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Vacuum Metallurgy - ALD Vacuum Technologies

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<strong>Vacuum</strong> Systems and <strong>Technologies</strong> for<br />

<strong>Metallurgy</strong><br />

Heat Treatment


SOLUTIONS ARE OUR BUSINESS<br />

<strong>ALD</strong> <strong>Vacuum</strong> <strong>Technologies</strong> AG supplies systems<br />

and processes for thermal and thermochemical<br />

treatment of metallic materials in solid and liquid<br />

form. The company`s competence consists on the<br />

one hand of its mastery in vacuum process technology<br />

and on the other hand of its know-how in<br />

engineering custom-tailored system solutions.<br />

WORLDWIDE TECHNOLOGY<br />

AND MARKET LEADER IN:<br />

<strong>Vacuum</strong> <strong>Metallurgy</strong>:<br />

Engineering and supply of systems and processes for treating<br />

metallic materials in liquid form – particularly vacuum systems for<br />

the melting, casting and remelting of metals and alloys, as well as<br />

special coating equipment for turbine blades.<br />

<strong>Vacuum</strong> Heat Treatment and Sintering:<br />

Processes and systems for heat treating metallic materials, brazing<br />

and sintering.<br />

<strong>ALD</strong> is noted for its superb know-how basis,<br />

leadership in research and development and its<br />

strategic alliances. Close collaborations with<br />

“blue chip customers” have strengthened its<br />

position as a supplier of key technologies to<br />

major growth markets.


<strong>Vacuum</strong> <strong>Metallurgy</strong><br />

<strong>Vacuum</strong> metallurgy is presently entering a new phase wherein it is reevaluating the experience gained from<br />

continuously developing established processes and joining together new process combinations. Advanced<br />

vacuum processes such as, steel degassing and ladle metallurgy, melting and remelting, as well as precision<br />

casting and metal-powder technology, have led to high-quality metallurgical products.<br />

The use of these special metal-making processes in<br />

modern, efficiently functioning production systems<br />

greatly reduces costs. The recycling of revert from<br />

the processing of costly materials contributes to the<br />

economy´s cost-effectiveness. Examples of the products<br />

that have been derived from these technologies include<br />

highly alloyed special steels and superalloys, refractory<br />

and reactive metals with ultrahigh purity and a fine<br />

grain structure, precision castings with directional and<br />

single-crystal structures, forgings in near net shape,<br />

and high-purity powder for homogeneous, highstrength<br />

parts.<br />

16 ton VIDP<br />

melting chamber in pouring position<br />

The resulting materials of high strength and reliability<br />

contribute to demanding applications in the aircraft<br />

industries and power generation, while the high-purity<br />

products contribute to new developments in electronics.<br />

The proper selection of technology is the most<br />

demanding task the plant builder has to solve in close<br />

dialogue with the producer of the materials and the<br />

consumer. This particular challenge is the keystone of<br />

the business philosophy of <strong>ALD</strong> <strong>Vacuum</strong><br />

<strong>Technologies</strong> AG, Hanau/Germany.<br />

EB/PVD coater for mass production<br />

20 ton ESR furnace capable of melting<br />

under protective atmosphere


<strong>Vacuum</strong> Heat Treatment and Sintering<br />

Heat treatment is a sequence of heat<br />

treatment steps in which a workpiece is<br />

exposed completely to time-temperature<br />

sequences in order to change its internal<br />

structure so as to achieve the required<br />

features.<br />

Overpressure vacuum sintering furnace type<br />

VKPgr 50/50/170, 1,600 °C, 60 bar, maximum<br />

gross charge weight up to 1,700 kg.<br />

Hardening and Tempering<br />

The hardening process is a type of heat treatment<br />

comprising austenitizing and quenching of the part.<br />

The necessary requirements are selected in which<br />

the austenitic structure is changed into martensitic<br />

structure. The part undergoes tempering treatment<br />

after hardening in order to obtain high ductility and<br />

toughness.<br />

Brazing<br />

Brazing is a process for combining similar metals,<br />

whereby a liquid phase is created between them by<br />

melting additional material/brazing alloy. Hereby,<br />

the solidus temperature of the base metal is not<br />

reached. The lower pressure reduces the oxides on the<br />

surface of the workpiece and thus creates the requirements<br />

for wetting by the liquid alloy.<br />

Case Hardening<br />

<strong>Vacuum</strong> carburizing processes with or without<br />

plasma are used in the gear industry as well as for<br />

producing fuel/ diesel injection systems to withstand<br />

highest mechanical stresses and to lower manufacturing<br />

cost.<br />

Multi-chamber vacuum furnace with 8 treatment<br />

modules for carburizing automotive gear parts<br />

After the highly efficient vacuum carburizing<br />

step the parts are quenched with inert gases under<br />

higher pressures. This dry quenching method saves<br />

subsequent cleaning steps and reduces distortion<br />

of the quenched parts which saves or reduces cost<br />

intensive hard machining. Beside these advantages<br />

this newly developed and already introduced technology<br />

enables new manufacturing strategies and<br />

is environmentally friendly.<br />

Sintering<br />

The sintering process takes place in vacuum or<br />

under protective gas at the appropriate temperature<br />

for the material. A defined, reproducible sintering<br />

atmosphere without atmospheric oxygen is important.<br />

At certain pressures and temperatures the process<br />

gas feed during sintering with argon, N 2 , H 2 , CH 4 ,<br />

CO 2 and others influences the structure and chemical<br />

composition of the workpiece.<br />

ModulTherm<br />

Highest flexibility of process and<br />

production volume are a result of the modular design<br />

Following the vacuum sintering process, 6 to 10 MPa<br />

argon gas may be introduced into the furnace at<br />

sintering temperature to further reduce porosity and<br />

to ensure the material quality of high-performance<br />

hard metal tools and other sintered parts.


Delivery Programm<br />

VACUUM METALLURGY<br />

PRODUCTION SYSTEMS FOR<br />

■ VACUUM INDUCTION MELTING AND CASTING (VIM/VIDP)<br />

<strong>Vacuum</strong> Induction Melting Furnaces for Charge Weights from 1 kg up to 30 tons<br />

■ ELECTROSLAG REMELTING (ESR)<br />

■ VACUUM ARC REMELTING (VAR)<br />

■ ELECTRON BEAM MELTING (EB)<br />

■ VACUUM PRECISION CASTING<br />

<strong>Vacuum</strong> Induction Melting and Casting with Ceramic Crucibles<br />

Liquid Metal Cooling for DS/SX Solidification<br />

Cold Crucible Induction Melting and Casting<br />

<strong>Vacuum</strong> Arc Melting and Casting<br />

■ VACUUM INERT GAS METAL POWDER TECHNOLOGY<br />

<strong>Vacuum</strong> Induction Melting and Inert Gas Atomization<br />

Ceramic-Free Metal Powder Production<br />

Inert Gas Recycling<br />

■ VACUUM ISOTHERMAL FORGING<br />

Hot Isothermal Forging for “Near Net Shape” <strong>Technologies</strong><br />

■ INDUCTION HEATED QUARTZ TUBE FURNACES (IWQ)<br />

For special applications<br />

■ VACUUM TURBINE BLADE COATING<br />

Electron Beam/Physical Vapor Deposition (EB/PVD) of Protective (MCrAlY) and<br />

Thermal Barrier Coatings (TBC)<br />

VACUUM HEAT TREATMENT<br />

AND SINTERING<br />

■ VACUUM HARDENING, TEMPERING<br />

AND BRAZING<br />

<strong>Vacuum</strong> Heat Treatment of Cold and Hot<br />

Work Steels as well as High Speed Steels,<br />

Single-Chamber <strong>Vacuum</strong> Heat Treatment<br />

Systems in Horizontal and Vertical Design<br />

for different load sizes and charge weights<br />

from some kgs up to several tons, but also<br />

multi chamber systems for treating low<br />

alloyed materials.<br />

■ VACUUM CASE HARDENING<br />

<strong>Vacuum</strong> carburizing with or without<br />

plasma and subsequent high pressure gas<br />

quenching in batch and multi chamber<br />

systems for production volumes of some<br />

kgs per hour up to mass production. Full<br />

product range from single chamber, double<br />

chamber, inline multi to linked chamber<br />

systems are available.<br />

■ VACUUM SINTERING<br />

<strong>Vacuum</strong> sintering systems for cemented<br />

carbides and rare earth magnets, overpressure<br />

sintering furnaces for sintering cemented<br />

carbides at pressures up to 100 bar, all<br />

in different sizes for loads up to more than<br />

2 tons.


Customer Support by <strong>ALD</strong> – Worldwide<br />

Engineering Facilities & Operator Companies<br />

Sales Offices<br />

Territories Covered by Representatives<br />

<strong>ALD</strong> systems are built for operation around the<br />

clock, seven days per week. As and when the need<br />

for service arises, a global network is available to<br />

send urgently needed spare parts or experienced<br />

service technicians. <strong>ALD</strong> has daughter companies<br />

in 6 countries worldwide and representations in<br />

many others. Our marketing and service network<br />

and spare part stocks at strategic locations enable<br />

us to react at short notice. Additionally, our headquarters<br />

in Germany operate a customer support<br />

center with experts who assist whenever special<br />

know-how is required.<br />

<strong>ALD</strong> services include professional support in emergencies<br />

as well as preventive maintenance for plant<br />

equipment and the refurbishment of older systems to<br />

boost plant availability to the highest possible level.<br />

Our services at a glance:<br />

■ Delivery of spare parts and consumables<br />

■ Repair service<br />

■ Maintenance and inspection<br />

■ Equipment refurbishment<br />

<strong>ALD</strong> <strong>Vacuum</strong> <strong>Technologies</strong> AG<br />

Wilhelm-Rohn-Strasse 35<br />

D-63450 Hanau<br />

Phone +49 (0) 6181- 307-0<br />

Fax +49 (0) 6181- 307-3290<br />

e-mail: info@ald-vt.de<br />

Internet: www.ald-vt.de<br />

China<br />

<strong>ALD</strong> China Liaison Office<br />

C&K Development Co., Ltd.<br />

Unit C, 17/F., Seabright Plaza,<br />

9-23 Shell St., HK North Point<br />

Phone +85 (21) 257 - 84888<br />

Fax +85 (21) 257 - 87118<br />

e-mail: cnkchina@online.sh.cn<br />

Far East<br />

<strong>ALD</strong> Thermo <strong>Technologies</strong><br />

Far East Co., Ltd.<br />

Shinjuku Nomura Building, 6 F.<br />

1-26-2 Nishi-Shinjuku, Shinjuku-Ku<br />

Tokyo 163-0558 Japan<br />

Phone +81 (3) 33 40 37 26<br />

Fax +81 (3) 33 40 37 27<br />

e-mail: ald-fe@cello.ocn.ne.jp<br />

Great Britain<br />

<strong>ALD</strong> <strong>Vacuum</strong> <strong>Technologies</strong> Ltd.<br />

The Frensham Suite<br />

13-21 High Street<br />

Guildford, Surrey GU1 3DG<br />

Phone +44 (1483) 45 44 34<br />

Fax +44 (1483) 30 66 41<br />

e-mail: ald.vactech@btclick.com<br />

USA / Canada<br />

<strong>ALD</strong> <strong>Vacuum</strong> <strong>Technologies</strong>, Inc.<br />

18, Thompson Road<br />

East Windsor CT 06088<br />

Phone +1 (860) 386-72 27<br />

Fax +1 (860) 386-72 20<br />

e-mail: rschumann@ald-usa.com

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