Schedule B3 - COAG Standing Council on Environment and Water

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7.6 Organic carbon 25 7.6.1 Scope and application 25 7.6.2 Interferences 25 8 Metals ..............................................................................................................................................26 8.1 Aqua regia digestible metals 26 8.1.1 Scope and application 26 8.1.2 Principle 26 8.2 Acid digestible metals in sediments, sludges and soils 26 8.2.1 Scope and application 26 8.2.2 Principle 27 8.2.2.1 For FAAS and ICP-AES 27 8.2.2.2 For GFAAS and ICP-MS 27 8.3 Metals by microwave assisted acid digestion of sediments, sludges, soils and oils 27 8.3.1 Scope and application 27 8.3.2 Principle 27 8.4 Mercury 27 8.4.1 Scope and application 27 8.4.2 Principle 28 8.5 Hexavalent chromium 28 8.5.1 Scope and application 28 8.5.2 Principle 28 9 Halides.............................................................................................................................................29 9.1 Bromide 29 9.1.1 Scope and application 29 9.1.2 Principle 29 9.2 Fluoride 29 9.2.1 Scope and application 29 9.2.2 Principle 29 10 Non-metals (cyanide and sulphur) ............................................................................................30 10.1 Total cyanide 30 10.1.1 Scope and application 30 10.1.2 Principle 30 10.2 Total sulfur 30 10.2.1 Scope and application 30 10.2.2 Principle 30 10.3 Sulfate 30 10.3.1 Scope and application 30 10.3.2 Principle 31 10.4 Sulfide 31 10.4.1 Scope and application 31 10.4.2 Principle 31
11 Organics ..........................................................................................................................................32 11.1 Volatile organics 33 11.1.1 Scope and application 33 11.2 Monocyclic aromatic hydrocarbons (MAH) 33 11.2.1 Preliminary screening 33 11.2.2 Sample extraction 33 11.2.3 Sample clean-up 33 11.2.4 Sample analysis 34 11.3 Volatile halogenated compounds 34 11.3.1 Sample extraction 34 11.3.2 Sample clean-up 34 11.3.3 Sample analysis 35 11.4 Miscellaneous volatile organic compounds 35 11.4.1 Sample extraction 35 11.4.2 Sample clean-up 35 11.4.3 Sample analysis 36 11.5 Volatile total recoverable hydrocarbons (vTRH) 36 11.6 Volatile total recoverable hydrocarbons (vTRH) by purge and trap analysis 36 11.6.1 Scope 36 11.6.2 Sample extraction 36 11.6.3 Extract clean-Up 36 11.6.4 Extract analysis 36 11.7 Semi-volatile organics 37 11.7.1 Scope and application 37 11.8 Semi-volatile chlorinated hydrocarbons 37 11.8.1 Sample extraction 38 11.8.2 Extract clean-up 38 11.8.3 Extract analysis 39 11.9 Polycyclic aromatic hydrocarbons by solvent extraction 39 11.9.1 Sample extraction 39 11.9.2 Sample clean-up 40 11.9.3 Extract analysis 40 11.10 Polycyclic aromatic hydrocarbons by supercritical fluid extraction 40 11.10.1 Sample extraction 40 11.10.2 Extract clean-up 41 11.10.3 Extract analysis 41 11.11 Organochlorine pesticides and polychlorinated biphenyls 41 11.11.1 Sample extraction 41 11.11.2 Extract analysis 43 11.12 Organophosphorus pesticides 43 11.12.1 Sample extraction 43 11.12.2 Extract clean-up (not usually necessary) 44 11.12.3 Sample Analysis 44
Page 1 and 2: National Environment Protection (As
Page 3 and 4: The following guideline provides ge
Page 5: 4.4 Sample control 12 4.5 Documenta
Page 9 and 10: 15.2 Method A1: Determination of vo
Page 11 and 12: 2 Laboratory analysis of potentiall
Page 13 and 14: 3 Determinative methods This guidel
Page 15 and 16: 3.4 Use of results Effective site a
Page 17 and 18: 4.2.2 Analysis blank This refers to
Page 19 and 20: The minimum validation data require
Page 21 and 22: 4.3.4.2 Practical quantitation limi
Page 23 and 24: 5 Sample preparation and storage 5.
Page 25 and 26: The effect of drying temperature on
Page 27 and 28: 5.2.2 Preparation of field-moist sa
Page 29 and 30: After taking a sub-sample from a 12
Page 31 and 32: 6 Analytical methods This section d
Page 33 and 34: The same 1:5 soil-water suspension
Page 35 and 36: 8 Metals 8.1 Aqua regia digestible
Page 37 and 38: 8.4.2 Principle Mercury is digested
Page 39 and 40: 10 Non-metals (cyanide and sulphur)
Page 41 and 42: 11 Organics The table below lists t
Page 43 and 44: 11.2.4 Sample analysis The table be
Page 45 and 46: 11.4.3 Sample analysis The table be
Page 47 and 48: 11.8.1 Sample extraction The table
Page 49 and 50: * Ensure samples don’t overheat;
Page 51 and 52: 3550C Ultrasonic extraction* using:
Page 53 and 54: 3550C Ultrasonic extraction* using:
Page 55 and 56: TRH can be defined as all chromatog
Page 57 and 58:
11.14.1 Sample extraction The table
Page 59 and 60:
11.15.2 Extract clean-up 3650B Acid
Page 61 and 62:
11.17 Dioxins and furans 11.17.1 Sc
Page 63 and 64:
12 Leachable contaminants 12.1 Scop
Page 65 and 66:
13 Bibliography Adam, AJ & Anderson
Page 67 and 68:
Legget, GE and Argyle, DP 1985, ‘
Page 69 and 70:
US EPA SW-846, Method 5030B, Purge
Page 71 and 72:
14.2 Application of HSLs HSLs have
Page 73 and 74:
The same situation applies for larg
Page 75 and 76:
15 Appendix 2: Determination of tot
Page 77 and 78:
15.1.3.1 Hydrocarbon product linear
Page 79 and 80:
Calibration verification standard s
Page 81 and 82:
15.3 Method A2 : Determination of s
Page 83 and 84:
• Exchange an aliquot of sample e
Page 85 and 86:
16 Shortened forms ANCE ASE© ASLP
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Schedule B3 - COAG Standing Council on Environment and Water

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