX $ 55 / 1 x 1 mL<br />

5 mg/mL each in MeOH 3 comps.<br />

90<br />

Gasoline - Regular, unleaded<br />

Gasoline - Premium (1.66 mg/mL<br />

Gasoline - Regular, leaded (1.67 mg/mL)<br />

Gasoline - Regular, unleaded (1.67 mg/mL)<br />

VPH Primary Dilution Standard<br />

with Surrogate<br />

WA-VPH-10X-SS $ 35 / 1 x 1 mL<br />

WA-VPH-10X-SS-PAKSAVE 20% $ 140 / 5 x 1 mL<br />

2,000 µg/mL each in MeOH 16 comps.<br />

Benzene<br />

Ethylbenzene<br />

Toluene<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene<br />

MtBE<br />

n-Pentane<br />

n-Hexane<br />

n-Octane<br />

n-Decane<br />

n-Dodecane<br />

1-Methylnaphthalene<br />

Naphthalene<br />

1,2,3-Trimethylbenzene<br />

2,5-Dibromotoluene (surrogate)<br />

VPH Surrogate Standard<br />

GRH-004-SS $ 10 / 1 x 1 mL<br />

GRH-004-SS-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

50 µg/mL in MeOH<br />

GRH-004-SS-10X $ 20 / 1 x 1 mL<br />

GRH-004-SS-10X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

500 µg/mL in MeOH<br />

GRH-004-SS-100X $ 20 / 1 x 1 mL<br />

GRH-004-SS-100X-PAKSAVE 20% $ 80 / 5 x 1 mL<br />

5,000 µg/mL in MeOH<br />

2,5-Dibromotoluene<br />

Stock Concentrate VPH Solutions<br />

WA-VPH-10X $ 30 / 1 x 1 mL<br />

WA-VPH-10X-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

2,000 µg/mL each in MeOH 15 comps.<br />

WA-VPH-100X $ 35 / 1 x 1 mL<br />

WA-VPH-100X-PAK SAVE 20% $ 140 / 5 x 1 mL<br />

20.0 mg/mL each in MeOH 15 comps.<br />

Benzene<br />

Ethylbenzene<br />

Toluene<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene<br />

MtBE<br />

n-Pentane<br />

n-Pentane<br />

n-Hexane<br />

n-Octane<br />

n-Hexane<br />

n-Octane<br />

n-Decane<br />

n-Dodecane<br />

1-Methylnaphthalene<br />

Naphthalene<br />

1,2,3-Trimethylbenzene<br />

VPH Retention Time Marker<br />

WA-VPH-RT $ 20 / 1 x 1 mL<br />

WA-VPH-RT-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

2,000 µg/mL each in MeOH 6 comps.<br />

n-Decane<br />

n-Dodecane<br />

n-Tridecane<br />

1,2,3-Trimethylbenzene Standard<br />

V-028S-D-10X $ 20 / 1 x 1 mL<br />

V-028S-D-10X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

1000 µg/mL each in CH 2Cl 2<br />

Technical Notes<br />

1,2,3-Trimethylbenzene<br />

Simultaneous BTEX / Gasoline QA/QC<br />

AccuStandard's QA/QC department has certified the benzene, toluene, ethyl<br />

benzene and xylene concentrations in our unleaded gasoline Standard.<br />

(GA-001-20X-BTEX and in AK-101.0-GCS-BTEX). Use of either standard allows<br />

the analytical chemist in a single injection to verify that the QA/QC requirements<br />

are being met for the BTEX analytes as well as for the gasoline.<br />

Since formulating the <strong>Standards</strong> for the TPH methods and because of numerous<br />

laboratory requests, we have added a new multi source certified BTEX in<br />

gasoline composite mix (AK-101.0-GCS-BTEX). The BTEX values for this multi<br />

source calibration standard have been determined through in-house analysis<br />

against a BTEX multi level calibration curve.<br />

AccuStandard's Product Development Team continues to look for innovative<br />

approaches to save the analytical laboratory time and money.<br />

Washington EPH <strong>Standards</strong> on Next Page<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


Washington Method Determination of Extractable Petroleum Hydrocarbons (EPH)<br />

EPH Aromatic/PAH Standard<br />

WA-EPH-10X $ 75 / 1 x 1 mL<br />

WA-EPH-10X-PAK SAVE 20% $ 300 / 5 x 1 mL<br />

1.0 mg/mL each in CH2Cl2 18 comps.<br />

Acenaphthene<br />

Acenaphthylene<br />

Anthracene<br />

Benz[a]anthracene<br />

Benzo[a]pyrene<br />

Benzo[b]fluoranthene<br />

Benzo[g,h,i]perylene<br />

Benzo[k]fluoranthene<br />

Chrysene<br />

Acenaphthene<br />

Anthracene<br />

Benzo[g,h,i]perylene<br />

Benzo[a]pyrene<br />

n-Decane<br />

n-Dodecane<br />

n-Hexadecane<br />

n-Heneicosane<br />

Naphthalene<br />

Pyrene<br />

Wisconsin Method<br />

Wisconsin DNR - Gasoline Range Hydrocarbons<br />

GRH-003S $ 35 / 1 x 1 mL<br />

GRH-003S-PAK SAVE 20% $ 140 / 5 x 1 mL<br />

2.0 mg/mL each in MeOH 10 comps.<br />

Benzene<br />

Ethylbenzene<br />

MtBE<br />

Naphthalene<br />

Toluene<br />

Dibenz[a,h]anthracene<br />

Fluoranthene<br />

Fluorene<br />

Indeno[1,2,3-cd]pyrene<br />

2-Methylnaphthalene<br />

Naphthalene<br />

Phenanthrene<br />

Pyrene<br />

1,2,3-Trimethylbenzene<br />

Internal Standard<br />

GRH-IS $ 15 / 1 x 1 mL<br />

1,000 µg/mL in CH 2Cl 2<br />

GRH-IS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

1,000 µg/mL in CH 2Cl 2<br />

GRH-IS-10X $ 30 / 1 x 1 mL<br />

10.0 mg/mL in CH 2Cl 2<br />

5-alpha Androstane<br />

EPH Surrogate Spike<br />

DRH-MA-SS $ 10 / 1 x 1 mL<br />

20 µg/mL each in Acetone 2 comps.<br />

DRH-MA-SS-10X $ 20 / 1 x 1 mL<br />

200 µg/mL each in Acetone 2 comps.<br />

DRH-MA-SS-100X $ 20 / 1 x 1 mL<br />

DRH-MA-SS-100X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

2,000 µg/mL each in Acetone 2 comps.<br />

1-Chlorooctadecane o-Terphenyl<br />

EPH Matrix Spike<br />

WA-EPH-MS2-20ML $ 30 / 1 x 20 mL<br />

WA-EPH-MS2-20ML-PAK<br />

25 µg/mL each in Acetone 10 comps.<br />

LUFT/LUST <strong>Standards</strong><br />

State Methods<br />

n-Octane<br />

n-Decane<br />

n-Dodecane<br />

1,2,4-Trimethylbenzene<br />

1,3,5-Trimethylbenzene<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene<br />

EPH Aliphatic Check Mix<br />

WA-EPH-ALI $ 20 / 1 x 1 mL<br />

WA-EPH-ALI-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

1.0 mg/mL each in CH2Cl2 5 comps.<br />

Acenaphthene<br />

Benzo[g,h,i]perylene<br />

Naphthalene<br />

n-Octane<br />

n-Decane<br />

n-Dodecane<br />

Acenaphthene<br />

Benzo[g,h,i]perylene<br />

Naphthalene<br />

n-Hexadecane<br />

n-Heneicosane<br />

EPH Aromatic Check Mix<br />

WA-EPH-ARO $ 30 / 1 x 1 mL<br />

WA-EPH-ARO-PAKSAVE 20% $ 120 / 5 x 1 mL<br />

1.0 mg/mL each in CH2Cl2 5 comps.<br />

Pyrene<br />

1,2,3-Trimethylbenzene<br />

Revised EPH Aliphatic<br />

Check Mix<br />

WA-EPH-ALI-R1 $ 20 / 1 x 1 mL<br />

WA-EPH-ALI-R1-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

1.0 mg/mL each in CH2Cl2 6 comps.<br />

n-Hexadecane<br />

n-Heneicosane<br />

n-Tetratriacontane<br />

Revised EPH Aromatic<br />

Check Mix<br />

WA-EPH-ARO-R1 $ 30 / 1 x 1 mL<br />

WA-EPH-ARO-R1-PAK $ 120 / 5 x 1 mL<br />

1.0 mg/mL each in CH2Cl2 6 comps.<br />

Pyrene<br />

1,2,3-Trimethylbenzene<br />

Toluene<br />

Aliphatic Surrogate<br />

DRH-007-SS $ 15 / 1 x 1 mL<br />

DRH-007-SS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

1.0 mg/mL in Hexane<br />

1-Chlorooctadecane<br />

Aromatic Surrogate<br />

DRH-006-SS $ 15 / 1 x 1 mL<br />

DRH-006-SS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

1.0 mg/mL in CH 2Cl 2<br />

o-Terphenyl<br />

EPH Fractionation Check Solution<br />

WA-EPH-FCS $ 45 / 1 x 1 mL<br />

WA-EPH-FCS-PAK SAVE 20% $ 180 / 5 x 1 mL<br />

25 µg/mL each in Hexane 24 comps.<br />

Acenaphthene<br />

Acenaphthylene<br />

Anthracene<br />

Benz[a]anthracene<br />

Benzo[a]pyrene<br />

Benzo[b]fluoranthene<br />

Benzo[g,h,i]perylene<br />

Benzo[k]fluoranthene<br />

Chrysene<br />

Dibenz[a,h]anthracene<br />

Fluoranthene<br />

Fluorene<br />

Acenaphthene<br />

Acenaphthylene<br />

Anthracene<br />

Benz[a]anthracene<br />

Benzo[a]pyrene<br />

Benzo[b]fluoranthene<br />

Benzo[g,h,i]perylene<br />

Benzo[k]fluoranthene<br />

Chrysene<br />

Dibenz[a,h]anthracene<br />

Fluoranthene<br />

Fluorene<br />

Indeno[1,2,3-cd]pyrene<br />

2-Methylnaphthalene<br />

Naphthalene<br />

Phenanthrene<br />

Pyrene<br />

n-Decane<br />

n-Dodecane<br />

n-Tetradecane<br />

n-Hexadecane<br />

n-Octadecane<br />

n-Eicosane<br />

n-Heneicosane<br />

Revised EPH Fractionation Check<br />

Solution<br />

WA-EPH-FCS-R1 $ 45 / 1 x 1 mL<br />

WA-EPH-FCS-R1-PAKSAVE 20% $ 180 / 5 x 1 mL<br />

25 µg/mL each in Hexane 23 comps<br />

Indeno[1,2,3-cd]pyrene<br />

2-Methylnaphthalene<br />

Naphthalene<br />

Phenanthrene<br />

Pyrene<br />

n-Octane<br />

n-Decane<br />

n-Dodecane<br />

n-Hexadecane<br />

n-Heneicosane<br />

n-Tetratriacontane<br />

1,2,3-Trimethylbenzene Standard<br />

V-028S-D-10X $ 20 / 1 x 1 mL<br />

V-028S-D-10X-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

1000 µg/mL each in CH 2Cl 2<br />

1,2,3-Trimethylbenzene<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

LUFT/LUST<br />

Washington<br />

Wisconsin<br />

91<br />

LUFT/LUST


LUFT/LUST TPH<br />

LUFT/LUST<br />

LUFT/LUST <strong>Standards</strong><br />

Complete Set of Total Petroleum Hydrocarbon (TPH) Pattern Recognition <strong>Standards</strong><br />

AccuStandard has assembled the following sets to identify specific petroleum product types found during LUFT/LUST investigations. The sets<br />

can be purchased using one convenient Cat. No. or as individuals.<br />

TPH-SET $ 535 / 33 x 1 mL (includes TPH-001-SET, TPH-002-SET, TPH-003-SET, TPH-004-SET)<br />

Motor Fuels & Lubricating Oils Set<br />

TPH-001-SET $ 180 / 11 x 1 mL (Set includes Cat. No.'s listed in Bold)<br />

Heating Fuel Oils Set<br />

TPH-002-SET $ 115 / 7 x 1 mL (Set includes Cat. No.'s listed in Bold)<br />

92<br />

Conc. 1 mL<br />

Description (mg/mL) Solv. Cat. No. Price<br />

Regular unleaded 0.5 MeOH GA-001 $ 10<br />

20 MeOH GA-001-40X 20<br />

20 CH 2Cl 2 GA-001-D-40X 20<br />

Regular leaded 0.5 MeOH GA-002 10<br />

20 MeOH GA-002-40X 20<br />

20 CH 2Cl 2 GA-002-D-40X 20<br />

Premium 0.5 MeOH GA-003 10<br />

20 MeOH GA-003-40X 20<br />

20 CH 2Cl 2 GA-003-D-40X 20<br />

RFA Gasoline 0.5 MeOH GA-005 10<br />

(oxygenate free) 20 MeOH GA-005-40X 20<br />

20 CH 2Cl 2 GA-005-D-40X 20<br />

#2 Diesel 0.5 MeOH FU-009 10<br />

(conventional) 20 MeOH FU-009-40X 20<br />

20 CH 2Cl 2 FU-009-D-40X 20<br />

#1 Diesel 0.5 MeOH FU-013 10<br />

(low sulfur) 20 MeOH FU-013-40X 20<br />

20 CH 2Cl 2 FU-013-D-40X 20<br />

#2 Diesel 0.5 MeOH FU-017 10<br />

(extra low sulfur) 20 MeOH FU-017-40X 20<br />

20 CH 2Cl 2 FU-017-D-40X 20<br />

Arctic Diesel 0.5 MeOH FU-023 10<br />

20 MeOH FU-023-40X 20<br />

20 CH 2Cl 2 FU-023-D-40X 20<br />

SAE 30 W motor oil 0.5 Hexane FU-018-H 10<br />

20 Hexane FU-018-H-40X 20<br />

20 CH 2Cl 2 FU-018-D-40X 20<br />

SAE 40 W motor oil 0.5 Hexane FU-019-H 10<br />

20 Hexane FU-019-H-40X 20<br />

20 CH 2Cl 2 FU-019-D-40X 20<br />

SAE 50 W motor oil 0.5 Hexane FU-021-H 10<br />

20 Hexane FU-021-H-40X 20<br />

20 CH 2Cl 2 FU-021-D-40X 20<br />

Conc. 1 mL<br />

Description (mg/mL) Solv. Cat. No. Price<br />

#1 Fuel Oil 0.5 MeOH FU-001 $ 10<br />

20 MeOH FU-001-40X 20<br />

20 CH 2Cl 2 FU-001-D-40X 20<br />

#2 Fuel Oil 0.5 MeOH FU-002 10<br />

20 MeOH FU-002-40X 20<br />

20 CH 2Cl 2 FU-002-D-40X 20<br />

#3 Fuel Oil 0.5 Hexane FU-003 10<br />

20 Hexane FU-003-40X 20<br />

20 CH 2Cl 2 FU-003-D-40X 20<br />

#4 Fuel Oil 0.5 Hexane FU-004 10<br />

20 Hexane FU-004-40X 20<br />

20 CH 2Cl 2 FU-004-D-40X 20<br />

#5 Fuel Oil 0.5 Hexane FU-007 10<br />

20 Hexane FU-007-40X 20<br />

20 CH 2Cl 2 FU-007-D-40X 20<br />

#6 Fuel Oil 0.5 Hexane FU-008 10<br />

20 Hexane FU-008-40X 20<br />

20 CH 2Cl 2 FU-008-D-40X 20<br />

Kerosene 0.5 MeOH FU-005 10<br />

20 MeOH FU-005-40X 20<br />

20 CH 2Cl 2 FU-005-D-40X 20<br />

Aviation Fuels & Oils Set<br />

TPH-003-SET $ 160 / 10 x 1 mL (Set includes Cat. No.'s listed in Bold)<br />

Conc. 1 mL<br />

Description (mg/mL) Solv. Cat. No. Price<br />

Aviation (gas) 0.5 MeOH GA-004 $ 10<br />

Grade 100 LL 20 MeOH GA-004-40X 20<br />

20 CH 2Cl 2 GA-004-D-40X 20<br />

JP-4 Fuel 0.5 MeOH FU-010 10<br />

20 MeOH FU-010-40X 20<br />

20 CH 2Cl 2 FU-010-D-40X 20<br />

JP-5 Fuel 0.5 MeOH FU-012 10<br />

20 MeOH FU-012-40X 20<br />

20 CH 2Cl 2 FU-012-D-40X 20<br />

JP-7 Fuel 0.5 MeOH FU-014 10<br />

20 MeOH FU-014-40X 20<br />

20 CH 2Cl 2 FU-014-D-40X 20<br />

JP-8 Fuel 0.5 MeOH FU-015 10<br />

20 MeOH FU-015-40X 20<br />

20 CH 2Cl 2 FU-015-D-40X 20<br />

JP-10 Fuel 0.5 MeOH FU-022 10<br />

(Cruise Missile) 20 MeOH FU-022-40X 20<br />

20 CH 2Cl 2 FU-022-D-40X 20<br />

JP-TS 0.5 MeOH FU-016 10<br />

20 MeOH FU-016-40X 20<br />

20 CH 2Cl 2 FU-016-D-40X 20<br />

Jet Fuel (type 1) 0.5 MeOH FU-011 10<br />

20 MeOH FU-011-40X 20<br />

20 CH 2Cl 2 FU-011-D-40X 20<br />

Turbine (Jet A) Fuel 0.5 MeOH FU-006 10<br />

20 MeOH FU-006-40X 20<br />

20 CH 2Cl 2 FU-006-D-40X 20<br />

Hydraulic oil 0.5 Hexane FU-020-H 10<br />

20 Hexane FU-020-H-40X 20<br />

20 CH 2Cl 2 FU-020-D-40X 20<br />

Household & Industrial Solvent Set<br />

TPH-004-SET $ 80 / 5 x 1 mL (Set includes Cat. No.'s listed in Bold)<br />

Conc. 1 mL<br />

Description (mg/mL) Solv. Cat. No. Price<br />

Lacquer thinner 1 gram Neat HS-001N $ 10<br />

0.5 MeOH HS-001S 10<br />

20.0 MeOH HS-001S-40X 20<br />

20.0 CH 2Cl 2 HS-001S-D-40X 20<br />

Mineral spirits 1 gram Neat HS-002N 10<br />

0.5 MeOH HS-002S 10<br />

20.0 MeOH HS-002S-40X 20<br />

20.0 CH 2Cl 2 HS-002S-D-40X 20<br />

Naphtha 1 gram Neat HS-003N 10<br />

0.5 MeOH HS-003S 10<br />

20.0 MeOH HS-003S-40X 20<br />

20.0 CH 2Cl 2 HS-003S-D-40X 20<br />

Turpentine 1 gram Neat HS-004N 10<br />

0.5 MeOH HS-004S 10<br />

20.0 MeOH HS-004S-40X 20<br />

20.0 CH 2Cl 2 HS-004S-D-40X 20<br />

Stoddard 1 gram Neat HS-005N 10<br />

0.5 MeOH HS-005S 10<br />

20.0 MeOH HS-005S-40X 20<br />

20.0 CH 2Cl 2 HS-005S-D-40X 20<br />

Motor Oil & Weathered Fuels <strong>Standards</strong> on Next Page<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


Motor Oil <strong>Standards</strong><br />

Conc. 1 mL<br />

Description (mg/mL) Solv. Cat. No. Price<br />

SAE 5W 30 0.5 Hexane FU-025-H $ 10<br />

Motor Oil 20.0 Hexane FU-025-H-40X 20<br />

20.0 CH 2Cl 2 FU-025-D-40X 20<br />

SAE 10W 30 0.5 Hexane FU-026-H 10<br />

Motor Oil 20.0 Hexane FU-026-H-40X 20<br />

20.0 CH 2Cl 2 FU-026-D-40X 20<br />

Weathered Fuels<br />

LUFT/LUST <strong>Standards</strong><br />

Conc. 1 mL<br />

Description (mg/mL) Solv. Cat. No. Price<br />

SAE 10W 40 0.5 Hexane FU-027-H $ 10<br />

Motor Oil 20.0 Hexane FU-027-H-40X 20<br />

20.0 CH 2Cl 2 FU-027-D-40X 20<br />

SAE 20W 50 0.5 Hexane FU-028-H 10<br />

Motor Oil 20.0 Hexane FU-028-H-40X 20<br />

20.0 CH 2Cl 2 FU-028-D-40X 20<br />

Weathered LUFT/LUST Fuels<br />

Petroleum Products contain many different chemicals, plus synthetic product additives. Typically, these petroleum products are subdivided into<br />

two groups based on their volatility: [a] gasoline related products (more volatile) and [b] fuel related products (less volatile such as kerosene,<br />

aviation fuels, diesel fuels and heating oils).<br />

Most analytical methods for petroleum products focus on several items: the level of BTEX, the total petroleum hydrocarbon number (TPH), and<br />

the fingerprint of the petroleum product. Depending on the volatility of the petroleum product spilled, the nature of the contaminated soil, and<br />

the age of the spill, analysis becomes even more difficult. Weathering, evaporation, and the migration of the lighter volatiles at the contamination<br />

site can affect the fingerprint identification portion of the fuel products analysis.<br />

AccuStandard designed the weathered fuel line to artificially mimic the weathering, evaporation, and migration process. Use of these standards<br />

can help in the identification of the fuel type if it has been present in the ground for some time, in a sandy type soil with possible evaporation<br />

loss, or has migrated from the plume point of origin.<br />

Weathered Gasoline Set<br />

WGU-SET $ 85 / 4 x 1 mL<br />

Gasoline - Regular, unleaded 5.0 mg/mL in MeOH GA-001-10X $ 20 / 1 x 1 mL<br />

Gasoline - Regular, unleaded (25% Weathered) 5.0 mg/mL in MeOH GA-W25-10X $ 25 / 1 x 1 mL<br />

Gasoline - Regular, unleaded (50% Weathered) 5.0 mg/mL in MeOH GA-W50-10X $ 25 / 1 x 1 mL<br />

Gasoline - Regular, unleaded (75% Weathered) 5.0 mg/mL in MeOH GA-W75-10X $ 25 / 1 x 1 mL<br />

Weathered Kerosene Set<br />

WFK-SET $ 85 / 4 x 1 mL<br />

Kerosene 5.0 mg/mL in CH 2Cl 2 FU-005-D-10X $ 20 / 1 x 1 mL<br />

Kerosene (25% Weathered) 5.0 mg/mL in CH 2Cl 2 FK-W25-10X $ 25 / 1 x 1 mL<br />

Kerosene (50% Weathered) 5.0 mg/mL in CH 2Cl 2 FK-W50-10X $ 25 / 1 x 1 mL<br />

Kerosene (75% Weathered) 5.0 mg/mL in CH 2Cl 2 FK-W75-10X $ 25 / 1 x 1 mL<br />

Weathered #2 Diesel (extra Low Sulfur Content) Set<br />

WFD2-SET $ 85 / 4 x 1 mL<br />

#2 Diesel fuel (extra Low Sulfur) 5.0 mg/mL in CH 2Cl 2 FU-017-D-10X $ 20 / 1 x 1 mL<br />

#2 Diesel fuel (extra Low Sulfur) (25% Weathered) 5.0 mg/mL in CH 2Cl 2 FD2-W25-10X $ 25 / 1 x 1 mL<br />

#2 Diesel fuel (extra Low Sulfur) (50% Weathered) 5.0 mg/mL in CH 2Cl 2 FD2-W50-10X $ 25 / 1 x 1 mL<br />

#2 Diesel fuel (extra Low Sulfur) (75% Weathered) 5.0 mg/mL in CH 2Cl 2 FD2-W75-10X $ 25 / 1 x 1 mL<br />

Weathered #2 Diesel (Conventional) Set<br />

WFD2-R1-SET $ 85 / 4 x 1 mL<br />

#2 Diesel fuel (Conventional) 5.0 mg/mL in CH 2Cl 2 FU-009-D-10X $ 20 / 1 x 1 mL<br />

#2 Diesel fuel (Conventional) (25% Weathered) 5.0 mg/mL in CH 2Cl 2 FD2-W25-R1-10X $ 25 / 1 x 1 mL<br />

#2 Diesel fuel (Conventional) (50% Weathered) 5.0 mg/mL in CH 2Cl 2 FD2-W50-R1-10X $ 25 / 1 x 1 mL<br />

#2 Diesel fuel (Conventional) (75% Weathered) 5.0 mg/mL in CH 2Cl 2 FD2-W75-R1-10X $ 25 / 1 x 1 mL<br />

Total Petroleum Hydrocarbon Pattern Recognition <strong>Standards</strong><br />

This book contains chromatography for the various petroleum products typically found during<br />

LUFT/LUST site investigations. The chromatography shows each fuel pattern in a 25 minute analytical<br />

run for early eluting petroleum products like gasoline to late eluting products like motor oil. In<br />

addition, an n-alkane standard (DRH-008S) analyzed under identical conditions has been overlaid on<br />

each petroleum product chromatogram. Use of the book will assist the chemist’s identification of the<br />

fuel for pattern recognition.<br />

The n-alkane standard (DRH-008S) overlay provides n-alkane reference points between the standard<br />

and the unknown sample. These beginning and ending n-alkane reference points can be used to<br />

establish gross hydrocarbon concentrations. By comparing the specific n-alkane range of the closest<br />

identified petroleum standard to that of the unknown sample, a reproducible gross hydrocarbon number<br />

can be achieved.<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

Motor Oil Composite<br />

Standard<br />

MO-COMP-D-40X $ 30 / 1 x 1 mL<br />

5000 µg/mL each in CH2Cl2 4 comps.<br />

5w30 Motor oil<br />

10w30 Motor oil<br />

10w40 Motor oil<br />

20w50 Motor oil<br />

To Order:<br />

TPH Book<br />

BOOK-TPH $ 35<br />

LUFT/LUST TPH<br />

Weathered<br />

Fuels<br />

93<br />

LUFT/LUST


LUFT/LUST GRH<br />

LUFT/LUST<br />

Gasoline Range Hydrocarbon Analysis<br />

EPA Method - Gasoline Range Hydrocarbons<br />

Gasoline Standard<br />

GRH-002S $ 25 / 1 x 1 mL<br />

At stated conc. in MeOH 10 comps.<br />

2-Methylpentane (1.5 mg/mL)<br />

2,2,4-Trimethylpentane (1.5 mg/mL)<br />

Heptane (0.5 mg/mL)<br />

Benzene (0.5 mg/mL)<br />

Toluene (1.5 mg/mL)<br />

LUFT/LUST <strong>Standards</strong><br />

Gasoline Range<br />

Ethylbenzene (0.5 mg/mL)<br />

m-Xylene (1.0 mg/mL)<br />

p-Xylene (1.0 mg/mL)<br />

o-Xylene (1.0 mg/mL)<br />

1,2,4-Trimethylbenzene (1.0 mg/mL)<br />

Internal Standard<br />

GARH-IS $15 / 1 x 1 mL<br />

1.0 mg/mL in CH2Cl2 Chloro-4-fluorobenzene<br />

Surrogate Standard<br />

GARH-SS $ 20 / 1 x 1 mL<br />

2.5 mg/mL in Acetone<br />

4-Bromofluorobenzene<br />

Gasoline Additives<br />

GAD-001 $ 20 / 1 x 1 mL<br />

GAD-001-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

0.2 mg/mL each in MeOH 4 comps.<br />

Dibromomethane<br />

1,2-Dibromoethane<br />

Benzene<br />

Ethyl benzene<br />

Toluene<br />

1,2-Dichloroethane<br />

Methyl t-butyl ether<br />

Certified BTEX in Unleaded Gasoline<br />

GA-001-20X-BTEX $ 55 / 1 x 1 mL<br />

10.0 mg/mL in MeOH<br />

Hexadecane Extraction Volatiles<br />

CLP-BTEX $ 30 / 1 x 1 mL<br />

CLP-BTEX-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

0.2 mg/mL each in MeOH 6 comps.<br />

CLP-BTEX-10X $ 30 / 1 x 1 mL<br />

CLP-BTEX-10X-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

2.0 mg/mL each in MeOH 6 comps.<br />

94<br />

Regular unleaded gasoline<br />

Technical Note<br />

Simultaneous BTEX/Gasoline QA/QC<br />

AccuStandard's QA/QC department has certified the benzene,<br />

toluene, ethyl benzene and xylene concentrations in our<br />

unleaded gasoline standard. Use of GA-001-20X-BTEX allows<br />

the analytical chemist in a single injection to verify that QA/QC<br />

requirements are being met for the BTEX analytes as well as<br />

the gasoline.<br />

AccuStandard's Product Development Team continues to look<br />

for innovative approaches to save the analytical laboratory time<br />

and money.<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene<br />

California - Gasoline Range Hydrocarbons<br />

S-603A-10X $ 25 / 1 x 1 mL<br />

S-603A-10X-PAK SAVE 25% $ 90 / 5 x 1 mL<br />

2.0 mg/mL each in MeOH 7 comps.<br />

Benzene<br />

Ethylbenzene<br />

Methyl t-butyl ether<br />

Toluene<br />

Los Angeles County Well Investigation and<br />

Monitoring Program<br />

Purgeable Aromatics - Gasoline ID<br />

M-602-GAS-10X $ 30 / 1 x 1 mL<br />

2.0 mg/mL each in MeOH 11 comps.<br />

Benzene<br />

Chlorobenzene<br />

1,2-Dichlorobenzene<br />

1,3-Dichlorobenzene<br />

1,4-Dichlorobenzene<br />

Ethylbenzene<br />

Oxygenate Gasoline Additive Standard<br />

OGAD-001 $ 30 / 1 x 1 mL<br />

OGAD-001-PAK $ 120 / 1 x 1 mL<br />

At stated conc. in MeOH 5 comps.<br />

MtBE (2000 µg/mL)<br />

ETBE (2000 µg/mL)<br />

Isopropyl ether (2000 µg/mL)<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene<br />

Toluene<br />

o-Xylene<br />

p-Xylene<br />

m-Xylene<br />

MtBE<br />

TAME (2000 µg/mL)<br />

t-Butanol (10000 µg/mL)<br />

Ethanol<br />

M-8015B/5031-11 $ 25 / 1 x 1 mL<br />

10 mg/mL in Water<br />

Methanol<br />

M-8015B/5031-17 $ 20 / 1 x 1 mL<br />

10 mg/mL in Water<br />

Pennsylvania DER - Gasoline Range Hydrocarbons<br />

GRH-001S $ 25 / 1 x 1 mL<br />

GRH-001S-PAK SAVE 20% $ 100 / 1 x 1 mL<br />

1.0 mg/mL each in MeOH 10 comps.<br />

Benzene<br />

Ethylbenzene<br />

Heptane<br />

2-Methyl pentane<br />

Toluene<br />

Benzene<br />

Ethylbenzene<br />

MtBE<br />

Naphthalene<br />

Toluene<br />

1,2,4-Trimethylbenzene<br />

2,2,4-Trimethylpentane<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene<br />

Wisconsin DNR - Gasoline Range Hydrocarbons<br />

GRH-003S $ 35 / 1 x 1 mL<br />

GRH-003S-PAK SAVE 20% $ 140 / 5 x 1 mL<br />

2.0 mg/mL each in MeOH 10 comps.<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

1,2,4-Trimethylbenzene<br />

1,3,5-Trimethylbenzene<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene


Diesel Range Hydrocarbon Analysis<br />

D-2887 Calibration Solution<br />

LUFT/LUST <strong>Standards</strong><br />

Diesel Range<br />

EPA Method - Diesel Range Hydrocarbons<br />

DRH-001S $ 20 / 1 x 1 mL<br />

0.2 mg/mL each in CH2Cl2 : Hexane (1:1) 10 comps.<br />

DRH-001S-10X $ 30 / 1 x 1 mL<br />

2.0 mg/mL each in CH2Cl2 : Hexane (1:1) 10 comps.<br />

n-Decane C 10<br />

n-Dodecane C 12<br />

n-Tetradecane C 14<br />

n-Docosane C 22<br />

n-Tetracosane C 24<br />

n-Hexacosane C 26<br />

n-Octacosane C 28<br />

Surrogate Standard<br />

GRH-SS $ 15 / 1 x 1 mL<br />

GRH-SS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

2.0 mg/mL in Acetone<br />

o-Terphenyl (OTP)<br />

Internal Standard<br />

GRH-IS $ 15 / 1 x 1 mL<br />

GRH-IS-PAK SAVE 20% $ 60 / 5 x 1 mL<br />

1.0 mg/mL in CH2Cl2 5-alpha Androstane<br />

Hexane (600 µg/mL)<br />

Heptane (600 µg/mL)<br />

Octane (800 µg/mL)<br />

Nonane (800 µg/mL)<br />

Decane (1,200 µg/mL)<br />

Undecane (1,200 µg/mL)<br />

n-Hexadecane C 16<br />

n-Octadecane C 18<br />

n-Eicosane C 20<br />

Calibration/Window Defining Hydrocarbon Standard<br />

DRH-004S-5X $ 50 / 1 x 1 mL<br />

1.0 mg/mL each in CH 2Cl 2 : CS 2 (1:1) 17 comps.<br />

Octane C 8<br />

Decane C 10<br />

Dodecane C 12<br />

Tetradecane C 14<br />

Tetracosane C 24<br />

Hexacosane C 26<br />

Octacosane C 28<br />

Triacontane C 30<br />

Dotriacontane C 32<br />

Tetratriacontane C 34<br />

Hexatriacontane C 36<br />

Octatriacontane C 38<br />

Tetracontane C 40<br />

Surrogate Standard<br />

DRH-SS $ 30 / 1 x 1 mL<br />

DRH-SS-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

5.0 mg/mL in THF<br />

n-Triacontane-d 62<br />

Hexadecane C 16<br />

Octadecane C 18<br />

Eicosane C 20<br />

Docosane C 22<br />

Calibration Solution<br />

DRH-002S $ 45 / 1 x 1 mL<br />

At stated conc. in CS2 17 comps.<br />

Dodecane (1,200 µg/mL)<br />

Tetradecane (1,200 µg/mL)<br />

Hexadecane (1,000 µg/mL)<br />

Octadecane (500 µg/mL)<br />

Eicosane (200 µg/mL)<br />

Tetracosane (200 µg/mL)<br />

Octacosane (100 µg/mL)<br />

Dotriacontane (100 µg/mL)<br />

Hexatriacontane (100 µg/mL)<br />

Tetracontane (100 µg/mL)<br />

Tetratetracontane (100 µg/mL)<br />

Column Test Mixture<br />

<strong>ASTM</strong>-D2887 $ 10 / 1 x 1 mL<br />

1% v/v in n-Octane 2 comps.<br />

n-Hexadecane n-Octadecane<br />

Wisconsin Diesel Range Hydrocarbons<br />

DRH-003S $ 20 / 1 x 1 mL<br />

0.2 mg/mL each in Hexane 11 comps.<br />

n-Decane C 10<br />

n-Undecane C 11<br />

n-Dodecane C 12<br />

n-Tridecane C 13<br />

n-Tetradecane C 14<br />

n-Pentadecane C 15<br />

n-Hexadecane C 16<br />

n-Heptadecane C 17<br />

n-Octadecane C 18<br />

n-Nonadecane C 19<br />

n-Eicosane C 20<br />

Complete Hydrocarbon Analysis<br />

Multi-State Hydrocarbon Window Defining Standard<br />

DRH-008S-R2 $ 65 / 1 x 1 mL<br />

DRH-008S-R2-PAK SAVE 20% $ 260 / 5 x 1 mL<br />

500 µg/mL each in Chloroform 35 comps.<br />

Octane<br />

Nonane<br />

Decane<br />

Undecane<br />

Dodecane<br />

Tridecane<br />

Tetradecane<br />

Pentadecane<br />

Hexadecane<br />

Heptadecane<br />

Octadecane<br />

Hydrocarbon Window Defining Standard Set<br />

DRH-FTRPH-SET $ 80 / 2 x 1 mL<br />

DRH-FTRPH-SET-PAK SAVE 20% $ 320 / 5 (2 x 1 mL)<br />

500 µg/mL each in Hexane<br />

FTRPH Calibration/Window Defining Standard<br />

DRH-FTRPH $ 35 / 1 x 1 mL<br />

DRH-FTRPH-PAK SAVE 15% $ 150 / 5 x 1 mL<br />

500 µg/mL each in Hexane 17 comps.<br />

n-Octane<br />

n-Decane<br />

n-Dodecane<br />

n-Tetradecane<br />

n-Hexadecane<br />

n-Hexatriacontane<br />

n-Octatriacontane<br />

n-Tetracontane<br />

Hydrocarbon Window Defining Standard<br />

DRH-FTRPH2 $ 45 / 1 x 1 mL<br />

DRH-FTRPH2-PAK SAVE 20% $ 180 / 5 x 1 mL<br />

500 µg/mL each in Hexane 18 comps.<br />

n-Nonane<br />

n-Undecane<br />

n-Tridecane<br />

n-Pentadecane<br />

n-Heptadecane<br />

Heptadecane<br />

Pristane<br />

Octadecane<br />

Phytane<br />

Nonadecane<br />

Eicosane<br />

Heneicosane<br />

Docosane<br />

Tricosane<br />

n-Octadecane<br />

n-Eicosane<br />

n-Docosane<br />

n-Tetracosane<br />

n-Hexacosane<br />

Pristane<br />

Phytane<br />

n-Nonadecane<br />

n-Heneicosane<br />

n-Tricosane<br />

Tetracosane<br />

Pentacosane<br />

Hexacosane<br />

Heptacosane<br />

Octacosane<br />

Nonacosane<br />

Triacontane<br />

n-Hentriacontane<br />

Dotriacontane<br />

Technical Note<br />

n-Octacosane<br />

n-Triacontane<br />

n-Dotriacontane<br />

n-Tetratriacontane<br />

n-Pentacosane<br />

n-Heptacosane<br />

n-Nonacosane<br />

n-Hentriacontane<br />

Tritriacontane<br />

Tetratriacontane<br />

Pentatriacontane<br />

Hexatriacontane<br />

Heptatriacontane<br />

Octatriacontane<br />

Nonatriacontane<br />

Tetracontane<br />

AccuStandard offers a hydrocarbon window defining standard<br />

with the C 8 to C 40 odd and even Alkanes. Use of this one<br />

standard should meet the numerous State to State variations for<br />

hydrocarbon validation and reporting. As an added benefit<br />

AccuStandard included pristane and phytane in the formulation.<br />

Again, use of this one standard can meet numerous LUFT/LUST<br />

programs requiring that the C 17/ pristane and C 18/ phytane ratio<br />

be used to estimate subsurface degradation of fuel oil spills.<br />

If you prefer, AccuStandard has also developed a fuel oil<br />

degradation mixture containing just the four required analytes to<br />

determine the C 17/pristane and C 18/ phytane ratio. Cat. No.<br />

DRH-005S-10X<br />

Fuel Oil Degradation/Retention Time Mixture for<br />

quantification of C 17/Pristane and C 18/Phytane ratios<br />

DRH-005S-10X $ 20 / 1 x 1 mL<br />

2.0 mg/mL each in CH 2Cl 2 : CS 2 (1:1) 4 comps.<br />

Phytane (2,6,10,14-Tetramethylhexadecane)<br />

Pristane (2,6,10,14-Tetramethylpentadecane)<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

n-Tritriacontane<br />

n-Pentatriacontane<br />

n-Heptatriacontane<br />

n-Nonatriacontane<br />

LUFT/LUST DRH<br />

95<br />

LUFT/LUST


LUFT/LUST PT<br />

QC<br />

LUFT/LUST<br />

LUFT/LUST Proficiency Test Samples<br />

Suffix Key<br />

Petro PT Samples<br />

"AS" = Formal PT Study<br />

"AT" = Pre-Test, Quick TAT<br />

"AV" = Values Included<br />

New PT Samples Gasoline & Diesel<br />

The new Gasoline PT sample allows laboratories to test for gasoline TPH. This sample can also be used to test for the BTEX<br />

concentrations so the lab can use this product for method 602, 8020, 8021 and 8015 modified. The sample can also be used<br />

to reduce analytical bias by using the recommended calibration standard listed with the PT sample when conducting PT studies.<br />

AccuStandard is the one ISO 9001 standard manufacturer capable of supplying not only the PT sample(s), but also a wide<br />

variety of calibration standards to meet your specific TPH Method requirement.<br />

Oxygenate PT Sample<br />

With MtBE contamination problems in drinking water, numerous states<br />

are now requiring certification for Oxygenate monitoring. Join<br />

AccuStandard’s next study for Oxygenate analysis. Our timely PT<br />

schedule easily allows your lab to be proactive in new regulatory<br />

requirements. The analytes in the standard and the PT sample have<br />

been drawn from the California list of known prevalent oxygenates in<br />

gasoline. These new Oxygenate PT samples and standards allow your<br />

Lab to:<br />

• Expand testing capabilities<br />

• Generate new testing revenue<br />

• Eliminate standard preparation<br />

• Easily combine with other AccuStandard Volatile standards.<br />

WS-PT Oxygenates<br />

*<br />

OPE-OXY-001-AS $ 47 / 2 mL<br />

OPE-OXY-001-AT $ 47 / 2 mL<br />

OPE-OXY-001-AV $ 47 / 2 mL<br />

Sample conc. after prep 5.0-50 µg/L<br />

Contains 4 analytes listed below<br />

96<br />

ETBE<br />

Diisopropylether<br />

MTBE<br />

TAME<br />

Suggested Calibration Standard<br />

Oxygenate Gasoline Additive Standard<br />

OGAD-001 $ 30 / 1 x 1 mL<br />

NEW<br />

OGAD-001-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

At stated conc. in MeOH 5 comps.<br />

MtBE (2000 µg/mL) TAME (2000 µg/mL)<br />

ETBE (2000 µg/mL) t-Butanol (10000 µg/mL)<br />

Isopropyl ether (2000 µg/mL)<br />

Lab Code 200389-0<br />

WP-PT Oil, Grease & TPH<br />

*<br />

IPE-OILG-001-AS $ 32 / 5 mL<br />

IPE-OILG-001-AT $ 32 / 5 mL<br />

IPE-OILG-001-AV<br />

Sample conc. after prep<br />

Contains 2 analytes listed below<br />

$ 32 / 5 mL<br />

Analyte List Sample range<br />

Total Oil & Grease † 5-100 mg/L<br />

TPH 5-100 mg/L<br />

Technical Note<br />

This PT sample can be used by gravimetric oil and grease<br />

methods. In addition, it can also be used for TPH analysis by<br />

gravimetric methods including the EPA method 1664. The<br />

sample contains real world material commonly found at<br />

petroleum containment sites.<br />

Suggested Calibration Standard<br />

Oil and Grease<br />

WC-OILG-10X-1 $ 45 / 100 mL<br />

1000 µg/mL Total Oil and Grease in n-Propanol<br />

Contains 500 µg/mL vegetable oil and 500 µg/mL of petroleum oil. Shake<br />

well before use.<br />

* Designed for NELAC/CA<br />

† indicates these are included in the NVLAP Scope of Accreditation<br />

†† indicates kits. See individual Cat. No.s for Accreditation status of analytes<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard


Method 1664 Oil, Grease & Total Petroleum Hydrocarbon Determination<br />

Precision and Recovery (PAR) Spiking Solution<br />

M-1664-5ML $ 15 / 1 x 5 mL<br />

M-1664-5ML-PAK SAVE 20% $ 60 / 5 x 5 mL<br />

4.0 mg/mL each in Acetone 2 comps.<br />

M-1664-20ML $ 25 / 1 x 20 mL<br />

M-1664-20ML-PAK SAVE 20% $ 100 / 5 x 20 mL<br />

4.0 mg/mL each in Acetone 2 comps.<br />

Hexadecane Stearic acid<br />

Method 413.2 & 418.1 Total Petroleum Hydrocarbon Analysis by IR<br />

Oil, Grease & Petroleum Hydrocarbon<br />

Concentrates Mix<br />

Chlorobenzene (25.0)<br />

Isooctane (37.5)<br />

Method 8440 Total Petroleum Hydrocarbon Analysis<br />

Chlorobenzene (0.10 w/w %)<br />

n-Hexadecane (0.15 w/w %)<br />

LUFT/LUST <strong>Standards</strong><br />

Oil, Grease & TPH<br />

M-418-CON $ 35 / 1 x 1 mL<br />

% by volume 3 comps.<br />

Hexadecane (37.5)<br />

Total Recoverable Petroleum Hydrocarbon Mix<br />

M-8440 $ 20 / 1 x 1 mL<br />

M-8440-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

At stated conc. in Tetrachloroethene 3 comps.<br />

Isooctane (0.15 w/w %)<br />

Silica Gel Cleanup Calibration Solution<br />

M-8440-SGC $ 10 / 1 x 1 mL<br />

M-8440-SGC-PAK SAVE 20% $ 40 / 5 x 1 mL<br />

10.0 mg/mL in Tetrachloroethene<br />

Corn Oil<br />

Leaking Underground Storage Tank<br />

Retention Time Standard<br />

This product can be used to screen a sample to<br />

determine what type of petroleum spill that may have<br />

caused the contamination.<br />

Retention Time Standard<br />

DRH-010S $ 20 / 1 x 1 mL<br />

DRH-010S-PAK SAVE 20% $ 80 / 5 x 1 mL<br />

25 µg/mL each in CH2Cl2 7 comps.<br />

n-Hexane<br />

n-Decane<br />

n-Dodecane<br />

n-Tetracosane<br />

n-Octacosane<br />

Technical Note<br />

n-Triacontane<br />

n-Tetracontane<br />

NEW<br />

A sample showing peaks in the C6-C10 range generally<br />

indicates a gasoline spill. Samples with the peaks in the C24-<br />

C12 range are indicative of a diesel spill while samples with<br />

the higher carbon numbers above C24 are typically oils or<br />

lubricants. Once the initial screen is complete, more detailed<br />

work can be done to further identify the contaminant.<br />

Oil, Grease and Petroleum<br />

Hydrocarbon Total Recoverable (IR Method)<br />

M-418 $ 30 / 1 x 1 mL<br />

M-418-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

Total 4.15 mg/mL in Freon 113, (Parts by volume) 3 comps.<br />

Chlorobenzene (10.0)<br />

n-Hexadecane (15.0)<br />

Technical Note<br />

AccuStandard's Precison and Recovery (PAR) Spiking Solution was<br />

developed for the new Method 1664. This performance based method was<br />

developed to replace previous gravimetric procedures which incorporated<br />

Freon-113 as the extraction solvent for the determination of Oil and Grease<br />

and Total Petroleum Hydrocarbons. Each standard is packaged in a flame<br />

sealed ampule conveniently sized for quality control of the analytical batch.<br />

Chlorobenzene (25.0 vol %)<br />

n-Hexadecane (37.5 vol %)<br />

Isooctane (15.0)<br />

Total Petroleum Hydrocarbon Concentrate Mix<br />

M-8440-CON $ 30 / 1 x 1 mL<br />

M-8440-CON-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

3 comps.<br />

Isooctane (37.5 vol %)<br />

Total Petroleum Hydrocarbon<br />

Pattern Recognition <strong>Standards</strong><br />

This book contains chromatography for the<br />

various petroleum products typically found<br />

during LUFT/LUST site investigations. The<br />

chromatography shows each fuel pattern in a<br />

25 minute analytical run for early eluting<br />

petroleum products like gasoline to late<br />

eluting products like motor oil. In addition,<br />

an n-alkane standard (DRH-008S) analyzed<br />

under identical conditions has been overlaid<br />

on each petroleum product chromatogram.<br />

Use of the book will assist the chemist’s<br />

identification of the fuel for pattern<br />

recognition.<br />

The n-alkane standard (DRH-008S) overlay provides n-alkane reference<br />

points between the standard and the unknown sample. These beginning and<br />

ending n-alkane reference points can be used to establish gross hydrocarbon<br />

concentrations. By comparing the specific n-alkane range of the closest<br />

identified petroleum standard to that of the unknown sample a reproducible<br />

gross hydrocarbon number can be achieved. To Order, BOOK-TPH $ 35<br />

Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com<br />

Method 1664<br />

413 & 418<br />

8440<br />

97<br />

LUFT/LUST


LUFT/LUST<br />

Method 1004 Carbonyl Compounds as DNPH deriv. by HPLC<br />

Acetaldehyde (1000 µg/mL)<br />

Acetone (500 µg/mL)<br />

Acrolein (500 µg/mL)<br />

Benzaldehyde (500 µg/mL)<br />

<strong>ASTM</strong> E-1387 Resolution Check Mix for Fire Debris Analysis<br />

<strong>ASTM</strong> E-1618 Resolution Check Mix for Fire Debris Analysis<br />

98<br />

n-Decane<br />

n-Dodecane<br />

n-Eicosane<br />

o-Ethyltoluene<br />

m-Ethyltoluene<br />

n-Hexadecane<br />

n-Hexane<br />

n-Octadecane<br />

n-Octane<br />

Butyraldehyde (500 µg/mL)<br />

Formaldehyde (1500 µg/mL)<br />

Propionaldehyde (500µg/mL)<br />

Reference Gas Oil Sample<br />

RGS-001 $ 20 / 1 x 1 mL<br />

Hydrocarbon Mixture<br />

(boiling point range 250-850 °F)<br />

Resolution Check Mix<br />

<strong>ASTM</strong>-E1387 $ 30 / 1 x 1 mL<br />

<strong>ASTM</strong>-E1387-PAK SAVE 20% $ 120 / 5 x 1 mL<br />

2.0 mg/mL each in CH2Cl2 13 comps.<br />

Decane<br />

Dodecane<br />

Eicosane<br />

2-Ethyltoluene<br />

3-Ethyltoluene<br />

Hexadecane<br />

Hexane<br />

Octadecane<br />

Octane<br />

LUFT/LUST <strong>Standards</strong><br />

Automotive Engine Exhaust, Refinery Waste (Skinner List)<br />

Alcohol Oxidation Products in Automotive Engine Exhaust by HPLC of DNPH derivatives<br />

The California Air Resources Board, in conjunction with some of the larger automobile manufacturers, has developed an HPLC method in<br />

which the 2,4-Dinitrophenylhydrazine derivatives of the by-products are quantitated.<br />

Carbonyl Compounds as DNPH deriv. by HPLC<br />

California Air Resources Board Method 1004<br />

M-1004 $ 25 / 1 x 1 mL<br />

At stated conc. in AcCN 13 comps.<br />

M-1004-10X $ 35 / 1 x 1 mL<br />

At 10 times the stated conc. in AcCN 13 comps.<br />

Carbonyl Compound DNPH Derivative<br />

Acetaldehyde (3.0 µg/mL) (15.3 µg/mL)<br />

Acetone (3.0 µg/mL) (12.3 µg/mL)<br />

Acrolein (3.0 µg/mL) (12.7 µg/mL)<br />

Benzaldehyde (3.0 µg/mL) (8.1 µg/mL)<br />

2-Butanone (MEK) (3.0 µg/mL) (10.5 µg/mL)<br />

n-Butyraldehyde (3.0 µg/mL) (10.5 µg/mL)<br />

Crotonaldehyde (3.0 µg/mL) (10.7 µg/mL)<br />

Formaldehyde (3.0 µg/mL) (21.0 µg/mL)<br />

Hexanal (3.0 µg/mL) (8.4 µg/mL)<br />

Methacrolein (3.0 µg/mL) (10.7 µg/mL)<br />

Propionaldehyde (3.0 µg/mL) (12.3 µg/mL)<br />

m-Tolualdehyde (3.0 µg/mL) (7.5 µg/mL)<br />

Valeraldehyde (3.0 µg/mL) (9.3 µg/mL)<br />

CAR-DNPH $ 20 / 1 x 1 mL<br />

At stated conc. in AcCN as DNPH derivatives 7 comps.<br />

Tetradecane<br />

Toluene<br />

1,2,4-Trimethylbenzene<br />

p-Xylene<br />

Test Mix for Fire Debris Analysis<br />

<strong>ASTM</strong>-E1618 $ 35 / 1 x 1 mL<br />

<strong>ASTM</strong>-E1618-PAK SAVE 20% $ 140 / 5 x 1 mL<br />

0.05% v/v (0.50 µL/mL) each in CH2Cl2 13 comps.<br />

n-Tetradecane<br />

Toluene<br />

1,2,4-Trimethylbenzene<br />

p-Xylene<br />

Skinner List for Refinery Waste<br />

Benzene<br />

Carbon disulfide<br />

Chlorobenzene<br />

Chloroform<br />

1,2-Dichloroethane<br />

1,4-Dioxane<br />

Ethyl benzene<br />

Semi-Volatiles<br />

Base/Neutral Extractables<br />

M-005B 0.2 mg/mL each in CH2Cl2 $ 150 / 1 x 1 mL<br />

M-005B-PAK 0.2 mg/mL each in CH2Cl2 SAVE 20% $ 600 / 5 x 1 mL<br />

M-005B-10X 2.0 mg/mL each in CH2Cl2 $ 200 / 1 x 1 mL<br />

M-005B-10X-PAK 2.0 mg/mL each in CH2Cl2 SAVE 20% $ 1,000 / 5 x 1 mL<br />

27 comps.<br />

Anthracene<br />

Benzo[a]anthracene<br />

Benzo[b]fluoranthene<br />

Benzo[k]fluoranthene<br />

Benzo[a]pyrene<br />

bis(2-Ethylhexyl)phthalate<br />

Butyl benzyl phthalate<br />

Chrysene<br />

Dibenz[a,h]acridine<br />

Dibenz[a,h]anthracene<br />

o-Dichlorobenzene<br />

m-Dichlorobenzene<br />

p-Dichlorobenzene<br />

Diethyl phthalate<br />

Acid Extractables<br />

M-005A 0.2 mg/mL each in CH2Cl2 $ 35 / 1 x 1 mL<br />

M-005A-PAK 0.2 mg/mL each in CH2Cl2 SAVE 20% $ 140 / 5 x 1 mL<br />

M-005A-10X 2.0 mg/mL each in CH2Cl2 $ 40 / 1 x 1 mL<br />

M-005A-10X-PAK 2.0 mg/mL each in CH2Cl2 SAVE 20% $ 160 / 5 x 1 mL<br />

o-Cresol<br />

m-Cresol<br />

p-Cresol<br />

2,4-Dimethylphenol<br />

2,4-Dinitrophenol<br />

4-Nitrophenol<br />

Phenol<br />

Thiophenol<br />

Volatiles<br />

M-005V 0.2 mg/mL each in MeOH $ 35 / 1 x 1 mL<br />

M-005V-PAK 0.2 mg/mL each in MeOH SAVE 20% $ 140 / 5 x 1 mL<br />

M-005V-10X 2.0 mg/mL each in MeOH $ 40 / 1 x 1 mL<br />

M-005V-10X-PAK 2.0 mg/mL each in MeOH SAVE 20% $ 160 / 5 x 1 mL<br />

14 comps.<br />

Ethylene dibromide<br />

Methyl ethyl ketone<br />

Styrene<br />

Toluene<br />

o-Xylene<br />

m-Xylene<br />

p-Xylene<br />

Quality System is Certified to comply with the International ISO 9001 Quality Standard<br />

7,12-Dimethylbenz[a]anthracene<br />

Dimethyl phthalate<br />

Di-n-butyl phthalate<br />

Di-n-octyl phthalate<br />

Indene<br />

Fluoranthene<br />

6-Methylchrysene<br />

1-Methylnaphthalene<br />

Naphthalene<br />

Phenanthrene<br />

Pyrene<br />

Pyridine<br />

Quinoline<br />

8 comps.


AA01N-1 73<br />

AA01N-5 73<br />

AA01N-1 26<br />

AA01N-10X-20ML 73<br />

AA01N-25X-20ML 73<br />

AA01N-5 26<br />

AA02N-1 73<br />

AA02N-5 73<br />

AA02W-10X-20ML 73<br />

AA03N-10X-20ML 73<br />

AA03N-25X-20ML 73<br />

AA03N-1 73<br />

AA03N-5 73<br />

AA04N-1 73<br />

AA04N-5 73<br />

AA04N-10X-20ML 73<br />

AA04N-25X-20ML 73<br />

AA05N-1 73<br />

AA05N-10X-20ML 73<br />

AA05N-5 73<br />

AA06N-1 73<br />

AA06N-10X-20ML 73<br />

AA06N-25X-20ML 73<br />

AA06N-5 73<br />

AA07W-1 73<br />

AA07W-10X-20ML 73<br />

AA07W-5 73<br />

AA08N-1 73<br />

AA08N-5 73<br />

AA08N-10X-20ML 73<br />

AA08N-25X-20ML 73<br />

AA09N-1 73<br />

AA09N-5 73<br />

AA09N-1 26<br />

AA09N-10X-20ML 73<br />

AA09N-25X-20ML 73<br />

AA09N-5 26<br />

AA11N-1 73<br />

AA11N-10X-20ML 73<br />

AA11N-25X-20ML 73<br />

AA11N-5 73<br />

AA12N-1 73<br />

AA12N-10X-20ML 73<br />

AA12N-25X-20ML 73<br />

AA12N-5 73<br />

AA13N-1 73<br />

AA13N-5 73<br />

AA13N-10X-20ML 73<br />

AA13N-25X-20ML 73<br />

AA14N-1 73<br />

AA14N-5 73<br />

AA14N-10X-20ML 73<br />

AA14N-25X-20ML 73<br />

AA15N-1 73<br />

AA15N-10X-20ML 73<br />

AA15N-25X-20ML 73<br />

AA15N-5 73<br />

AA16N-1 73<br />

AA16N-10X-20ML 73<br />

AA16N-25X-20ML 73<br />

AA16N-5 73<br />

AA17N-1 73<br />

AA17N-10X-20ML 73<br />

AA17N-25X-20ML 73<br />

AA18N-1 73<br />

AA18N-10X-20ML 73<br />

AA18N-25X-20ML 73<br />

AA18N-5 73<br />

AA19N-1 73<br />

AA19N-10X-20ML 73<br />

AA19N-25X-20ML 73<br />

AA19N-5 73<br />

AA20N-1 73<br />

AA20N-10X-20ML 73<br />

AA20N-5 73<br />

AA21W-1 73<br />

AA21W-10X-20ML 73<br />

AA21W-5 73<br />

Catalog Number Index<br />

AA22H-1 73<br />

AA22H-10X-20ML 73<br />

AA22H-25X-20ML 73<br />

AA22H-5 73<br />

AA23N-1 74<br />

AA23N-10X-20ML 74<br />

AA23N-25X-20ML 74<br />

AA23N-5 74<br />

AA24N-1 74<br />

AA24N-10X-20ML 74<br />

AA24N-25X-20ML 74<br />

AA24N-5 74<br />

AA25N-1 74<br />

AA25N-10X-20ML 74<br />

AA25N-25X-20ML 74<br />

AA25N-5 74<br />

AA26H-1 74<br />

AA26H-10X-20ML 74<br />

AA26H-5 74<br />

AA27N-1 74<br />

AA27N-5 74<br />

AA27N-1 26<br />

AA27N-10X-20ML 74<br />

AA27N-25X-20ML 74<br />

AA27N-5 26<br />

AA28N-1 74<br />

AA28N-10X-20ML 74<br />

AA28N-25X-20ML 74<br />

AA28N-5 74<br />

AA29N-1 74<br />

AA29N-10X-20ML 74<br />

AA29N-25X-20ML 74<br />

AA29N-5 74<br />

AA30N-1 17, 74<br />

AA30N-5 17, 74<br />

AA30N-10X-20ML 74<br />

AA30N-25X-20ML 74<br />

AA31N-1 74<br />

AA31N-10X-20ML 74<br />

AA31N-25X-20ML 74<br />

AA31N-5 74<br />

AA32N-1 74<br />

AA32N-5 74<br />

AA32N-10X-20ML 74<br />

AA32N-25X-20ML 74<br />

AA33N-1 74<br />

AA33N-5 74<br />

AA33N-10X-20ML 74<br />

AA33N-25X-20ML 74<br />

AA34N-1 74<br />

AA34N-10X-20ML 74<br />

AA34N-25X-20ML 74<br />

AA34N-5 74<br />

AA35W-1 74<br />

AA35W-10X-20ML 74<br />

AA35W-25X-20ML 74<br />

AA35W-5 74<br />

AA36N-1 74<br />

AA36N-10X-20ML 74<br />

AA36N-25X-20ML 74<br />

AA36N-5 74<br />

AA37N-1 26<br />

AA37N-1 74<br />

AA37N-10X-20ML 74<br />

AA37N-25X-20ML 74<br />

AA37N-5 26<br />

AA37N-5 74<br />

AA38W-1 74<br />

AA38W-10X-20ML 74<br />

AA38W-25X-20ML 74<br />

AA38W-5 74<br />

AA40H-1 74<br />

AA40H-10X-20ML 74<br />

AA40H-25X-20ML 74<br />

AA40H-5 74<br />

AA41W-1 74<br />

AA41W-10X-20ML 74<br />

AA41W-5 74<br />

AA42H-1 74<br />

AA42H-10X-20ML 74<br />

AA42H-25X-20ML 74<br />

AA42H-5 74<br />

AA43N-1 74<br />

AA43N-5 74<br />

AA43N-10X-20ML 74<br />

AA43N-25X-20ML 74<br />

AA44N-1 74<br />

AA44N-10X-20ML 74<br />

AA44N-25X-20ML 74<br />

AA44N-5 74<br />

AA45W-1 74<br />

AA45W-10X-20ML 74<br />

AA45W-25X-20ML 74<br />

AA45W-5 74<br />

AA46H-1 74<br />

AA46H-10X-20ML 74<br />

AA46H-25X-20ML 74<br />

AA46H-5 74<br />

AA47N-1 74<br />

AA47N-10X-20ML 74<br />

AA47N-25X-20ML 74<br />

AA47N-5 74<br />

AA48H-1 74<br />

AA48H-10X-20ML 74<br />

AA48H-25X-20ML 74<br />

AA48H-5 74<br />

AA49N-1 75<br />

AA49N-10X-20ML 75<br />

AA49N-25X-20ML 75<br />

AA49N-5 75<br />

AA50N-1 75<br />

AA50N-10X-20ML 75<br />

AA50N-25X-20ML 75<br />

AA50N-5 75<br />

AA51N-1 75<br />

AA51N-10X-20ML 75<br />

AA51N-25X-20ML 75<br />

AA51N-5 75<br />

AA52W-1 26, 75<br />

AA-52W-10X-20ML 75<br />

AA52W-5 26, 75<br />

AA53N-1 75<br />

AA53N-10X-20ML 75<br />

AA53N-25X-20ML 75<br />

AA53N-5 75<br />

AA54N-1 17, 75<br />

AA54N-5 17, 75<br />

AA54N-1 26<br />

AA54N-10X-20ML 75<br />

AA54N-25X-20ML 75<br />

AA54N-5 26<br />

AA55N-1 75<br />

AA55N-10X-20ML 75<br />

AA55N-25X-20ML 75<br />

AA55N-5 75<br />

AA56W-1 75<br />

AA56W-10X-20ML 75<br />

AA56W-25X-20ML 75<br />

AA56W-5 75<br />

AA57W-1 75<br />

AA57W-10X-20ML 75<br />

AA57W-25X-20ML 75<br />

AA57W-5 75<br />

AA58H-1 75<br />

AA58H-10X-20ML 75<br />

AA59N-1 75<br />

AA59N-10X-20ML 75<br />

AA59N-25X-20ML 75<br />

AA59N-5 75<br />

AA60N-1 75<br />

AA60N-10X-20ML 75<br />

AA60N-25X-20ML 75<br />

AA60N-5 75<br />

AA61N-1 75<br />

AA61N-5 75<br />

AA62N-1 75<br />

AA62N-10X-20ML 75<br />

AA62N-25X-20ML 75<br />

AA62N-5 75<br />

AA63H-1 75<br />

AA63H-5 75<br />

AA63N-10X-20ML 75<br />

AA63N-25X-20ML 75<br />

AA64W-1 75<br />

AA64W-10X-20ML 75<br />

AA64W-5 75<br />

AA65W-1 75<br />

AA65W-10X-20ML 75<br />

AA65W-5 75<br />

AA66N-1 75<br />

AA66N-5 75<br />

AA67N-1 26, 75<br />

AA67N-10X-20ML 75<br />

AA67N-25X-20ML 75<br />

AA67N-5 26, 75<br />

AA68N-1 75<br />

AA68N-10X-20ML 75<br />

AA68N-25X-20ML 75<br />

AA68N-5 75<br />

AA69N-1 75<br />

AA69N-10X-20ML 75<br />

AA69N-25X-20ML 75<br />

AA69N-5 75<br />

AA70N-1 75<br />

AA70N-10X-20ML 75<br />

AA70N-25X-20ML 75<br />

AA70N-5 75<br />

AA71N-1 75<br />

AA71N-10X-20ML 75<br />

AA71N-25X-20ML 75<br />

AA71N-5 75<br />

AK-101.0-GCS 82<br />

AK-101.0-GCS-BTEX 82, 90<br />

AK-101.0-GCS-PAK 82<br />

AK-101.0-IS-10X 82<br />

AK-101.0-IS-10X-PAK 82<br />

AK-101.0-LCS 82<br />

AK-101.0-LCS-PAK 82<br />

AK-101.0-NAS-10X 82<br />

AK-101.0-NAS-10X-PAK 82<br />

AK-101.0-SS 82<br />

AK-101.0-SS-100X 82<br />

AK-101.0-SS-100X-PAK 82<br />

AK-101.0-SS-10X 82<br />

AK-101.0-SS-10X-PAK 82<br />

AK-101.0-SS-PAK 82<br />

AK-101AA-ARO 82<br />

AK-101AA-ARO-PAK 82<br />

AK-101-GSC-R1 82<br />

AK-101-GSC-R1-PAK 82<br />

AK-102.0-DCS 83<br />

AK-102.0-DCS-10X 83<br />

AK-102.0-DCS-10X-PAK 83<br />

AK-102.0-DCS-PAK 83<br />

AK-102.0-DCS-R1-10X 83<br />

AK-102.0-DCS-R1-10X-PAK 83<br />

AK-102.0-IS 83<br />

AK-102.0-IS-PAK 83<br />

AK-102.0-LCS 83<br />

AK-102.0-LCS-10X 83<br />

AK-102.0-LCS-10X-PAK 83<br />

AK-102.0-LCS-PAK 83<br />

AK-102.0-LCS-R1-10X 83<br />

AK-102.0-LCS-R1-10X-PAK 83<br />

AK-102.0-NAS-10X 83, 86<br />

AK-102.0-NAS-10X-PAK 83, 86<br />

AK-102.0-SS 83<br />

AK-102.0-SS-10X 83, 85<br />

AK-102.0-SS-10X-PAK 83, 85<br />

AK-102.0-SS-PAK 83<br />

AK-102/103AA-RT 84<br />

AK-102/103AA-RT-PAK 84<br />

AK-102/103AA-SS 84<br />

AK-102/103AA-SS-PAK 84<br />

AK-102AA-DRO 84<br />

AK-102AA-DRO-PAK 84<br />

AK-103.0-LCS 84<br />

AK-103.0-LCS-5X 84<br />

AK-103.0-LCS-5X-PAK 84<br />

AK-103.0-LCS-PAK 84<br />

AK-103.0-RCS 84<br />

AK-103.0-RCS-PAK 84<br />

AK-103.0-SS-PAK 84<br />

AK-103AA-RRO 84<br />

AK-103AA-RRO-PAK 84<br />

<strong>ASTM</strong>-D2887 14<br />

<strong>ASTM</strong>-D2887 95<br />

<strong>ASTM</strong>-D3710 20<br />

<strong>ASTM</strong>-D3710-PAK 20<br />

<strong>ASTM</strong>-E1387 98<br />

<strong>ASTM</strong>-E1387-PAK 98<br />

<strong>ASTM</strong>-E1618 98<br />

<strong>ASTM</strong>-E1618-PAK 98<br />

<strong>ASTM</strong>-FUEL-QCS-01-PAK 1,40<br />

<strong>ASTM</strong>-FUEL-QCS-02-PAK 1,40<br />

<strong>ASTM</strong>-P-0010-PAK 11<br />

<strong>ASTM</strong>-P-0020-PAK 11<br />

<strong>ASTM</strong>-P-0030 12,13<br />

<strong>ASTM</strong>-P-0031 13<br />

<strong>ASTM</strong>-P-0032 13<br />

<strong>ASTM</strong>-P-0033 13<br />

<strong>ASTM</strong>-P-0034 13<br />

<strong>ASTM</strong>-P-0035 13<br />

<strong>ASTM</strong>-P-0036 12<br />

<strong>ASTM</strong>-P-0037 12<br />

<strong>ASTM</strong>-P-0038 14<br />

<strong>ASTM</strong>-P-0050 15<br />

<strong>ASTM</strong>-P-0051N-2G 56<br />

<strong>ASTM</strong>-P-0051N-2G 15<br />

<strong>ASTM</strong>-P-0052 15<br />

<strong>ASTM</strong>-P-0052-PAK 15<br />

<strong>ASTM</strong>-P-0053N-2G 56<br />

<strong>ASTM</strong>-P-0053N-2G 15<br />

<strong>ASTM</strong>-P-0061-SET 37<br />

<strong>ASTM</strong>-P-0062-SET 37<br />

<strong>ASTM</strong>-P-0063-SET 37<br />

<strong>ASTM</strong>-P-0064-SET 37<br />

<strong>ASTM</strong>-P-0065-SET 37<br />

<strong>ASTM</strong>-P-0066-SET 37<br />

<strong>ASTM</strong>-P-0067-SET 37<br />

<strong>ASTM</strong>-P-0068-SET 37<br />

<strong>ASTM</strong>-P-0069-SET 37<br />

<strong>ASTM</strong>-P-0070-10X 23, 40<br />

<strong>ASTM</strong>-P-0070-1X 23, 40<br />

<strong>ASTM</strong>-P-0070-20X 23, 40<br />

<strong>ASTM</strong>-P-0070-2X 23, 40<br />

<strong>ASTM</strong>-P-0070-4X 23, 40<br />

<strong>ASTM</strong>-P-0070-BL 23, 40<br />

<strong>ASTM</strong>-P-0070-SET 23, 40<br />

<strong>ASTM</strong>-P-0071-01 23, 40<br />

<strong>ASTM</strong>-P-0071-02 23, 40<br />

<strong>ASTM</strong>-P-0071-03 23, 40<br />

<strong>ASTM</strong>-P-0071-BL 23, 40<br />

<strong>ASTM</strong>-P-0071-SET 23, 40<br />

<strong>ASTM</strong>-P-0080 55<br />

<strong>ASTM</strong>-P-0080-PAK 55<br />

<strong>ASTM</strong>-P-0081 55<br />

<strong>ASTM</strong>-P-0081-PAK 55<br />

<strong>ASTM</strong>-P-0082 55<br />

<strong>ASTM</strong>-P-0082-PAK 55<br />

<strong>ASTM</strong>-P-0082-R1 55<br />

<strong>ASTM</strong>-P-0082-R1-PAK 55<br />

<strong>ASTM</strong>-P-0090-01 66<br />

<strong>ASTM</strong>-P-0090-02 66<br />

<strong>ASTM</strong>-P-0090-03 66<br />

<strong>ASTM</strong>-P-0090-04 66<br />

<strong>ASTM</strong>-P-0090-05 66<br />

<strong>ASTM</strong>-P-0090-06 66<br />

<strong>ASTM</strong>-P-0090-07 66<br />

<strong>ASTM</strong>-P-0090-08 66<br />

<strong>ASTM</strong>-P-0090-09 66<br />

<strong>ASTM</strong>-P-0090-10 66<br />

INDEX<br />

i


INDEX<br />

ii<br />

<strong>ASTM</strong>-P-0090-11 66<br />

<strong>ASTM</strong>-P-0090-12 66<br />

<strong>ASTM</strong>-P-0090-13 66<br />

<strong>ASTM</strong>-P-0090-14 66<br />

<strong>ASTM</strong>-P-0090-15 66<br />

<strong>ASTM</strong>-P-0090-16 66<br />

<strong>ASTM</strong>-P-0090-SET 66<br />

<strong>ASTM</strong>-P-0091-01-10X 38<br />

<strong>ASTM</strong>-P-0091-02-10X 38<br />

<strong>ASTM</strong>-P-0091-03-10X 38<br />

<strong>ASTM</strong>-P-0091-04-10X 38<br />

<strong>ASTM</strong>-P-0091-05-10X 38<br />

<strong>ASTM</strong>-P-0091-06-10X 38<br />

<strong>ASTM</strong>-P-0091-07-10X 38<br />

<strong>ASTM</strong>-P-0091-08-10X 38<br />

<strong>ASTM</strong>-P-0091-09-10X 38<br />

<strong>ASTM</strong>-P-0091-10-10X 38<br />

<strong>ASTM</strong>-P-0091-10X-SET 38<br />

<strong>ASTM</strong>-P-0091-11-10X 38<br />

<strong>ASTM</strong>-P-0091-12-10X 38<br />

<strong>ASTM</strong>-P-0091-13-10X 38<br />

<strong>ASTM</strong>-P-0091-14-10X 38<br />

<strong>ASTM</strong>-P-0091-15-10X 38<br />

<strong>ASTM</strong>-P-0091-16-10X 38<br />

<strong>ASTM</strong>-P-0091-17-10X 38<br />

<strong>ASTM</strong>-P-0091-18-10X 38<br />

<strong>ASTM</strong>-P-0091-19-10X 38<br />

<strong>ASTM</strong>-P-0091-20-10X 38<br />

<strong>ASTM</strong>-P-0091-21-10X 38<br />

<strong>ASTM</strong>-P-0091-22-10X 38<br />

<strong>ASTM</strong>-P-0092-0.1X 66<br />

<strong>ASTM</strong>-P-0092-100X 66<br />

<strong>ASTM</strong>-P-0092-10X 66<br />

<strong>ASTM</strong>-P-0092-1X 66<br />

<strong>ASTM</strong>-P-0092-500X 66<br />

<strong>ASTM</strong>-P-0092-5X 66<br />

<strong>ASTM</strong>-P-0092-BL 66<br />

<strong>ASTM</strong>-P-0092-SET 66<br />

<strong>ASTM</strong>-P-0100-01 62<br />

<strong>ASTM</strong>-P-0100-02 62<br />

<strong>ASTM</strong>-P-0100-03 62<br />

<strong>ASTM</strong>-P-0100-04 62<br />

<strong>ASTM</strong>-P-0100-05 62<br />

<strong>ASTM</strong>-P-0100-06 62<br />

<strong>ASTM</strong>-P-0100-07 62<br />

<strong>ASTM</strong>-P-0100-08 62<br />

<strong>ASTM</strong>-P-0100-09 62<br />

<strong>ASTM</strong>-P-0100-10 62<br />

<strong>ASTM</strong>-P-0100-11 62<br />

<strong>ASTM</strong>-P-0100-12 62<br />

<strong>ASTM</strong>-P-0100-SET 62<br />

<strong>ASTM</strong>-P-0101-01 62<br />

<strong>ASTM</strong>-P-0101-02 62<br />

<strong>ASTM</strong>-P-0101-03 62<br />

<strong>ASTM</strong>-P-0101-04 62<br />

<strong>ASTM</strong>-P-0101-05 62<br />

<strong>ASTM</strong>-P-0101-06 62<br />

<strong>ASTM</strong>-P-0101-07 62<br />

<strong>ASTM</strong>-P-0101-08 62<br />

<strong>ASTM</strong>-P-0101-09 62<br />

<strong>ASTM</strong>-P-0101-10 62<br />

<strong>ASTM</strong>-P-0101-11 62<br />

<strong>ASTM</strong>-P-0101-12 62<br />

<strong>ASTM</strong>-P-0102-01 62<br />

<strong>ASTM</strong>-P-0102-02 62<br />

<strong>ASTM</strong>-P-0102-03 62<br />

<strong>ASTM</strong>-P-0102-04 62<br />

<strong>ASTM</strong>-P-0102-05 62<br />

<strong>ASTM</strong>-P-0102-06 62<br />

<strong>ASTM</strong>-P-0102-07 62<br />

<strong>ASTM</strong>-P-0102-08 62<br />

<strong>ASTM</strong>-P-0102-09 62<br />

<strong>ASTM</strong>-P-0102-10 62<br />

<strong>ASTM</strong>-P-0102-11 62<br />

<strong>ASTM</strong>-P-0102-12 62<br />

<strong>ASTM</strong>-P-0102-SET 39<br />

<strong>ASTM</strong>-P-0102-SET 62<br />

<strong>ASTM</strong>-P-0103-01 39<br />

<strong>ASTM</strong>-P-0103-01 62<br />

<strong>ASTM</strong>-P-0103-02 39<br />

<strong>ASTM</strong>-P-0103-02 62<br />

<strong>ASTM</strong>-P-0103-03 39<br />

<strong>ASTM</strong>-P-0103-03 62<br />

<strong>ASTM</strong>-P-0103-04 39<br />

<strong>ASTM</strong>-P-0103-04 62<br />

<strong>ASTM</strong>-P-0103-05 39<br />

<strong>ASTM</strong>-P-0103-05 62<br />

<strong>ASTM</strong>-P-0103-06 39<br />

<strong>ASTM</strong>-P-0103-06 62<br />

<strong>ASTM</strong>-P-0103-07 39<br />

<strong>ASTM</strong>-P-0103-07 62<br />

<strong>ASTM</strong>-P-0103-08 39<br />

<strong>ASTM</strong>-P-0103-08 62<br />

<strong>ASTM</strong>-P-0103-09 39<br />

<strong>ASTM</strong>-P-0103-09 62<br />

<strong>ASTM</strong>-P-0103-10 39<br />

<strong>ASTM</strong>-P-0103-10 62<br />

<strong>ASTM</strong>-P-0103-11 39<br />

<strong>ASTM</strong>-P-0103-11 62<br />

<strong>ASTM</strong>-P-0103-12 39<br />

<strong>ASTM</strong>-P-0103-12 62<br />

<strong>ASTM</strong>-P-0103-SET 39<br />

<strong>ASTM</strong>-P-0103-SET 62<br />

<strong>ASTM</strong>-P-0104-01 62<br />

<strong>ASTM</strong>-P-0104-02 62<br />

<strong>ASTM</strong>-P-0104-03 62<br />

<strong>ASTM</strong>-P-0104-04 62<br />

<strong>ASTM</strong>-P-0104-05 62<br />

<strong>ASTM</strong>-P-0104-06 62<br />

<strong>ASTM</strong>-P-0104-07 62<br />

<strong>ASTM</strong>-P-0104-08 62<br />

<strong>ASTM</strong>-P-0104-09 62<br />

<strong>ASTM</strong>-P-0105-01 62<br />

<strong>ASTM</strong>-P-0105-02 62<br />

<strong>ASTM</strong>-P-0105-03 62<br />

<strong>ASTM</strong>-P-0105-04 62<br />

<strong>ASTM</strong>-P-0105-05 62<br />

<strong>ASTM</strong>-P-0105-06 62<br />

<strong>ASTM</strong>-P-0105-07 62<br />

<strong>ASTM</strong>-P-0106-01 62<br />

<strong>ASTM</strong>-P-0106-02 62<br />

<strong>ASTM</strong>-P-0106-03 62<br />

<strong>ASTM</strong>-P-0106-04 62<br />

<strong>ASTM</strong>-P-0106-05 62<br />

<strong>ASTM</strong>-P-0106-06 62<br />

<strong>ASTM</strong>-P-0106-07 62<br />

<strong>ASTM</strong>-P-0107-5 62<br />

<strong>ASTM</strong>-P-0108-01 63<br />

<strong>ASTM</strong>-P-0108-02 63<br />

<strong>ASTM</strong>-P-0108-03 63<br />

<strong>ASTM</strong>-P-0108-04 63<br />

<strong>ASTM</strong>-P-0108-05 63<br />

<strong>ASTM</strong>-P-0108-06 63<br />

<strong>ASTM</strong>-P-0108-07 63<br />

<strong>ASTM</strong>-P-0108-08 63<br />

<strong>ASTM</strong>-P-0108-09 63<br />

<strong>ASTM</strong>-P-0108-10 63<br />

<strong>ASTM</strong>-P-0108-11 63<br />

<strong>ASTM</strong>-P-0108-12 63<br />

<strong>ASTM</strong>-P-0108-13 63<br />

<strong>ASTM</strong>-P-0108-14 63<br />

<strong>ASTM</strong>-P-0108-15 63<br />

<strong>ASTM</strong>-P-0108-16 63<br />

<strong>ASTM</strong>-P-0108-17 63<br />

<strong>ASTM</strong>-P-0108-SET 63<br />

<strong>ASTM</strong>-P-0109-01 63<br />

<strong>ASTM</strong>-P-0109-02 63<br />

<strong>ASTM</strong>-P-0109-03 63<br />

<strong>ASTM</strong>-P-0109-04 63<br />

<strong>ASTM</strong>-P-0109-05 63<br />

<strong>ASTM</strong>-P-0109-06 63<br />

<strong>ASTM</strong>-P-0109-07 63<br />

<strong>ASTM</strong>-P-0109-08 63<br />

<strong>ASTM</strong>-P-0109-09 63<br />

<strong>ASTM</strong>-P-0109-10 63<br />

<strong>ASTM</strong>-P-0109-11 63<br />

<strong>ASTM</strong>-P-0109-12 63<br />

<strong>ASTM</strong>-P-0109-13 63<br />

<strong>ASTM</strong>-P-0109-14 63<br />

<strong>ASTM</strong>-P-0109-15 63<br />

<strong>ASTM</strong>-P-0109-16 63<br />

<strong>ASTM</strong>-P-0109-17 63<br />

<strong>ASTM</strong>-P-0109-SET 63<br />

<strong>ASTM</strong>-P-0110-01 63<br />

<strong>ASTM</strong>-P-0110-02 63<br />

<strong>ASTM</strong>-P-0110-03 63<br />

<strong>ASTM</strong>-P-0110-04 63<br />

<strong>ASTM</strong>-P-0110-05 63<br />

<strong>ASTM</strong>-P-0110-06 63<br />

<strong>ASTM</strong>-P-0110-07 63<br />

<strong>ASTM</strong>-P-0110-08 63<br />

<strong>ASTM</strong>-P-0110-09 63<br />

<strong>ASTM</strong>-P-0110-10 63<br />

<strong>ASTM</strong>-P-0110-11 63<br />

<strong>ASTM</strong>-P-0110-12 63<br />

<strong>ASTM</strong>-P-0110-13 63<br />

<strong>ASTM</strong>-P-0110-14 63<br />

<strong>ASTM</strong>-P-0110-15 63<br />

<strong>ASTM</strong>-P-0110-16 63<br />

<strong>ASTM</strong>-P-0110-17 63<br />

<strong>ASTM</strong>-P-0110-SET 25<br />

<strong>ASTM</strong>-P-0110-SET 63<br />

<strong>ASTM</strong>-P-0111-01 63<br />

<strong>ASTM</strong>-P-0111-02 63<br />

<strong>ASTM</strong>-P-0111-03 63<br />

<strong>ASTM</strong>-P-0111-04 63<br />

<strong>ASTM</strong>-P-0111-05 63<br />

<strong>ASTM</strong>-P-0111-06 63<br />

<strong>ASTM</strong>-P-0111-07 63<br />

<strong>ASTM</strong>-P-0111-08 63<br />

<strong>ASTM</strong>-P-0111-09 63<br />

<strong>ASTM</strong>-P-0111-10 63<br />

<strong>ASTM</strong>-P-0111-11 63<br />

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D-4929-94-100X 25<br />

D-4929-94-100X-PAK 25<br />

D-4929-94-PAK 25<br />

D-5059-A-01 27<br />

D-5059-A-02 27<br />

D-5059-A-03 27<br />

D-5059-A-04 27<br />

D-5059-A-05 27<br />

D-5059-A-06 27<br />

D-5059-A-07 27<br />

D-5059-A-CAL-SET 27<br />

D-5059-C-01 27<br />

D-5059-C-02 27<br />

D-5059-C-03 27<br />

D-5059-C-04 27<br />

D-5059-C-05 27<br />

D-5059-C-06 27<br />

D-5059-C-07 27<br />

D-5059-C-CAL-SET 27<br />

D-5059-IS-10ML-PAK 27<br />

D-5059-IS-4 27<br />

D-5134-92-ALK 27<br />

D-5134-92-CEM 27<br />

D-5134-92-LCM 27<br />

D-5134-92-NAP 27<br />

D-5134-92-REF 27<br />

D-5134-92-SET 27<br />

D-5184-91-AL-1 28<br />

D-5184-91-AL-5 28<br />

D-5184-91-SI-1 28<br />

D-5184-91-SI-5 28<br />

D-5184-91-TA-5 28<br />

D-5186-96-DLC-25X 28<br />

D-5186-96-DLC-50X 28<br />

D-5186-96-DLC-SET 28<br />

D-5186-96-PM 28<br />

D-5186-96-PM-PAK 28<br />

D-5307-CR 29<br />

D-5307-CR-PAK 29<br />

D-5307-IS-10ML 29<br />

D-5307-IS-10ML-PAK 29<br />

D-5307-QUAL 29<br />

D-5307-QUAL-PAK 29<br />

D-5307-QUANT 29<br />

D-5307-QUANT-PAK 29<br />

D-5441 30<br />

D-5441-10X 30<br />

D-5441-10X-5ML 30<br />

D-5441-10X-5ML-PAK 30<br />

D-5441-10X-PAK 30<br />

D-5441-5ML 30<br />

D-5441-5ML-PAK 30<br />

D-5441-PAK 30<br />

D-5441-QUAL 30<br />

D-5441-QUANT 30<br />

D-5441-RES 30<br />

D-5441-RES-5ML 30<br />

D-5441-RES-5ML-PAK 30<br />

D-5441-RES-PAK 30<br />

D-5442-CR-PAK 31<br />

D-5442-PAK 31<br />

D-5442-RT1 31<br />

D-5442-RT2 31<br />

D-5443-93-HTM 31<br />

D-5453-HL-01 31<br />

D-5453-HL-02 31<br />

D-5453-HL-03 31<br />

D-5453-HL-04 31<br />

D-5453-HL-BL 31<br />

D-5453-HL-SET 31<br />

D-5453-LL-01 31<br />

D-5453-LL-02 31<br />

D-5453-LL-03 31<br />

D-5453-LL-04 31<br />

D-5453-LL-BL 31<br />

D-5453-LL-SET 31<br />

D-5453-ML-01 31<br />

D-5453-ML-02 31<br />

D-5453-ML-03 31<br />

D-5453-ML-04 31<br />

D-5453-ML-05 31<br />

D-5453-ML-BL 31<br />

D-5453-ML-SET 31<br />

D-5480-CR-100X-PAK 32<br />

D-5480-CR-PAK 32<br />

D-5480-IS-5ML 32<br />

D-5480-IS-5ML-PAK 32<br />

D-5501-94-01 32<br />

D-5501-94-02 32<br />

D-5501-94-03 32<br />

D-5501-94-04 32<br />

D-5501-94-05 32<br />

D-5501-94-06 32<br />

D-5501-94-07 32<br />

D-5580-95-CAL-IS-SET 32<br />

D-5580-95-CAL-SET-10ML 32<br />

D-5580-QC 33<br />

D-5580-QC-PAK 33<br />

D-5580-QC-R1 33<br />

D-5580-QC-R1-PAK 33<br />

D-5600-01-1 37<br />

D-5600-BLH-5 37<br />

D-5600-BLH-L 37<br />

D-5600-LIB-1 37<br />

D-5600-LIB-5 37<br />

D-5708-A-10X 39<br />

D-5708-B-10X-1 39<br />

D-5708-B-10X-5 39<br />

D-5708-B-5 39<br />

D-5762-95-100X 40<br />

D-5762-95-10X 40<br />

D-5762-95-1X 40<br />

D-5762-95-500X-PAK 40<br />

D-5762-95-50X 40<br />

D-5762-95-5X 40<br />

D-5762-95-BL 40<br />

D-5762-95-CAL-SET 40<br />

D-5769-ADD/IS 47<br />

D-5769-ADD/IS-R 48<br />

D-5769-ADD/IS-R2 49<br />

D-5769-ADD-10ML 46<br />

D-5769-ADD-5ML 46<br />

D-5769-CAL/IS-R2-SET 49<br />

D-5769-CAL/IS-R-SET 48<br />

D-5769-CAL/IS-SET 47<br />

D-5769-CAL-SET-10ML 46<br />

D-5769-CAL-SET-5ML 46<br />

D-5769-QC/IS-5ML 47<br />

D-5769-QC/IS-5ML-PAK 47<br />

D-5769-QC/IS-R2-5ML 49<br />

D-5769-QC/IS-R2-5ML-PAK 49<br />

D-5769-QC/IS-R-5ML 48<br />

D-5769-QC/IS-R-5ML-PAK 48<br />

D-5769-QC-10ML 46<br />

D-5769-QC-10ML-PAK 46<br />

D-5863-95A-10X-1 52<br />

D-5863-95B-10X 52<br />

D-611-01 4<br />

D-611-02 4<br />

D-611-03 4<br />

D-611-04 4<br />

D-611-05 4<br />

D-611E-01 4<br />

D-611E-02 4<br />

D-611E-03 4<br />

D-611E-SET 4<br />

D-611-SET 4<br />

D-6258-01 54<br />

D-6258-02 54<br />

D-6258-03 54<br />

D-6258-04 54<br />

D-6258-05 54<br />

D-6258-BL 54<br />

D-6258-CAL-SET-5ML 54<br />

D-6258-CONC-5ML 54<br />

D-6296-BL 55<br />

D-6296-CAL1 55<br />

D-6296-CAL1-PAK 55<br />

D-6296-CAL2 55<br />

D-6296-CAL2-PAK 55<br />

D-6296-VER1 55<br />

D-6296-VER2 55<br />

D-6296-VER-SET 55<br />

D-6296-VER-SET-PAK 55<br />

D-6379-SET 57<br />

D-6379-SET-PAK 57<br />

D-6379-SRS 57<br />

D-6379-SRS-PAK 57<br />

D-6428-0.1X 57<br />

D-6428-0.1X-4 57<br />

D-6428-0.5X 57<br />

D-6428-0.5X-4 57<br />

D-6428-100X 57<br />

D-6428-100X-4 57<br />

D-6428-10X 57<br />

D-6428-10X-4 57<br />

D-6428-1X 57<br />

D-6428-1X-4 57<br />

D-6428-2.5X 57<br />

D-6428-2.5X-4 57<br />

D-6428-25X 57<br />

D-6428-25X-4 57<br />

D-6428-50X 57<br />

D-6428-50X-4 57<br />

D-6428-5X 57<br />

D-6428-5X-4 57<br />

D-6428-75X 57<br />

D-6428-75X-4 57<br />

D-6428-BL 57<br />

D-6428-BL-4 57<br />

D-6428-R1-4-SET 57<br />

D-6428-R1-SET 57<br />

D-6428-R2-4-SET 57<br />

D-6428-R2-SET 57<br />

D-6550-CONC 58<br />

D-6550-CONC-5ML 58<br />

DRH/GRH-FL-SS 86<br />

DRH/GRH-FL-SS-PAK 86<br />

DRH/GRH-FL-SS-R2 86<br />

DRH/GRH-FL-SS-R2-PAK 86<br />

DRH-001S 95<br />

DRH-001S-10X 95<br />

DRH-002N 56<br />

DRH-002N 14<br />

DRH-002N-10X 56<br />

DRH-002N-10X 14<br />

DRH-002S 95<br />

DRH-002S-R1 14, 20<br />

DRH-002S-R1-PAK 14, 20<br />

DRH-002S-R2 14<br />

DRH-002S-R2-PAK 14<br />

DRH-003S 95<br />

DRH-004S-5X 86, 95<br />

DRH-004S-5X-PAK 86<br />

DRH-005S-10X 14<br />

DRH-005S-10X 95<br />

DRH-006-CAL-10X 87<br />

DRH-006-CAL-1X 87<br />

DRH-006-CAL-20X 87<br />

DRH-006-CAL-40X 87<br />

DRH-006-CAL-4X 87<br />

DRH-006-CAL-SET 87<br />

DRH-006S 87<br />

DRH-006S-PAK 87<br />

DRH-006-SS 88, 91<br />

DRH-006-SS-PAK 88, 91<br />

DRH-007-CAL-10X 87<br />

DRH-007-CAL-1X 87<br />

DRH-007-CAL-20X 87<br />

DRH-007-CAL-40X 87<br />

DRH-007-CAL-4X 87<br />

DRH-007-CAL-SET 87<br />

DRH-007S 87<br />

DRH-007S-PAK 87<br />

DRH-007-SS 87, 91<br />

DRH-007-SS-PAK 87, 91<br />

DRH-008S-R1 14, 56, 86, 95<br />

DRH-008S-R1-PAK 14, 56, 86,<br />

95<br />

DRH-009S 85<br />

DRH-009S-PAK 85<br />

DRH-010S 97<br />

DRH-010S-PAK 97<br />

DRH-FL-SS 86<br />

DRH-FL-SS-3X 86<br />

DRH-FL-SS-3X-PAK 86<br />

DRH-FL-SS-PAK 86<br />

DRH-FTRPH 86, 95<br />

DRH-FTRPH2 95<br />

DRH-FTRPH2-PAK 95<br />

DRH-FTRPH-PAK 86, 95<br />

CLP-BLMA-L 71 iii<br />

INDEX


INDEX<br />

iv<br />

DRH-FTRPH-SET 95<br />

DRH-FTRPH-SET-PAK 95<br />

DRH-MA-FSS-10ML 88<br />

DRH-MA-FSS-50X 88<br />

DRH-MA-FSS-50X-PAK 88<br />

DRH-MA-MS 87<br />

DRH-MA-MS-10X 87<br />

DRH-MA-MS-10X-PAK 87<br />

DRH-MA-MS-40X 87<br />

DRH-MA-MS-40X-PAK 87<br />

DRH-MA-MS-PAK 87<br />

DRH-MA-SS 87, 91<br />

DRH-MA-SS-100X 87, 91<br />

DRH-MA-SS-100X-PAK 87, 91<br />

DRH-MA-SS-10X 87, 91<br />

DRH-MS-ASL 88<br />

DRH-MS-ASL-PAK 88<br />

DRH-PA-001 89<br />

DRH-PA-001-PAK 89<br />

DRH-SS 86<br />

DRH-SS-PAK 86<br />

DRH-TX-001-10X 89<br />

DRH-TX-001-10X-PAK 89<br />

DRH-TX-002-10X 89<br />

DRH-TX-002-10X-PAK 89<br />

DRH-TX-002-D-0.4X-10ML 89<br />

DRH-TX-002-D-40X 89<br />

DRH-TX-002-D-40X-PAK 89<br />

DRH-TX-002-D-SET 89<br />

DRH-TX-003-CNM 89<br />

DRH-TX-003-CNM-PAK 89<br />

DRH-TX-003-FCS 89<br />

DRH-TX-003-FCS-PAK 89<br />

DRH-TX-003-SET 89<br />

DRH-TX-003-SS1 89<br />

DRH-TX-003-SS1-PAK 89<br />

FD2-W25-10X 93<br />

FD2-W25-R1-10X 93<br />

FD2-W50-10X 93<br />

FD2-W50-R1-10X 93<br />

FD2-W75-10X 93<br />

FD2-W75-R1-10X 93<br />

FIA-ARO 4<br />

FIA-ARO-5ML 4<br />

FIA-CAL-SET 4<br />

FIA-OLE 4<br />

FIA-OLE-5ML 4<br />

FIA-PAR 4<br />

FIA-PAR-5ML 4<br />

FK-W25-10X 93<br />

FK-W50-10X 93<br />

FK-W75-10X 93<br />

FU-001 92<br />

FU-001-40X 92<br />

FU-001-D-40X 92<br />

FU-002 92<br />

FU-002-40X 92<br />

FU-002-D-40X 92<br />

FU-003 92<br />

FU-003-40X 92<br />

FU-003-D-40X 92<br />

FU-004 92<br />

FU-004-40X 92<br />

FU-004-D-40X 92<br />

FU-005 92<br />

FU-005-40X 92<br />

FU-005-D-10X 93<br />

FU-005-D-40X 92<br />

FU-006 92<br />

FU-006-40X 92<br />

FU-006-D-40X 92<br />

FU-007 92<br />

FU-007-40X 92<br />

FU-007-D-40X 92<br />

FU-008 92<br />

FU-008-40X 92<br />

FU-008-D-40X 92<br />

FU-009 92<br />

FU-009-40X 92<br />

FU-009-D-10X 93<br />

FU-009-D-40X 92<br />

FU-010 92<br />

FU-010-40X 92<br />

FU-010-D-40X 92<br />

FU-011 92<br />

FU-011-40X 92<br />

FU-011-D-40X 92<br />

FU-012 92<br />

FU-012-40X 92<br />

FU-012-D-40X 92<br />

FU-013 92<br />

FU-013-40X 92<br />

FU-013-D-40X 92<br />

FU-014 92<br />

FU-014-40X 92<br />

FU-014-D-40X 92<br />

FU-015 92<br />

FU-015-40X 92<br />

FU-015-D-40X 92<br />

FU-016 92<br />

FU-016-40X 92<br />

FU-016-D-40X 92<br />

FU-017 92<br />

FU-017-40X 92<br />

FU-017-D-10X 93<br />

FU-017-D-40X 92<br />

FU-018-D-40X 92<br />

FU-018-H 92<br />

FU-018-H-40X 92<br />

FU-019-D-40X 92<br />

FU-019-H 92<br />

FU-019-H-40X 92<br />

FU-020-D-40X 92<br />

FU-020-H 92<br />

FU-020-H-40X 92<br />

FU-021-D-40X 92<br />

FU-021-H 92<br />

FU-021-H-40X 92<br />

FU-022 92<br />

FU-022-40X 92<br />

FU-022-D-40X 92<br />

FU-023 92<br />

FU-023-40X 92<br />

FU-023-D-40X 92<br />

FU-025-D-40X 93<br />

FU-025-H 93<br />

FU-025-H-40X 93<br />

FU-026-D-40X 93<br />

FU-026-H 93<br />

FU-026-H-40X 93<br />

FU-027-D-40X 93<br />

FU-027-H 93<br />

FU-027-H-40X 93<br />

FU-028-D-40X 93<br />

FU-028-H 93<br />

FU-028-H-40X 93<br />

GA-001 92<br />

GA-001-10X 93<br />

GA-001-20X-BTEX 82, 88, 90,<br />

94<br />

GA-001-40X 92<br />

GA-001-D-40X 92<br />

GA-002 92<br />

GA-002-40X 92<br />

GA-002-D-40X 92<br />

GA-003 92<br />

GA-003-40X 92<br />

GA-003-D-40X 92<br />

GA-004 92<br />

GA-004-40X 92<br />

GA-004-D-40X 92<br />

GA-005 92<br />

GA-005-40X 92<br />

GA-005-D-40X 92<br />

GAD-001 94<br />

GAD-001-PAK 94<br />

GARH-IS 94<br />

GARH-SS 94<br />

GA-W25-10X 93<br />

GA-W50-10X 93<br />

GA-W75-10X 93<br />

GRH-001S 94<br />

GRH-001S-PAK 94<br />

GRH-002S 94<br />

GRH-003S 91, 94<br />

GRH-003S-PAK 91, 94<br />

GRH-004-MS 88<br />

GRH-004-MS-100X 88<br />

GRH-004-MS-100X-PAK 88<br />

GRH-004-MS-10X 88<br />

GRH-004-MS-10X-PAK 88<br />

GRH-004-MS-PAK 88<br />

GRH-004S/SS 88<br />

GRH-004S/SS-PAK 88<br />

GRH-004S-10X 88<br />

GRH-004S-10X-PAK 88<br />

GRH-004-SS 88, 90<br />

GRH-004-SS-100X 88, 90<br />

GRH-004-SS-100X-PAK 88, 90<br />

GRH-004-SS-10X 88, 90<br />

GRH-004-SS-10X-PAK 88, 90<br />

GRH-004-SS-PAK 88, 90<br />

GRH-IS 85-86, 88, 91, 95<br />

GRH-IS-10X 88, 91<br />

GRH-IS-PAK 85-86, 88, 91, 95<br />

GRH-PA-001 89<br />

GRH-PA-001-PAK 89<br />

GRH-SS 85-86, 95<br />

GRH-SS-PAK 85-86, 95<br />

HS-001N 92<br />

HS-001S 92<br />

HS-001S-40X 92<br />

HS-001S-D-40X 92<br />

HS-002N 92<br />

HS-002S 92<br />

HS-002S-40X 92<br />

HS-002S-D-40X 92<br />

HS-003N 92<br />

HS-003S 92<br />

HS-003S-40X 92<br />

HS-003S-D-40X 92<br />

HS-004N 92<br />

HS-004S 92<br />

HS-004S-40X 92<br />

HS-004S-D-40X 92<br />

HS-005N 92<br />

HS-005S 92<br />

HS-005S-40X 92<br />

HS-005S-D-40X 92<br />

IC-ACET-10X-1 79<br />

IC-ACET-10X-5 79<br />

IC-ACET-1X-1 79<br />

IC-ACET-1X-5 79<br />

IC-AN-KIT-10X-1 76<br />

IC-AN-KIT-10X-5 76<br />

IC-AN-KIT-1X-1 76<br />

IC-AN-KIT-1X-5 76<br />

IC-AN-KIT-2X-1 76<br />

IC-AN-KIT-2X-5 76<br />

IC-AN-KIT-R-10X-1 79<br />

IC-AN-KIT-R-10X-5 79<br />

IC-BA-10X-1 78<br />

IC-BA-10X-5 78<br />

IC-BA-1X-1 78<br />

IC-BA-1X-5 78<br />

IC-BA-2X-1 78<br />

IC-BA-2X-5 78<br />

IC-BR-10X-1 76<br />

IC-BR-1X-1 76<br />

IC-BR-1X-5 76<br />

IC-BR-2X-1 76<br />

IC-BR-2X-5 76<br />

IC-CA-10X-1 78<br />

IC-CA-10X-5 78<br />

IC-CA-1X-1 78<br />

IC-CA-1X-5 78<br />

IC-CA-2X-1 78<br />

IC-CA-2X-5 78<br />

IC-CAT-KIT-10X-1 78<br />

IC-CAT-KIT-10X-5 78<br />

IC-CAT-KIT-1X-1 78<br />

IC-CAT-KIT-1X-5 78<br />

IC-CAT-KIT-2X-1 78<br />

IC-CAT-KIT-2X-5 78<br />

IC-CHLR-10X-1 79<br />

IC-CHLR-10X-5 79<br />

IC-CHLR-1X-1 79<br />

IC-CHLR-1X-5 79<br />

IC-CHRM-10X-1 79<br />

IC-CHRM-10X-5 79<br />

IC-CHRM-1X-1 79<br />

IC-CHRM-1X-5 79<br />

IC-Cl-10X-1 76<br />

IC-Cl-10X-5 76<br />

IC-Cl-1X-1 76<br />

IC-Cl-1X-5 76<br />

IC-Cl-2X-1 76<br />

IC-Cl-2X-5 76<br />

IC-ELU-01-0.5 79<br />

IC-ELU-01-0.5-PAK 79<br />

IC-ELU-01-1 79<br />

IC-ELU-01-1-PAK 79<br />

IC-ELU-02-0.5 79<br />

IC-ELU-02-0.5-PAK 79<br />

IC-ELU-02-1 79<br />

IC-ELU-02-1-PAK 79<br />

IC-ELU-03-0.5 79<br />

IC-ELU-03-0.5-PAK 79<br />

IC-ELU-03-1 79<br />

IC-ELU-03-1-PAK 79<br />

IC-F-10X-1 76<br />

IC-F-10X-5 76<br />

IC-F-1X-1 76<br />

IC-F-1X-5 76<br />

IC-F-2X-1 76<br />

IC-FORM-10X-1 79<br />

IC-FORM-10X-5 79<br />

IC-FORM-1X-1 79<br />

IC-FORM-1X-5 79<br />

IC-K-10X-1 78<br />

IC-K-10X-5 78<br />

IC-K-1X-1 78<br />

IC-K-1X-5 78<br />

IC-K-2X-1 78<br />

IC-K-2X-5 78<br />

IC-LI-10X-1 78<br />

IC-LI-10X-5 78<br />

IC-LI-1X-1 78<br />

IC-LI-1X-5 78<br />

IC-LI-2X-1 78<br />

IC-LI-2X-5 78<br />

IC-MAN-01-1 77<br />

IC-MAN-02-1 77<br />

IC-MAN-03-1 77<br />

IC-MAN-04-1 77<br />

IC-MAN-05-R1-1 77<br />

IC-MAN-05-SET 77<br />

IC-MAN-06-R1-1 77<br />

IC-MAN-06-SET 77<br />

IC-MAN-07-R1-1 77<br />

IC-MAN-07-SET 77<br />

IC-MAN-08-R1-1 77<br />

IC-MAN-08-SET 77<br />

IC-MAN-09-R1-1 77<br />

IC-MAN-09-SET 77<br />

IC-MAN-10-R1-1 77<br />

IC-MAN-10-SET 77<br />

IC-MAN-11-1 77<br />

IC-MAN-12-1 77<br />

IC-MAN-13-1 77<br />

IC-MAN-14-R2-1 77, 79<br />

IC-MAN-14-R2-SET 77, 79<br />

IC-MAN-14-R3-1 77<br />

IC-MAN-14-SET 77<br />

IC-MAN-15-R2-1 77<br />

IC-MAN-15R-SET 77<br />

IC-MAN-16-R1-1 77<br />

IC-MAN-16-SET 77<br />

IC-MAN-17-R1-1 77<br />

IC-MAN-17-SET 77<br />

IC-MAN-18-R1-1 77<br />

IC-MAN-18-SET 77<br />

IC-MAN-CAL-SET 77<br />

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IC-MCA-05-1 78<br />

IC-MCA-06-1 78<br />

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IC-NA-2X-5 78<br />

IC-NH4-10X-1 78<br />

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IC-NH4-1X-1 78<br />

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IC-NO2-1X-5 76<br />

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ICP-12N-0.5-10X 68


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ICP-25N-25X-20ML 69<br />

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ICP-27N-10X-20ML 69<br />

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ICP-27N-25X-20ML 69<br />

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ICP-28N-1-10X 69<br />

ICP-28N-25X-20ML 69<br />

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ICP-MS-01N-0.1X-1 72<br />

ICP-MS-01N-1 72<br />

ICP-MS-02N-0.01X-1 72<br />

ICP-MS-02N-0.1X-1 72<br />

ICP-MS-02N-1 72<br />

ICP-MS-03N-0.01X-1 72<br />

ICP-MS-03N-0.1X-1 72<br />

ICP-MS-03N-1 72<br />

ICP-MS-04N-0.01X-1 72<br />

ICP-MS-04N-0.1X-1 72<br />

ICP-MS-04N-1 72<br />

ICP-MS-05N-0.01X-1 72<br />

ICP-MS-05N-0.1X-1 72<br />

ICP-MS-05N-1 72<br />

ICP-MS-06N-0.01X-1 72<br />

ICP-MS-06N-0.1X-1 72<br />

ICP-MS-06N-1 72<br />

ICP-MS-08N-0.01X-1 72<br />

ICP-MS-08N-0.1X-1 72<br />

ICP-MS-08N-1 72<br />

ICP-MS-09N-0.01X-1 72<br />

ICP-MS-09N-0.1X-1 72<br />

ICP-MS-09N-1 72<br />

ICP-MS-13N-0.01X-1 72<br />

ICP-MS-13N-0.1X-1 72<br />

ICP-MS-13N-1 72<br />

ICP-MS-14N-0.01X-1 72<br />

ICP-MS-14N-0.1X-1 72<br />

ICP-MS-14N-1 72<br />

ICP-MS-15N-0.01X-1 72<br />

ICP-MS-15N-1 72<br />

ICP-MS-21W-0.01X-1 72<br />

ICP-MS-21W-0.1X-1 72<br />

ICP-MS-21W-1 72<br />

ICP-MS-22H-0.01X-1 72<br />

ICP-MS-22H-0.1X-1 72<br />

ICP-MS-22H-1 72<br />

ICP-MS-25N-0.01X-1 72<br />

ICP-MS-25N-0.1X-1 72<br />

ICP-MS-25N-1 72<br />

ICP-MS-27N-0.01X-1 72<br />

ICP-MS-27N-0.1X-1 72<br />

ICP-MS-27N-1 72<br />

ICP-MS-29N-0.01X-1 72<br />

ICP-MS-29N-0.1X-1 72<br />

ICP-MS-29N-1 72<br />

ICP-MS-30N-0.01X-1 72<br />

ICP-MS-30N-0.1X-1 72<br />

ICP-MS-30N-1 72<br />

ICP-MS-32N-0.01X-1 72<br />

ICP-MS-32N-0.1X-1 72<br />

ICP-MS-32N-1 72<br />

ICP-MS-33N-0.01X-1 72<br />

ICP-MS-33N-0.1X-1 72<br />

ICP-MS-33N-1 72<br />

ICP-MS-34N-0.01X-1 72<br />

ICP-MS-34N-0.1X-1 72<br />

ICP-MS-34N-1 72<br />

ICP-MS-35W-0.01X-1 72<br />

ICP-24N-25X-20ML 69 v<br />

INDEX


INDEX<br />

vi<br />

ICP-MS-35W-0.1X-1 72<br />

ICP-MS-35W-1 72<br />

ICP-MS-37N-0.01X-1 72<br />

ICP-MS-37N-0.1X-1 72<br />

ICP-MS-37N-1 72<br />

ICP-MS-41W-0.01X-1 72<br />

ICP-MS-41W-0.1X-1 72<br />

ICP-MS-41W-1 72<br />

ICP-MS-43N-0.01X-1 72<br />

ICP-MS-43N-0.1X-1 72<br />

ICP-MS-43N-1 72<br />

ICP-MS-46H-0.01X-1 72<br />

ICP-MS-46H-0.1X-1 72<br />

ICP-MS-46H-1 72<br />

ICP-MS-50N-0.01X-1 72<br />

ICP-MS-50N-0.1X-1 72<br />

ICP-MS-50N-1 72<br />

ICP-MS-51N-0.01X-1 72<br />

ICP-MS-51N-0.1X-1 72<br />

ICP-MS-51N-1 72<br />

ICP-MS-53N-0.01X-1 72<br />

ICP-MS-53N-0.1X-1 72<br />

ICP-MS-53N-1 72<br />

ICP-MS-54N-0.01X-1 72<br />

ICP-MS-54N-0.1X-1 72<br />

ICP-MS-54N-1 72<br />

ICP-MS-55N-0.01X-1 72<br />

ICP-MS-55N-0.1X-1 72<br />

ICP-MS-55N-1 72<br />

ICP-MS-56W-0.01X-1 72<br />

ICP-MS-56W-0.1X-1 72<br />

ICP-MS-56W-1 72<br />

ICP-MS-59N-0.01X-1 72<br />

ICP-MS-59N-0.1X-1 72<br />

ICP-MS-59N-1 72<br />

ICP-MS-60N-0.01X-1 72<br />

ICP-MS-60N-0.1X-1 72<br />

ICP-MS-60N-1 72<br />

ICP-MS-61N-0.01X-1 72<br />

ICP-MS-61N-0.1X-1 72<br />

ICP-MS-63N-0.01X-1 72<br />

ICP-MS-63N-0.1X-1 72<br />

ICP-MS-63N-1 72<br />

ICP-MS-64W-0.01X-1 72<br />

ICP-MS-64W-0.1X-1 72<br />

ICP-MS-64W-1 72<br />

ICP-MS-66N-0.01X-1 72<br />

ICP-MS-66N-0.1X-1 72<br />

ICP-MS-67N-0.01X-1 72<br />

ICP-MS-67N-0.1X-1 72<br />

ICP-MS-67N-1 72<br />

ICP-MS-69N-0.01X-1 72<br />

ICP-MS-69N-0.1X-1 72<br />

ICP-MS-69N-1 72<br />

ICP-MS-70N-0.01X-1 72<br />

ICP-MS-70N-0.1X-1 72<br />

ICP-MS-70N-1 72<br />

IC-PO4-10X-1 76<br />

IC-PO4-10X-5 76<br />

IC-PO4-1X-1 76<br />

IC-PO4-1X-5 76<br />

IC-PO4-2X-1 76<br />

IC-PO4-2X-5 76<br />

IC-PO4-P-10X-1 79<br />

IC-PO4-P-10X-5 79<br />

IC-PO4-P-1X-1 79<br />

IC-PO4-P-1X-5 79<br />

IC-SO4-10X-1 76<br />

IC-SO4-10X-5 76<br />

IC-SO4-1X-1 76<br />

IC-SO4-1X-5 76<br />

IC-SO4-2X-1 76<br />

IC-SO4-2X-5 76<br />

IC-SO4-S-10X-1 79<br />

IC-SO4-S-10X-5 79<br />

IC-SO4-S-1X-1 79<br />

IC-SO4-S-1X-5 79<br />

IC-SR-10X-1 78<br />

IC-SR-10X-5 78<br />

IC-SR-1X-1 78<br />

IC-SR-1X-5 78<br />

IC-SR-2X-1 78<br />

IC-SR-2X-5 78<br />

IPE-OILG-001-AS 2<br />

IPE-OILG-001-AS 96<br />

IPE-OILG-001-AT 2<br />

IPE-OILG-001-AT 96<br />

IPE-OILG-001-AV 2<br />

IPE-OILG-001-AV 96<br />

IS-7281-2OZ 59<br />

KF-0.6X-5ML-VAP 5<br />

KF-10X-20ML-PAK 5<br />

KF-10X-2ML-VAP 5<br />

KF-10X-5ML-VAP 5<br />

KF-1X-20ML-PAK 5<br />

KF-1X-2ML-VAP 5<br />

KF-1X-5ML-VAP 5<br />

KF-50X-20ML-PAK 5<br />

KF-50X-2ML-VAP 5<br />

KF-50X-5ML-VAP 5<br />

M-005A 98<br />

M-005A-10X 98<br />

M-005A-10X-PAK 98<br />

M-005A-PAK 98<br />

M-005B 98<br />

M-005B-10X 98<br />

M-005B-10X-PAK 98<br />

M-005B-PAK 98<br />

M-005V 98<br />

M-005V-10X 98<br />

M-005V-10X-PAK 98<br />

M-005V-PAK 98<br />

M-1004 98<br />

M-1004-10X 98<br />

M-1664-20ML 97<br />

M-1664-20ML-PAK 97<br />

M-1664-5ML 97<br />

M-1664-5ML-PAK 97<br />

M-418 97<br />

M-418-CON 97<br />

M-418-PAK 97<br />

M-602-GAS-10X 85, 94<br />

M-8015B/5031-11 85, 94<br />

M-8015B/5031-17 85, 94<br />

M-8440 97<br />

M-8440-CON 97<br />

M-8440-CON-PAK 97<br />

M-8440-PAK 97<br />

M-8440-SGC 97<br />

M-8440-SGC-PAK 97<br />

MA-900-4 59<br />

MA-900-8 59<br />

M-GRA-ADD/IS 44<br />

M-GRA-ADD/IS-R 45<br />

M-GRA-CAL/IS-SET 44<br />

M-GRA-CAL-R/IS-R-SET 45<br />

M-GRA-FP 47-49<br />

M-GRA-FP-PAK 47-49<br />

M-GRA-IS 44, 47, 50<br />

M-GRA-IS-5ML 44, 46-47, 50<br />

M-GRA-IS-5ML-PAK 44, 46-47,<br />

50<br />

M-GRA-IS-AS-5ML 33<br />

M-GRA-IS-AS-5ML-PAK 33<br />

M-GRA-IS-R 45, 48<br />

M-GRA-IS-R-10ML 45-46, 48,<br />

50<br />

M-GRA-IS-R-10ML-PAK 45-46,<br />

48, 50<br />

M-GRA-IS-R2 49<br />

M-GRA-IS-R2-25ML 49<br />

M-GRA-IS-R2-SET 49<br />

M-GRA-K1 43<br />

M-GRA-K2 43<br />

M-GRA-K4 43<br />

M-GRA-MSR 47<br />

M-GRA-MSR-PAK 47<br />

M-GRA-QC/IS-5ML 44<br />

M-GRA-QC/IS-5ML-PAK 44<br />

M-GRA-QC/IS-R-5ML 45<br />

M-GRA-QC/IS-R-5ML-PAK 45<br />

M-GRA-QC-10ML 44-45, 53<br />

M-GRA-QC-10ML-PAK 44-45,<br />

53<br />

M-GRA-QC-R/IS-5ML 50<br />

M-GRA-QC-R/IS-5ML-PAK 50<br />

M-GRA-QC-R/IS-R-5ML 50<br />

M-GRA-QC-R/IS-R-5ML-PAK<br />

50<br />

M-GRA-QC-R-10ML 50<br />

M-GRA-QC-R-10ML-PAK 50<br />

M-GRA-RES 47-49<br />

M-GRA-RES-PAK 47-49<br />

M-GRA-SCS-AS 33<br />

M-GRA-SCS-AS-PAK 33<br />

M-GRA-ST 44-45, 47-49<br />

M-GRA-ST-PAK 44-45, 47-49<br />

M-GRA-VT/IS-AS 33<br />

M-GRA-VT/IS-AS-PAK 33<br />

M-GRA-VT-AS-10ML 33<br />

M-GRA-VT-AS-10ML-PAK 33<br />

M-GRO-BLNK/IS-10ML 35<br />

M-GRO-BLNK/IS-10ML-PAK 35<br />

M-GRO-BLNK-10ML 35-37<br />

M-GRO-BLNK-10ML 24<br />

M-GRO-BLNK-10ML-PAK35-36<br />

M-GRO-BLNK-10ML-PAK 24<br />

M-GRO-CAL/IS-SET 34<br />

M-GRO-CAL/IS-SET-PAK 34<br />

M-GRO-CAL-EPA-SET-10ML<br />

36<br />

M-GRO-CAL-IS/EPA-SET 36<br />

M-GRO-CAL-SET 34<br />

M-GRO-EPA-CC/IS-5ML 36<br />

M-GRO-EPA-CC/IS-5MLPAK36<br />

M-GRO-EPA-CC-10ML 36<br />

M-GRO-EPA-CC-10ML-PAK 36<br />

M-GRO-EPA-SP-5ML 36<br />

M-GRO-EPA-SP-5ML-PAK 36<br />

M-GRO-IS-5ML 35-36<br />

M-GRO-IS-5ML 24<br />

M-GRO-IS-5ML-PAK 35-36<br />

M-GRO-IS-5ML-PAK 24<br />

M-GRO-QC/IS-5ML 35<br />

M-GRO-QC/IS-5ML-PAK 35<br />

M-GRO-QC-10ML 35<br />

M-GRO-QC-10ML-PAK 35<br />

M-GRO-QC-R/IS-5ML 35<br />

M-GRO-QC-R/IS-5ML-PAK 35<br />

M-GRO-QC-R-10ML 35<br />

M-GRO-QC-R-10ML-PAK 35<br />

MO-COMP-D-40X 93<br />

MOSOL-20-16 59<br />

MOSOL-75-16 59<br />

OGAD-001 2<br />

OGAD-001 85, 94, 96<br />

OGAD-001-PAK 2<br />

OGAD-001-PAK 85, 94, 96<br />

OMT-001 66<br />

OMT-001-PAK 66<br />

OMT-002 66<br />

OMT-002-PAK 66<br />

OMT-003 66<br />

OMT-003-PAK 66<br />

OMT-004 66<br />

OMT-004-PAK 66<br />

OMT-005 66<br />

OMT-005-PAK 66<br />

OMT-006 66<br />

OMT-006-PAK 66<br />

OPE-OXY-001-AS 2<br />

OPE-OXY-001-AS 96<br />

OPE-OXY-001-AT 2<br />

OPE-OXY-001-AT 96<br />

OPE-OXY-001-AV 2<br />

OPE-OXY-001-AV 96<br />

RGS-001 98<br />

S-3571 12<br />

S-603A-10X 85, 94<br />

S-603A-10X-PAK 85, 94<br />

SBPT-AROM 2, 41<br />

SBPT-BENZ 2, 41<br />

SBPT-COMP 1, 41<br />

SBPT-LSGAS 1, 31, 41<br />

SBPT-OLEFIN 2, 41<br />

SBPT-OLEFINSFC 1, 41<br />

SBPT-SDF 1, 41<br />

SBPT-SGAS 2, 41<br />

SBPT-SWMO 1, 41<br />

SCO-100X-4 11<br />

SCO-10X-4 11<br />

SCO-200X-4 11<br />

SCO-25X-4 11<br />

SCO-300X-4 11<br />

SCO-400X-4 11<br />

SCO-500X-4 11<br />

SCO-50X-4 11<br />

SCO-CAL-SET-4 11<br />

SDF-100X-4 8<br />

SDF-100X-SHOT 8<br />

SDF-10X-4 8<br />

SDF-10X-SHOT 8<br />

SDF-150X-4 8<br />

SDF-150X-SHOT 8<br />

SDF-15X-4 8<br />

SDF-15X-SHOT 8<br />

SDF-1X-4 8<br />

SDF-1X-SHOT 8<br />

SDF-200X-4 8<br />

SDF-200X-SHOT 8<br />

SDF-2X-4 8<br />

SDF-2X-SHOT 8<br />

SDF-300X-4 8<br />

SDF-300X-SHOT 8<br />

SDF-30X-4 8<br />

SDF-30X-SHOT 8<br />

SDF-3X-4 8<br />

SDF-3X-SHOT 8<br />

SDF-400X-4 8<br />

SDF-400X-SHOT 8<br />

SDF-4X-4 8<br />

SDF-4X-SHOT 8<br />

SDF-500X-4 8<br />

SDF-500X-SHOT 8<br />

SDF-50X-4 8<br />

SDF-50X-SHOT 8<br />

SDF-5X-4 8<br />

SDF-5X-SHOT 8<br />

SDF-600X-4 8<br />

SDF-600X-SHOT 8<br />

SDF-7.5X-4 8<br />

SDF-7.5X-SHOT 8<br />

SDF-70X-4 8<br />

SDF-70X-SHOT 8<br />

SDF-BL-4 8<br />

SDF-BL-SHOT 8<br />

SDF-CAL-SET-4 8<br />

SK-100X-4 9<br />

SK-100X-SHOT 9<br />

SK-10X-4 9<br />

SK-10X-SHOT 9<br />

SK-1X-4 9<br />

SK-1X-SHOT 9<br />

SK-200X-4 9<br />

SK-200X-SHOT 9<br />

SK-20X-4 9<br />

SK-20X-SHOT 9<br />

SK-30X-4 9<br />

SK-30X-SHOT 9<br />

SK-3X-4 9<br />

SK-3X-SHOT 9<br />

SK-40X-4 9<br />

SK-40X-SHOT 9<br />

SK-50X-4 9<br />

SK-50X-SHOT 9<br />

SK-5X-4 9<br />

SK-5X-SHOT 9<br />

SK-7.5X-4 9<br />

SK-7.5X-SHOT 9<br />

SK-BL-4 9<br />

SK-BL-SHOT 9<br />

SK-CAL-SET-4 9<br />

SK-HD-100X-4 9<br />

SK-HD-10X-4 9<br />

SK-HD-150X-4 9<br />

SK-HD-15X-4 9<br />

SK-HD-1X-4 9<br />

SK-HD-200X-4 9<br />

SK-HD-20X-4 9<br />

SK-HD-2X-4 9<br />

SK-HD-300X-4 9<br />

SK-HD-30X-4 9<br />

SK-HD-3X-4 9<br />

SK-HD-400X-4 9<br />

SK-HD-40X-4 9<br />

SK-HD-4X-4 9<br />

SK-HD-500X-4 9<br />

SK-HD-50X-4 9<br />

SK-HD-5X-4 9<br />

SK-HD-600X-4 9<br />

SK-HD-7.5X-4 9<br />

SK-HD-70X-4 9<br />

SK-HD-BL-4 9<br />

SK-HD-CAL-SET-4 9<br />

SRO-100X-4 11<br />

SRO-150X-4 11<br />

SRO-200X-4 11<br />

SRO-300X-4 11<br />

SRO-35X-4 11<br />

SRO-400X-4 11<br />

SRO-70X-4 11<br />

SRO-CAL-SET-4 11<br />

STP-100X-4 10<br />

STP-10X-4 10<br />

STP-1X-4 10<br />

STP-200X-4 10<br />

STP-20X-4 10<br />

STP-2X-4 10<br />

STP-300X-4 10<br />

STP-30X-4 10<br />

STP-3X-4 10<br />

STP-40X-4 10<br />

STP-5X-4 10<br />

STP-60X-4 10<br />

STP-BL-4 10<br />

STP-CAL-SET 10<br />

SWMO-100X-4 8<br />

SWMO-100X-SHOT 8<br />

SWMO-10X-4 8<br />

SWMO-10X-SHOT 8<br />

SWMO-150X-4 8<br />

SWMO-150X-SHOT 8<br />

SWMO-15X-4 8<br />

SWMO-15X-SHOT 8<br />

SWMO-1X-4 8<br />

SWMO-1X-SHOT 8<br />

SWMO-200X-4 8<br />

SWMO-200X-SHOT 8<br />

SWMO-2X-4 8<br />

SWMO-2X-SHOT 8<br />

SWMO-300X-4 8<br />

SWMO-300X-SHOT 8<br />

SWMO-30X-4 8<br />

SWMO-30X-SHOT 8<br />

SWMO-3X-4 8<br />

SWMO-3X-SHOT 8<br />

SWMO-400X-4 8<br />

SWMO-400X-SHOT 8<br />

SWMO-4X-4 8<br />

SWMO-4X-SHOT 8<br />

SWMO-500X-4 8<br />

SWMO-500X-SHOT 8<br />

SWMO-50X-4 8<br />

SWMO-50X-SHOT 8<br />

SWMO-5X-4 8<br />

SWMO-5X-SHOT 8<br />

SWMO-600X-4 8<br />

SWMO-600X-SHOT 8<br />

SWMO-7.5X-4 8<br />

SWMO-7.5X-SHOT 8<br />

SWMO-70X-4 8<br />

SWMO-70X-SHOT 8<br />

SWMO-BL-4 8<br />

SWMO-BL-SHOT 8<br />

SWMO-CAL-SET-4 8<br />

SWMO-LT-100X-4 8<br />

SWMO-LT-100X-SHOT 8<br />

SWMO-LT-10X-4 8<br />

SWMO-LT-10X-SHOT 8<br />

SWMO-LT-150X-4 8<br />

SWMO-LT-150X-SHOT 8<br />

SWMO-LT-15X-4 8<br />

SWMO-LT-15X-SHOT 8<br />

SWMO-LT-1X-4 8<br />

SWMO-LT-1X-SHOT 8<br />

SWMO-LT-200X-4 8<br />

SWMO-LT-200X-SHOT 8<br />

SWMO-LT-2X-4 8<br />

SWMO-LT-2X-SHOT 8<br />

SWMO-LT-300X-4 8<br />

SWMO-LT-300X-SHOT 8<br />

SWMO-LT-30X-4 8<br />

SWMO-LT-30X-SHOT 8<br />

SWMO-LT-3X-4 8<br />

SWMO-LT-3X-SHOT 8<br />

SWMO-LT-400X-4 8<br />

SWMO-LT-400X-SHOT 8<br />

SWMO-LT-4X-4 8<br />

SWMO-LT-4X-SHOT 8<br />

SWMO-LT-500X-4 8<br />

SWMO-LT-500X-SHOT 8<br />

SWMO-LT-50X-4 8<br />

SWMO-LT-50X-SHOT 8<br />

SWMO-LT-5X-4 8<br />

SWMO-LT-5X-SHOT 8<br />

SWMO-LT-600X-4 8<br />

SWMO-LT-600X-SHOT 8<br />

SWMO-LT-7.5X-4 8<br />

SWMO-LT-7.5X-SHOT 8<br />

SWMO-LT-70X-4 8<br />

SWMO-LT-70X-SHOT 8<br />

SWMO-LT-BL-4 8<br />

SWMO-LT-BL-SHOT 8<br />

SWMO-LT-CAL-SET-4 8<br />

T-W130 21<br />

V-028S-D-10X 90-91<br />

V-028S-D-10X-PAK 90-91<br />

WA-EPH-10X 91<br />

WA-EPH-10X-PAK 91<br />

WA-EPH-ALI 91


WA-EPH-ALI-PAK 91<br />

WA-EPH-ALI-R1 91<br />

WA-EPH-ALI-R1-PAK 91<br />

WA-EPH-ARO 91<br />

WA-EPH-ARO-PAK 91<br />

WA-EPH-ARO-R1 91<br />

WA-EPH-ARO-R1-PAK 91<br />

WA-EPH-FCS 91<br />

WA-EPH-FCS-PAK 91<br />

WA-EPH-FCS-R1 91<br />

WA-EPH-FCS-R1-PAK 91<br />

WA-EPH-MS2-20ML 91<br />

WA-EPH-MS2-20ML-PAK 91<br />

WA-VPH 90<br />

WA-VPH-100X 90<br />

WA-VPH-100X-PAK 90<br />

WA-VPH-10X 90<br />

WA-VPH-10X-PAK 90<br />

WA-VPH-10X-SS 90<br />

WA-VPH-10X-SS-PAK 90<br />

WA-VPH-MS 90<br />

WA-VPH-MS-PAK 90<br />

WA-VPH-PAK 90<br />

WA-VPH-RT 90<br />

WA-VPH-RT-PAK 90<br />

WC-OILG-10X-1 2, 96<br />

WFD2-R1-SET 93<br />

WFD2-SET 93<br />

WFK-SET 93<br />

WGU-SET 93<br />

WM-11-NMS-10X-1 61<br />

WM-11-NMS-1X-1 61<br />

WM-11-NMS-30X-1 61<br />

WM-11-NMS-3X-1 61<br />

WM-11-NMS-50X-1 61<br />

WM-11-NMS-5X-1 61<br />

WM-11-NMS-90X-1 61<br />

WM-11-NMS-SET-1 61<br />

WM-12-10X-4 59<br />

WM-12-10X-8 59<br />

WM-12-1X-4 59<br />

WM-12-1X-8 59<br />

WM-12-30X-4 59<br />

WM-12-30X-8 59<br />

WM-12-3X-4 59<br />

WM-12-3X-8 59<br />

WM-12-50X-4 59<br />

WM-12-50X-8 59<br />

WM-12-5X-4 59<br />

WM-12-5X-8 59<br />

WM-12-90X-4 59<br />

WM-12-90X-8 59<br />

WM-12-NMS-10X-1 61<br />

WM-12-NMS-1X-1 61<br />

WM-12-NMS-30X-1 61<br />

WM-12-NMS-3X-1 61<br />

WM-12-NMS-50X-1 61<br />

WM-12-NMS-5X-1 61<br />

WM-12-NMS-SET-1 61<br />

WM-12-SET-4 59<br />

WM-12-SET-8 59<br />

WM-20CST-01 59<br />

WM-20CST-02 59<br />

WM-20CST-03 59<br />

WM-20CST-04 59<br />

WM-20CST-06 59<br />

WM-20CST-07 59<br />

WM-20CST-08 59<br />

WM-20CST-09 59<br />

WM-20CST-13 59<br />

WM-20CST-15 59<br />

WM-20CST-27 59<br />

WM-20CST-29 59<br />

WM-20CST-30 59<br />

WM-20CST-32 59<br />

WM-20CST-33 59<br />

WM-20CST-34 59<br />

WM-20CST-35 59<br />

WM-20CST-37 59<br />

WM-20CST-41 59<br />

WM-20CST-43 59<br />

WM-20CST-50 59<br />

WM-20CST-52 59<br />

WM-20CST-53 59<br />

WM-20CST-54 59<br />

WM-20CST-55 59<br />

WM-20CST-60 59<br />

WM-20CST-63 59<br />

WM-20CST-64 59<br />

WM-20CST-70 59<br />

WM-20CST-71 59<br />

WM-20-NMS-10X-1 26, 61<br />

WM-20-NMS-1X-1 26, 61<br />

WM-20-NMS-30X-1 26, 61<br />

WM-20-NMS-3X-1 26, 61<br />

WM-20-NMS-50X-1 26, 61<br />

WM-20-NMS-5X-1 26, 61<br />

WM-20-NMS-90X-1 26, 61<br />

WM-20-NMS-SET-1 26, 61<br />

WM-21-10X-4 59<br />

WM-21-10X-8 59<br />

WM-21-1X-4 59<br />

WM-21-1X-8 59<br />

WM-21-30X-4 59<br />

WM-21-30X-8 59<br />

WM-21-3X-4 59<br />

WM-21-3X-8 59<br />

WM-21-50X-4 59<br />

WM-21-50X-8 59<br />

WM-21-5X-4 59<br />

WM-21-5X-8 59<br />

WM-21-90X-4 59<br />

WM-21-90X-8 59<br />

WM-21-NMS-10X-1 28<br />

WM-21-NMS-10X-1 61<br />

WM-21-NMS-1X-1 28<br />

WM-21-NMS-1X-1 61<br />

WM-21-NMS-30X-1 28<br />

WM-21-NMS-30X-1 61<br />

WM-21-NMS-3X-1 28<br />

WM-21-NMS-3X-1 61<br />

WM-21-NMS-50X-1 28<br />

WM-21-NMS-50X-1 61<br />

WM-21-NMS-5X-1 28<br />

WM-21-NMS-5X-1 61<br />

WM-21-NMS-SET-1 28<br />

WM-21-NMS-SET-1 61<br />

WM-21-SET-4 59<br />

WM-21-SET-8 59<br />

WM-75CST-01-5X 59<br />

WM-75CST-02-5X 59<br />

WM-75CST-04-5X 59<br />

WM-75CST-06-5X 59<br />

WM-75CST-07-5X 59<br />

WM-75CST-08-5X 59<br />

WM-75CST-09-5X 59<br />

WM-75CST-13-5X 59<br />

WM-75CST-15-5X 59<br />

WM-75CST-27-5X 59<br />

WM-75CST-29-5X 59<br />

WM-75CST-30-5X 59<br />

WM-75CST-32-5X 59<br />

WM-75CST-33-5X 59<br />

WM-75CST-35-5X 59<br />

WM-75CST-37-5X 59<br />

WM-NMS-14 26, 28<br />

WM-NMS-14-5X 26, 28<br />

Z-008 21<br />

Z-008S 54<br />

Z-008S-H-10X 54<br />

Z-008S-M 54<br />

WM-20CST-67 59 vii<br />

INDEX


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