Cours de Chromatographie en Phase Gazeuse (L2)
Chromatographie en Phase Gazeuse (CPG) - LISA
Chromatographie en Phase Gazeuse (CPG) - LISA
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signal FID (mV)<br />
<strong>Chromatographie</strong> <strong>en</strong> <strong>Phase</strong> <strong>Gazeuse</strong> Reproductibilié (CPG) < 8 %<br />
9400<br />
8900<br />
8400<br />
7900<br />
DL-val<br />
D-isoleu<br />
L-isoleu + DL-leu<br />
DL-ph<strong>en</strong>yl<br />
7400<br />
6900<br />
6400<br />
aci<strong>de</strong><br />
-am ino DL-ala<br />
α<br />
β<br />
-ala<br />
gly<br />
DLnorva<br />
DL-norleu<br />
aci<strong>de</strong> 4-amino<br />
DL-aci<strong>de</strong> aspa<br />
DL-aci<strong>de</strong> glu<br />
5900<br />
5400<br />
10 12 14 16 18 20 22 24 26 28 30<br />
tem ps (m in)<br />
Programme <strong>en</strong> température:70 °C, 5 min - 4 °C/min - 170 °C, 5 min. Colonne CHROMPACK<br />
10 m * 0,25 mm CP-Chirasil Dex. P=48 kPa. Split 1:100. Volume injecté : 1 microL.<br />
Université <strong>de</strong> Paris Val 12 <strong>de</strong> Val Marne <strong>de</strong> Marne Faculté <strong>de</strong>s Sci<strong>en</strong>ces et technologie Faculté <strong>de</strong> Sci<strong>en</strong>ces 9 et 16 Technologie mars 2009
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