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Get PDF - Chemistry - University of Rochester

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68<br />

both shorter articles (Notes) and lengthier ones (Articles),<br />

the covers <strong>of</strong> which continue to be a highly desired forum<br />

for authors to showcase art relating to their manuscripts.<br />

NEWS FROM THE SCIENTIFIC<br />

AND TECHNICAL STAFF:<br />

TERRY (TED) O’CONNELL started his twenty-eighth year<br />

with the <strong>Chemistry</strong> Department and enjoys his position as<br />

Director <strong>of</strong> Technical Operations. He is responsible for new<br />

equipment installations and any building renovations. In<br />

the past year, the department acquired and installed over<br />

$2,000,000 worth <strong>of</strong> research instrumentation, including: a<br />

Bruker EMX-Plus EPR spectrometer, a Thermo LTQ Velos Ion<br />

Trap LC/MS, a Bruker Fourier Transform Mass Spectrometer<br />

(FTMS); a Perkin Elmer 2400 CHN/S Analyzer, and a Bruker<br />

Aut<strong>of</strong>lex III MALDI-TOF. He works closely with Senior Lab<br />

Engineer PETE SERRINO and Research Scientist SANDIP<br />

SUR, as well as ERIC LOBENSTINE and RAY TENG.<br />

ERIC LOBENSTINE (Ph.D. ’81), Manager for Computers<br />

and Network spent a significant amount <strong>of</strong> his time this past<br />

year working with a <strong>University</strong> IT committee on a major<br />

upgrade for the email service for both graduate students<br />

and postdocs, to insure that our needs would be met. This<br />

transition went (reasonably) smoothly at the end <strong>of</strong> May; so<br />

many students were eager to play with the new system that it<br />

took almost a week to move all the users’ emails! Eric is very<br />

happy to announce that Hutchison Hall now has wireless<br />

network access. Since it was one <strong>of</strong> the last academic buildings<br />

on the River Campus without ubiquitous wireless access, Eric<br />

has been pushing hard for this service for several years now.<br />

On a personal note, Eric’s older Brian graduated Magna Cum<br />

Laude in May, with a B.A. in Financial Economics and minors<br />

in <strong>Chemistry</strong> and English. After an internship this summer at<br />

Global Crossing, Brian is attending the Simon School in the fall<br />

Eric Lobenstine with son, Brian, and wife, Jeanne<br />

to work on his M.B.A. Ethan, Eric’s younger son, now a Senior<br />

had a great summer working as an Orientation Leader for the<br />

1200+ students who arrived for the 2010-2011 academic year.<br />

RAY TENG (B.S. ’87, M.B.A. ’01) has been with the<br />

<strong>University</strong> since 1987 and joined <strong>Chemistry</strong> in 2004 as<br />

Research/Facility Coordinator. Ray brings many years <strong>of</strong><br />

experience to the Department, having previously worked<br />

in the Department <strong>of</strong> Physics and Astronomy, the Nuclear<br />

Structure Research Laboratory, and the Department <strong>of</strong> Earth<br />

and Environmental Sciences as Senior Technical Associate. In<br />

2009, minor renovations in Hutchison Hall were undertaken:<br />

Room 468 was converted to a computer lab, B25 was renovated<br />

for a new Bruker Low Temperature EPR, and <strong>of</strong>fice space<br />

(431) was renovated for our new faculty hire, Oleg Prezhdo.<br />

Ray continues to enjoy the daily interactions with faculty and<br />

students in addressing research and facilities issues. Soccer<br />

continues to play a big part in Ray’s spare time to which he<br />

has now added “the college search” for D3 soccer schools.<br />

Once a chemist has synthesized a new molecule, he or she<br />

needs to “characterize” it in order to prove to the scientific<br />

community that it really exists. Two <strong>of</strong> the most important<br />

and trusted means <strong>of</strong> characterization for solid samples are<br />

single crystal X-ray crystallography and combustion elemental<br />

analysis. The former technique determines the composition <strong>of</strong><br />

one crystal (like a sugar or salt crystal) and provides the chemist<br />

with the identity and arrangement <strong>of</strong> atoms in the sample. The<br />

latter technique involves burning a portion (about 2 mg) <strong>of</strong><br />

the bulk solid sample and measuring the amount <strong>of</strong> carbon<br />

dioxide, water, and nitrogen to provide the chemist with the<br />

absolute percentages <strong>of</strong> carbon, hydrogen, and nitrogen in<br />

the sample. Our crystallographer, BILL BRENNESSEL, has<br />

been busy with the management and operation <strong>of</strong> facilities<br />

dedicated to those two techniques. The X-ray Crystallography<br />

Facility continues its high turnout <strong>of</strong> results with, on average, a<br />

new sample run daily. In addition, undergraduate students get<br />

hands-on training as part <strong>of</strong> the inorganic techniques course,<br />

CHM 234, and graduate students learn the theory and full<br />

operation <strong>of</strong> the instrumentation in CHM 417. Students who<br />

have taken CHM 417 are <strong>of</strong>ficially trained users <strong>of</strong> the facility<br />

and can examine their own research samples. The new CENTC<br />

Elemental Analysis Facility, provided by a grant obtained<br />

through Pr<strong>of</strong>essor William Jones and CENTC (Center for<br />

Enabling New Technologies through Catalysis), has been<br />

running for nearly six months now. The instrumentation<br />

includes the combustion analyzer, a microbalance, and a<br />

high-end glovebox used to prepare samples that react with<br />

the oxygen or water in air. Despite the synthetic research<br />

community’s routine use <strong>of</strong> this technique, it is surprising that<br />

we are one <strong>of</strong> the few universities to have a facility on site. The<br />

in-house nature <strong>of</strong> the facility not only eliminates shipping

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