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Pesticide Standards Reference Guide - AccuStandard

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GPC Calibration Solution<br />

M-1600-GPC-5ML $ 35 / 1 x 5 mL<br />

At stated conc. in CH2Cl2 5 comps.<br />

Corn oil (300 mg/mL)<br />

bis(2-Ethylhexyl)phthalate (15 mg/mL)<br />

Pentachlorophenol (1.4 mg/mL)<br />

Perylene (0.1 mg/mL)<br />

Sulfur (0.5 mg/mL)<br />

M-1657-CAL-SET $ 195 / 4 x ( 3 x 1 mL )<br />

Contains all 4 calibration groups at the respective Low, Medium and High Ranges<br />

Calibration Group 1<br />

M-1657-01-R1-CAL-SET $ 60 / 3 x 1 mL<br />

All solutions in Isooctane 9 comps.<br />

Components Low Medium High<br />

(units in ng/mL) ( 1X ) ( 5X ) ( 20X )<br />

Azinphos methyl 100 500 2,000<br />

Dichlorvos 500 2,500 10,000<br />

Disulfoton 200 1,000 4,000<br />

Fenthion 200 1,000 4,000<br />

Merphos (A + B) 400 2,000 8,000<br />

Ronnel 200 1,000 4,000<br />

Sulprofos 200 1,000 4,000<br />

Tributyl phosphate 200 1,000 4,000<br />

Triphenyl phosphate 200 1,000 4,000<br />

Calibration Group 4<br />

M-1657-04-CAL-SET $ 60 / 3 x 1 mL<br />

All solutions in Isooctane 11 comps.<br />

Components Low Medium High<br />

(units in ng/mL) ( 1X ) ( 5X ) ( 20X )<br />

Coumaphos 500 2,500 10,000<br />

Diazinon 200 1,000 4,000<br />

EPN 200 1,000 4,000<br />

Ethion 200 1,000 4,000<br />

Ethoprop 200 1,000 4,000<br />

Malathion 200 1,000 4,000<br />

Phorate 200 1,000 4,000<br />

Tetrachlorvinphos 200 1,000 4,000<br />

Tributyl phosphate 200 1,000 4,000<br />

Trichloronate 200 1,000 4,000<br />

Triphenyl phosphate 200 1,000 4,000<br />

Calibration Group 2<br />

M-1657-02-CAL-SET $ 60 / 3 x 1 mL<br />

All solutions in Isooctane 12 comps.<br />

Components Low Medium High<br />

(units in ng/mL) ( 1X ) ( 5X ) ( 20X )<br />

Chlorfevinphos 200 1,000 4,000<br />

Chlorpyrifos 200 1,000 4,000<br />

Demeton (O + S) 400 2,000 8,000<br />

Dichlofenthion 200 1,000 4,000<br />

Dimethoate 100 500 2,000<br />

Famphur 500 2,500 10,000<br />

Leptophos 200 1,000 4,000<br />

Methyl parathion 200 1,000 4,000<br />

Tributyl phosphate 200 1,000 4,000<br />

Trichlorofon 500 2,500 10,000<br />

Tricresylphosphate 100 500 2,000<br />

Triphenyl phosphate 200 1,000 4,000<br />

Certificate of Analysis and MSDSs are available from www.<strong>AccuStandard</strong>.com<br />

Calibration Group 3<br />

M-1657-03-CAL-SET $ 65 / 3 x 1 mL<br />

All solutions in Isooctane 14 comps.<br />

Components Low Medium High<br />

(units in ng/mL) ( 1X ) ( 5X ) ( 20X )<br />

Azinphos ethyl 200 1,000 4,000<br />

Crotoxyphos 500 2,500 10,000<br />

DEF 200 1,000 4,000<br />

Fensulfothion 500 2,500 10,000<br />

Methyl chlorpyrifos 200 1,000 4,000<br />

Mevinphos 500 2,500 10,000<br />

Naled 500 2,500 10,000<br />

Parathion 200 1,000 4,000<br />

Phosmet 500 2,500 10,000<br />

Phosphamidon (E + Z) 100 500 2,000<br />

Sulfotepp 200 1,000 4,000<br />

Terbufos 200 1,000 4,000<br />

Tributyl phosphate 200 1,000 4,000<br />

Triphenyl phosphate 200 1,000 4,000<br />

Method 1659 is used to determine Dazomet by base hydrolysis to Methyl Isothiocyanate (MITC) and subsequent determination of MITC by widebore<br />

fused-silica capillary column gas chromatography with a Nitrogen Phophorus Detector (NPD).<br />

Recovery & Precision Solution<br />

M-1659-RPS $ 10 / 1 x 1 mL<br />

25 µg/mL in Acetone<br />

Methyl isothiocyanate (MITC)<br />

EPA Method 1600 Series<br />

<strong>Pesticide</strong> <strong>Standards</strong><br />

Method 1657 Organo-Phosphorus <strong>Pesticide</strong>s in Municipal & Industrial Wastewater by FPD<br />

Method 1657 is a consolidation of several EPA wastewater methods used to determine the organo-phosphorus pesticides associated with the Clean<br />

Water Act, the Resource and Conservation and Recovery Act, & the Comprehensive Environmental Response, Compensation and Liability Act; and<br />

other compounds amenable to extraction and analysis by wide-bore capillary column gas chromatography with a flame photometric detector (FPD).<br />

Solid-phase Extraction Cartridge<br />

Calibration Solution<br />

M-1600-SPE $ 10 / 1 x 1 mL<br />

0.1 mg/mL in Acetone<br />

2,4,6-Trichlorophenol<br />

Calibration Solutions and Suggested Calibration Groups<br />

Method 1659 Dazomet in Municipal & Industrial Wastewater by NPD<br />

Matrix Spiking Solution<br />

M-1659-MS $ 10 / 1 x 1 mL<br />

25 µg/mL in Acetone<br />

Dazomet<br />

Surrogate Spiking Solution<br />

M-1657-SS $ 20 / 1 x 1 mL<br />

0.2 mg/mL each in Acetone 2 comps.<br />

Tributyl phosphate<br />

Triphenyl phosphate<br />

Calibration Solutions<br />

M-1659-CAL-SET $ 25 / 3 x 1 mL<br />

M-1659-CAL-1X 0.2 mg/mL in Acetone 1 mL<br />

M-1659-CAL-5X 1.0 mg/mL in Acetone 1 mL<br />

M-1659-CAL-25X 5.0 mg/mL in Acetone 1 mL<br />

Methyl isothiocyanate (MITC)<br />

97

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