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反応ゲルの調製<br />

水熱合成 : 190℃, 1 h ~ 9 d<br />

水洗 : 超音波 2 h<br />

熱処理 : 600℃, 5 h<br />

評価 : XRD, SEM<br />

研究成果概要<br />

オートクレーブ<br />

テフロン容器<br />

反応ゲル<br />

SiO 2 : Al 2O 3 : TPAOH : NaOH : H 2O<br />

=1 : 0.02 : 0.07 : 0.30 : 22.48<br />

14

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