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VOLATILE ACIDITY (BY CASH STILL) - Sonic.net

VOLATILE ACIDITY (BY CASH STILL) - Sonic.net

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CALCULATIONS<br />

NOTES<br />

Volatile acidity (gm/100mL Acetic acid) =(0.60xmL NaOH x N NaOH)–(0.60 x mL I 2 x N I 2 )<br />

= 0.60x[(mL NaOH x N NaOH) - (mL I 2 x N I 2 )]<br />

If NaOH is 0.10N and Iodine is 0.02N = (mL NaOH x 0.06) - (mL I 2 x 0.012)<br />

DISPOSAL<br />

Boiling with a dilute solution of sodium hydroxide should clean the inner chamber of the<br />

still. Boil with distilled water to remove all traces of sodium hydroxide<br />

Samples must be degassed prior to analysis.<br />

A blank may be run with DI water as a QC check.<br />

Neutralize with Kolorsafe neutralizer and discard in sink.<br />

Main Office: 7795 Bell Road • Windsor, CA 95492 • (707) 838-6312 • FAX (707) 838-1765<br />

Central Coast: 2717 Aviation Way, Suite 100 • Santa Maria, CA 93455 • (805) 922-6321 • FAX (805) 922-1751<br />

Page 2 of 2 7/25/01

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