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On-line Concentration Measurement of Sulfuric acid - Anton Paar.com

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::: Application Report<br />

<strong>On</strong>-<strong>line</strong> <strong>Concentration</strong> <strong>Measurement</strong> <strong>of</strong><br />

<strong>Sulfuric</strong> <strong>acid</strong> “H2SO4”<br />

Relevant for:<br />

<strong>On</strong><strong>line</strong> concentration measurement <strong>of</strong> H2SO4 and Oleum<br />

Installation<br />

Depending on the requirements the density<br />

and/or sound velocity transducers can be<br />

installed at different sites in the process.<br />

0-90 % w/w<br />

For this application the DPRn sensor must be<br />

made <strong>of</strong> tantalum which shows an excellent<br />

resistance against sulfuric <strong>acid</strong> between 0-75 °C.<br />

For the measurement <strong>of</strong> oleum the DPRn<br />

transducer must be made <strong>of</strong> glass.<br />

DPRn<br />

Fig. 3: Bypass installation <strong>of</strong> the DPRn<br />

mPDS 1100<br />

TEMP+16.14 : °C<br />

PER-D: 2574.976 us<br />

DENS: 1.33317 g/cm3<br />

Ai-curr: 0.160 mA<br />

L<br />

06<br />

ESC<br />

ENTER<br />

mPDS 1100<br />

90-100 % w/w<br />

For H2SO4 concentration in the range <strong>of</strong> 90 to<br />

100 % w/w a gold plated SPRn sound velocity<br />

transducer is used. The gold plated SPRn<br />

transducer is inserted into the <strong>line</strong> using standard<br />

fittings (DIN 2633, DN40 PN16). All wetted parts <strong>of</strong><br />

the transducer are gold plated to prevent corrosion<br />

<strong>of</strong> the transducer material by sulfuric <strong>acid</strong>.<br />

4<br />

SPRn<br />

TEMP+16.14 : °C<br />

Fig. 4: In-<strong>line</strong> installation <strong>of</strong> the SPRn<br />

PER-D: 2574.976 us<br />

DENS: 1.33317 g/cm3<br />

Ai-curr: 0.160 mA<br />

L<br />

06<br />

ESC<br />

ENTER<br />

mPDS 1100<br />

Density or sound velocity and temperature are<br />

transferred to the mPDS 1100 by a two wire cable.<br />

The same cable powers the transducer and it can<br />

be <strong>of</strong> almost any length.<br />

90-110 %w/w<br />

For the measurement range over 100 % the DSRn<br />

sensor which delivers density, sound velocity and<br />

temperature is needed. As evaluation unit the<br />

mPDS 5 have to be connected. Because the<br />

DSRn is only available in Hastelloy the maximum<br />

temperature must not exceed 40 °C!<br />

DSRn<br />

Fig. 5: Bypass installation <strong>of</strong> the DSRn<br />

mPDS 1100

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