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for PalmSens handheld potentiostat/galvanostat - WonATech

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The available methods<br />

Voltammetric techniques:<br />

• Linear sweep voltammetry LSV<br />

• Differential pulse voltammetry DPV<br />

• Square wave voltammetry SWV<br />

• Normal pulse voltammetry NPV<br />

• ac Voltammetry acV<br />

• Cyclic voltammetry CV<br />

• Stripping chronopotentiometry (or PSA) SCP<br />

Note: these techniques can also be used <strong>for</strong> stripping voltammetry<br />

Techniques as a function of time:<br />

• Amperometric detection AD<br />

• Pulsed amperometric detection PAD<br />

• Multiple pulse amperometry MPAD<br />

• Fast amperometry FAMP<br />

• Potentiometry CP<br />

• Multistep Amperometry MA<br />

• Multistep Potentiometry MP<br />

The specifications of most of the relevant parameters<br />

General pretreatment:<br />

General voltammetric parameters:<br />

Apply conditioning potential <strong>for</strong>:<br />

Apply deposition potential <strong>for</strong>:<br />

Apply begin potential <strong>for</strong>:<br />

0 – 1600 s<br />

0 – 1600 s<br />

0 – 1600 s<br />

Begin potential: -2.000 V to + 2.000 V<br />

End potential: -2.000 V to + 2.000 V<br />

Step potential: 1 mV to 250 mV<br />

Conditioning potential:<br />

Deposition potential:<br />

Standby potential:<br />

-2.000 V to + 2.000 V<br />

-2.000 V to + 2.000 V<br />

-2.000 V to + 2.000 V<br />

Pulse potential: 1 mV to 250 mV<br />

ac-amplitude: 1 mV to 250 mV<br />

Limits of some technique specific parameters <strong>for</strong> <strong>PalmSens</strong><br />

DPV and NPV: Scan rate:<br />

Pulse time:<br />

1 mV/s (1mV step) to 50 mV/s (5 mV<br />

step)<br />

10 ms to 300 ms<br />

SWV: Frequency: 1 Hz to 400 Hz<br />

SCP: Sampling rate: Approx. 40 kHz., max. 100 s<br />

LSV and CV: Scan rate: 0.2 mV/s (1 mV step) to 5 V/s (5 mV<br />

step)<br />

acV:<br />

AD and PAD:<br />

MPAD:<br />

Fast amperometry:<br />

Scan rate:<br />

Frequency:<br />

Interval time:<br />

Pulse time:<br />

Run time:<br />

Mode:<br />

Maximum number of points:<br />

Pulse times:<br />

Run time:<br />

Number of potential levels:<br />

Maximum number of points:<br />

Interval time:<br />

Maximum run time:<br />

Maximum number of points:<br />

1 mV/s (1 mV step) to 25 mV/s (5 mV<br />

step)<br />

0.12 Hz to 250 Hz<br />

10 or 50 ms to 300 s<br />

1 ms to 1 s<br />

10 s to 100000 s<br />

dc-amperometry and normal<br />

pulse and differential pulse.<br />

65000<br />

100 ms to 2 s<br />

10 s to 100000 s<br />

3<br />

65000<br />

1 ms to 1 s<br />

30 s<br />

20000

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