Designing the killer experiment - PraxisUnico

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+ Lesson 1 – Moving takes time• Found great, local premises, but needed chemistry andholography lab’s• Holography lab’s require considerable attention to detail• Air circulation• Health & Safety - burns• Method of making Chalcogenides high H&S risk• Arsenes, phosphines – poisonous, explosive• Extensive building modifications were needed, with planningpermissions• H&S consultants used to ensure legal compliance andmaximise staff well-being
+ Setting up first experiments• First step was to establish a base-line set of materialperformance results• Tried to replicate University results using new, bigger facilities• Initial results not as good/varied• Takes time to “bed-in” new deposition equipment• Scale was different• Experimental processes needed modifications• H&S constraints more significant• Greater need for documentation – progress/corporate liability• First step was to achieve reproducibility• This would allow predictability of performance• A precursor to our “killer” experiments
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Page 9: + Summary• Designing the killer e

Designing the killer experiment - PraxisUnico

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