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Gama completa de equipos para análisis químicos de referencia

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Dedicated Analytical Solutions<br />

<strong>Gama</strong> <strong>completa</strong> <strong>de</strong> <strong>equipos</strong> <strong>para</strong><br />

<strong>análisis</strong> <strong>químicos</strong> <strong>de</strong> <strong>referencia</strong>


Pre<strong>para</strong>ción <strong>de</strong> la muestra<br />

Para obtener unos buenos resultados es imprescindible pre<strong>para</strong>r la muestra correctamente. La mayoría <strong>de</strong> los errores se<br />

producen en el proceso <strong>de</strong> elaboración <strong>de</strong> la muestra, mientras que los fallos en los <strong>equipos</strong> son prácticamente inexistentes.<br />

Una pre<strong>para</strong>ción incorrecta <strong>de</strong> la muestra ocasiona graves errores en el <strong>análisis</strong>. No existe ninguna solución estándar<br />

válida <strong>para</strong> todo tipo <strong>de</strong> muestras. La mayoría <strong>de</strong> los laboratorios precisan diferentes molinos trituradores <strong>de</strong>pendiendo<br />

<strong>de</strong> la muestra y el tipo <strong>de</strong> <strong>análisis</strong>. El molino triturador, a pesar <strong>de</strong> que muchas veces no se tiene en cuenta, es un elemento<br />

importante en el proceso analítico. FOSS lo consi<strong>de</strong>ra imprescindible, por eso lo ha incluido como parte integral <strong>de</strong>l<br />

sistema analítico.<br />

A variety of bla<strong>de</strong>s for<br />

different applications.<br />

Cemotec 1090<br />

El sistema Cemotec Sample Mill es un molino triturador especialmente<br />

diseñado <strong>para</strong> triturar el grano y las semillas <strong>de</strong> las muestras sin pérdida <strong>de</strong><br />

humedad. Es un triturador excelente <strong>para</strong> pre<strong>para</strong>r todo tipo <strong>de</strong> muestras que no<br />

requieran que el tamaño <strong>de</strong>l grano sea muy fino y uniforme.<br />

• Mantiene la humedad<br />

• Aprobado por el Departamento Sueco <strong>de</strong> Agricultura<br />

Disponibles repuestos <strong>de</strong>l disco <strong>de</strong> corte (10003965) y vasos <strong>de</strong> muestras <strong>de</strong><br />

150 ml en cajas <strong>de</strong> 100 (10003923) o en cajas <strong>de</strong> 500 (10003924).<br />

Cyclotec 1093<br />

El sistema Cyclotec Sample Mill es un molino triturador diseñado <strong>para</strong><br />

triturar <strong>de</strong> forma rápida y uniforme una gran variedad <strong>de</strong> alimentos, granos,<br />

hojas... etc, a<strong>de</strong>más <strong>de</strong> productos <strong>químicos</strong>, farmacéuticos y similares. El sistema<br />

Cyclotec nos ofrece una solución rápida y práctica <strong>para</strong> pre<strong>para</strong>r con precisión<br />

muestras <strong>para</strong> una gran variedad <strong>de</strong> técnicas <strong>de</strong> <strong>análisis</strong> como por ejemplo,<br />

digestión, extracción, fibra y NIR.<br />

•<br />

•<br />

•<br />

Gran velocidad- 4 g/s con granos<br />

Distribución <strong>de</strong>l tamaño <strong>de</strong> la partícula poco dispersa<br />

Válido <strong>para</strong> la pre<strong>para</strong>ción NIR (AOAC 4.2.10 16th ed.)<br />

Repuestos: Botellas <strong>de</strong> muestra <strong>de</strong> 125 ml (10003679) <strong>de</strong> 52 o 104 (1000893)<br />

unida<strong>de</strong>s por caja. Un lio dispositivo <strong>de</strong> entrada amplio (10002485) facilita el<br />

proceso <strong>para</strong> triturar forraje, ensilaje, paja, hojas... etc. El ensamblaje <strong>de</strong> la botella<br />

(10009833) tiene una capacidad <strong>para</strong> una botella <strong>de</strong> 500 ml (10013478).<br />

Homogeneizador 2094 (monofásico, 1500 rpm) Homogeneizador<br />

2096 (trifásico, 1500/3000 rpm)<br />

Los Homogeneizadores 2094 y 2096 están diseñados <strong>para</strong> macerar y homogeneizar<br />

una gran variedad <strong>de</strong> muestras altas en grasas, fibra y humedad en unos 20-60<br />

segundos. Ejemplos <strong>de</strong> aplicación: reducción <strong>de</strong>l forraje, <strong>de</strong> la comida seca y<br />

productos <strong>químicos</strong>; homogeneización <strong>de</strong> carne, pescado, fruta, verduras<br />

y comida precocinada, incluyendo pizza, empanadas y comida congelada.<br />

• Muestras <strong>de</strong>s<strong>de</strong> 0,2 a 2,5 kg (3,5 kg con el Homogenizador 2096)<br />

• El diseño <strong>de</strong> las cuchillas aseguran la homogenización vertical y<br />

horizontal.<br />

• Modo a pulsos <strong>para</strong> tratar las muestras congeladas.<br />

Knifetec 1095 ( 20.000 rpm, refrigerado)<br />

El sistema Knifetec 1095 Sample Mill es un molino triturador que ha siso<br />

diseñado <strong>para</strong> pre<strong>para</strong>r muestras con alto contenido en grasa, humedad y fibra<br />

como por ejemplo: semillas y plantas oleaginosas, comida precocinada, cárnicos,<br />

fruta, verduras, granos, semillas, piensos y comida <strong>de</strong> animales domésticos.<br />

• Triturador <strong>de</strong> alta velocidad con cronómetro automático.<br />

• 100 ml <strong>de</strong> muestra en 2,5 o 10 ciclos <strong>de</strong> segundos.<br />

Selección <strong>de</strong>l rotor <strong>de</strong> cuchillas <strong>para</strong> diferentes aplicaciones<br />

estándar- 10005980 incluido, afilado- 10008651, pequeño- 10013135<br />

y gránulos- 10013136) y ban<strong>de</strong>ja <strong>de</strong> acero inoxidable ( 10008467).<br />

Para más información sobre molinos trituradores consulte la hoja <strong>de</strong> datos 99990730.


Digestión<br />

El sistema <strong>de</strong> digestión Tecator <strong>para</strong> Kjeldahl y otros procesos <strong>de</strong> mineralización o reflujo se compone <strong>de</strong> un digestor<br />

con un control <strong>de</strong> precisión <strong>de</strong> la temperatura, hasta 440ºC, y soportes <strong>de</strong> 8 o 20 tubos <strong>de</strong> 100 ml o 250 ml . Para cumplir<br />

la normativa BPL (Good Practice Laboratory) y Salud y Seguridad (H&S) recomendamos que los digestores se usen<br />

junto con el colector <strong>de</strong>l extractor <strong>de</strong> humos o el cabezal <strong>de</strong> reflujo, ambos situados en la cabina <strong>de</strong> gases. El soporte <strong>de</strong><br />

tubos, el extractor o el cabezal <strong>de</strong> reflujo se colocan encima <strong>de</strong>l digestor sin ocupar un espacio adicional en el laboratorio.<br />

Sistemas autoelevadores<br />

Los sistemas autoelevadores facilitan los procesos automatizados y eliminan el<br />

peso y el riesgo que conlleva el manejo <strong>de</strong> productos <strong>químicos</strong> calientes.<br />

El soporte <strong>de</strong> 8 o 20 tubos se coloca en el elevador. La aplicación seleccionada<br />

en el software controla por completo todo el proceso. El exhaust se acopla con el<br />

soporte <strong>de</strong> tubos según <strong>de</strong>scien<strong>de</strong> hasta el digestor pre-calentado y el Scrubber,<br />

en caso <strong>de</strong> estar conectado, se pone en marcha. El software <strong>de</strong> comunicación <strong>de</strong>l<br />

digestor con el PC es bidireccional por medio <strong>de</strong>l cable RS232 que se incluye<br />

con el sistema. También se pue<strong>de</strong> conectar con un módulo opcional Bluetooth.<br />

Es posible registrar constantemente datos <strong>de</strong> tiempo, temperatura, aplicación que<br />

se usa, operador, número <strong>de</strong> lote y número <strong>de</strong> i<strong>de</strong>ntificación.<br />

Sistemas <strong>de</strong> soportes “autorack”<br />

Cuando se usa un sistema <strong>de</strong> soporte autorack en lugar <strong>de</strong> un sistema autoelevador<br />

se sigue el mismo procedimiento que en el sistema autoelevador, exceptuando<br />

que en el sistema autorack la colocación <strong>de</strong>l exhaust en el digestor y su<br />

se<strong>para</strong>ción se hace <strong>de</strong> forma manual al oír la señal. La aplicación seleccionada<br />

controla todas las funciones al igual que en el sistema autoelevador.<br />

Sistemas básicos<br />

La temperatura y el tiempo <strong>para</strong> el proceso <strong>de</strong> digestión se seleccionan en el<br />

panel principal. Todos los <strong>de</strong>más procedimientos, incluyendo la conexión <strong>de</strong> la<br />

unidad <strong>de</strong> limpieza, son manuales.<br />

Sistemas <strong>de</strong> extracción y contención <strong>de</strong> humos<br />

Los sistemas <strong>de</strong> extracción <strong>de</strong> humos especialmente diseñados <strong>para</strong> cada Unidad<br />

<strong>de</strong> Digestión facilitan la eliminación y contención <strong>de</strong> humos. Recomendamos su<br />

uso en todos los procesos <strong>de</strong> digestión, evita el tener que reemplazar la cabina <strong>de</strong><br />

gases. Se recomienda el uso <strong>de</strong> los sistemas <strong>de</strong> digestión y extracción <strong>de</strong> humos<br />

<strong>de</strong>ntro <strong>de</strong> cabinas <strong>de</strong> gases. De esta forma cumple con la normativa BPL (Good<br />

Practice Laboratory) y <strong>de</strong> Salud y Seguridad (H&S).<br />

Unidad <strong>de</strong> Neutralización y Limpieza <strong>de</strong> humos (Scrubber)<br />

La Unidad Scrubber <strong>de</strong> Tecator es compacta, <strong>de</strong> succión in<strong>de</strong>pendiente y por<br />

tanto no se ve afectada por el flujo <strong>de</strong> agua. Durante la digestión los gases ácidos<br />

se eliminan mediante la Unidad <strong>de</strong> Neutralización/Limpieza. Primero los vapores<br />

se con<strong>de</strong>nsan y se diluyen en una amplia trampa <strong>para</strong> ácidos, <strong>de</strong>spués, se limpian<br />

y se neutralizan antes <strong>de</strong> pasar por una segunda trampa <strong>para</strong> ácidos que protege<br />

la bomba <strong>de</strong> vacio en caso <strong>de</strong> que los neutralizantes se agoten. Después el aire<br />

limpio sale por la salida <strong>de</strong>l tubo. Para cumplir con la normativa BPL (Good<br />

Practice Laboratory) y <strong>de</strong> Salud y Seguridad (H&S) dicho tubo <strong>de</strong> ventilación<br />

<strong>de</strong>bería orientarse a la cabina <strong>de</strong> gases. Cuando el Scrubber se conecta a un sistema<br />

automático el programa controlará por completo toda la función incluyendo<br />

los ajustes <strong>de</strong> mayor o menor aspiración.<br />

Para más información sobre la gama <strong>de</strong> digestores consulte la hoja <strong>de</strong> datos 99990720.


Destilación<br />

Las sistemas Kjeltec han sido diseñados <strong>para</strong> conseguir la mayor precisión posible en los <strong>análisis</strong> Kjeldahl y otras <strong>de</strong>stilaciones.<br />

Para cumplir con los diferentes requisitos analíticos, la gama Kjeltec incluye una gran variedad <strong>de</strong> <strong>equipos</strong>, <strong>de</strong>s<strong>de</strong><br />

unida<strong>de</strong>s simples <strong>de</strong> <strong>de</strong>stilación hasta sistemas con automuestreador <strong>completa</strong>mente automáticos. La prestación patentada<br />

SAFE (Steam Addition for Equilibration) reduce la capacidad <strong>de</strong> reacción entre los ácidos concentrados y el álcali.<br />

Todos los <strong>equipos</strong> tienen un cabezal <strong>de</strong> expansión <strong>de</strong> polipropileno resistente al álcali y bombas <strong>de</strong> fuelle <strong>para</strong> dispensar<br />

reactivos con precisión. Las aplicaciones químicas optimizadas le proporcionan un coste muy reducido en cada <strong>análisis</strong><br />

realizado.<br />

Kjeltec 2100<br />

Es una unidad económica y semiautomática <strong>para</strong> <strong>análisis</strong> Kjeldahl y otras <strong>de</strong>stilaciones<br />

químicas como por ejemplo, dióxido <strong>de</strong> azufre, alcohol, fenoles, ácidos<br />

volátiles...etc. La muestra digerida en el tubo se pue<strong>de</strong> diluir manualmente,<br />

en caso necesario, y luego se coloca en la unidad. El álcali (u otro reactivo) se<br />

dispensa automáticamente iniciándose la <strong>de</strong>stilación automática que se produce<br />

durante el tiempo seleccionado. Una válvula <strong>de</strong> antiretorno evita que el <strong>de</strong>stilado<br />

retroceda al final <strong>de</strong>l ciclo. La muestra <strong>de</strong>stilada se valora manualmente o con un<br />

valorador externo.<br />

Para más información sobre Kjeltec 2100 consulte la hoja <strong>de</strong> datos 99990217.<br />

Kjeltec 2200<br />

Es una unidad versátil y <strong>completa</strong>mente automática <strong>para</strong> el <strong>análisis</strong> Kjeldahl<br />

y otras <strong>de</strong>stilaciones . El tubo que contiene la muestra digerida se coloca en la<br />

unidad y se cierra la puerta <strong>de</strong> seguridad. El sistema diluye automáticamente la<br />

muestra, controla el agua <strong>de</strong> refrigeración, aña<strong>de</strong> álcali (u otro reactivo), <strong>de</strong>stila<br />

la muestra en el periodo <strong>de</strong> tiempo seleccionado y vacía el vaso <strong>de</strong> reactivo al<br />

final <strong>de</strong>l ciclo. Se pue<strong>de</strong> añadir solución receptora <strong>de</strong> forma automática con el kit<br />

opcional (10000041). Una válvula <strong>de</strong> antiretorno evita que el <strong>de</strong>stilado retroceda<br />

al final <strong>de</strong>l ciclo. La muestra <strong>de</strong>stilada se valora manualmente o con un valorador<br />

externo que se pue<strong>de</strong> conectar con el kit opcional (10011403).<br />

Para más información sobre Kjeltec 2200 consulte la hoja <strong>de</strong> datos 99990213.<br />

Kjeltec 2300<br />

Es un analizador <strong>completa</strong>mente automático <strong>para</strong> el <strong>análisis</strong> Kjeldahl y otros procesos<br />

similares..Incluye todas las prestaciones el Kjeltec 2200 a<strong>de</strong>más <strong>de</strong> la<br />

valoración automática on-line que se produce simultáneamente a la <strong>de</strong>stilación,<br />

ahorrando <strong>de</strong> este modo un tiempo valioso. Los resultados aparecen en pantalla<br />

en las unida<strong>de</strong>s <strong>de</strong>seadas. La impresora opcional (10007913) le proporciona una<br />

copia impresa <strong>de</strong> los resultados. Permite <strong>de</strong>scargar datos a un PC . Un test <strong>de</strong><br />

recuperación incorporado permite validar los resultados con patrones conocidos<br />

<strong>para</strong> que <strong>de</strong> este modo genere datos fiables.<br />

Para más información sobre Kjeltec 2300 consulte la hoja <strong>de</strong> datos 99990214<br />

Kjeltec 2400 con Autosampler (Automuestreador) automático <strong>de</strong><br />

60 muestras<br />

Es un analizador <strong>completa</strong>mente automático con automuestreador <strong>para</strong> el <strong>análisis</strong><br />

automático <strong>de</strong> las digestiones Kjeldahl y otros procesos similares. El analizador<br />

Kjeltec 2400, sin muestreador, tiene las mismas prestaciones que el analizador<br />

Kjeltec 2300 a<strong>de</strong>más <strong>de</strong> la posibilidad <strong>de</strong> añadir el muestreador y la conexión<br />

a una balanza <strong>de</strong> precisión.<br />

El Autosampler 2460 tiene capacidad <strong>para</strong> tres gradillas <strong>de</strong> veinte muestras. Se<br />

pue<strong>de</strong>n añadir gradillas nuevas en cualquier momento y analizar muestras urgentes<br />

in<strong>de</strong>pendientes. Una vez que todas las muestras se han procesado el sistema<br />

realiza <strong>de</strong> forma automática un ciclo <strong>de</strong> limpieza antes <strong>de</strong> apagarse.<br />

Para más información sobre Kjeltec 2400/2460 consulte la hoja <strong>de</strong> datos 99990218


Equipos <strong>para</strong> extracción con disolvente e hidrólisis<br />

La gama <strong>de</strong> <strong>equipos</strong> <strong>de</strong> extracción Soxtec es muy amplia, <strong>de</strong>s<strong>de</strong> el sistema básico Soxtec 2045- <strong>de</strong> dos posiciones manual,<br />

hasta el sistema totalmente automático Soxtec 2050 <strong>de</strong> seis posiciones. En todos los casos las muestras se manejan<br />

por lotes <strong>para</strong> que el proceso <strong>de</strong> <strong>análisis</strong> sea lo más fácil y seguro posible. No importa el tipo <strong>de</strong> extracción que requiera<br />

su sistema Soxhlet, siempre tenemos la solución a<strong>de</strong>cuada que pue<strong>de</strong> reemplazarlo consumiendo menos disolvente y<br />

entre tres y cinco veces más rápido. No existe ningún otro extractor Soxhlet que gaste tan poco disolvente. Normalmente,<br />

gracias a la recuperación <strong>de</strong> disolvente, se consumen solo unos 16 ml <strong>de</strong> disolvente por muestra, lo que reduce el coste<br />

por prueba y la eliminación <strong>de</strong> disolvente. La seguridad siempre ha sido muy importante <strong>para</strong> nosotros, por tanto, la única<br />

parte eléctrica <strong>de</strong> la unidad <strong>de</strong> Extracción, que es la placa caliente, está diseñada a prueba <strong>de</strong> chispas. Los sensores dobles<br />

<strong>de</strong> seguridad evitan que, en ningún caso, se alcance la temperatura <strong>de</strong> ignición <strong>de</strong>l disolvente..<br />

Soxtec 2045 – Sistema <strong>de</strong> extracción manual <strong>de</strong> 2 muestras<br />

Incluye una unidad <strong>de</strong> extracción <strong>de</strong> 2 muestras y una unidad <strong>de</strong> control in<strong>de</strong>pendiente.<br />

Emplea <strong>de</strong> 50 a 60 ml <strong>de</strong> disolvente por prueba (se recupera hasta el 80%).<br />

El sistema estándar incluye: Vasos <strong>de</strong> extracción <strong>de</strong> aluminio (juego <strong>de</strong> 2)<br />

Dedales <strong>de</strong> celulosa <strong>de</strong> 33 mm (65 ml) caja <strong>de</strong> 25<br />

Opcional: Vasos <strong>de</strong> extracción <strong>de</strong> cristal (juego <strong>de</strong> 2)<br />

Dedales <strong>de</strong> celulosa <strong>de</strong> 45 mm (120 ml) caja <strong>de</strong> 25<br />

Dedales <strong>de</strong> celulosa <strong>de</strong> 26 mm (30 ml) caja <strong>de</strong> 25<br />

Para más información sobre Soxtec 2045 consulte la hoja <strong>de</strong> datos 99990310.<br />

Soxtec 2043 – Sistema <strong>de</strong> extracción manual <strong>de</strong> 6 muestras<br />

Incluye una unidad <strong>de</strong> extracción <strong>de</strong> 6 muestras y una unidad <strong>de</strong> control in<strong>de</strong>pendiente.<br />

Emplea <strong>de</strong> 40 a 50 ml <strong>de</strong> disolvente por prueba (se recupera hasta el 80%).<br />

El sistema estándar incluye: Vasos <strong>de</strong> extracción <strong>de</strong> aluminio (juego <strong>de</strong> 6)<br />

Dedales <strong>de</strong> celulosa <strong>de</strong> 26 mm (30 ml) (caja <strong>de</strong> 25)<br />

Opcional: Vasos <strong>de</strong> extracción <strong>de</strong> cristal (juego <strong>de</strong> 6)<br />

Para más información sobre Soxtec 2043 consulte la hoja <strong>de</strong> datos 99990312<br />

Soxtec 2055 – Sistema <strong>de</strong> extracción semiautomática <strong>de</strong> muestras<br />

Incluye una unidad <strong>de</strong> extracción <strong>de</strong> 6 muestras y una unidad <strong>de</strong> control in<strong>de</strong>pendiente<br />

y programable. Emplea <strong>de</strong> 70 a 90 ml <strong>de</strong> disolvente por prueba (se recupera<br />

hasta el 80%)<br />

El sistema estándar incluye: Vasos <strong>de</strong> extracción <strong>de</strong> aluminio (3 juegos <strong>de</strong> 6)<br />

Dedales <strong>de</strong> celulosa <strong>de</strong> 33 mm (65 ml) (caja <strong>de</strong> 25)<br />

Opcional: Vasos <strong>de</strong> extracción <strong>de</strong> cristal (juego <strong>de</strong> 6)<br />

Dedales <strong>de</strong> celulosa <strong>de</strong> 26 mm (30 ml) (caja <strong>de</strong> 25)<br />

Para más información sobre Soxtec 2055 consulte la hoja <strong>de</strong> datos 99990306.<br />

Soxtec 2050 – Sistema <strong>de</strong> extracción automática <strong>de</strong> 6 muestras<br />

Incluye una unidad <strong>de</strong> extracción <strong>de</strong> 6 muestras, una unidad <strong>de</strong> control in<strong>de</strong>pendiente<br />

y programable y una unidad <strong>de</strong> operación <strong>para</strong> facilitar el proceso automático.<br />

Emplea <strong>de</strong> 70 a 90 ml <strong>de</strong> disolvente por prueba (recuperación <strong>de</strong> hasta el 80%).<br />

El sistema estándar incluye: Vasos <strong>de</strong> extracción <strong>de</strong> aluminio (3 juegos <strong>de</strong> 6)<br />

Dedales <strong>de</strong> celulosa <strong>de</strong> 33 mm (65 ml) (caja <strong>de</strong> 25)<br />

Para más información sobre Soxtec 2050 consulte la hoja <strong>de</strong> datos 99990306.<br />

SoxCap 2047 – Sistema manual <strong>de</strong> hidrólisis ácida <strong>de</strong> 6 muestras.<br />

Análisis <strong>de</strong> grasa total.<br />

El sistema SoxCap 2047 forma parte <strong>de</strong> los sistemas Soxtec . Dicho sistema<br />

permite <strong>de</strong>terminar la grasa total siguiendo los métodos reconocidos. El sistema<br />

SoxCap realiza la hidrólisis, filtración y lavado sin ninguna transferencia <strong>de</strong> muestra.<br />

Esta técnica patentada ofrece un alto rendimiento y evita, en la mayoría <strong>de</strong> los<br />

casos, la manipulación manual usando herramientas <strong>para</strong> el manejo por lotes. El<br />

sistema SoxCap es compatible con Soxtec 2045, 2050 y 2055.<br />

Para más información sobre SoxCap 2047 consulte la hoja <strong>de</strong> datos 99990311.


Análisis <strong>de</strong> fibra cruda, <strong>de</strong>tergente y alimentaria<br />

Con los métodos tradicionales <strong>de</strong> <strong>análisis</strong> <strong>de</strong> fibra hay que realizar repetidos tratamientos <strong>de</strong> la muestra, transferir y filtrar,<br />

así como manejar varios reactivos, en ocasiones calientes. Cada uno <strong>de</strong> estos procesos implica un margen alto <strong>de</strong> error y<br />

un riesgo <strong>para</strong> el usuario. Los sistemas Fibertec reducen el porcentaje <strong>de</strong> error y mejoran la seguridad. La muestra no<br />

sufre ninguna transferencia durante todos los procesos lo que reduce la manipulación <strong>de</strong> reactivos y se asegura la filtración<br />

rápida y eficaz usando los sistemas integrados <strong>de</strong> vacio y presión.<br />

Los sistemas <strong>de</strong> <strong>análisis</strong> <strong>de</strong> fibra cruda y <strong>de</strong>tergente relacionados con la nutrición animal y la fibra dietética son la solución<br />

a sus necesida<strong>de</strong>s.<br />

Sistema Fibertec 2021/2023 Fibercap <strong>de</strong> 6 o 18 muestras<br />

Los sistemas manuales <strong>de</strong> bajo coste se basan en el principio <strong>de</strong> una única cápsula<br />

<strong>de</strong> inmersión <strong>para</strong> <strong>de</strong>terminar las fracciones <strong>de</strong> fibra cruda o <strong>de</strong>tergente (NDF,<br />

ADF Y ADL) siguiendo los procedimientos oficiales según lo indica la normativa<br />

AOAC, ISO, AACC, AOCS y EC.<br />

Para más información sobre Fibertec 2021/2023 consulte la hoja <strong>de</strong> datos 99990407.<br />

Fibertec M6- Sistema manual <strong>de</strong> 6 muestras<br />

Determina la cantidad <strong>de</strong> fibra según Ween<strong>de</strong>, Van Soest, etc, incluyendo el<br />

proceso <strong>de</strong> ebullición usando reactivos externos precalentados, el proceso <strong>de</strong><br />

aclarado y filtración en condiciones <strong>de</strong> reproducibilidad controladas.<br />

Incluye las siguientes unida<strong>de</strong>s:<br />

Fibertec 1020 Hot Extraction Unit – Sistema <strong>de</strong> extracción en caliente <strong>de</strong><br />

6 muestras <strong>para</strong> hidrólisis y extracción con sistemas integrados <strong>para</strong> calentar y<br />

filtrar reduciendo el contacto con los reactivos.<br />

Fibertec 1021 Cold Extraction Unit – Sistema <strong>de</strong> extracción en frío <strong>de</strong> 6<br />

muestras <strong>para</strong> <strong>de</strong>sengrasado y extracción a temperatura ambiente, por ejemplo,<br />

<strong>de</strong>terminación <strong>de</strong> lignina y <strong>de</strong>sengrasado <strong>de</strong> residuos <strong>de</strong> fibras.<br />

Para más información sobre Fibertec M6 consulte la hoja <strong>de</strong> datos 99990401.<br />

Fibertec 2010 – Sistema automático <strong>de</strong> 6 muestras<br />

El sistema Fibertec 2010 se compone <strong>de</strong> los siguientes módulos básicos:<br />

Fibertec 2010 Hot Extraction Unit- Sistema <strong>de</strong> extracción en caliente <strong>para</strong><br />

los procesos <strong>de</strong> hidrólisis y filtración con precalentamiento automático y adición<br />

<strong>de</strong> reactivos, ebullición y filtración. El sistema cumple los requisitos <strong>de</strong>l inicio<br />

<strong>de</strong>l tiempo <strong>de</strong> ebullición <strong>para</strong> fibra cruda siguiendo la normativa ISO y EC. La<br />

unidad controla <strong>de</strong> forma automática el agua <strong>de</strong> refrigeración.<br />

Fibertec 1021 Cold Extraction Unit- Sistema <strong>de</strong> extracción en frío <strong>de</strong> 6<br />

muestras <strong>para</strong> <strong>de</strong>sengrasado y extracción a temperatura ambiente, por ejemplo,<br />

<strong>de</strong>terminación <strong>de</strong> lignina y <strong>de</strong>sengrasado <strong>de</strong> residuos <strong>de</strong> fibras.<br />

Para más información sobre Fibertec 2010 consulte la hoja <strong>de</strong> datos 99990405.<br />

Fibertec E<br />

El sistema Fibertec E ha sido diseñado <strong>para</strong> <strong>de</strong>terminar <strong>de</strong> forma rápida<br />

y práctica la cantidad total <strong>de</strong> fibra alimentaria soluble e insoluble según los<br />

métodos enzimáticos establecidos, incluidos los aprobados por AOAC, AACC,<br />

NMKL y Asp. También es un sistema práctico en la pre<strong>para</strong>ción <strong>de</strong> la muestra<br />

<strong>para</strong> realizar estudios <strong>de</strong>tallados <strong>de</strong> las fracciones <strong>de</strong> fibra, por ejemplo, mediante<br />

técnicas colorimétricas o cromatográficas.<br />

El sistema incluye: una Unidad <strong>de</strong> Filtración <strong>para</strong> filtrar varias fracciones<br />

<strong>de</strong> forma rápida durante el <strong>análisis</strong>; la unidad Shaking Water Bath 1024, baño<br />

<strong>de</strong> agua con agitación, empleado <strong>para</strong> los procesos incubación enzimática. Se<br />

requiere también un sistema <strong>de</strong> baño maría ( no incluido).<br />

Para más información sobre Fibertec E 1023 consulte la hoja <strong>de</strong> datos 99990403.


Análisis mediante sistemas <strong>de</strong> inyección <strong>de</strong> flujo (FIA)<br />

La unidad FIAstar 5000 es un sistema totalmente automático <strong>para</strong> <strong>de</strong>terminar la cantidad <strong>de</strong> amonio, nitrato/nitritos,<br />

nitrógeno total, fosfatos, fósforo total y otros parámetros mediante métodos utilizados y aprobados por la normativa ISO.<br />

Se pue<strong>de</strong>n analizar hasta 3 parámetros <strong>de</strong> forma simultánea. Cada analizador lleva incorporado un <strong>de</strong>tector digital <strong>de</strong><br />

doble longitud <strong>de</strong> onda <strong>para</strong> suprimir el efecto <strong>de</strong> índice <strong>de</strong> refracción y las burbujas <strong>de</strong> aire, un termostato, una válvula<br />

<strong>de</strong> inyección y una bomba. Todo el sistema se controla mediante el software SoFIA en Windows ®, incluyendo los<br />

ajustes rutinarios según la normativa ISO 8466.<br />

Sistema FIAstar – mono canal<br />

Sistema básico <strong>para</strong> analizar un parámetro con presentación manual <strong>de</strong> la<br />

muestra. Se pue<strong>de</strong>n <strong>de</strong>terminar diferentes parámetros intercambiando el<br />

casete <strong>de</strong> método. Es necesario un PC <strong>para</strong> que funcione el software y el<br />

sistema.<br />

Requisitos <strong>de</strong>l PC<br />

PC con Windows 98, 2000 o XP.<br />

Al menos 32 Mb <strong>de</strong> memoria RAM y 40 mb <strong>de</strong> espacio disponible en el<br />

disco duro, diskette <strong>de</strong> 1,44 mb o CD.<br />

Puerto USB <strong>para</strong> cada módulo FIA que se conecte.<br />

Puerto RS232 <strong>para</strong> conectar el Sampler 5027 (Muestreador 5027)<br />

Puerto adicional RS 232 <strong>para</strong> transferir datos a LIMS.<br />

Casetes <strong>de</strong> método “conectar y analizar”<br />

Los casetes <strong>de</strong> método configurados previamente se insertan y/o se intercambian<br />

fácilmente en el modulo, la conexión y <strong>de</strong>sconexión es simple y<br />

rápida.. Tan solo se tarda unos minutos en iniciar y cerrar el sistema. Existe<br />

un casete <strong>de</strong> método en blanco <strong>para</strong> configurar aplicaciones especiales.<br />

Sistema FIAstar – 3 canales con Sampler (Muestreador)<br />

Sistema <strong>completa</strong>mente automático <strong>para</strong> analizar 3 parámetros simultáneamente<br />

en una única muestra. Gracias a la función stand-by se alarga la<br />

duración <strong>de</strong> los tubos <strong>de</strong> la bomba y se ahorra una gran cantidad <strong>de</strong> reactivos<br />

(< 3 ml <strong>de</strong> reactivo/ 24 h), teniendo la posibilidad <strong>de</strong> realizar el <strong>análisis</strong><br />

automático y <strong>de</strong>satendido incluso durante toda la noche.<br />

Autosampler 5027 (Automuestreador 5027)<br />

Ban<strong>de</strong>jas <strong>de</strong> muestras: <strong>para</strong> 64 o 120 muestras<br />

Ban<strong>de</strong>ja segmentada: 4 rejillas individuales<br />

Tamaño <strong>de</strong> la muestra: 12,30 ml<br />

Ban<strong>de</strong>ja lateral: 10 posiciones <strong>para</strong> patrones y QC<br />

Software SoFIA<br />

Puntos <strong>de</strong> calibración: hasta 10 patrones<br />

Ajuste <strong>de</strong> la curva <strong>de</strong><br />

calibración: lineal o <strong>de</strong> segundo or<strong>de</strong>n según la normativa ISO<br />

Rutinas <strong>de</strong> seguridad y<br />

buen uso <strong>de</strong>l laboratorio: comprobar las muestras, ejecutar muestras<br />

múltiples y estándar, recalibración automática,<br />

advertencias <strong>de</strong> ausencia <strong>de</strong> reactivo, <strong>de</strong><br />

muestra y fuera <strong>de</strong> rango. Biblioteca <strong>de</strong> métodos<br />

pre<strong>de</strong>finidos.<br />

Para más información sobre FIAstar 5000 consulte la hoja <strong>de</strong> datos 99990912.


Consumibles, accesorios y piezas <strong>de</strong> repuesto<br />

We consi<strong>de</strong>r consumables, accessories and original spare parts as an integral part of our support to our customers.<br />

Everything is specially <strong>de</strong>signed and manufactured to fit your systems and to ensure safe, accurate and simple laboratory<br />

work.<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Kjeltabs<br />

Amplia selección <strong>de</strong> catalizadores en forma <strong>de</strong> pastilla <strong>para</strong> los<br />

procesos <strong>de</strong> digestión ácida.<br />

Tubos <strong>de</strong> digestión y <strong>de</strong>stilación <strong>para</strong> Kjeltec<br />

Los tubos <strong>para</strong> Kjeldahl y otros <strong>análisis</strong> se emplean en los sistemas<br />

<strong>de</strong> digestión Tecator y Kjeltec . Capacidad disponible:<br />

100,250 y 750 ml. Pare<strong>de</strong>s rectas, aforados y juntas esféricas.<br />

Dedales <strong>de</strong> celulosa <strong>para</strong> Soxtec<br />

Celulosa pura <strong>de</strong> grosor simple o doble. Disponible en 26 (30),<br />

33 (65) y 45 (120) mm (ml). Versión <strong>de</strong> pureza extra <strong>para</strong><br />

aplicaciones medioambientales.<br />

FiberCap <strong>para</strong> Fibertec 2021/2023<br />

Cápsula <strong>de</strong> un solo uso <strong>para</strong> mayor seguridad , rapi<strong>de</strong>z y<br />

simplificar el <strong>análisis</strong>. Disponible en envases <strong>de</strong> 100 y 500.<br />

Crisoles <strong>para</strong> Fibertec<br />

Crisoles <strong>de</strong> cristal <strong>de</strong> varias porosida<strong>de</strong>s <strong>para</strong> Fibertec M6,<br />

2010 y 1023.<br />

FOSS ESPAÑA<br />

Josep Tarra<strong>de</strong>llas, 8-10<br />

08029-Barcelona<br />

Tel. 934949940<br />

Fax: 4052176<br />

general@foss.es<br />

Catálogo <strong>de</strong> consumibles,<br />

accesorios y<br />

piezas <strong>de</strong> repuesto<br />

Para facilitarle la búsqueda<br />

<strong>de</strong> nuestros productos y<br />

resolver sus necesida<strong>de</strong>s <strong>de</strong><br />

recambios y consumibles,<br />

en este catálogo encontrará<br />

los listados por grupos <strong>de</strong><br />

productos <strong>de</strong> los componentes<br />

<strong>para</strong> sus sistemas<br />

CA, incluyendo los<br />

correspondientes a <strong>equipos</strong><br />

discontinuados.<br />

P/N 9999 0502, Issue 1 ES, Oct 2005


Características<br />

• Registro <strong>de</strong> muestras, incluyendo i<strong>de</strong>ntificación<br />

• Instrumentos controlados <strong>de</strong>s<strong>de</strong> PC<br />

• Conforme a rutinas GLP<br />

• Impresión <strong>de</strong> informes<br />

• Exportación <strong>de</strong> datos, por ej. a Word, Excel,<br />

Acrobat<br />

• Importación/exportación LIMS<br />

• Conectable en red, visión <strong>de</strong> resultados en varias<br />

estaciones<br />

• Conexión simple a periféricos<br />

Descripción:<br />

El analizador Kjeltec 8400 tiene dos sistemas <strong>de</strong><br />

software distintos. Uno es el software incorporado<br />

que controla el <strong>análisis</strong> y contiene todas las funciones<br />

necesarias <strong>para</strong> manejar el sistema en el día a día. Este<br />

sistema se instala en fábrica en el analizador.<br />

Dedicated Analytical Solutions<br />

Compass<br />

Software <strong>de</strong> gestión <strong>de</strong> datos<br />

Software Compass <strong>para</strong> el registro rápido y fiable y trazabilidad <strong>de</strong> las muestras según las rutinas GLP, incluyendo la conexión sin problemas <strong>de</strong><br />

todos los periféricos, como balanza, impresora y PC, con in<strong>de</strong>pen<strong>de</strong>ncia <strong>de</strong>l fabricante El complemento perfecto <strong>para</strong> su nuevo Kjeltec TM 8400.<br />

El otro es un sistema opcional, Compass (Composition<br />

Analysis Software System), una aplicación <strong>de</strong><br />

PC. Este software maneja el analizador Kjeltec 8400<br />

y el muestreador, si existe, permitiendo el registro<br />

rápido y fiable y el rastreo <strong>de</strong> muestras según las<br />

rutinas GLP, incluyendo la conexión sin problemas<br />

<strong>de</strong> todos los periféricos, como balanza, impresora y<br />

PC, con in<strong>de</strong>pen<strong>de</strong>ncia <strong>de</strong>l fabricante .<br />

Compass proporciona una comunicación bidireccional<br />

con el analizador a través <strong>de</strong> Ethernet con comandos<br />

<strong>de</strong> usuario. Esta comunicación también facilita<br />

la conexión a diversos paquetes LIMS (Sistema <strong>de</strong><br />

gestión <strong>de</strong> información <strong>de</strong> laboratorio, Laboratory<br />

Information Management System) propietarios o<br />

personalizados.<br />

Las tareas realizadas con frecuencia se pue<strong>de</strong>n realizar<br />

rápidamente utilizando las nueve teclas <strong>de</strong> acceso<br />

directo <strong>de</strong> la barra <strong>de</strong> herramientas <strong>de</strong> comandos. A<br />

estos comandos se pue<strong>de</strong> acce<strong>de</strong>r también <strong>de</strong>s<strong>de</strong> el<br />

menú principal.


Número <strong>de</strong> pedido:<br />

60031632 Compass Data Management Software<br />

Requisitos <strong>de</strong> sistema <strong>de</strong>l PC:<br />

Por favor, tenga en cuenta que los requisitos indicados a continuación<br />

son únicamente <strong>para</strong> la Aplicación/Base <strong>de</strong> datos<br />

Compass y que los requisitos <strong>de</strong>l sistema operativo <strong>de</strong>l usuario<br />

podrían ser superiores.<br />

Aplicación Compass<br />

• Windows® 2000 Service Pack 4/Windows® Server 2003<br />

Service Pack 1/Windows® XP Service Pack 2/Windows®<br />

Vista con SP 1<br />

• Pentium III 600 MHz o superior (recomendado 1 GHz)<br />

• 192 MB RAM (recomendado 512 MB)<br />

• 1025 MB <strong>de</strong> espacio disponible en el disco duro<br />

• Un puerto Ethernet <strong>para</strong> comunicación con el Analizador<br />

Base <strong>de</strong> datos <strong>de</strong> Compass<br />

• Windows® 2000 Service Pack 4/Windows® Server 2003<br />

Service Pack 1/Windows® XP Service Pack 2/Windows®<br />

Vista con SP 1<br />

• .NET Framework 2.01)<br />

• Microsoft SQL Server 2005 Express<br />

• Pentium III 600 MHz o superior (recomendado 1 GHz)<br />

• 192 MB RAM (recomendado 512 MB)<br />

• 1025 MB <strong>de</strong> espacio disponible en el disco duro<br />

• Un puerto Ethernet <strong>para</strong> comunicación con la aplicación<br />

Compass<br />

1)<br />

Se pue<strong>de</strong> <strong>de</strong>scargar <strong>de</strong> la página web <strong>de</strong> Microsoft®. .NET Framework 2.0<br />

<strong>de</strong>be instalarse antes que Microsoft® SQL Server 2005 Express<br />

FOSS Analytical<br />

Slangerupga<strong>de</strong> 69<br />

DK-3400 Hilleroed<br />

Dinamarca<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Comunicación con la balanza:<br />

El PC <strong>de</strong>be conectarse a la balanza mediante un cable serie<br />

(RS-232) (no incluido) según las especificaciones <strong>de</strong>l fabricante<br />

<strong>de</strong> la balanza <strong>para</strong> la comunicación con el PC.<br />

Los comandos enumerados son compatibles con los siguientes<br />

mo<strong>de</strong>los <strong>de</strong> balanzas:<br />

Mo<strong>de</strong>los Sartorius A120S, A200S, A210P<br />

GetWeight: ESC P CR LF<br />

GetStableWeight: ESC P CR LF<br />

Mo<strong>de</strong>los Sartorius CP, GC y GP<br />

GetWeight: ESC P CR LF<br />

GetStableWeight: ESC P CR LF<br />

Mo<strong>de</strong>los Mettler Toledo Excellence Plus XP (XP105DR,<br />

XP205, XP205DR, XP204, XP504, XP504DR)<br />

GetWeight: SI CR LF<br />

GetStableWeight: S CR LF<br />

Comunicaciones LIMS<br />

Exportación <strong>de</strong> datos <strong>de</strong> resultados a archivos con formato *.txt,<br />

*.xml o *.csv <strong>para</strong> lectura por LIMS<br />

Importación <strong>de</strong> datos <strong>de</strong> muestras <strong>de</strong> archivos con formato<br />

*.xml creados por LIMS<br />

Cables necesarios, no suministrados en el paquete Compass:<br />

• Cable serie – (RS-232) conexión a la balanza conforme a<br />

las especificaciones <strong>de</strong>l fabricante <strong>de</strong> la misma<br />

• Cable <strong>de</strong> red – Instalación en red<br />

• Cable cruzado – Conexión directa al Analizador<br />

P/N 1026228, Edición 1 ES, Enero 2009


Tecator Digestion Unit Auto Lift 20 together with the Scrubber, for<br />

fully unatten<strong>de</strong>d operation.<br />

Features and benefits:<br />

Tecator Digestion units, with integrated programmable controllers,<br />

can be combined with a range of accessories offering:<br />

• fully automated digestion with user interface adapting to<br />

actual product configuration<br />

• convenient, safe and flexible operation<br />

• GLP-support through two way PC communication<br />

• economy of chemicals, energy, labour, space and time<br />

• efficient fume containment through optional exhaust<br />

• efficient fume removal through optional scrubber<br />

The systems, with extensive application support, are compatible<br />

with Kjeltec Distilling Units.<br />

General Description:<br />

The products <strong>de</strong>scribed in this brochure can be combined to<br />

match individual needs, from units capable of handling just a<br />

few samples a day up to fully automated systems for high sample<br />

throughput. Three configurations; Auto Lift, Auto Rack,<br />

and Basic; are available for either 250 ml or 100 ml digestion<br />

tubes; which must be specified when or<strong>de</strong>ring; <strong>de</strong>pendant on<br />

the application required.<br />

A Digestion System is based on a Digestion Unit and tube<br />

rack with capacity for either eight or twenty tubes. For most<br />

Kjeldahl digestions straight 250 ml tubes are recommen<strong>de</strong>d.<br />

To comply with GLP and Health & Safety requirements we<br />

recommend that all Digestion Units are used with an Exhaust<br />

Manifold or Reflux Head, and are located in a fume cupboard.<br />

An optional Scrubber Unit creates a fully integrated system.<br />

Dedicated Analytical Solutions<br />

Tecator Digestion Systems<br />

Auto Lift versions, with exhaust docking facility, allow fully<br />

automated unatten<strong>de</strong>d operation contributing to safety and convenience<br />

by eliminating handling of hot chemicals and saving<br />

valuable bench space. Auto Rack versions allow automated<br />

digestions but require manual placement of Tube Rack and<br />

Exhaust Manifold which are stored above the Digestion Unit<br />

in a similar position to the Auto Lift. All Auto mo<strong>de</strong>ls have an<br />

integrated programmer which precisely controls temperature(s)<br />

and timing together with connected components. The analysis<br />

cycle is clearly monitored on the graphical display. Auto mo<strong>de</strong>ls<br />

can be connected to a PC for data logging and downloading<br />

of standard, and user <strong>de</strong>fined, applications. The programmer<br />

has various password protected access levels to prevent unauthorised<br />

modification and comply with accreditation procedures.<br />

Basic versions have built in, user <strong>de</strong>finable, temperature<br />

and time control clearly viewed on the display.<br />

Auto Rack versions can be upgra<strong>de</strong>d to Auto Lift systems to<br />

spread the investment across fiscal periods.<br />

The Basic version can be fitted with a rack system at any<br />

time to save valuable bench space.<br />

Various accessories are available to make routine analysis<br />

safe and simple. They inclu<strong>de</strong> a range of test tubes, tube racks,<br />

retainer plates for washing, fume removal systems, boiling<br />

rods and catalyst tablets.<br />

Digestion system products and accessories are <strong>de</strong>scribed in<br />

more <strong>de</strong>tail on the following pages.


All Digestion Systems are based on one of the “four” Digestion Units for either 250 ml or 100 ml tubes*.<br />

* Tube volume to be specified when or<strong>de</strong>ring your digestion unit.<br />

Digestion Units<br />

The Digestion Units are insulated to minimise heat transfer to<br />

the surroundings and allow fast, even heating, thus giving good<br />

working conditions as well as saving energy. They are <strong>de</strong>signed<br />

for batches of either eight or twenty test tubes with three different<br />

levels of control.<br />

The Auto versions have an integrated all activity controller,<br />

that adapts to the actual product configuration and is programmable<br />

using the software supplied. When a Lift or Scrubber<br />

Unit is connected they are controlled by the selected application<br />

program, which is stored in the Digestion Unit memory, allowing<br />

fully unatten<strong>de</strong>d operation.<br />

The Basic versions have a built in, user <strong>de</strong>finable, time and<br />

temperature controller and display.<br />

Software for Auto Lift and Auto Rack systems<br />

There are two se<strong>para</strong>te software systems in Auto versions. The<br />

embed<strong>de</strong>d software controls all necessary functions of the digestion<br />

system on a routine basis. The PC Application software,<br />

<strong>de</strong>livered on CD, is system management software which enables<br />

<strong>de</strong>fault values to be modified according to the needs of the authorised<br />

user. To process different type of samples a wi<strong>de</strong> range<br />

of Tecator applications can be downloa<strong>de</strong>d from the database<br />

inclu<strong>de</strong>d on the CD. Up to 254 Applications can be stored in the<br />

digestion unit at any one time, of which half can be standard<br />

Tecator format and half can be user <strong>de</strong>fined. Each application<br />

can control up to 23 steps including all Temperature; ramp and<br />

time; Lift and Scrubber steps.<br />

The software supports Good Laboratory Practice (GLP)<br />

routines and accreditation procedures. Data for date, time,<br />

temperature, application used, operator, batch number, and ID<br />

number are constantly logged. The 32 most recent Data Logs<br />

can be stored in the Digestion Unit. All this information can be<br />

transferred to a PC for archiving and generation of up to seven<br />

different reports. Original Tecator Applications cannot be<br />

changed. They can be adapted and saved as different files or the<br />

user can <strong>de</strong>sign their own applications. To prevent unauthorised<br />

changes, and comply with GLP routines, the software is password<br />

protected at different authority levels.<br />

Audible alerts<br />

Audible ‘’ready’’ or ‘’cycle over’’ alerts advise the user when the<br />

digestion application is completed<br />

Audible ‘’alarm’’ alerts advise the user when errors/interruptions<br />

occur within the running application program<br />

Alerts can be adjusted High, Low or Off.<br />

Power failure or interruption of power supply<br />

In the event of power failure the digestion unit operation is automatically<br />

handled in the safest way. If the failure or interruption<br />

occurs at any time up to or during preheating, before digestion<br />

has started, the cycle will continue when power is restored. Following<br />

a power failure or interruption, after the digestion cycle<br />

has started, the unit stops heating immediately and the Lift goes<br />

to the cooling position with exhaust in place, upon restoration of<br />

power. This complies with GLP and Health & Safety routines.<br />

These interruptions will be recor<strong>de</strong>d in the data logging function.<br />

Communication with PC<br />

The PC Application software has two way communication<br />

with the Digestion Unit via the serial RS232 cable supplied as<br />

standard. Alternatively communication can be achieved through<br />

Bluetooth TDK blu2i modules, or equivalent, available from your<br />

computer supplier.<br />

Language versions<br />

The software is available in the following languages:-<br />

Chinese (simplified), Dutch, English, French, German, Italian,<br />

Japanese, Korean, Polish, Russian, Spanish, and Swedish. Other<br />

languages can be accommodated in co-operation with your local<br />

supplier.<br />

Auto Lift Systems<br />

Auto Lift systems facilitate highly automated procedures,<br />

eliminating heavy and risky handling of hot chemicals. Valuable<br />

bench space is saved, as the Tube Rack and Exhaust Manifold are<br />

positioned above the Digestion Unit.<br />

A Tube Rack with 8 or 20 tubes is placed in the Lift. The application<br />

selected then fully controls the entire process. The Exhaust<br />

Manifold docks automatically with the Tube Rack as they<br />

move down into the preheated Digestion Unit; and the Scrubber<br />

Unit, if connected, starts.<br />

The scrubber capacity is automatically adjusted during the<br />

cycle to contain fumes and minimise acid losses. When the<br />

digestion is completed the combined Tube Rack and Exhaust<br />

Manifold move to the cooling position with the Scrubber Unit<br />

still running until no further fumes are evolved. An adjustable<br />

audible signal in the Digestion Unit indicates “cycle over”.<br />

To avoid any spillage a drip tray, supplied with the Exhaust<br />

Manifold, is inserted un<strong>de</strong>rneath the Exhaust Manifold when it is<br />

se<strong>para</strong>ted from the Tube Rack after cooling.


The Lift eliminates heavy handling. The Rack System saves space.<br />

Auto Rack Systems<br />

When an Auto Rack system is used in place of an Auto Lift<br />

system the typical procedure is as with the Auto Lift system with<br />

the exception that the combining/se<strong>para</strong>ting of Tube Rack and<br />

Exhaust Manifold and the movement to the cooling position is<br />

performed manually when the signal is heard. The application<br />

selected controls all other functions as with the Auto Lift system.<br />

Basic Systems<br />

The temperature and time for the digestion are selected on the<br />

front panel. All other procedures, including operation of a connected<br />

scrubber, are then performed by the operator once the<br />

digestion unit has reached the selected temperature.<br />

Fume Removal and Containment Systems<br />

Exhaust Manifolds<br />

Many digestion applications, e.g. Kjeldahl, produce fumes that<br />

are unpleasant and corrosive. Exhaust Manifolds <strong>de</strong>signed for<br />

each Digestion Unit facilitate fume removal and containment and<br />

are strongly recommen<strong>de</strong>d for use with all digestion procedures.<br />

The cost of replacement of a fume cupboard which has been<br />

corro<strong>de</strong>d by inefficient fume handling is very much greater than<br />

the relatively low cost of an approved exhaust. Whilst many users<br />

choose to operate integrated systems in the open laboratory, we<br />

strongly recommend the use of both exhaust systems and fume<br />

cupboards for these operations. This is simply Good Laboratory<br />

Practice (GLP) and avoids conflict with local Health & Safety<br />

(H&S) requirements.<br />

The Exhaust Manifolds should be connected to the water aspirator<br />

supplied, or to a suitable Scrubber Unit.<br />

Scrubber Unit<br />

Where water is a scarce or expensive commodity, or simply when<br />

a higher level of automation is <strong>de</strong>sired, the water aspirator should<br />

be replaced with an efficient Scrubber Unit. Exhaust Manifolds<br />

and Scrubber Units which require an external water source are<br />

subject to variation in vacuum efficiency due to fluctuations in<br />

local water pressure.<br />

The compact bench top Tecator Scrubber Unit is self contained<br />

and is therefore unaffected by water supply issues. During<br />

digestion moist, acidic fumes from the connected exhaust are<br />

drawn through the Scrubber Unit. Acid vapours are first con<strong>de</strong>nsed<br />

and diluted in a large acid trap. Any residual fumes are<br />

collected, washed and neutralised before passing through a second<br />

small acid trap which protects the vacuum pump in the event<br />

that the scrubbing agents are exhausted. The cleaned air is then<br />

There is an Exhaust for each Digestion Unit.<br />

The Scrubber neutralizes the corrosive fumes.


There are Reflux Heads for 250 ml Digestion Units.<br />

Select the correct tube for your application.<br />

Kjeltabs, salt and catalyst in tablet form.<br />

vented via a tubing outlet. In the interest of GLP and H&S this<br />

venting tube should be directed into a fume cupboard. When the<br />

Scrubber Unit is connected to an Auto Lift or Auto Rack system<br />

the program will fully control the function including switching<br />

from high to low aspiration settings.<br />

Reflux Heads<br />

When a digestion unit is used for reflux chemistries, such as<br />

Chemical Oxygen Demand (COD), a Reflux Head connected to a<br />

suitable cold water supply should be used in place of the Exhaust<br />

Manifold. Tecator Reflux Heads are conveniently mounted in<br />

handling racks which match the tube rack in the Digestion Unit.<br />

The ball jointed con<strong>de</strong>nsers are <strong>de</strong>signed for use with ball jointed<br />

digestion tubes. The Reflux Heads are compatible with Auto Lift,<br />

Auto Rack and Basic systems.<br />

Digestion Tubes<br />

To suit different applications and manual/automatic handling<br />

systems, tubes for the Digestion Units are available in two sizes<br />

(250 ml and 100 ml) and three shapes. Straight si<strong>de</strong>d tubes<br />

are recommen<strong>de</strong>d for the majority of digestion applications.<br />

Volumetric tubes with a constriction at the neck are recommen<strong>de</strong>d<br />

for applications where the digestate requires dilution to<br />

a fixed volume before analyses such as FIA, SFA, and AA etc.<br />

Ball jointed tubes, available in 250 ml size only, are required for<br />

reflux chemistries using the reflux con<strong>de</strong>nser heads. The larger<br />

250 ml straight si<strong>de</strong>d tubes are recommen<strong>de</strong>d for Kjeldahl, as<br />

they can hold samples of wi<strong>de</strong>ly varying sizes. Samples of heterogeneous<br />

material often need to be fairly large to ensure that<br />

they are representative. There is no lower limit of sample size in<br />

the 250 ml tubes; they simply allow greater flexibility for most<br />

type of samples.<br />

The 100 ml straight si<strong>de</strong>d tubes can be used where the material<br />

is homogeneous and small samples are fully representative or<br />

where they are specified by the approved method.<br />

Kjeltabs<br />

A salt, to increase the boiling point, and a catalyst, to increase<br />

the speed of reaction, are used for Kjeldahl digestions. As a convenient<br />

way to obtain the correct dosage, FOSS supplies Kjeltabs<br />

– tablets containing Potassium Sulphate and a catalyst (Copper,<br />

Selenium, or Copper/Titanium). Digestion time may <strong>de</strong>pend on<br />

the catalyst used. Historically Mercury has been used as the most<br />

efficient catalyst. Today it has been replaced largely by Copper,<br />

or other metals, due to safety and environmental consi<strong>de</strong>rations.<br />

Kjeltabs are supplied in two sizes; 3.5 g and 1.5 g. One or more<br />

tablets are combined with the acid to obtain an optimal salt/acid<br />

ratio. The smaller 1.5 g size is <strong>de</strong>signed for the 100 ml tubes.


Or<strong>de</strong>ring information:*<br />

Digestion Units:<br />

All mo<strong>de</strong>ls are <strong>de</strong>livered with a Tube Rack with integrated<br />

heat shields. They should always be combined with a matching<br />

Exhaust Manifold or Reflux Head and Test Tubes – 100 or 250<br />

ml volume.<br />

For Kjeldahl digestions the 2501-001 Scrubber Unit should<br />

always be consi<strong>de</strong>red for safe and efficient neutralisation of<br />

corrosive gases. This replaces the water aspirator, supplied as<br />

standard.<br />

Auto Lift mo<strong>de</strong>ls, complete with 2515-001 Lift and integrated<br />

controller for fully automatic control of digestion applications,<br />

including the operation of the Lift and a 2501-001 Scrubber<br />

Unit (optional extra). The digestion unit can be connected to<br />

PC for application updates, traceability and logging purposes.<br />

NOTE. An appropriate exhaust manifold or reflux head<br />

MUST be ad<strong>de</strong>d for an automatic system.<br />

Auto Rack mo<strong>de</strong>ls, complete with 2515-011 Rack and<br />

integrated controller for full control of digestion applications,<br />

including the operation of a 2501-001 Scrubber (optional extra).<br />

The digestion unit can be connected to PC for application<br />

updates, traceability and logging purposes.<br />

Can be upgra<strong>de</strong>d to an Auto Lift system by addition of the<br />

2515-001 Lift.<br />

NOTE. An appropriate exhaust manifold or reflux head<br />

MUST be ad<strong>de</strong>d for an automatic system.<br />

Basic mo<strong>de</strong>ls, with built in electronics for control of temperature<br />

and time only.<br />

Can not be upgra<strong>de</strong>d to Auto mo<strong>de</strong>ls but are compatible with<br />

2515-011 Rack.<br />

Tecator Auto Digestion Units<br />

Auto mo<strong>de</strong>ls with integrated all activity controller and graphical<br />

display.<br />

Versions for 250 ml tubes<br />

2508-001 Tecator Digestion Unit 8 – Auto Lift system,<br />

250 ml tubes, 230 V 50-60 Hz<br />

2508-002 Same as above but for 110 V 50-60 Hz<br />

2508-011 Tecator Digestion Unit 8 – Auto Rack system,<br />

250 ml tubes, 230 V 50-60 Hz<br />

2508-012 Same as above but for 110 V 50-60 Hz<br />

2520-001 Tecator Digestion Unit 20 – Auto Lift system,<br />

250 ml tubes, 230 V 50-60 Hz<br />

2520-011 Tecator Digestion Unit 20 – Auto Rack system,<br />

250 ml tubes, 230 V 50-60 Hz<br />

Versions for 100 ml tubes<br />

2508-006 Tecator Digestion Unit 8 – Auto Lift system,<br />

100 ml tubes, 230 V 50-60 Hz<br />

2508-007 Same as above but for 110 V 50-60 Hz<br />

2508-016 Tecator Digestion Unit 8 – Auto Rack system,<br />

100 ml tubes, 230 V 50-60 Hz<br />

2508-017 Same as above but for 110 V 50-60 Hz<br />

2520-006 Tecator Digestion Unit 20 – Auto Lift system,<br />

100 ml tubes, 230 V 50-60 Hz<br />

2520-016 Tecator Digestion Unit 20 – Auto Rack system,<br />

100 ml tubes, 230 V 50-60 Hz<br />

Tecator Digestion Units<br />

Basic mo<strong>de</strong>ls with built in electronics for control of temperature<br />

and time.<br />

Versions for 250 ml tubes<br />

2508-051 Tecator Digestion Unit 8 – Basic, 250 ml tubes,<br />

230 V 50-60 Hz<br />

2508-052 Same as above but for 110 V 50-60 Hz<br />

2520-051 Tecator Digestion Unit 20 – Basic 250 ml tubes,<br />

230 V 50-60 Hz<br />

Versions for 100 ml tubes<br />

2508-056 Tecator Digestion Unit 8 – Basic, 100 ml tubes,<br />

230 V 50-60 Hz<br />

2508-057 Same as above but for 110 V 50-60 Hz<br />

2520-056 Tecator Digestion Unit 20 – Basic 100 ml tubes,<br />

230 V 50-60 Hz<br />

Fume Removal & Containment Systems<br />

2508-020 Exhaust Manifold for Digestion Units 2508, if 250<br />

ml tubes are used.<br />

Complete with Water Aspirator and Drip Tray.<br />

2508-021 Exhaust Manifold for Digestion Units 2508, if 100<br />

ml tubes are used.<br />

Complete with Water Aspirator and Drip Tray.<br />

2520-020 Exhaust Manifold for Digestion Units 2520, if 250<br />

ml tubes are used.<br />

Complete with Water Aspirator and Drip Tray.<br />

2520-021 Exhaust Manifold for Digestion Units 2520, if 100<br />

ml tubes are used.<br />

Complete with Water Aspirator and Drip Tray.<br />

2501-001 Scrubber Unit 110/230 V 50-60 Hz.<br />

For neutralization of fumes in acid digestions. It<br />

can be combined with any of the Exhaust Manifolds.<br />

Up to 100 samples without changing of<br />

reagent. Fully automatic operation when connected<br />

to an Auto Digestion Unit.<br />

Lift & Rack Systems<br />

2515-001 LIFT for the AUTO version of Digestion Unit<br />

2508 and 2520.<br />

The Application run in the Digestion Unit fully<br />

controls the LIFT.<br />

The Lift can only be connected to Auto version<br />

Digestion Unit.<br />

2515-011 RACK System for all versions of Digestion Unit<br />

2508 and 2520 without LIFT.<br />

Enables manual positioning of components in a<br />

similar way as the Auto Lift.<br />

Reflux con<strong>de</strong>nsers<br />

2508-030 Reflux Head COD Digestion Unit 2508.<br />

Water-cooled Con<strong>de</strong>nsers for 8x250 ml tubes.<br />

2520-030 Reflux Head COD Digestion Unit 2520.<br />

Water-cooled Con<strong>de</strong>nsers for 20x250 ml tubes.<br />

10000254 Reflux Con<strong>de</strong>nser, Air Cooled.<br />

700 mm. With ground joint for 250 ml tubes.


Cont. Or<strong>de</strong>ring information:*<br />

Handling Systems<br />

Digestion Units are <strong>de</strong>livered complete with one Tube Rack.<br />

It may be found convenient to or<strong>de</strong>r extra so that all tubes<br />

normally in use in the laboratory are placed in a rack.<br />

All Tube Racks fit the Kjeltec 2460 Sampler.<br />

10014245 Tube Rack for 8 Digestion Tubes 250 ml.<br />

10014248 Tube Rack for 8 Digestion Tubes 100 ml.<br />

10014240 Tube Rack for 20 Digestion Tubes 250 ml.<br />

10014246 Tube Rack for 20 Digestion Tubes 100 ml.<br />

10014006 Retainer Plate for Washing; Digestor 2520, 250 ml<br />

Tubes.<br />

10014007 Retainer Plate for Washing; Digestor 2520, 100 ml<br />

Tubes.<br />

10000460 Boiling Rod<br />

To avoid bumping when digesting large volumes of water.<br />

10000897 Handling Device for Digestion Tube<br />

10007117 Dispenser 2-10 ml, 1000 ml Bottle<br />

10007118 Dispenser 10-30 ml, 2000 ml Bottle<br />

Test tubes<br />

Straight mo<strong>de</strong>l Test Tubes, often used for Kjeldahl <strong>de</strong>termination.<br />

10014311 Digestion Tubes Straight 100 ml 8/pkg<br />

10014312 Digestion Tubes Straight 100 ml 20/pkg<br />

10014278 Digestion Tubes Straight 250 ml 8/pkg<br />

10000158 Digestion Tubes Straight 250 ml 20/pkg<br />

With constriction and volume mark, used in applications where<br />

the digest is diluted to volume and an aliquot is taken for<br />

analysis.<br />

10014313 Digestion Tubes With Mark 100 ml 8/pkg<br />

10014314 Digestion Tubes With Mark 100 ml 20/pkg<br />

10014315 Digestion Tubes With Mark 250 ml 8/pkg<br />

10000157 Digestion Tubes With Mark 250 ml 20/pkg<br />

With ground joint for air-cooled Reflux Con<strong>de</strong>nsers.<br />

10014316 Digestion Tubes - Ground Joint 250 ml 8/pkg<br />

10000159 Digestion Tubes - Ground Joint 250 ml 20/pkg<br />

With ball joint for water-cooled Reflux Con<strong>de</strong>nsers.<br />

10014317 Digestion Tubes - Ball Joint 250 ml 8/pkg<br />

10000611 Digestion Tubes - Ball Joint 250 ml 20/pkg<br />

Kjeltabs:<br />

Most types are <strong>de</strong>livered in boxes of 1000.<br />

15270001 Selenium, Tablets with 1.5 g K 2 SO 4 + 7.5 mg Se.<br />

15270002 Selenium, Tablets with 5 g K 2 SO 4 + 5 mg Se.<br />

15270003 Selenium, Tablets with 3.5 g K 2 SO 4 + 3.5 mg Se.<br />

15270056 Selenium, Tablets with 1 g Na 2 SO 4 + 0.05 g Se.<br />

15270010 Copper/Titanium, Tablets with 5 g K 2 SO 4 + 0.15 g<br />

CuSO 4 .5H 2 O + 0.15 g TiO 2 .<br />

15270020 Copper/Titanium, Tablets with 3.5 g K 2 SO 4 +<br />

0.105 g CuSO 4 .5H 2 O + 0.105 g TiO 2 .<br />

15270018 Copper, Tablets with 3.5 g K 2 SO 4 + 0.4 g<br />

CuSO 4 .5H 2 O.<br />

15270034 Copper, Tablets with 1.5 g K 2 SO 4 + 0.15 g<br />

CuSO 4 .5H 2 O.<br />

15270057 Copper, Tablets with 4.5 g K 2 SO 4 + 0.5 g<br />

CuSO 4 .5H 2 O.<br />

Other types are available upon request


Installation requirements:<br />

Digestion Unit 2508 Auto<br />

Power Supply: 200 - 240 V or 100 - 115 V,<br />

50 - 60 Hz<br />

Power consumption: 1100 W<br />

Water supply: See Exhaust Manifolds. If<br />

Scrubber connected - None<br />

Weight: 10 kg<br />

Dimensions, W × D × H: 300 × 500 × 697 mm (incl. Rack<br />

system)<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Exhaust system and Fume hood<br />

Recommen<strong>de</strong>d bench space: 1 m, or 0.4 m if a Lift or Racking<br />

System is used<br />

Digestion Unit 2508 Basic<br />

Power Supply: 200 - 240 V or 100 - 115 V,<br />

50 - 60 Hz<br />

Power consumption: 1100 W<br />

Water supply: See Exhaust Manifolds. If<br />

Scrubber connected - None<br />

Weight: 10 kg<br />

Dimensions, W × D × H: 300 × 390 × 140 mm<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Exhaust system and Fume hood<br />

Recommen<strong>de</strong>d bench space: 1 m, or 0.4 m if a Racking System<br />

is used<br />

Digestion Unit 2520 Auto<br />

Power Supply: 200 - 240 V, 50 - 60 Hz<br />

Power consumption: 2300 W<br />

Water supply: See Exhaust Manifolds. If<br />

Scrubber connected - None<br />

Weight: 18 kg<br />

Dimensions, W × D × H: 300 × 660 × 697 mm (incl. Rack<br />

system)<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Exhaust system and Fume hood<br />

Recommen<strong>de</strong>d bench space: 1 m, or 0.4 m if a Lift or Rack<br />

System is used<br />

Digestion Unit 2520 Basic<br />

Power Supply: 200 - 240 V, 50 - 60 Hz<br />

Power consumption: 2300 W<br />

Water supply: See Exhaust Manifolds. If<br />

Scrubber connected - None<br />

Weight: 18 kg<br />

Dimensions, W × D × H: 300 × 550 × 140 mm<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Exhaust system and Fume hood<br />

Recommen<strong>de</strong>d bench space: 1 m, or 0.4 m if a Rack System is<br />

used<br />

Scrubber<br />

Power Supply: 100 to 240 V, 50 - 60 Hz, Self<br />

selecting<br />

Power consumption: 50 W<br />

Water supply: No<br />

Weight: 19 kg<br />

Dimensions, W × D × H: 335 × 485 × 395 mm<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Outlet tubing preferably into sink<br />

in fume hood<br />

Recommen<strong>de</strong>d bench space: 0.6 m<br />

Exhaust 2508<br />

Water supply: 3 - 5 l/min for 5 minutes, then<br />

1 l/min<br />

Exhaust 2520<br />

Water supply: 10 - 12 l/min for 5 minutes, then<br />

3 - 5 l/min<br />

Lift<br />

Power Supply: None. Powered from the Digestion<br />

Unit Auto<br />

Power consumption: 10 W<br />

Weight: 7 kg<br />

Dimensions, W × D × H: 300 × 550 × 697 mm (Mounted<br />

on Digestion Unit)<br />

Ambient temperature: max 40�C<br />

Ventilation requirement: No<br />

Recommen<strong>de</strong>d bench space: 0 m. Lift is mounted on the<br />

Digestion Unit


Performance data:<br />

2508 Auto 2508 Basic 2520 Auto 2520 Basic<br />

Temperature range Ambient - 440°C 100 - 440°C Ambient - 440°C 100 - 440°C<br />

Temperature setting<br />

repeatability<br />

1°C 1°C 1°C 1°C<br />

Temperature readout Digital Digital Digital Digital<br />

Heater indication LED LED LED LED<br />

Heater warning Text in display Text in display Text in display Text in display<br />

Over temperature<br />

protection<br />

Yes Yes Yes Yes<br />

Temperature stability at<br />

100°C<br />

± 2°C ± 5°C ± 2°C ± 5°C<br />

Temperature stability at<br />

400°C<br />

± 1°C ± 2°C ± 1°C ± 2°C<br />

Heating time 20 to<br />

400°C at 230 V<br />

~35 min ~35 min ~40 min ~40 min<br />

Time setting per step 1 - 999 min 1 - 1199 min 1 - 999 min 1 - 1199 min<br />

Ramp control (Rate of<br />

heating)<br />

Yes No Yes No<br />

Digestion applications<br />

memory<br />

Up to 254 No Up to 254 No<br />

Digestion steps per<br />

application<br />

Up to 23 1, Manual control Up to 23 1, Manual control<br />

Lift connection Yes, full control No Yes, full control No<br />

Scrubber Yes, full control Yes, man control Yes, full control Yes, man control<br />

Tubes / batch<br />

Typical sample capacity<br />

8 8 20 20<br />

Tube size 250 ml 250 ml 250 ml 250 ml<br />

Sample size* solids up to 5 g up to 5 g up to 5 g up to 5 g<br />

Sample size* liquids up to 15 ml up to 15 ml up to 15 ml up to 15 ml<br />

Tube size 100 ml 100 ml 100 ml 100 ml<br />

Sample size* solids up to 1 g up to 1 g up to 1 g up to 1 g<br />

Sample size* liquids up to 3 ml up to 3 ml up to 3 ml up to 3 ml<br />

*Note: Larger samples require special procedures. Please see the relevant Application Notes or consult our Customer Service Laboratory.<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

P/N 9999 0720E, Issue 2 GB, August 2005


Analizador FIAstar ® 5000. ”Conectar y Analizar”, la máxima sencillez en <strong>análisis</strong> <strong>químicos</strong> por vía húmeda.<br />

Características y Beneficios<br />

• Beneficioso inclusive con lotes pequeños <strong>de</strong><br />

muestras, <strong>de</strong>bido a:<br />

- Puesta en marcha y apagado rápido (10 min.).<br />

- Resultados inmediatos (menos <strong>de</strong> 1 min.).<br />

• Casetes <strong>de</strong> Método ”Conectar y Analizar” rápido<br />

y sencillo.<br />

• Software Windows ® 98/2000 incluyendo rutinas<br />

<strong>de</strong> calibración según ISO 8466.<br />

• Detector Digital <strong>de</strong> Doble Longitud <strong>de</strong> Onda<br />

(DDW) <strong>para</strong> eliminar los efectos <strong>de</strong>l índice <strong>de</strong> refracción<br />

y <strong>de</strong> las burbujas <strong>de</strong> aire.<br />

• Rango dinámico amplio y bajos límites <strong>de</strong> <strong>de</strong>tección.<br />

• Función <strong>de</strong> stand-by (


Información <strong>de</strong> Pedidos*:<br />

5000-001 Módulo Analizador FIAstar 5000 (26 V DC), unidad<br />

<strong>de</strong> <strong>análisis</strong> con válvula <strong>de</strong> inyección, bomba, soporte <strong>de</strong><br />

casete, termostato incorporado, <strong>de</strong>tector DDW, conexión<br />

USB y adaptador <strong>de</strong> voltaje (100-240 V, 50-60<br />

Hz).<br />

5000-010 Casete <strong>de</strong> Método Nitrato/Nitrito y Nitrógeno Total,<br />

con filtros, tubos <strong>de</strong> la bomba, columnas <strong>de</strong> reducción,<br />

botellas <strong>para</strong> reactivo / enjuague y soporte <strong>de</strong> casete.<br />

5000-020 Casete <strong>de</strong> Método Amonio, con filtros, tubos <strong>de</strong> la<br />

bomba, membranas <strong>de</strong> difusión <strong>de</strong> gas, mezcla indicadora,<br />

botellas <strong>para</strong> reactivo / enjuague y soporte <strong>de</strong> casete.<br />

5000-030 Casete <strong>de</strong> Método Fosfato/Fósforo Total, con filtros,<br />

tubos <strong>de</strong> la bomba, botellas <strong>para</strong> reactivo / enjuague y<br />

soporte <strong>de</strong> casete.<br />

5000-040 Casete <strong>de</strong> Método TKN (Nitrógeno Kjeldahl Total),<br />

con filtros, tubos <strong>de</strong> la bomba, membranas <strong>de</strong> difusión<br />

<strong>de</strong> gas, mezcla indicadora, botellas <strong>de</strong> reactivo / enjuague<br />

y porta casete.<br />

5000-100 Programa SoFIA <strong>para</strong> FIAstar 5000 en entorno<br />

Windows ®<br />

5027-003 Muestreador 5027 <strong>para</strong> FIAstar con ban<strong>de</strong>ja <strong>para</strong> 120<br />

muestras, vasos <strong>de</strong> 12 mL y ban<strong>de</strong>ja se<strong>para</strong>da <strong>para</strong> patrones<br />

<strong>de</strong> calibración y <strong>de</strong> QC.<br />

5027-004 Í<strong>de</strong>m, pero con ban<strong>de</strong>ja <strong>para</strong> 64 muestras, 30 mL<br />

Datos <strong>de</strong> Operación:<br />

Analizador FIAstar ® 5000<br />

Principio <strong>de</strong> operación: Análisis por Inyección en Flujo (FIA)<br />

Inyector: Inyector rotatorio <strong>de</strong> 6 vías, volumen variable<br />

Volumen <strong>de</strong> muestras: 20 - 400 µl<br />

Bomba: Bomba peristáltica <strong>de</strong> 2 ´ 4 canales con<br />

velocidad variable y función <strong>de</strong> alerta<br />

Termostato: Termostato incorporado, 30°C - 90°C ±<br />

1°C<br />

Casete <strong>de</strong> Método: Consumo <strong>de</strong> reactivos 0.3 - 2 mL/<br />

muestra<br />

Detector: Fotómetro Digital <strong>de</strong> Doble Longitud <strong>de</strong><br />

Onda con corrección automática <strong>de</strong> fondo<br />

Celda <strong>de</strong> Flujo: Paso 10 mm; volumen 18 µL<br />

Rango <strong>de</strong> Longitud <strong>de</strong> 400 - 1,000nm<br />

Onda:<br />

Intervalo <strong>de</strong> Absorbancia: 0 - 2.5 UA<br />

Requerimientos <strong>de</strong> Instalación<br />

Analizador FIAstar ® 5000<br />

Suministro eléctrico: 100 - 240 V CA, 50-60 Hz (26 V CC)<br />

Dimensiones: 450 ´ 310 ´ 145 mm<br />

(con soporte <strong>de</strong> reactivos 625 ´ 310 ´<br />

145)<br />

Peso: 8,7 kg<br />

Consumo <strong>de</strong> energía: 70 vatios<br />

Conexión a PC: USB (Universal Serial Bus)<br />

Especificaciones <strong>de</strong>l PC:<br />

Or<strong>de</strong>nador en entorno Windows ® 98 o 2000 instalado<br />

Mínimo 32 Mb <strong>de</strong> memoria RAM<br />

*Información <strong>de</strong> pedidos: Utilice los Números <strong>de</strong> Catálogo y texto correspondiente <strong>de</strong>tallados arriba.<br />

Foss Tecator AB<br />

Box 70, SE-263 21 Höganäs, Suecia<br />

Tel: +46 42 36 15 00<br />

Fax: +46 42 34 03 49<br />

e-mail info@foss.tecator.se<br />

Página web: www.foss.dk<br />

Representantes en 100 países<br />

Sistemas completos<br />

Analizador FIAstar 5000 <strong>para</strong> Nitritos / Nitratos, con 1 Módulo<br />

Analizador FIAstar 5000, 1 software SoFIA, 1 casete NO 2 / NO 3 ,<br />

1 Muestreador 5027 (120 posiciones).<br />

Analizador FIAstar 5000 <strong>de</strong> Dos Canales <strong>para</strong> Nitrógeno en Suelos,<br />

con 2 Módulos Analizadores FIAstar 5000, 1 software SoFIA, 1<br />

hub USB, 1 casete NO 2 /NO 3 , 1 casete NH4 y 1 Muestreador 5027<br />

(120 posiciones).<br />

5000-700 Sistema FIAstar 5000 <strong>de</strong> Tres Canales <strong>para</strong> Análisis<br />

<strong>de</strong> Agua, con 3 módulos Analizadores FIAstar 5000,<br />

1 software SoFIA, 1 hub USB, 1 casete NO2 / NO 3,<br />

1 casete NH 4, 1 casete P y 1 muestreador 5027 (120<br />

posiciones).<br />

Accesorios y consumibles<br />

50003139 Columnas <strong>de</strong> Cadmio pre-empaquetadas, caja <strong>de</strong> 3 unida<strong>de</strong>s<br />

50000295 Mezcla indicadora <strong>para</strong> Amonio<br />

50002875 Membranas <strong>de</strong> Difusión <strong>de</strong> Gases <strong>para</strong> Amonio<br />

10004593 Membranas <strong>de</strong> Difusión <strong>de</strong> Gases <strong>para</strong> TKN<br />

5000-050 Casete <strong>de</strong> Método en blanco <strong>para</strong> otras aplicaciones,<br />

con tubos <strong>de</strong> la bomba y conjunto <strong>de</strong> bucles <strong>de</strong> mezcla.<br />

Los filtros <strong>de</strong>ben ser pedidos se<strong>para</strong>damente<br />

Resolución: 0.001 mUA<br />

Reproducibilidad: Mejor que 1% r.s.d.<br />

Software SoFIA<br />

Puntos <strong>de</strong> Calibración: Hasta 10 patrones<br />

Ajuste <strong>de</strong> curva <strong>de</strong><br />

calibración: Lineal o segundo or<strong>de</strong>n ISO 8466<br />

Rutinas QC y GLP: Verificación <strong>de</strong> muestras; <strong>análisis</strong> estándar<br />

y muestras múltiples; recalibración<br />

automática; alarmas <strong>de</strong> falta <strong>de</strong> reactivo,<br />

falta <strong>de</strong> muestras y fuera <strong>de</strong> rango<br />

Métodos pre-<strong>de</strong>finidos<br />

Muestreador 5027<br />

Principio <strong>de</strong> operación: Circular<br />

Ban<strong>de</strong>jas <strong>de</strong> muestras: Para 64 o 120 muestras<br />

División <strong>de</strong> la ban<strong>de</strong>ja: 4 gradillas individuales<br />

Tamaño <strong>de</strong> muestra: 12, 30 mL<br />

Ban<strong>de</strong>ja lateral: 10 posiciones <strong>para</strong> patrones y QC<br />

Espacio disponible en disco duro 40 MB<br />

Disquetera <strong>de</strong> 1.44 Mb o lector <strong>de</strong> CD<br />

Una puerta USB <strong>para</strong> cada módulo FIA conectado<br />

Una puerta RS 232 <strong>para</strong> comunicación con el muestreador 5027<br />

Puerta RS 232 adicional <strong>para</strong> transferencia <strong>de</strong> datos a un sistema<br />

LIMS<br />

Muestreador 5027<br />

Suministro eléctrico: 100/115/130/200/240 V, 50-60 Hz<br />

Dimensiones: 450 ´ 400 ´ 260 mm<br />

(con ban<strong>de</strong>ja se<strong>para</strong>da 625 ´ 400 ´ 260)<br />

Peso: 14 kg<br />

Consumo <strong>de</strong> energía: 20 vatios<br />

In the interest of product <strong>de</strong>velopment we reserve the right to alter specifications without prior notice.<br />

Part no 9999 0912ES / 0006 DOT Graphic AB, Malmö, Swe<strong>de</strong>n


A modular system for simple analysis of cru<strong>de</strong> and <strong>de</strong>tergent fiber.<br />

Features and benefits<br />

• 18 & 6 position systems for cru<strong>de</strong> fibre, NDF,<br />

ADF & ADL<br />

• Results in agreement with official procedures<br />

• Low investment cost giving unique performance/<br />

price ratio<br />

• FiberCap capsule <strong>de</strong>sign ensures accurate<br />

analysis and superior precision<br />

• Batch handling with no sample transfer<br />

• Rapid filtration for all sample types saves time<br />

• Multiple systems are easily operated for high<br />

throughput<br />

• Small bench space nee<strong>de</strong>d<br />

Description<br />

The FiberCap system is specifically <strong>de</strong>signed to<br />

provi<strong>de</strong> a low cost, high capacity solution for fibre<br />

<strong>de</strong>termination in accordance with the Ween<strong>de</strong> and<br />

van Soest methods. Batch handling, with no sample<br />

transfer, is used throughout the procedure. Defatting,<br />

boiling, rinsing and filtration are performed<br />

un<strong>de</strong>r reproducible and controlled conditions.<br />

Dedicated Analytical Solutions<br />

FiberCap 2021/2023<br />

Fibre Analysis System<br />

The system offers substantial savings both in<br />

manual handling and time as well as improved analytical<br />

precision compared to manual methods.<br />

The capsule is a polypropylene container with a<br />

simple snap on lid, once sealed, there is no sample<br />

transfer. The different chemical properties of the<br />

membranes used in the capsule and the lid ensure<br />

free flow of reagent through the FiberCap during<br />

analysis. This feature guarantees repeatable conditions<br />

for all sample types, even high starch samples<br />

can easily be <strong>de</strong>termined. Filtration or washing is<br />

done in seconds for all sample types.<br />

Two versions of capsules are available, having<br />

different mesh size, offers the possibility to match<br />

results either with the filter paper method (white<br />

capsule) or the crucible method (green capsule).<br />

The FiberCap is available in either 18 or 6 position<br />

systems and one operator can easily handle<br />

several systems simultaneously giving a very high<br />

throughput. For example, 4 batches with the 18 position<br />

system give 72 finished extractions in 1,5 h.


FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Weighing De-fatting Batch transfer Extraction<br />

System <strong>de</strong>scription<br />

2021 0001 FiberCap 2021 (6 position) 230 V, 50 Hz.<br />

Including all accessories necessary for analysis<br />

whereof 100 pcs of capsules (white)<br />

2021 0004 FiberCap 2021, 115 V, 50-60 Hz. As above.<br />

2021 0011 FiberCap 2021 230 V, 50 Hz. Including all<br />

accessories necessary for analysis whereof<br />

100 pcs of capsules (green)<br />

2021 0014 FiberCap 2021, 115 V, 50-60 Hz. As above.<br />

2023 0001 FiberCap 2023 (18 position) 230 V, 50 Hz.<br />

Including all accessories necessary for analysis<br />

whereof 100 pcs of capsules (white)<br />

2023 0003 FiberCap 2023, 115 V, 50-60 Hz. As above.<br />

2023 0011 FiberCap 2023 230 V, 50 Hz. Including all<br />

accessories necessary for analysis whereof<br />

100 pcs of capsules (green)<br />

2023 0013 FiberCap 2023, 115 V, 50-60 Hz. As above.<br />

Performance data:<br />

Sample size: 0,5 - 3 g<br />

Measuring range: 0,1 - 100 %<br />

Capacity per batch: 6 samples or 18 samples simultane-<br />

ously<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

Accessories:<br />

1524 0010 2022 Hot Plate 230 V, 50 Hz<br />

1524 0011 2022 Hot Plate 115 V, 50 - 60 Hz<br />

1001 0332 Boiling Stand<br />

1001 0224 Capsule Tray, 6 position<br />

1001 0334 Capsule Tray, 18 position<br />

1001 0137 Extraction Beaker, 6 position<br />

1001 0546 Extraction Beaker, 18 position<br />

1001 0331 Drying Stand<br />

1001 0347 FiberCap capsules, 100 pcs<br />

1001 0346 FiberCap capsules, 500 pcs<br />

1001 0262 Stopper, 6 position<br />

1001 0335 Stopper, 18 position<br />

� � � � � � � �<br />

Capacity per day: Up to 216 analyses (Cru<strong>de</strong> fibre)<br />

(6 batches) using six Fibertec 2021 Systems in<br />

<strong>para</strong>llell, 108 analyses (Cru<strong>de</strong> fibre)<br />

using one Fibertec 2023.<br />

Repeatability: ± 1 % relative at 5 - 30 % fibre level<br />

Installation requirements:<br />

Equipment Power supply Power consumption Dimensions Weight Water supply<br />

w × d × h<br />

2022 Hot Plate 230 V, 50 Hz 500 W 20 × 30 × 35 cm 2,5 kg 0,4 l/min<br />

115 V, 50 - 60 Hz<br />

Furnace Note; the furnace used during the analysis must be well ventilated, due to the build up of smoke.<br />

Applications:<br />

• Cru<strong>de</strong> Fibre • NDF (Neutral Detergent Fibre) • ADF (Acid Detergent Fibre) & ADL (Acid Detergent Lignin)<br />

The Fibertec 2021 and 2023 System are also suitable for use with almost any chemical.<br />

Materials used are glass, PTFE; PEEK, PP, PET & PA.<br />

P/N 9999 0407, Issue 2 GB, Nov 2007


Extraction System for simple <strong>de</strong>termination of Cru<strong>de</strong> Fibre, Detergent Fibre, Cellulose,<br />

Hemicelluloses, Lignin and related Parameters in plant materials, compound feed, food, etc.<br />

Benefits<br />

•<br />

•<br />

•<br />

•<br />

•<br />

•<br />

•<br />

•<br />

•<br />

Six samples processed simultaneously.<br />

Accessories for batch handling.<br />

Integral extraction and filtration.<br />

No sample transfer and no loss of sample.<br />

Se<strong>para</strong>te unit for solvent <strong>de</strong>hydration, lignin <strong>de</strong>termination<br />

and <strong>de</strong>fatting.<br />

Extensive application service.<br />

High reproducibility of conditions and results.<br />

Saves time, energy and laboratory space.<br />

Official approval: ISO 6865, 92/89 EEC and<br />

AOAC 2002.04 (feed).<br />

Description<br />

The Fibertec System M6 is <strong>de</strong>dicated for fibre<br />

<strong>de</strong>terminations according to Ween<strong>de</strong>, van Soest,<br />

etc. Single or sequential extractions including boiling,<br />

using externally preheated reagents, rinsing<br />

and filtration are performed un<strong>de</strong>r reproducible and<br />

controlled conditions.<br />

Dedicated Analytical Solutions<br />

Fibertec M6<br />

Fibre Analysis System<br />

The basic modules of a Fibertec M6 are:<br />

• 1020 Hot Extraction Unit, for hot hydrolysis and<br />

extraction with built-in systems for heating and<br />

filtration<br />

• 1021 Cold Extraction Unit, for <strong>de</strong>fatting samples,<br />

extraction at ambient temperature e.g. lignin <strong>de</strong>termination,<br />

and for solvent <strong>de</strong>hydration of fibre<br />

residues.<br />

Both units are adapted to the same crucible<br />

system that permits the sample, whenever required,<br />

to be dried and weighed between extractions. In<br />

the system the samples are handled in specially<br />

<strong>de</strong>signed filter crucibles, which are used both as an<br />

integral part of an extraction assembly during extraction,<br />

rinsing and filtering, and as a sample vessel<br />

during the weighing, drying and ashing steps.<br />

The Fibertec M6 permits handling of six samples<br />

at a time by the use of accessory tools for batch<br />

handling. Filtration problems are overcome by the<br />

unique vacuum/reverse air flow system.<br />

The Fibertec M6 offers a most time saving and<br />

convenient solution for more reproducible fibre<br />

<strong>de</strong>terminations.


System <strong>de</strong>scription:<br />

Fibertec M6 (200-230V):<br />

• Hot Extraction Unit comprising: Hot Extractor, Reflector,<br />

Reagent Bottles, Hot Water Sprayer, Beaker, Funnel, Water<br />

Suction Pump, Antifoaming Agent, Tubing, Hol<strong>de</strong>r for 6<br />

crucibles, Stand for 6 crucibles, Crucibles (P2 standard, 2<br />

sets of 6), Manual.<br />

• Cold Extraction Unit comprising: Cold Extractor, Spray<br />

Bottle, Tubing, T-tube, Spare Part Kit, Stand for 6 crucibles,<br />

Crucibles (P2 standard 40 - 100 µm, set of 6),<br />

Antifoaming Agent (octanol), Celite, 1 l<br />

Performance data:<br />

Sample size: 0.5 - 3 g (1 g normal)<br />

Measuring range: 0.1 - 100%<br />

Repeatability: < 1% relative at 5 - 30 % fibre level<br />

Accuracy: According to official methods<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Also choose from the following accessories:<br />

1093 Cyclotec Sample Mill, cyclone mill<br />

1090 Cemotec Sample Mill, moisture mill<br />

2094 Homogenizer, blen<strong>de</strong>r type<br />

2096 Homogenizer, blen<strong>de</strong>r type<br />

1095 Knifetec, water cooled sample mill<br />

Hot plate 2022<br />

Filter Crucibles:<br />

Crucible, P1 (100 - 160 µm), set of 6<br />

Crucible, P2 (40 - 100 µm), set of 6, standard<br />

Crucible, P3 (16 - 40 µm), set of 6<br />

Crucible, P0 (160 - 250 µm), set of 6<br />

Crucible P2 US, (40 - 60 µm) set of 6<br />

Capacity per batch: 6 samples simultaneously<br />

Capacity per day: Up to 36 analyses (Cru<strong>de</strong> Fibre<br />

method acc. to Ween<strong>de</strong>) per day<br />

Installation requirements:<br />

Equipment Power supply Power Dimensions Weight Water supply<br />

consumption w × d × h<br />

1020 Hot Extraction Unit 200 - 230V ± 10% 1 000 kW 56 × 38 × 57 28 kg Tap water for<br />

50 - 60 Hz con<strong>de</strong>nsors (appr. 2 l/min)<br />

and water aspirator (during<br />

filtration)<br />

1021 Cold Extraction Unit - - 56 × 38 × 28 4 kg Tap water for water aspira<br />

tor (during filtration)<br />

Applications:<br />

• Cru<strong>de</strong> Fibre (acc. to Ween<strong>de</strong>). • Neutral Detergent Fibre.<br />

• Acid Detergent Fibre. • Acid Detergent Lignin.<br />

In addition, most other chemical extraction methods except methods including acetic acid, trichloracetic acid and/or nitric acid,<br />

may be employed. For specific method information, please ask for <strong>de</strong>tailed FOSS Analytical Application Notes.<br />

Fibertec Systems for any fibre <strong>de</strong>termination needs:<br />

Low fat samples<br />

1093 Cyclotec Mill<br />

Medium fat samples<br />

1090 Cemotec Mill<br />

High fat samples<br />

2094/2096 Homogenizer<br />

1095 Knifetec<br />

Balance<br />

Method<br />

Enzymatic<br />

Chemical<br />

Fibertec E<br />

High workloads<br />

Fibertec 2010<br />

Medium workloads<br />

Fibertec M6<br />

Drying Oven Balance Muffle furnance<br />

Balance<br />

P/N 9999 0401E, Issue 1 GB, Dec 2004


Semi-automated incubation and se<strong>para</strong>tion system for quantitative <strong>de</strong>termination of<br />

dietary fibre in processed food, cereal products, fruits and vegetables, health food,<br />

feedstuffs, plant materials, etc.<br />

Benefits<br />

• Free choice of methods like AOAC, AACC,<br />

NMKL and Asp.<br />

• Determines total, soluble and insoluble dietary<br />

fibre.<br />

• Rapid filtration of six samples simultaneously.<br />

• Specially <strong>de</strong>signed incubation flasks<br />

• High incubation and se<strong>para</strong>tion capacity.<br />

• Repeatable readings, S.D. < 0.5% absolute.<br />

• Easy and convenient to use.<br />

• Saves time, space and manual work.<br />

Description<br />

The Fibertec E is <strong>de</strong>signed for rapid and rational<br />

<strong>de</strong>termination of dietary fibre according to established<br />

enzymatic methods, including those approved<br />

by AOAC, AACC, NMKL and Asp.<br />

The Fibertec E <strong>de</strong>termines total dietary fibre as<br />

well as the insoluble and soluble fibres se<strong>para</strong>tely.<br />

It is also useful in sample pre<strong>para</strong>tion for <strong>de</strong>tailed<br />

studies of fibre fractions, e.g. by chromatographic<br />

or colorimetric techniques.<br />

Dedicated Analytical Solutions<br />

Fibertec E<br />

Dietary Fibre Analysis System<br />

The basic Fibertec E inclu<strong>de</strong>s a Shaking Water<br />

Bath and a Filtration Module. The Shaking Water<br />

Bath incubates 12 samples in each batch. The<br />

temperature range is from ambient to 80°C and it is<br />

possible to preset three temperatures. The shaking<br />

frequency and amplitu<strong>de</strong> are continously adjustable.<br />

The Filtration Module filters and collects 6<br />

sample solutions batchwise and inclu<strong>de</strong>s a system<br />

for rapid <strong>de</strong>hydration. The filtration step is spee<strong>de</strong>d<br />

up through built-in “Pressure Mo<strong>de</strong>”. Reversed<br />

pressure is applied to facilitate filtration by breaking<br />

up clogged filter residues during filtration.<br />

Filtration time varies according to sample type, but<br />

on average it is 2-4 minutes for 100 ml of digested<br />

solution.<br />

The reproducibility (standard <strong>de</strong>viation) of the<br />

Fibertec E in <strong>de</strong>termining total, insoluble and<br />

soluble dietary fibre is < 0.5% absolute.


System <strong>de</strong>scription:<br />

Fibertec E<br />

• Filtration Module complete, comprising: Filtration Module,<br />

Incubation Flasks (4 sets of 6), Standard Crucibles<br />

(P2, 2 sets of 6), Basket for Incubation Flasks, 2 Stands for<br />

Crucibles, 2 Spray bottles, 2 Water aspiration pumps, Filter<br />

aid, Tubing, Shaking Water Bath, complete, comprising: a<br />

tray for 12 Incubation Flasks and a hinged inclined lid.<br />

In addition, we recommend:<br />

Incubation Flask (set of 6), at least 4 sets<br />

Crucible, P2 (40 - 100 µm) set of 6, at least 2 sets<br />

Basket for 12 Incubation Flasks, at least 1<br />

Total Dietary Fibre Kit for 200 <strong>de</strong>terminations<br />

Termamyl 300 L, 100 ml Boiling Water Bath Pipette 100 µl<br />

Muffle or incineratron furnace ~525°C<br />

Performance data:<br />

Filtration Module:<br />

Filtration and <strong>de</strong>-<br />

hydration capacity: 6 samples/batch<br />

Filtration rate: 2-4 ml/100 ml of digested solution,<br />

<strong>de</strong>pending on sample type<br />

Repeatability: S.D. < 0.5% absolute<br />

Flask volume: 600 ml<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Shaking Water Bath:<br />

Capacity: 12 flasks/batch<br />

Temperature range: ambient to 80°C<br />

Temperature accuracy: ± 0.1°C<br />

Shaking frequency: 0-150 strokes/minute<br />

Stroke length: 0-50 mm<br />

Installation requirements:<br />

Equipment Power supply Power consumption Dimensions Weight, kg<br />

w × d × h<br />

1023 Filtration Module 100-120 V, 50-60 Hz 8 770 × 280 × 500 24<br />

210-230 V, 50-60 Hz<br />

1024 Shaking Water Bath 100-120 V, 50-60 Hz 1500 890 × 370 × 320 24<br />

210-230 V, 50-60 Hz<br />

A comple analytical scheme for dietary fibre <strong>de</strong>termination consists of:<br />

Samples with a low<br />

fat content<br />

1093 Cyclotec Mill<br />

1090 Cemotec Mill<br />

Samples with a high<br />

fat content<br />

2094 Homogenizers<br />

1095 Knifetec<br />

Balance<br />

Water Bath<br />

Boiling<br />

Shaking Water<br />

Bath 1024<br />

Accessories:<br />

Alternative filter crucibles:<br />

Crucible, P0 (160 - 250 µm), set of 6<br />

Crucible, P1 (90 - 150 µm), set of 6<br />

Crucible, P3 (15 - 40 µm), set of 6<br />

Stand for 6 Crucibles<br />

1093 Cyclotec Sample Mill<br />

1090 Cemotec Sample Mill<br />

1095 Knifetec Sample Mill for high fat, high fibre samples<br />

For protein <strong>de</strong>termination we recommend our Kjeltec analyzers.<br />

Alternative flask trays for other applications, e.g. biochemical<br />

work:<br />

Tray for E**-flasks, 50 ml<br />

Tray for E**-flasks, 100 ml<br />

Tray for E**-flasks, 250 ml<br />

Tray for E**-flasks, 500 ml<br />

** Erlenmeyer<br />

Filtration Module<br />

1023<br />

Drying Oven Balance<br />

Correction<br />

Muffle furnance Kjeltec<br />

P/N 9999 0403E, Issue 1 GB, Dec 2004


A semi-automated extraction system for simple <strong>de</strong>termination of cru<strong>de</strong> fibre, <strong>de</strong>tergent<br />

fibre and related <strong>para</strong>meters in plant materials, compound feeds, foodstuffs etc.<br />

Features and benefits<br />

Safety<br />

• Automated heating of reagents in an integrated, closed<br />

system<br />

• Automated addition of preheated reagents<br />

Precision<br />

• Fulfils boiling start time requirements for cru<strong>de</strong> fibre specified<br />

in ISO and EC standards<br />

• Enhances precision thanks to integrated extraction and filtration,<br />

thus avoiding sample transfer<br />

• Ensures same extraction condition in each analysis by means<br />

of timer function<br />

• Official approval: ISO 6865, 92/89 EEC and AOAC 2002.04<br />

(feed).<br />

Value<br />

•<br />

•<br />

•<br />

Automatic water filling/topping up<br />

Batch handling <strong>de</strong>vices for simple transfer of samples to<br />

balance, furnace etc<br />

Water-saving <strong>de</strong>vice reduces consumption<br />

Dedicated Analytical Solutions<br />

Fibertec 2010<br />

Auto Fibre Analysis System<br />

Description<br />

The Fibertec 2010 is specifically <strong>de</strong>signed for fibre <strong>de</strong>termination<br />

in accordance with the Ween<strong>de</strong>, van Soest and other<br />

recognized methods. Single or sequential extractions including<br />

boiling, use of internally preheated reagents, rinsing and<br />

filtration are performed un<strong>de</strong>r reproducible and controlled<br />

conditions.<br />

The Fibertec 2010 is available with the following basic<br />

modules:<br />

Fibertec 2010 Hot Extraction Unit, for hot hydrolysis and<br />

extraction, featuring built-in systems for heating and filtration,<br />

and for automatic preheating and addition of reagents<br />

Fibertec 1021 Cold Extraction Unit, for <strong>de</strong>-fatting samples,<br />

extraction at ambient temperatures (e.g. in lignin <strong>de</strong>termination)<br />

and solvent <strong>de</strong>hydration of fibre residues<br />

Both modules use the same crucible system, permitting samples<br />

to be dried and weighed between extractions if required.<br />

Samples are handled in specially <strong>de</strong>signed filter crucibles. Crucibles<br />

are used both as an integral part of the assembly during<br />

extraction, rinsing and filtration and as sample vessels during<br />

weighing, drying and ashing.<br />

The Fibertec method is as <strong>de</strong>scribed in the relevant ISO and<br />

EC standards. It is thus the reference method and is a sound<br />

choice for the future.


System <strong>de</strong>scription:<br />

• Fibertec 2010, 240V, 50 Hz comprising; Hot Extraction<br />

Unit, Cold Extraction Unit, crucibles, crucible stand,<br />

crucible hol<strong>de</strong>r, reflector, spray bottle, tubing, anti-foaming<br />

agent and water supply tank, crucible seals<br />

• Fibertec 2010, 240V, 60 Hz specifications. As above.<br />

• Fibertec 2010, 240V, 60 Hz specifications<br />

• Fibertec 2010 Hot Extraction Unit (240V, 50 Hz) same as<br />

2010 but without Cold Extraction Unit<br />

Accessories:<br />

Crucible stand for 6 crucibles. At least two stands recommen<strong>de</strong>d.<br />

Crucible hol<strong>de</strong>r for 6 crucibles<br />

Water Aspirator Pump<br />

Performance data:<br />

Sample size: 0,5 - 3 g<br />

Measuring range: 0,1% - 100%<br />

Capacity per batch: Up to 6 samples simultaneously<br />

Capacity per day: Up to 36 analyses (cru<strong>de</strong> fibre<br />

method). Up to 60 analyses using<br />

modified procedure<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Anti-foaming agent (octanol)<br />

Filtering agent (celite 545), 1 l<br />

Optional accessories:<br />

Crucibles, P0 (porosity 160-250 µm), set of 6<br />

Crucibles, P1 (porosity 100-160 µm), set of 6<br />

Crucibles, P2 standard (porosity 40-100 µm), set of 6<br />

Crucibles, P3 (porosity 16-40 µm), set of 6<br />

Sample pre<strong>para</strong>tion equipment:<br />

1093 Cyclotec, Sample mill<br />

1090 Cemotec, Sample mill<br />

2094 Homogenizer, blen<strong>de</strong>r type<br />

2096 Homogenizer, blen<strong>de</strong>r type<br />

1095 Knifetec, water cooled<br />

Repeatability: ±1 % relative at 5% - 30% fibre level<br />

Reagent preheating<br />

time: 10-20 min<br />

Heating-up time from<br />

preheated temperature<br />

to boiling: 5-7 min<br />

Installation requirements:<br />

Equipment Power supply Power Dimensions Weight Water supply<br />

consumption w × d × h<br />

2010 Hot Extraction Unit 200 - 240V ± 10% 50 Hz or<br />

200 - 240V ± 10% 60 Hz 2.3 kW 75 × 40 × 68 65 kg Tap water* appr. 2 l/min<br />

1021 Cold Extraction Unit<br />

with water aspirator - - 58 × 38 × 28 14 kg Tap water<br />

* When Fibertec 2010 is in standby mo<strong>de</strong> the tap water supply is closed down.<br />

Applications:<br />

• Cru<strong>de</strong> Fibre (acc. to Ween<strong>de</strong>). • Neutral Detergent Fibre.<br />

• Acid Detergent Fibre. • Acid Detergent Lignin.<br />

The Fibertec 2010 is also suitable for use with most other chemical extraction methods except those that involve the use<br />

of acetic acid, trichloracetic acid and/or nitric acid. For specific method information, please ask for <strong>de</strong>tailed FOSS Analytical<br />

Application Notes.<br />

Fibertec Systems for any fibre <strong>de</strong>termination needs:<br />

Low fat samples<br />

1093 Cyclotec Mill<br />

Medium fat samples<br />

1090 Cemotec Mill<br />

High fat samples<br />

2094/2096 Homogenizer<br />

1095 Knifetec<br />

Balance<br />

Method<br />

Enzymatic<br />

Chemical<br />

Fibertec E<br />

High workloads<br />

Fibertec 2010<br />

Medium workloads<br />

Fibertec M6<br />

Drying Oven Balance Muffle furnance<br />

Balance<br />

P/N 9999 0405E, Issue 1 GB, Dec 2004


Semi-automated incubation and se<strong>para</strong>tion system for quantitative <strong>de</strong>termination of<br />

dietary fibre in processed food, cereal products, fruits and vegetables, health food,<br />

feedstuffs, plant materials, etc.<br />

Benefits<br />

• Free choice of methods like AOAC, AACC,<br />

NMKL and Asp.<br />

• Determines total, soluble and insoluble dietary<br />

fibre.<br />

• Rapid filtration of six samples simultaneously.<br />

• Specially <strong>de</strong>signed incubation flasks<br />

• High incubation and se<strong>para</strong>tion capacity.<br />

• Repeatable readings, S.D. < 0.5% absolute.<br />

• Easy and convenient to use.<br />

• Saves time, space and manual work.<br />

Description<br />

The Fibertec E is <strong>de</strong>signed for rapid and rational<br />

<strong>de</strong>termination of dietary fibre according to established<br />

enzymatic methods, including those approved<br />

by AOAC, AACC, NMKL and Asp.<br />

The Fibertec E <strong>de</strong>termines total dietary fibre as<br />

well as the insoluble and soluble fibres se<strong>para</strong>tely.<br />

It is also useful in sample pre<strong>para</strong>tion for <strong>de</strong>tailed<br />

studies of fibre fractions, e.g. by chromatographic<br />

or colorimetric techniques.<br />

Dedicated Analytical Solutions<br />

Fibertec E<br />

Dietary Fibre Analysis System<br />

The basic Fibertec E inclu<strong>de</strong>s a Shaking Water<br />

Bath and a Filtration Module. The Shaking Water<br />

Bath incubates 12 samples in each batch. The<br />

temperature range is from ambient to 80°C and it is<br />

possible to preset three temperatures. The shaking<br />

frequency and amplitu<strong>de</strong> are continously adjustable.<br />

The Filtration Module filters and collects 6<br />

sample solutions batchwise and inclu<strong>de</strong>s a system<br />

for rapid <strong>de</strong>hydration. The filtration step is spee<strong>de</strong>d<br />

up through built-in “Pressure Mo<strong>de</strong>”. Reversed<br />

pressure is applied to facilitate filtration by breaking<br />

up clogged filter residues during filtration.<br />

Filtration time varies according to sample type, but<br />

on average it is 2-4 minutes for 100 ml of digested<br />

solution.<br />

The reproducibility (standard <strong>de</strong>viation) of the<br />

Fibertec E in <strong>de</strong>termining total, insoluble and<br />

soluble dietary fibre is < 0.5% absolute.


System <strong>de</strong>scription:<br />

Fibertec E<br />

• Filtration Module complete, comprising: Filtration Module,<br />

Incubation Flasks (4 sets of 6), Standard Crucibles<br />

(P2, 2 sets of 6), Basket for Incubation Flasks, 2 Stands for<br />

Crucibles, 2 Spray bottles, 2 Water aspiration pumps, Filter<br />

aid, Tubing, Shaking Water Bath, complete, comprising: a<br />

tray for 12 Incubation Flasks and a hinged inclined lid.<br />

In addition, we recommend:<br />

Incubation Flask (set of 6), at least 4 sets<br />

Crucible, P2 (40 - 100 µm) set of 6, at least 2 sets<br />

Basket for 12 Incubation Flasks, at least 1<br />

Total Dietary Fibre Kit for 200 <strong>de</strong>terminations<br />

Termamyl 300 L, 100 ml Boiling Water Bath Pipette 100 µl<br />

Muffle or incineratron furnace ~525°C<br />

Performance data:<br />

Filtration Module:<br />

Filtration and <strong>de</strong>-<br />

hydration capacity: 6 samples/batch<br />

Filtration rate: 2-4 ml/100 ml of digested solution,<br />

<strong>de</strong>pending on sample type<br />

Repeatability: S.D. < 0.5% absolute<br />

Flask volume: 600 ml<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Shaking Water Bath:<br />

Capacity: 12 flasks/batch<br />

Temperature range: ambient to 80°C<br />

Temperature accuracy: ± 0.1°C<br />

Shaking frequency: 0-150 strokes/minute<br />

Stroke length: 0-50 mm<br />

Installation requirements:<br />

Equipment Power supply Power consumption Dimensions Weight, kg<br />

w × d × h<br />

1023 Filtration Module 100-120 V, 50-60 Hz 8 770 × 280 × 500 24<br />

210-230 V, 50-60 Hz<br />

1024 Shaking Water Bath 100-120 V, 50-60 Hz 1500 890 × 370 × 320 24<br />

210-230 V, 50-60 Hz<br />

A comple analytical scheme for dietary fibre <strong>de</strong>termination consists of:<br />

Samples with a low<br />

fat content<br />

1093 Cyclotec Mill<br />

1090 Cemotec Mill<br />

Samples with a high<br />

fat content<br />

2094 Homogenizers<br />

1095 Knifetec<br />

Balance<br />

Water Bath<br />

Boiling<br />

Shaking Water<br />

Bath 1024<br />

Accessories:<br />

Alternative filter crucibles:<br />

Crucible, P0 (160 - 250 µm), set of 6<br />

Crucible, P1 (90 - 150 µm), set of 6<br />

Crucible, P3 (15 - 40 µm), set of 6<br />

Stand for 6 Crucibles<br />

1093 Cyclotec Sample Mill<br />

1090 Cemotec Sample Mill<br />

1095 Knifetec Sample Mill for high fat, high fibre samples<br />

For protein <strong>de</strong>termination we recommend our Kjeltec analyzers.<br />

Alternative flask trays for other applications, e.g. biochemical<br />

work:<br />

Tray for E**-flasks, 50 ml<br />

Tray for E**-flasks, 100 ml<br />

Tray for E**-flasks, 250 ml<br />

Tray for E**-flasks, 500 ml<br />

** Erlenmeyer<br />

Filtration Module<br />

1023<br />

Drying Oven Balance<br />

Correction<br />

Muffle furnance Kjeltec<br />

P/N 9999 0403E, Issue 1 GB, Dec 2004


Extraction System for simple <strong>de</strong>termination of Cru<strong>de</strong> Fibre, Detergent Fibre, Cellulose,<br />

Hemicelluloses, Lignin and related Parameters in plant materials, compound feed, food, etc.<br />

Benefits<br />

•<br />

•<br />

•<br />

•<br />

•<br />

•<br />

•<br />

•<br />

•<br />

Six samples processed simultaneously.<br />

Accessories for batch handling.<br />

Integral extraction and filtration.<br />

No sample transfer and no loss of sample.<br />

Se<strong>para</strong>te unit for solvent <strong>de</strong>hydration, lignin <strong>de</strong>termination<br />

and <strong>de</strong>fatting.<br />

Extensive application service.<br />

High reproducibility of conditions and results.<br />

Saves time, energy and laboratory space.<br />

Official approval: ISO 6865, 92/89 EEC and<br />

AOAC 2002.04 (feed).<br />

Description<br />

The Fibertec System M6 is <strong>de</strong>dicated for fibre<br />

<strong>de</strong>terminations according to Ween<strong>de</strong>, van Soest,<br />

etc. Single or sequential extractions including boiling,<br />

using externally preheated reagents, rinsing<br />

and filtration are performed un<strong>de</strong>r reproducible and<br />

controlled conditions.<br />

Dedicated Analytical Solutions<br />

Fibertec M6<br />

Fibre Analysis System<br />

The basic modules of a Fibertec M6 are:<br />

• 1020 Hot Extraction Unit, for hot hydrolysis and<br />

extraction with built-in systems for heating and<br />

filtration<br />

• 1021 Cold Extraction Unit, for <strong>de</strong>fatting samples,<br />

extraction at ambient temperature e.g. lignin <strong>de</strong>termination,<br />

and for solvent <strong>de</strong>hydration of fibre<br />

residues.<br />

Both units are adapted to the same crucible<br />

system that permits the sample, whenever required,<br />

to be dried and weighed between extractions. In<br />

the system the samples are handled in specially<br />

<strong>de</strong>signed filter crucibles, which are used both as an<br />

integral part of an extraction assembly during extraction,<br />

rinsing and filtering, and as a sample vessel<br />

during the weighing, drying and ashing steps.<br />

The Fibertec M6 permits handling of six samples<br />

at a time by the use of accessory tools for batch<br />

handling. Filtration problems are overcome by the<br />

unique vacuum/reverse air flow system.<br />

The Fibertec M6 offers a most time saving and<br />

convenient solution for more reproducible fibre<br />

<strong>de</strong>terminations.


System <strong>de</strong>scription:<br />

Fibertec M6 (200-230V):<br />

• Hot Extraction Unit comprising: Hot Extractor, Reflector,<br />

Reagent Bottles, Hot Water Sprayer, Beaker, Funnel, Water<br />

Suction Pump, Antifoaming Agent, Tubing, Hol<strong>de</strong>r for 6<br />

crucibles, Stand for 6 crucibles, Crucibles (P2 standard, 2<br />

sets of 6), Manual.<br />

• Cold Extraction Unit comprising: Cold Extractor, Spray<br />

Bottle, Tubing, T-tube, Spare Part Kit, Stand for 6 crucibles,<br />

Crucibles (P2 standard 40 - 100 µm, set of 6),<br />

Antifoaming Agent (octanol), Celite, 1 l<br />

Performance data:<br />

Sample size: 0.5 - 3 g (1 g normal)<br />

Measuring range: 0.1 - 100%<br />

Repeatability: < 1% relative at 5 - 30 % fibre level<br />

Accuracy: According to official methods<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Also choose from the following accessories:<br />

1093 Cyclotec Sample Mill, cyclone mill<br />

1090 Cemotec Sample Mill, moisture mill<br />

2094 Homogenizer, blen<strong>de</strong>r type<br />

2096 Homogenizer, blen<strong>de</strong>r type<br />

1095 Knifetec, water cooled sample mill<br />

Hot plate 2022<br />

Filter Crucibles:<br />

Crucible, P1 (100 - 160 µm), set of 6<br />

Crucible, P2 (40 - 100 µm), set of 6, standard<br />

Crucible, P3 (16 - 40 µm), set of 6<br />

Crucible, P0 (160 - 250 µm), set of 6<br />

Crucible P2 US, (40 - 60 µm) set of 6<br />

Capacity per batch: 6 samples simultaneously<br />

Capacity per day: Up to 36 analyses (Cru<strong>de</strong> Fibre<br />

method acc. to Ween<strong>de</strong>) per day<br />

Installation requirements:<br />

Equipment Power supply Power Dimensions Weight Water supply<br />

consumption w × d × h<br />

1020 Hot Extraction Unit 200 - 230V ± 10% 1 000 kW 56 × 38 × 57 28 kg Tap water for<br />

50 - 60 Hz con<strong>de</strong>nsors (appr. 2 l/min)<br />

and water aspirator (during<br />

filtration)<br />

1021 Cold Extraction Unit - - 56 × 38 × 28 4 kg Tap water for water aspira<br />

tor (during filtration)<br />

Applications:<br />

• Cru<strong>de</strong> Fibre (acc. to Ween<strong>de</strong>). • Neutral Detergent Fibre.<br />

• Acid Detergent Fibre. • Acid Detergent Lignin.<br />

In addition, most other chemical extraction methods except methods including acetic acid, trichloracetic acid and/or nitric acid,<br />

may be employed. For specific method information, please ask for <strong>de</strong>tailed FOSS Analytical Application Notes.<br />

Fibertec Systems for any fibre <strong>de</strong>termination needs:<br />

Low fat samples<br />

1093 Cyclotec Mill<br />

Medium fat samples<br />

1090 Cemotec Mill<br />

High fat samples<br />

2094/2096 Homogenizer<br />

1095 Knifetec<br />

Balance<br />

Method<br />

Enzymatic<br />

Chemical<br />

Fibertec E<br />

High workloads<br />

Fibertec 2010<br />

Medium workloads<br />

Fibertec M6<br />

Drying Oven Balance Muffle furnance<br />

Balance<br />

P/N 9999 0401E, Issue 1 GB, Dec 2004


Kjeltec – el estándar<br />

<strong>para</strong> el <strong>análisis</strong> preciso,<br />

seguro y fácil <strong>de</strong> la<br />

proteína


EXACTITUD<br />

Con el enfoque en la exactitud<br />

2<br />

Alcanzar la mayor exactitud posible es el objetivo<br />

<strong>de</strong> todo <strong>análisis</strong>. Ésta ha sido siempre la<br />

pauta <strong>de</strong> FOSS en el <strong>de</strong>sarrollo <strong>de</strong> nuevos instrumentos<br />

y sistemas.<br />

Hoy, 30 años <strong>de</strong>spués <strong>de</strong> que se lanzara el<br />

primer Kjeltec, FOSS mantiene una posición<br />

lí<strong>de</strong>r en el <strong>análisis</strong> <strong>de</strong> nitrógeno/proteína.<br />

Nuestra meta fundamental es usar la tecnología<br />

disponible <strong>para</strong> eliminar los factores humanos y<br />

técnicos que causan errores en los resultados, o<br />

que cambian el funcionamiento <strong>de</strong> los analizadores<br />

con el tiempo.<br />

Un Kjeltec <strong>de</strong> FOSS hace fácil y fiable el <strong>análisis</strong><br />

<strong>de</strong> rutina.


La generación Serie Azul <strong>de</strong> Kjeltec esta diseñada<br />

<strong>para</strong> lograr la mayor exactitud y precisión posible en<br />

el <strong>análisis</strong> Kjeldahl <strong>de</strong> nitrógeno. Para correspon<strong>de</strong>r<br />

a todos los tipos <strong>de</strong> requisitos analíticos, la gama<br />

cuenta con varios instrumentos, <strong>de</strong>s<strong>de</strong> unida<strong>de</strong>s <strong>de</strong><br />

<strong>de</strong>stilación manual a sistemas totalmente automatizados,<br />

con auto-muestreo, <strong>para</strong> el funcionamiento<br />

<strong>de</strong>satendido.<br />

Una <strong>de</strong> las características que aseguran la más<br />

alta exactitud es el software interactivo, que ayuda<br />

al operario a evitar errores. El funcionamiento <strong>de</strong>l<br />

analizador pue<strong>de</strong> verificarse fácilmente usando el<br />

test <strong>de</strong> recuperación <strong>de</strong> rutina incorporado.<br />

Las superiores prestaciones se basan en el uso <strong>de</strong> que una<br />

precisa reacción ácido-base <strong>para</strong> la <strong>de</strong>tección <strong>de</strong>l punto<br />

final <strong>de</strong> la valoración. Esta reacción será la misma día a día<br />

y año a año. No está afectada por factores externos como el<br />

tiempo, la <strong>de</strong>riva o el factor humano<br />

Otro ejemplo es la posibilidad <strong>de</strong> pre<strong>de</strong>finir un<br />

amplio número <strong>de</strong> procedimientos automatizados,<br />

especialmente útil en laboratorios que usan varios<br />

métodos <strong>de</strong> <strong>de</strong>stilación.<br />

El único con tritación colorimétrica incorporada<br />

proporciona una exactitud incom<strong>para</strong>ble y es la<br />

metodología recomendada por las recientes normas<br />

AOAC, ISO/IDF y otras organizaciones <strong>de</strong> estandarización.<br />

Las bombas <strong>de</strong> fuelle mi<strong>de</strong>n el volumen<br />

real <strong>de</strong> reactivo que se dosifica, lo que asegura la<br />

exactitud constantemente. Las ventajas adicionales<br />

son la estabilidad a largo plazo, el amplio rango <strong>de</strong><br />

trabajo, velocidad <strong>de</strong> respuesta, simplicidad y ninguna<br />

necesidad <strong>de</strong> calibraciones.<br />

El método Kjeldahl es la técnica más versátil<br />

disponible <strong>para</strong> el <strong>análisis</strong> <strong>de</strong> nitrógeno.<br />

De hecho, éste es el único método<br />

que pue<strong>de</strong> ser usado <strong>para</strong> <strong>análisis</strong> tanto<br />

<strong>de</strong> amonio como contenido <strong>de</strong> nitrógeno/<br />

proteína en todo tipo <strong>de</strong> muestras<br />

3


SEGURIDAD<br />

4<br />

La seguridad es una responsabilidad<br />

La seguridad en su trabajo diario en el laboratorio<br />

es su responsabilidad. Sin embargo, es nuestra res-<br />

ponsabilidad <strong>de</strong>sarrollar instrumentos que hagan su<br />

tarea tan simple como sea posible <strong>para</strong> lograr sus<br />

objetivos.<br />

Cuanta más seguridad incorporemos en el instrumento,<br />

menos tendrá usted que preocuparse al manejarlo.<br />

Un Kjeltec <strong>de</strong> FOSS hace el <strong>análisis</strong> rutinario<br />

más seguro.


La gama <strong>de</strong> Kjeltec <strong>de</strong> FOSS cumple con las normas<br />

<strong>de</strong> seguridad en el <strong>análisis</strong> <strong>de</strong> nitrógeno/proteína por<br />

método Kjeldahl. Los instrumentos están equipados<br />

con un conjunto <strong>de</strong> elementos <strong>de</strong> seguridad incorporados,<br />

tales como sensores que <strong>de</strong>tectan si el tubo<br />

está en su sitio o no, si la puerta y/o la tapa frontal<br />

están abiertas, y si el nivel <strong>de</strong> reactivo es <strong>de</strong>masiado<br />

alto o bajo. También están equipados con un rápido<br />

y fiable sistema <strong>de</strong> vaciado <strong>de</strong> tubos, que sustituye<br />

el manejo manual <strong>de</strong> reactivos calientes <strong>de</strong>spués <strong>de</strong><br />

la <strong>de</strong>stilación. Cuando cualquiera <strong>de</strong> los sensores se<br />

activa, el sistema se <strong>de</strong>tiene y muestra en la pantalla<br />

y/o imprime la razón <strong>de</strong> esta interrupción. El mensaje<br />

obtenido indica la acción correctiva necesaria.<br />

El analizador Kjeltec contiene numerosos sensores<br />

<strong>para</strong> asegurar un manejo seguro. Cuando<br />

los sensores <strong>de</strong>l sistema indican un error, el<br />

sistema se <strong>de</strong>tiene y muestra la razón <strong>de</strong> la interrupción<br />

por pantalla y/o por listado.<br />

La tecnología patentada SAfE (Steam Addition for<br />

Equilibration) mejora la seguridad <strong>de</strong>l analizador<br />

a través <strong>de</strong> un procedimiento <strong>de</strong> mezclado <strong>de</strong> los<br />

reactivos especial. Después <strong>de</strong> la adición <strong>de</strong>l agua,<br />

comienza el vapor, se mezclan los contenidos <strong>de</strong>l<br />

tubo, y las gradientes <strong>de</strong> concentración se reducen<br />

al mínimo. Se agrega el álcali y se produce un cambio<br />

gradual <strong>de</strong> ácido a las condiciones alcalinas,<br />

mientras la pasta <strong>de</strong> sal se disuelve. El procedimiento<br />

SAfE ahorra tiempo, mejora la seguridad y previene<br />

la pérdida potencial <strong>de</strong> nitrógeno.<br />

A<strong>de</strong>más, la nueva tecnología patentada SAfE<br />

(Steam Addition for Equilibration) mejora la seguridad<br />

<strong>de</strong>l analizador a través <strong>de</strong> un procedimiento<br />

<strong>de</strong> mezclado <strong>de</strong> los reactivos especial que reduce la<br />

reacción exotérmica cuando se aña<strong>de</strong> el álcali a la<br />

mezcla <strong>de</strong> digestión, y elimina la necesidad <strong>de</strong><br />

predilución manual <strong>de</strong> muestras.<br />

Las pastas semisólidas <strong>de</strong> la mezcla sal/ácido restantes<br />

<strong>de</strong> la digestión, se disuelven con suavidad.<br />

Si un instrumento pue<strong>de</strong><br />

funcionar con sus puertas y<br />

cubiertas abiertas, no garantiza<br />

la seguridad durante la<br />

operación .<br />

Si el instrumento continúa<br />

con el <strong>análisis</strong> incluso si no<br />

hay tubo en la posición, ese<br />

instrumento es inseguro tenga<br />

puertas o no.<br />

AGUA<br />

ÁLCALI<br />

DELAY SAfE PATENTED<br />

SAL/ÁCIDO SAL/ÁCIDO<br />

Los gradientes <strong>de</strong><br />

reactivos permanecen<br />

La mezcla <strong>de</strong> reactivos<br />

minimiza el gradiente<br />

AGUA/ÁLCALI<br />

5


... Esto es lo que obtiene<br />

Un coste más bajo <strong>de</strong>l <strong>análisis</strong><br />

Gracias a aplicaciones <strong>de</strong> rutina optimizadas los<br />

costes <strong>de</strong> funcionamiento se mantienen bajos.<br />

Eficacia más alta<br />

El tiempo <strong>de</strong> inactividad y gastos <strong>de</strong> mantenimiento<br />

se reducen al mínimo gracias al empleo <strong>de</strong> una cuidadosa<br />

selección <strong>de</strong> componentes <strong>de</strong> larga duración.<br />

El equipo está construido <strong>de</strong> modo que las superficies<br />

expuestas a reactivos están fabricadas con<br />

plásticos resistentes a materiales <strong>químicos</strong> y libres <strong>de</strong><br />

corrosión, etiquetados <strong>para</strong> el reciclaje. Naturalmente<br />

todas las partes que son expuestas a las sustancias<br />

químicas son fáciles <strong>para</strong> limpiar. Los programas <strong>de</strong><br />

mantenimiento rutinario se estipulan <strong>de</strong> acuerdo con<br />

las rutinas GLP.<br />

Rendimiento más alto<br />

Las muestras se pue<strong>de</strong>n manejar en lotes, lo que simplifica<br />

la carga y la capacidad <strong>de</strong> trazabilidad <strong>de</strong> las<br />

muestras.<br />

Con un Analizador Kjeltec, el <strong>análisis</strong> rutinario se hace<br />

muy sencillo. La documentación y el soporte técnico <strong>de</strong><br />

FOSS aseguran resultados exactos, disminuyen el tiempo<br />

<strong>de</strong> inactividad y reducen gastos operacionales.<br />

La precisión es el criterio más importante <strong>para</strong> una<br />

buena economía <strong>de</strong> por vida. El ejemplo está en la industria<br />

<strong>de</strong> la alimentación, don<strong>de</strong> el coste <strong>de</strong> materia<br />

prima afecta a la rentabilidad <strong>de</strong>l productor consi<strong>de</strong>rablemente.<br />

En combinación con nuestro sistema <strong>de</strong> auto-<br />

muestreo, Kjeltec asegura el proceso <strong>de</strong> hasta 60<br />

muestras, sin transferencia <strong>de</strong> la muestra. Simplemente<br />

cargue los porta-muestras directamente <strong>de</strong>s<strong>de</strong><br />

el bloque <strong>de</strong> digestión y el Kjeltec realizará el <strong>análisis</strong><br />

exacto y <strong>de</strong>satendido durante 4 horas. Hay que<br />

mencionar <strong>de</strong> nuevo, que al ser el único equipo con<br />

titración colorimétrica incorporada no requiere esfuerzos<br />

<strong>de</strong> calibración.<br />

Conocimiento mejorado<br />

A<strong>de</strong>más, cuando usted escoge FOSS como su compañero<br />

en el laboratorio adquiere algo que pue<strong>de</strong><br />

significar la diferencia entre éxito y fracaso. Adquiere<br />

acceso a toda la experiencia <strong>de</strong> una empresa <strong>de</strong><br />

<strong>análisis</strong> lí<strong>de</strong>r mundial <strong>de</strong>ntro <strong>de</strong>l campo <strong>de</strong> alimentos,<br />

piensos y <strong>análisis</strong> <strong>de</strong> agua. FOSS está representado<br />

en más <strong>de</strong> 100 países.<br />

El Kjeltec <strong>de</strong> FOSS ofrece una relación calidadprecio<br />

sin igual y hace beneficioso el <strong>análisis</strong> rutinario.<br />

Simplemente cargue los porta-muestras directamente <strong>de</strong>s<strong>de</strong><br />

el bloque <strong>de</strong> digestión y el Kjeltec realizará el <strong>análisis</strong> exacto<br />

y <strong>de</strong>satendido durante 4 horas. Se pue<strong>de</strong>n cargar hasta<br />

un máximo <strong>de</strong> 60 muestras.<br />

Un 1% <strong>de</strong> Diferencia<br />

COMPONENTE (%) SOBRE PRECIO VENTA<br />

Materia Prima 80 79<br />

Costes Fijos 10 10<br />

Costes Mano <strong>de</strong> Obra 5 5<br />

Beneficio 5 6 (=20% aumento beneficio)<br />

7


La gama Kjeltec <strong>de</strong> FOSS<br />

UNIDAD DE DESTILACION KJELTEC 2100 KJELTEC 2200 KJELTEC 2300 KJELTEC 2400 KJELTEC 2400/2460<br />

Generador automático <strong>de</strong> vapor estándar estándar estándar estándar estándar<br />

Programable 1 programa 5 programas 10 programas 10 programas 5 programas<br />

Sistema <strong>de</strong> ahorro <strong>de</strong> agua estándar estándar estándar estándar estándar<br />

Cabezal <strong>de</strong> expansion <strong>de</strong> polipropeno estándar estándar estándar estándar estándar<br />

Recipiente <strong>de</strong> vaciado <strong>de</strong> tubos <strong>de</strong><br />

polipropeno – estándar estándar estándar estándar<br />

Tiempo <strong>de</strong> <strong>de</strong>stilación


Funciones & Ventajas:<br />

• Facilidad <strong>de</strong> uso con la dilución, adición <strong>de</strong> álcali, <strong>de</strong>stilación<br />

y vaciado <strong>de</strong>l tubo automáticos.<br />

• El generador variable <strong>de</strong>l vapor <strong>de</strong> salida amplía el área <strong>de</strong><br />

aplicación a otros componentes volátiles.<br />

• Procedimientos oficiales y precisos (ISO, AOAC, EPA, DIN,<br />

etc.) que simplifican la validación.<br />

• Función SAfE* patentada <strong>para</strong> la <strong>de</strong>stilación segura <strong>de</strong><br />

tubos con presencia <strong>de</strong> precipitados.<br />

• Sistemas <strong>de</strong> seguridad incorporados <strong>para</strong> protección <strong>de</strong><br />

usuarios.<br />

• El control con ajuste automático <strong>de</strong>l agua <strong>de</strong> refrigeración<br />

ahorra agua y reduce costes.<br />

• Bombas <strong>de</strong> fuelle <strong>para</strong> la dispensación precisa <strong>de</strong> reactivos.<br />

• Cabezal <strong>de</strong> expansión <strong>de</strong> plástico resistente al álcali <strong>para</strong><br />

larga vida útil.<br />

Dedicated Analytical Solutions<br />

Kjeltec 8100<br />

Unidad <strong>de</strong> <strong>de</strong>stilación manual<br />

Unidad <strong>de</strong> <strong>de</strong>stilación sencilla <strong>de</strong> utilizar <strong>para</strong> el <strong>análisis</strong> Kjeldahl <strong>de</strong> nitrógeno/proteína, amonio-nitrógeno, TKN, Destilación directa (DD),<br />

ácidos/bases volátiles, etc.(en la foto también se muestra; Tecator TM Digestor 20 Auto Elevador y el Lavador)<br />

Descripción:<br />

La Unidad <strong>de</strong> Destilación Kjeltec 8100 es una solución simple<br />

y fiable <strong>de</strong> <strong>de</strong>stilación segura y semiautomática.<br />

La posibilidad <strong>de</strong> preprogramar los tiempos <strong>de</strong> la adición <strong>de</strong><br />

álcali y <strong>de</strong> la <strong>de</strong>stilación ayuda a conseguir resultados precisos<br />

con in<strong>de</strong>pen<strong>de</strong>ncia <strong>de</strong>l operador.<br />

Las bombas <strong>de</strong> fuelle <strong>de</strong> precisión proporcionan una estabilidad<br />

a largo plazo en la dispensación <strong>de</strong> reactivos. La unidad va<br />

equipada <strong>de</strong> sensores <strong>para</strong> la puerta <strong>de</strong> seguridad, plataforma<br />

<strong>de</strong>l tubo y temperatura <strong>de</strong>l <strong>de</strong>stilado, así como sensores <strong>de</strong> nivel<br />

y sobrepresión <strong>para</strong> el generador variable <strong>de</strong>l vapor <strong>de</strong> salida.<br />

La tecnología patentada SAfE* mejora la seguridad mediante un<br />

procedimiento <strong>de</strong> mezclado, reduciendo la reacción exotérmica<br />

entre el álcali y el ácido durante la <strong>de</strong>stilación.<br />

El usuario está totalmente protegido por la puerta <strong>de</strong> seguridad<br />

<strong>de</strong> rotación única que <strong>de</strong>be estar cerrada con un tubo en su sitio<br />

antes <strong>de</strong> que la unidad pue<strong>de</strong> funcionar. La puerta <strong>de</strong> seguridad y<br />

la ban<strong>de</strong>ja <strong>de</strong> goteo pue<strong>de</strong>n extraerse fácilmente <strong>para</strong> su limpieza.<br />

El agua <strong>de</strong> refrigeración se utiliza únicamente durante el <strong>análisis</strong><br />

lo que permite ahorros adicionales mediante la función automática<br />

<strong>de</strong> control <strong>de</strong> flujo.<br />

El conjunto <strong>de</strong> aplicaciones optimizadas hace que los costes<br />

<strong>de</strong> ejecución se reduzcan aún más. Mediante la utilización <strong>de</strong><br />

componentes seleccionados se minimizan los costes <strong>de</strong> <strong>para</strong>da y<br />

mantenimiento. El programa <strong>de</strong> mantenimiento rutinario permite<br />

incluir rutinas <strong>de</strong> Buenas Prácticas <strong>de</strong> Laboratorio (BPL).<br />

* Adición <strong>de</strong> vapor <strong>para</strong> homogenización


Números <strong>de</strong> pedido:<br />

81000001 Unidad <strong>de</strong> Destilación Manual, 200 – 240 V,<br />

50 – 60 Hz que incluye:<br />

Unidad <strong>de</strong> <strong>de</strong>stilación controlada por microprocesador<br />

con drenaje <strong>de</strong> tubo y adición automática<br />

<strong>de</strong> agua y álcali.<br />

Generador <strong>de</strong> vapor incorporado <strong>para</strong> agua <strong>de</strong>ionizada<br />

o agua corriente.<br />

Completa con tanques <strong>de</strong> álcali/agua/residuos con<br />

sensores <strong>de</strong> nivel, matraz <strong>de</strong> receptor, adaptador<br />

combi <strong>para</strong> tubos <strong>de</strong> 100, 250, 400 & 750 ml y<br />

tubos <strong>de</strong> digestión <strong>de</strong> 100 & 250 ml.<br />

Datos <strong>de</strong> funcionamiento a 230 V:<br />

Tiempo <strong>de</strong> <strong>de</strong>stilación: 3,5 min a 30 mg N<br />

(6,5 min a 200 mg N)<br />

Capacidad <strong>de</strong>stilación: ~ 40 ml/min<br />

Rango medición: 1 – 200 mg N<br />

Reproducibilidad: 1% RSD (incluyendo paso <strong>de</strong><br />

digestión)<br />

Recuperación: > 99,5 % a niveles nitrógeno entre<br />

1 - 200 mg N<br />

Drenaje <strong>de</strong>l tubo: 200 ml en menos <strong>de</strong> 10 s<br />

Volúmenes bomba reactivos: 0 - 150 ml en intervalos <strong>de</strong> 10 ml<br />

Retardo: 0 - 1800 s<br />

SAfE Patented : 0 - 15 s<br />

FOSS Analytical<br />

Slangerupga<strong>de</strong> 69<br />

DK-3400 Hilleroed<br />

Dinamarca<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Accesorios opcionales:<br />

Para instalar un sistema Kjeldahl completo, <strong>de</strong>be seleccionarse<br />

un Digestor con los accesorios a<strong>de</strong>cuados, como Aspirador,<br />

Lavador, tubos <strong>de</strong> <strong>de</strong> muestra y pastillas catalizadoras. Los<br />

<strong>de</strong>talles se pue<strong>de</strong>n encontrar en la hoja <strong>de</strong> datos técnicos <strong>de</strong> los<br />

sistemas Tecator Digestor.<br />

60032042 Tanque 20 l (álcali/agua/residuos) sin sensores <strong>de</strong><br />

nivel<br />

60032043 Kit <strong>de</strong> sensor <strong>de</strong> nivel <strong>para</strong> residuos<br />

60032044 Kit <strong>de</strong> sensor <strong>de</strong> nivel <strong>para</strong> reactivos<br />

1002-022 Unidad <strong>de</strong> valoración <strong>completa</strong>, 50 ml<br />

60030343 Adaptador <strong>para</strong> tubos Büchi<br />

10000089 Cesta <strong>para</strong> 20 matraces <strong>de</strong> receptor (250 ml)<br />

10000164 Matraces <strong>de</strong> receptor, 250 ml (juego <strong>de</strong> 10)<br />

10000897 Dispositivo <strong>para</strong> manejar tubos <strong>de</strong> digestión<br />

Requisitos <strong>de</strong> instalación:<br />

Fuente <strong>de</strong> alimentación: 200 - 240 V, 50 - 60 Hz<br />

Consumo eléctrico: 2.200 W<br />

Consumo <strong>de</strong> agua: 2 l/min a temperatura <strong>de</strong> agua <strong>de</strong> 30ºC<br />

(sólo durante <strong>de</strong>stilación) 1 l/min a temperatura <strong>de</strong> agua <strong>de</strong> 15ºC<br />

Temperatura ambiente: máx. 40ºC<br />

Humedad ambiente: máx. 80 % relativa<br />

Peso neto: 30 kg<br />

Dimensiones: A × P × Al = 480 × 580 × 690 mm<br />

Drenaje: Sólo <strong>para</strong> agua <strong>de</strong> refrigeración<br />

P/N 1026210, Edición 1 ES, Enero 2009


Dedicated Analytical Solutions<br />

Kjeltec 8200<br />

Unidad <strong>de</strong> Destilación Automática<br />

Destilación automática <strong>para</strong> el <strong>análisis</strong> Kjeldahl <strong>de</strong> nitrógeno/proteína, amonio-nitrógeno, TKN, Destilación directa (DD), ácidos/bases<br />

volátiles, etc. (En la foto tambien se muestra; Tecator TM Digestor 20 Auto Elevador y el Lavador)<br />

Funciones & Ventajas:<br />

• Facilidad <strong>de</strong> uso con la <strong>de</strong>stilación automática totalmente<br />

programable, que incluye la dilución <strong>de</strong> muestras, adición <strong>de</strong><br />

álcali & receptor, <strong>de</strong>stilación y drenaje <strong>de</strong>l tubo.<br />

• El generador variable <strong>de</strong>l vapor <strong>de</strong> salida amplía el área <strong>de</strong><br />

aplicación a otros componentes volátiles.<br />

• Procedimientos oficiales y precisos (ISO, AOAC, EPA, DIN,<br />

etc.) que simplifican la validación.<br />

• Función SAfE* patentada <strong>para</strong> la <strong>de</strong>stilación segura <strong>de</strong> tubos<br />

con presencia <strong>de</strong> precipitados.<br />

• Sistemas <strong>de</strong> seguridad incorporados <strong>para</strong> protección <strong>de</strong><br />

usuarios.<br />

• El control con ajuste automático <strong>de</strong>l agua <strong>de</strong> refrigeración<br />

ahorra agua y reduce costes.<br />

• El control <strong>de</strong> temperatura <strong>de</strong>l <strong>de</strong>stilado asegura la precisión<br />

<strong>de</strong> los resultados.<br />

• Bombas <strong>de</strong> fuelle <strong>para</strong> la dispensación precisa <strong>de</strong> reactivos.<br />

• Cabezal <strong>de</strong> expansion <strong>de</strong> plástico/recipiente <strong>de</strong> drenaje <strong>de</strong><br />

tubos resistentes al álcali <strong>para</strong> una larga vida útil.<br />

• Sistema <strong>de</strong>l analizador y muestreador actualizables <strong>de</strong> forma<br />

modular.<br />

Descripción:<br />

La unidad <strong>de</strong> Destilación Automática Kjeltec 8200 es la solución<br />

más avanzada <strong>de</strong> <strong>de</strong>stilación automática y segura. Las<br />

bombas <strong>de</strong> fuelle <strong>de</strong> precisión proporcionan una estabilidad a<br />

largo plazo en la dispensación <strong>de</strong> reactivos. La unidad va equipada<br />

con sensores <strong>para</strong> la puerta <strong>de</strong> seguridad, plataforma <strong>de</strong>l<br />

tubo y temperatura <strong>de</strong>l <strong>de</strong>stilado, así como sensores <strong>de</strong> nivel<br />

y sobrepresión <strong>para</strong> el generador variable <strong>de</strong>l vapor <strong>de</strong> salida.<br />

La tecnología patentada SAfE* mejora la seguridad mediante un<br />

procedimiento <strong>de</strong> mezclado, reduciendo la reacción exotérmica<br />

entre el álcali y el ácido durante la <strong>de</strong>stilación y eliminando la<br />

necesidad <strong>de</strong> predilución manual. Un sistema rápido <strong>de</strong> drenaje<br />

<strong>de</strong> tubos elimina la necesidad <strong>de</strong> manipular reactivos calientes<br />

tras la <strong>de</strong>stilación.<br />

El usuario está totalmente protegido por la puerta <strong>de</strong> seguridad<br />

<strong>de</strong> rotación, única en el mercado, que <strong>de</strong>be estar cerrada con un<br />

tubo en su sitio antes <strong>de</strong> que la unidad pue<strong>de</strong> funcionar. La puerta<br />

<strong>de</strong> seguridad y la ban<strong>de</strong>ja <strong>de</strong> goteo pue<strong>de</strong>n extraerse fácilmente<br />

<strong>para</strong> su limpieza.<br />

El agua <strong>de</strong> refrigeración se utiliza únicamente durante el <strong>análisis</strong><br />

lo que permite ahorros adicionales mediante la función automática<br />

<strong>de</strong> control <strong>de</strong> flujo.<br />

El Kjeltec 8200 ofrece la opción <strong>de</strong> actualizar la unidad a un<br />

analizador Kjeltec 8400 completo cuando lo requiera su negocio.<br />

También se pue<strong>de</strong> añadir al analizador un cambiador <strong>de</strong> muestras<br />

<strong>de</strong> 20 o 60 posiciones, lo que proporciona un funcionamiento<br />

<strong>de</strong>satendido totalmente automático.<br />

* Adición <strong>de</strong> vapor <strong>para</strong> homogenización


Números <strong>de</strong> pedido:<br />

82000001 Unidad <strong>de</strong> Destilación Automática, 200 – 240 V,<br />

50 – 60 Hz que incluye:<br />

Unidad <strong>de</strong> <strong>de</strong>stilación controlada por microprocesador<br />

con drenaje <strong>de</strong> tubo y adición automática<br />

<strong>de</strong> agua, álcali y solución receptora.<br />

Generador <strong>de</strong> vapor incorporado <strong>para</strong> agua <strong>de</strong>ionizada<br />

o agua corriente.<br />

Completa con tanques <strong>de</strong> álcali/agua/receptor/residuos<br />

con sensores <strong>de</strong> nivel, matraz <strong>de</strong> receptor,<br />

adaptador combi <strong>para</strong> tubos <strong>de</strong> 100, 250, 400 &<br />

750 ml y tubos <strong>de</strong> digestión <strong>de</strong> 100 & 250 ml,<br />

dispositivo <strong>de</strong> manejo <strong>de</strong> tubos <strong>de</strong> digestión.<br />

60032041 Kit <strong>para</strong> by pass <strong>de</strong> la <strong>de</strong>stilación<br />

60032073 Cable <strong>para</strong> conexión <strong>de</strong> valorador externo<br />

60032040 Kit <strong>para</strong> actualización <strong>de</strong> la unidad <strong>de</strong> Destilación<br />

Kjeltec 8200 a la unidad Analizador Kjeltec 8400<br />

Datos <strong>de</strong> funcionamiento a 230 V:<br />

Tiempo <strong>de</strong> <strong>de</strong>stilación: 3,5 min a 30 mg N<br />

(6,5 min a 200 mg N)<br />

Capacidad <strong>de</strong>stilación: ~ 40 ml/min<br />

Rango medición: 1 – 200 mg N<br />

Reproducibilidad: 1% RSD (incluyendo paso <strong>de</strong><br />

digestión)<br />

Recuperación: > 99,5 % a niveles nitrógeno entre<br />

1 - 200 mg N<br />

Drenaje <strong>de</strong>l tubo: 200 ml en menos <strong>de</strong> 10 s<br />

Volúmenes bomba reactivos: 0 - 150 ml en intervalos <strong>de</strong> 10 ml<br />

Retardo: 0 – 1800 segundos<br />

SAfE Patented : 0 – 15 segundos<br />

FOSS Analytical<br />

Slangerupga<strong>de</strong> 69<br />

DK-3400 Hilleroed<br />

Dinamarca<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Accesorios opcionales:<br />

Para instalar un sistema Kjeldahl completo, <strong>de</strong>be seleccionarse<br />

un Digestor con los accesorios a<strong>de</strong>cuados, como Aspirador,<br />

Lavador, tubos <strong>de</strong> muestra y pastillas catalizadoras. Los <strong>de</strong>talles<br />

se pue<strong>de</strong>n encontrar en la hoja <strong>de</strong> datos técnicos <strong>de</strong> los sistemas<br />

Tecator Digestor.<br />

60032042 Tanque 20 l (álcali/agua/residuos) sin sensores <strong>de</strong><br />

nivel<br />

60032043 Kit <strong>de</strong> sensor <strong>de</strong> nivel <strong>para</strong> residuos<br />

60032044 Kit <strong>de</strong> sensor <strong>de</strong> nivel <strong>para</strong> reactivos<br />

1002-022 Unidad <strong>de</strong> valoración <strong>completa</strong>, 50 ml<br />

60030343 Adaptador <strong>para</strong> tubos Büchi<br />

10000089 Cesta <strong>para</strong> 20 matraces <strong>de</strong> receptor (250 ml)<br />

10000164 Matraces <strong>de</strong> receptor, 250 ml (juego <strong>de</strong> 10)<br />

10000897 Dispositivo <strong>para</strong> manejar tubos <strong>de</strong> digestión<br />

Requisitos <strong>de</strong> instalación:<br />

Fuente <strong>de</strong> alimentación: 200 - 240 V, 50 - 60 Hz<br />

Consumo eléctrico: 2.200 W<br />

Consumo <strong>de</strong> agua: 2 l/min a temperatura <strong>de</strong> agua <strong>de</strong> 30 ºC<br />

(sólo durante <strong>de</strong>stilación) 1 l/min a temperatura <strong>de</strong> agua <strong>de</strong> 15 ºC<br />

Temperatura ambiente: máx. 40ºC<br />

Humedad ambiente: máx. 80 % relativa<br />

Peso neto: 30 kg<br />

Dimensiones: A × P × Al = 480 × 580 × 690 mm<br />

Drenaje: Sólo <strong>para</strong> agua <strong>de</strong> refrigeración<br />

P/N 1026216, Edición 1 ES, Enero 2009


Kjeltec 8400/8420/8460<br />

Sistemas automáticos <strong>de</strong> muestreo<br />

Análisis totalmente automático <strong>de</strong> nitrógeno/proteínas o TKN en digestiones Kjeldahl, nitrógeno <strong>de</strong> amoniaco, <strong>de</strong>stilación directa (DD) etc.<br />

(En la foto también se muestra: Tecator Digestor 20 Auto Elevador y el Lavador)<br />

Funciones & Ventajas:<br />

• Procesos totalmente automáticos <strong>de</strong> dilución, manejo <strong>de</strong><br />

reactivos, <strong>de</strong>stilación, valoración, cálculo e informes<br />

• El cambiador <strong>de</strong> muestras opcional <strong>de</strong> 20 o 60 posiciones<br />

proporciona un funcionamiento totalmente <strong>de</strong>satendido<br />

• Sistema <strong>de</strong> valoración colorimétrico acreditado oficialmente<br />

(AOAC, EPA, DIN, ISO) que simplifica la validación.<br />

• Sistemas <strong>de</strong> seguridad incorporados <strong>para</strong> protección <strong>de</strong><br />

usuarios.<br />

• Función SAfE* patentada <strong>para</strong> la <strong>de</strong>stilación segura <strong>de</strong><br />

muestras que forman precipitados.<br />

• El control <strong>de</strong> temperatura <strong>de</strong>l <strong>de</strong>stilado asegura resultados<br />

precisos<br />

• El autoajuste <strong>de</strong>l control <strong>de</strong> agua <strong>de</strong> enfriamiento ahorra<br />

agua<br />

• Bombas <strong>de</strong> fuelle <strong>para</strong> la dispensación precisa <strong>de</strong> reactivos<br />

• Cabezal <strong>de</strong> expansión <strong>de</strong> plástico/recipiente <strong>de</strong> drenaje <strong>de</strong><br />

tubos resistentes al álcali <strong>para</strong> una larga vida útil<br />

• Bureta intercambiable <strong>para</strong> el cambio sencillo <strong>de</strong>l valorante<br />

• La conexión Ethernet elimina los problemas <strong>de</strong> comunicación<br />

con impresoras y balanzas<br />

• Control completo <strong>de</strong>l PC <strong>de</strong> todos los registros e informes a<br />

través <strong>de</strong>l software opcional <strong>de</strong> gestión <strong>de</strong> datos<br />

Dedicated Analytical Solutions<br />

Descripción:<br />

Los sistemas Analizador Kjeltec 8400 y los Muestreadores<br />

8420 o 8460 son las soluciones más avanzadas <strong>de</strong> automatización<br />

en el laboratorio Kjeldahl con in<strong>de</strong>pen<strong>de</strong>ncia <strong>de</strong> la producción<br />

<strong>de</strong> muestras.<br />

El <strong>de</strong>sarrollo <strong>de</strong> rutinas <strong>de</strong> Buenas Prácticas <strong>de</strong> Laboratorio (BPL)<br />

se realiza mediante rutinas <strong>de</strong> registro <strong>de</strong> muestras y pruebas <strong>de</strong><br />

rendimiento y la documentación <strong>completa</strong> <strong>de</strong> todos los eventos<br />

realizados durante el <strong>análisis</strong> a través <strong>de</strong> la conexión Balanza/<br />

Impresora/LIMS.<br />

Las bombas <strong>de</strong> fuelle y una bureta rellenable <strong>de</strong> gran precisión<br />

proporcionan estabilidad a largo plazo en la dispensación <strong>de</strong><br />

reactivos. El flujo <strong>de</strong> agua <strong>de</strong> enfriamiento se controla automáticamente<br />

y un sensor <strong>de</strong> temperatura <strong>de</strong>tiene la unidad si el <strong>de</strong>stilado<br />

está <strong>de</strong>masiado caliente. Dispone <strong>de</strong> sensores que monitorizan<br />

que los tubos están en su sitio, puertas <strong>de</strong> seguridad, niveles <strong>de</strong><br />

reactivos, nivel <strong>de</strong> agua y sobrepresión en el generador <strong>de</strong> vapor,<br />

proporcionando todo ello condiciones seguras <strong>para</strong> los usuarios.<br />

La tecnología SAfE* reduce la reacción exotérmica entre el álcali<br />

y el ácido, lo que elimina la necesidad <strong>de</strong> predilución manual <strong>de</strong><br />

las muestras. Un sistema rápido <strong>de</strong> drenaje <strong>de</strong> tubos elimina la<br />

necesidad <strong>de</strong> manipular reactivos calientes.<br />

Los sistemas <strong>de</strong> muestreador toman los tubos directamente en<br />

sus ban<strong>de</strong>jas <strong>de</strong> digestión original, lo que limita la manipulación<br />

y los errores <strong>de</strong> transferencia <strong>de</strong> muestras.<br />

* Steam Addition for Equilibration (Adición <strong>de</strong> vapor <strong>para</strong> homogenización)


Números <strong>de</strong> pedido:<br />

84000001 Unidad Analizador Kjeltec 8400, 200 – 240 V,<br />

50 - 60 Hz que consta <strong>de</strong>:<br />

Unidad automática <strong>de</strong> <strong>de</strong>stilación / valoración con<br />

drenaje <strong>de</strong> tubo y generador <strong>de</strong> vapor incorporado<br />

<strong>para</strong> agua <strong>de</strong>ionizada o agua corriente, <strong>completa</strong><br />

con tanques <strong>de</strong> álcali/agua/receptor/residuos con<br />

sensores <strong>de</strong> nivel, adaptador combi <strong>de</strong> tubos <strong>de</strong><br />

100, 250, 400 y 750 ml <strong>para</strong> dispositivo <strong>de</strong> manejo<br />

<strong>de</strong> 100 & 250 ml<br />

84200001 Kjeltec 8400 / Muestreador Kjeltec 8420 200 –<br />

240 V, 50 - 60 Hz que consta <strong>de</strong>:<br />

Kjeltec 84000001 y 84200011 Muestreador<br />

Kjeltec 8420 <strong>para</strong> 20 muestras<br />

84600001 Kjeltec 8400 / Muestreador Kjeltec 8460 200 –<br />

240 V, 50 - 60 Hz que consta <strong>de</strong>:<br />

Kjeltec 84000001 y 84600011<br />

Muestreador Kjeltec 8460 <strong>para</strong> 60 muestras<br />

84200011 Muestreador Kjeltec 8420 200 – 240 V, 50 – 60 Hz<br />

con accesorios necesarios <strong>para</strong> conectarse y funcionar<br />

con Kjeltec 8400<br />

84600011 Muestreador Kjeltec 8460 200 – 240 V, 50 – 60 Hz<br />

con accesorios necesarios <strong>para</strong> conectarse y fun-<br />

cionar con Kjeltec 8400<br />

Con tanque <strong>de</strong> agua integrado<br />

Datos <strong>de</strong> funcionamiento a 230 V:<br />

Capacidad automuestreador: Muestreador Kjeltec 8420,<br />

1 ban<strong>de</strong>ja con 20 tubos Kjeldahl <strong>de</strong><br />

250 ml o 400 ml<br />

Muestreador Kjeltec 8460, 3 ban<strong>de</strong>-<br />

jas con 20 tubos Kjeldahl <strong>de</strong> 250 ml<br />

o 400 ml<br />

Capacidad almacenaje: 40 lotes (ilimitado con Compass)<br />

Tiempo <strong>de</strong> <strong>análisis</strong>: 3,5 min a 30 mg N<br />

(6,5 min a 200 mg N)<br />

Capacidad <strong>de</strong>stilación: ~ 40 ml/min<br />

Rango medición: 1 – 200 mg N<br />

Reproducibilidad: 1% RSD (incluyendo paso <strong>de</strong><br />

digestión)<br />

Recuperación: > 99,5 % a niveles nitrógeno entre<br />

1 - 200 mg N<br />

Drenaje <strong>de</strong>l tubo: 200 ml en menos <strong>de</strong> 10 segundos<br />

Volumen probeta: 35 ml<br />

Resolución probeta: 2.4 μl/intervalo<br />

Velocidad probeta: >0.5 ml/segundo<br />

Retardo: 0 – 1800 segundos<br />

SAfE Patented : 0 – 15 segundos<br />

FOSS Analytical<br />

Slangerupga<strong>de</strong> 69<br />

DK-3400 Hilleroed<br />

Dinamarca<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Accesorios opcionales:<br />

Para instalar un sistema Kjeldahl completo, <strong>de</strong>be seleccionarse<br />

un Digestor con los accesorios a<strong>de</strong>cuados, como Aspirador,<br />

Lavador, tubos <strong>de</strong> muestra y pastillas catalizadoras. Pue<strong>de</strong><br />

encontrar información adicional en la hoja <strong>de</strong> datos técnicos<br />

aparte <strong>de</strong> los sistemas Tecator Digestion.<br />

60031631 Compass, software <strong>de</strong> PC <strong>para</strong> la unidad Analizador<br />

Kjeltec 8400<br />

60028286 Tanque <strong>para</strong> valorante, completo con tubos<br />

60032074 Dispositivo <strong>de</strong> Dosificación <strong>de</strong> Bureta <strong>para</strong> la<br />

calibración <strong>de</strong> la bureta.<br />

10011512 Sensor <strong>de</strong> nivel <strong>para</strong> tanque <strong>de</strong> residuos<br />

10011513 Sensor <strong>de</strong> nivel <strong>para</strong> tanque <strong>de</strong> reactivos<br />

60032042 Tanque 20 l (álcali/agua/residuos) sin sensores <strong>de</strong><br />

nivel<br />

60032043 Kit <strong>de</strong> sensor <strong>de</strong> nivel <strong>para</strong> residuos<br />

60032044 Kit <strong>de</strong> sensor <strong>de</strong> nivel <strong>para</strong> reactivos<br />

60030343 Adaptador <strong>para</strong> tubos Büchi<br />

10000897 Dispositivo <strong>para</strong> manejar tubos <strong>de</strong> digestión<br />

Requisitos <strong>de</strong> instalación:<br />

Fuente <strong>de</strong> alimentación: 200 - 240 V, 50 - 60 Hz<br />

Variación tolerable tensión: ± 10 %<br />

Consumo eléctrico: 2.200 W<br />

Consumo <strong>de</strong> agua: 2 l/min a temperatura <strong>de</strong> agua <strong>de</strong> 30ºC<br />

(sólo durante <strong>de</strong>stilación) 1 l/min a temperatura <strong>de</strong> agua <strong>de</strong> 15 ºC<br />

Temperatura ambiente: máx. 40°C<br />

Humedad ambiente: máx. 80 % relativa<br />

Drenaje: Sólo <strong>para</strong> agua <strong>de</strong> refrigeración<br />

Peso neto:<br />

Kjeltec 8400 35 kg<br />

Muestreador Kjeltec 8420 71 kg<br />

Muestreador Kjeltec 8460 89 kg<br />

Dimensiones (A x P x Al):<br />

Kjeltec 8400 480 × 580 × 690 mm<br />

Muestreador Kjeltec 8420 645 × 840 × 900 mm<br />

Muestreador Kjeltec 8460 1000 × 800 × 900 mm<br />

P/N 1026222, Edición 1 ES, Enero 2009


The Mill collection<br />

Introduction<br />

Good results starts with sample pre<strong>para</strong>tion.<br />

Errors caused by analytical instruments are<br />

very small compared to the errors associated with<br />

sample pre<strong>para</strong>tion. Badly prepared samples will<br />

automatically result in large analytical errors.<br />

The laboratory sample mill is an important but<br />

often overlooked link in the chain of analysis; so<br />

important that at FOSS Tecator we regard it as an<br />

integral part of the analytical system.<br />

We have therefore <strong>de</strong>veloped mills of our own to<br />

assure the best analytical results. They are convenient<br />

and safe to use and they cover a broad range<br />

of grinding applications, including pre<strong>para</strong>tion for<br />

both traditional wet chemistry and NIR/NIT analyses,<br />

with assured high repeatability and reproducibility.<br />

General <strong>de</strong>scription<br />

This Mill collection fol<strong>de</strong>r presents high quality<br />

products that can ensure reliability and reproducibility<br />

of the analysis.<br />

The Cemotec is optimized for solid samples<br />

with a high moisture content, and the Cyclotec<br />

Dedicated Analytical Solutions<br />

Mill Collection<br />

for dry samples that require a uniform particle<br />

size. The Knifetec is suitable for small (100 ml)<br />

samples of dry, moist or wet materials, and the<br />

robust Homogenizer for larger (0.2-2.5 kg) samples<br />

with a high fat or oil content.<br />

Various accessories and consumables are available<br />

to make routine sample pre<strong>para</strong>tion simple.<br />

They inclu<strong>de</strong> a range of sample bottles, grinding<br />

rings, bla<strong>de</strong>s and impellers.<br />

Sample pre<strong>para</strong>tion is an important step in all<br />

analytical procedures. It is for example crucial to<br />

grind properly to obtain the highest quality of the<br />

analytical results.<br />

Analytical errors are more easily reduced in the<br />

sample pre<strong>para</strong>tion step than in any of the subsequent<br />

steps of the analysis.<br />

All samples should be prepared un<strong>de</strong>r the same<br />

conditions.<br />

On the following pages we show how our Mill<br />

collection can crush, grind, mix and homogenize<br />

dry samples to a consistency suitable for chemical<br />

analysis.


Cemotec 1090 Sample Mill<br />

Sample grinding without moisture loss.<br />

Cemotec Mill<br />

Cemotec Accessories<br />

Features:<br />

• Reliable classic working principle<br />

• Adjustable particle size<br />

• Low noise level<br />

Benefits:<br />

• No loss of moisture<br />

• Officially approved by the Swedish National Board<br />

of Agriculture for sample pre<strong>para</strong>tion prior to moisture<br />

analysis<br />

• Low maintenance <strong>de</strong>mand<br />

Description:<br />

The Cemotec Sample Mill is specially <strong>de</strong>signed to<br />

grind grain and seed samples without losing any of the<br />

moisture content. It is however an excellent mill for all<br />

types of sample pre<strong>para</strong>tion where the requirements<br />

for fineness and uniformity of particle size are mo<strong>de</strong>rate.<br />

The Cemotec works on the tried-and-true principle<br />

of grinding between two discs, one stationary and<br />

one turning. The sample is introduced at the centre of<br />

the stationary disc and is crushed between the discs.<br />

The distance between the discs is easily adjusted by a<br />

graduated knob to control the fineness of the grist.<br />

The Cemotec works silently and effectively at relatively<br />

low speed. The rate of grinding is about 3 grams<br />

per second. Low speed means low noise, and dust is<br />

effectively contained by the seal between the outlet<br />

and the sample container.


Features:<br />

• High grinding speed, 4 grams per second<br />

• Adjustable particle size<br />

• Low noise level (75 dBA)<br />

Benefits:<br />

• No thermal <strong>de</strong>gradation of the sample<br />

• Uniform particle size distribution<br />

• Easy handling of samples<br />

• High operator safety<br />

• Low maintenance <strong>de</strong>mand<br />

• Recommen<strong>de</strong>d by the Canadian Grain Commission<br />

prior to NIR analysis<br />

• Approved by AOAC prior to NIR analysis (4.2.10<br />

16th Ed.)<br />

Description:<br />

The Cyclotec Sample Mill is <strong>de</strong>signed for rapid,<br />

uniform grinding of a wi<strong>de</strong> variety of feeds, grains,<br />

leaves, etc. and also for grinding of chemicals, pharmaceuticals<br />

and similar products. Recovery of the<br />

sample is complete.<br />

Through its unique <strong>de</strong>sign the Cyclotec grinds<br />

samples by a high speed action. This action rolls the<br />

sample against the inner circumference of a durable<br />

grinding surface and then passes it through a fine<br />

mesh screen.<br />

The high volume air flow provi<strong>de</strong>s self cleaning<br />

action and minimum temperature rise; whole series of<br />

samples can be ground with minimal cross contamination<br />

and without cleanout between samples. Thermal<br />

<strong>de</strong>gradation is minimized to provi<strong>de</strong> more accurate<br />

results.<br />

The Cyclotec offers a very rapid and convenient<br />

solution to accurate sample pre<strong>para</strong>tion for a variety of<br />

analytical techniques, e.g. Kjeldahl, Infrared Reflectance,<br />

Direct Distillation, Cru<strong>de</strong> Fibre and Extraction.<br />

Cyclotec 1093 Sample Mill<br />

Rapid sample pre<strong>para</strong>tion for general laboratory analysis.<br />

Cyclotec Mill<br />

Cyclotec filled with hol<strong>de</strong>r for 500 ml sample bottle


2094 and 2096 Homogenizers<br />

Rapid maceration and homogenization of a variety of samples.<br />

Homogenizers<br />

The cutters<br />

Features:<br />

• Powerful cutting action at one or two speeds: 1500<br />

or 1500/3000 rpm<br />

• Sample size from 0.2 to 2.5 kg<br />

• A variety of angled knives for different sample types<br />

• Knives and bowl in stainless steel<br />

• Safety switch<br />

• Sample pre<strong>para</strong>tion of meat products according to<br />

AOAC 983.18<br />

Benefits:<br />

• Rapid and reproducible homogenization<br />

• Easy to clean<br />

• Robust construction<br />

Description:<br />

The 2094 and 2096 Homogenizers are <strong>de</strong>signed for<br />

macerating and homogenizing of a variety of highmoisture,<br />

high-fat and fibrous samples. Application<br />

examples inclu<strong>de</strong>: size reduction of forage and dry<br />

food and chemical products; homogenization of meat,<br />

fish, fruit, vegetables, prepared foods (such as pizza,<br />

meat pies and frozen meals) and chemical and pharmaceutical<br />

formulations.<br />

The Homogenizers allows frozen food samples to<br />

be homogenized in a short period of time, providing<br />

more accurate analyses of unstable constituents such<br />

as vitamins.<br />

A reproducible <strong>de</strong>gree of homogenization is achieved<br />

by the mixing action obtained by the angled knives.<br />

Homogenization is accomplished through the high<br />

speed combined with a powerful cutting action.<br />

Angled knife bla<strong>de</strong>s produce a vertical flow within the<br />

batch and facilitate rapid and thorough homogenization.<br />

Complete homogenization is normally achieved<br />

in 20 to 60 seconds.<br />

A magnetic safety switch prevents the 2094 and<br />

2096 Homogenizers from being operated without the<br />

transparent cover in the locked position.<br />

The 2094 and 2096 Homogenizers comes with a<br />

multipurpose micro-teeth cutter. For additional convenience<br />

extra stainless steel bowls and smooth bla<strong>de</strong><br />

cutters are available for both Homogenizers. For the<br />

2096 Homogenizer a scalloped cutter is also available.


Features:<br />

• 20 000 rpm rotor bla<strong>de</strong> for rapid grinding<br />

• Timer controlled<br />

• Sample size up to 100 ml initial volume<br />

• Water cooled<br />

• Safety switch stops rotor in less than 1 second<br />

Benefits:<br />

•<br />

•<br />

•<br />

1095 Knifetec Sample Mill<br />

Rapid sample pre<strong>para</strong>tion of high-fat, high-moisture and fibrous samples.<br />

Integral tilting system, fully removable lid and rotor<br />

bla<strong>de</strong> to facilitate cleaning<br />

Chamber cooling option reduces adhesion of sample<br />

to the wall of the grin<strong>de</strong>r<br />

No heat generated, making samples suitable for<br />

moisture analysis<br />

Description:<br />

The 1095 Knifetec Sample Mill is <strong>de</strong>signed for<br />

the pre<strong>para</strong>tion of high fat, high moisture and fibrous<br />

samples prior to analysis. Oilseeds, prepared foods,<br />

meat products, fruit, vegetables, grains, seeds and feed<br />

samples are examples of suitable sample types.<br />

The high speed rotor bla<strong>de</strong> and timer control ensure<br />

very fast and reproducible sample pre<strong>para</strong>tion time<br />

after time. The normal time to prepare samples is from<br />

two to ten seconds.<br />

A safety switch located in the lid prevents acci<strong>de</strong>ntal<br />

operation of the mill with the lid removed.<br />

The Knifetec is equipped with a grinding chamber<br />

cooling feature which enables it to be connected to<br />

a cold water tap or other laboratory chilling <strong>de</strong>vices.<br />

Samples containing high levels of fat have a ten<strong>de</strong>ncy<br />

to stick to the wall of the chamber as the fat softens<br />

during grinding, preventing a<strong>de</strong>quate homogenisation.<br />

Fibrous samples may generate heat due to friction.<br />

Utilizing the cooling option overcomes both these<br />

problems, ensuring satisfactory sample pre<strong>para</strong>tion.<br />

The fully removable lid, the stainless steel chamber<br />

and the removable rotor bla<strong>de</strong> of the Knifetec simplify<br />

sample removal and cleaning between samples.<br />

This saves a consi<strong>de</strong>rable amount of time compared<br />

to other techniques. An integral tilting system also<br />

simplifies emptying and cleaning.<br />

The <strong>de</strong>sign of the 1095 Knifetec ensures rapid,<br />

reproducible and safe pre<strong>para</strong>tion.<br />

Knifetec<br />

The sample tray and rotor bla<strong>de</strong>s


Or<strong>de</strong>ring information:<br />

Cemotec 1090 Sample Mill:<br />

1090-001 Cemotec 1090 Sample Mill complete with<br />

har<strong>de</strong>ned Grinding Discs, disposable Sample<br />

Bottles (20), Allen Keys 4 and 5 mm, Hopper<br />

with cover, Users’ Manual, 200-230 V, 50-60 Hz<br />

1090-002 Same as above but for 115 V, 50-60 Hz<br />

Accessories<br />

10003923 Disposable Sample Bottles (150 ml) of polypropylene<br />

with snap-on lid 100/pkg<br />

10003924 Disposable Sample Bottles (150 ml) of polypropylene<br />

with snap-on lid 500/pkg<br />

10003965 Grinding Discs (1 pair)<br />

10003922 Seal for Sample Bottle<br />

Cyclotec 1093 Sample Mill<br />

1093-001 Cyclotec 1093 Sample Mill complete with<br />

Sample Bottles (125 ml) with snap-on lid (2),<br />

screens 0.5 and 1.0 mm, Allen Keys 4 and 6 mm,<br />

Seal for Grinding Chamber, Paper Bag for Dust<br />

Collection, Seal for Sample Bottle, Users’<br />

Manual, 200-230 V, 50 Hz<br />

1093-002 Same as above but for 115 V 60 Hz<br />

1093-003 Same as above but for 200-230 V 60 Hz<br />

1093-004 Same as above but for 115 V 50 Hz<br />

Accessories<br />

10000893 Sample Bottles, dark glass for UV protection,<br />

125 ml, case of 104<br />

10003679 Sample Bottles, dark glass for UV protection,<br />

125 ml, case of 52<br />

15220023 Lid for Sample Bottles<br />

10002485 Large Inlet/Forage Assembly Kit<br />

10002488 Dust Collection with external connection<br />

10002537 Paper Bags for Dust Collection, pack of 10<br />

10002000 Dust Filter Pad<br />

10014484 Screen 0.3 mm (use together with 1 or 2 mm<br />

Screen)<br />

10000820 Screen 0.5 mm<br />

10005864 Screen 0.8 mm<br />

10001989 Screen 1.0 mm<br />

10002715 Screen 2.0 mm<br />

10001990 Seal for Sample Bottle<br />

10001992 Seal for Grinding Chamber<br />

10001993 Seal for Dust Filter Cover<br />

10008180 Seal Kit<br />

10001991 Impeller, Standard<br />

10002666 Impeller, Nickel-plated for mineral analysis<br />

10009833 Hol<strong>de</strong>r for 500 ml sample bottle<br />

10013478 Sample bottle 500 ml with lid, 1 pcs<br />

10004463 Grinding Ring, ma<strong>de</strong> of tungsten carbi<strong>de</strong> -<br />

Standard<br />

10013810 Grinding Ring for Hard sample<br />

10006680 Grinding Ring Heavy Metals 3/set<br />

*Or<strong>de</strong>ring information: Use the above specified Cat. Nos. together with the text.<br />

Homogenizer 2094<br />

2094-001 Homogenizer complete with stainless steel bowl<br />

(3.5 l), multipurpose cutter with microteeth<br />

bla<strong>de</strong>s, transparent lid and User’s Manual,<br />

1 500 rpm, 1 × 230 V, 50 Hz<br />

2094-002 Same as above but for 1 × 115 V, 60 Hz<br />

Accessories<br />

19000660 Stainless steel bowl. 3,5 l<br />

19000662 Transparent lid<br />

19000654 Cutter with smooth bla<strong>de</strong>s<br />

19000659 Cutter with microteeth bla<strong>de</strong>s<br />

19000634 Grindstone for bla<strong>de</strong>s<br />

Homogenizer 2096<br />

2096-001 Homogenizer complete with stainless steel bowl<br />

(5.5 l), multipurpose cutter with microteeth<br />

bla<strong>de</strong>s, transparent lid with integrated scraper and<br />

Users’s Manual, 1 500 / 3 000 rpm, 3 × 400 V,<br />

50 Hz<br />

2096-002 Same as above but only 1 500 rpm for 1-phase,<br />

115 V, 60 Hz<br />

Accessories<br />

19000605 Stainless steel bowl. 5,5 l<br />

19000655 Transparent lid with scraper<br />

19000656 Cutter with smooth bla<strong>de</strong>s<br />

19000657 Cutter with scalloped bla<strong>de</strong>s<br />

19000658 Cutter with microteeth bla<strong>de</strong>s<br />

19000634 Grindstone for bla<strong>de</strong>s<br />

Knifetec 1095 Sample Mill<br />

1095-001 Knifetec Sample Mill complete with rotor bla<strong>de</strong>,<br />

PVC tubing 4m, tubing clamp, Users’ Manual,<br />

230 V, 50-60 Hz<br />

1095-002 Same as above and also including Transformer<br />

for 115 V operation, 50-60 Hz<br />

Accessories<br />

10005980 Rotor bla<strong>de</strong> standard, complete<br />

10008651 Rotor bla<strong>de</strong> with sharp knives complete<br />

10013135 Rotor bla<strong>de</strong> for small volume<br />

10013136 Rotor bla<strong>de</strong> for pellets<br />

10005960 Distance for Rotor bla<strong>de</strong><br />

10003923 Disposable Sample Bottles (150 ml) of polypropylene<br />

with snap-on lid 100/set<br />

10003924 Disposable Sample Bottles (150 ml) of polypropylene<br />

with snap-on lid 500/set<br />

10008467 Stainless steel tray


Installation requirements:<br />

Cemotec 1090 Sample Mill<br />

Power supply: 200-230 V, 50-60 Hz<br />

115 V, 50-60 Hz<br />

Power consumption: 600 W<br />

Net weight: 18 kg<br />

Dimensions, L × D × H: 220 × 400 × 400 mm<br />

Rotor speed, grinding disc 3 000 rpm<br />

Cyclotec 1093 Sample Mill<br />

Power supply: 200-230 V 50 Hz<br />

115 V 60 Hz<br />

200-230 V 60 Hz<br />

115 V 50 Hz<br />

Power consumption: 600 W<br />

Net weight: 18 kg<br />

Dimensions, L × D × H: 220 × 300 × 400 mm<br />

Rotor speed, impeller 10 000 rpm<br />

Homogenizer 2094<br />

Power supply: 230 V 50 Hz 1-phase<br />

115 V 60 Hz 1-phase<br />

Power consumption: 500 W<br />

Net weight: 15 kg<br />

Capacity: 3,5 l bowl. Do not exceed<br />

1,5 l liquid content<br />

Rotor speed: 1 500 rpm<br />

Dimensions, L × D × H: 250 × 410 × 300 mm<br />

Homogenizer 2096<br />

Power supply: 400 V 50 Hz 3-phase<br />

115 V 60 Hz 1-phase<br />

Power consumption: 750 W 1-phase /<br />

1400 W 3-phase<br />

Net weight: 25,5 kg<br />

Capacity: 5,5 l bowl. Do not exceed<br />

2,5 l liquid content<br />

Rotor speed: 1 500 rpm (1-phase) /<br />

1 500 & 3 000 rpm<br />

(3-phase)<br />

Dimensions, L × D × H: 270 × 460 × 400 mm<br />

Knifetec 1095 Sample Mill<br />

Power supply: 230 V 50-60 Hz<br />

incl Transformer 115/230V<br />

Power consumption: 120 W<br />

Net weight: 7.5 kg<br />

Dimensions, L × D × H: 190 × 290 × 250 mm<br />

Rotor speed: 20 000 rpm<br />

Water supply: 2 l/min, 8-10°C<br />

Performance data:<br />

Feature Cemotec Cyclotec Homogenizer Knifetec<br />

Sample Type Dry samples prior to Dry samples prior to High-moisture, high- High-moisture, high-<br />

moisture analysis, up to wet chemistry or IR fat and fibrous samples fat and fibrous samples<br />

20 % moisture and/or analysis, up to 15%<br />

20% fat<br />

moisture and/or fat<br />

content up to 20%<br />

Applications Grains, seeds, feed, Grains, seeds, cereals, Forage, dry food, meat, Oilseeds, prepared<br />

beans, dry granular forage, feed, leaves, fish, vegetables, pre- foods, meat products,<br />

foods, fertilizer, tablets tablets, tobacco, lime, pared foods, chemical fruit, vegetables,<br />

coal<br />

and pharmaceutical<br />

formulations<br />

grains, seeds, and feed<br />

Sample Size Up to 14 mm ∅ Up to 10 mm, large 0.2 - 2.5 kg Maximum 100 ml (50<br />

inlet up to 40 mm<br />

- 150 g)<br />

Grinding Principle Two discs, one rotating<br />

one stationary<br />

Turbine and sieve Rotor knives Rotor bla<strong>de</strong><br />

Grinding Rate/Time Appr. 3 g/s Appr. 4 g/s 20 to 60 s 2 to 10 seconds<br />

Grinding Speed Grinding disc 3 000 Impeller 10 000 rpm Bla<strong>de</strong> 1 500 or 1 500 / Bla<strong>de</strong> 20 000 rpm<br />

rpm<br />

3 000 rpm<br />

Particle Size Coarse grist Fine and uniform grist<br />

with 0.5 mm screen:<br />

max 0.45 mm with 1.0<br />

mm screen: max 0.75<br />

mm<br />

Depending on sample Depending on sample<br />

Timer No No No Yes<br />

Safety Microswitch Microswitch Magnetic switch Microswitch<br />

Cleaning Low cross contamina- Low cross contamina- Manual Manual<br />

tiontion


Application overview<br />

Application Cemotec Cyclotec Homogenizer Knifetec<br />

Grains of wheat, oats,<br />

barley, rye<br />

+++ +++ + +++<br />

Soya beans + + + +++<br />

Rapeseed + + + +++<br />

Feed pellets +++ +++ + ++<br />

Hay/Straw ++ +<br />

Vegetables/Fruit +++ +<br />

Meat ++<br />

Meat products +++ +<br />

Mixed food +++ +<br />

Subsequent analysis<br />

Application<br />

Reference methods<br />

Cemotec Cyclotec Homogenizer Knifetec<br />

Protein +++ +++ +++ +++<br />

Fat low<br />

+++ +++ ++<br />

+++<br />

Fat high<br />

+++<br />

+++<br />

Fibre cru<strong>de</strong><br />

Fibre dietary<br />

+++ +++ + ++<br />

Moisture low & low fat<br />

+++<br />

+++<br />

++<br />

Moisture low & high fat<br />

++<br />

+++<br />

Moisture high & low fat<br />

++<br />

+++<br />

+++<br />

Moisture hig & high fat<br />

+++<br />

+++<br />

NIR/NIT + +++ +++ +++<br />

+++ excellent ++ very good + good<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

P/N 9999 0730E, Issue 2 GB, Nov 2005


Tecator Digestion Unit Auto Lift 20 together with the Scrubber, for<br />

fully unatten<strong>de</strong>d operation.<br />

Features and benefits:<br />

Tecator Digestion units, with integrated programmable controllers,<br />

can be combined with a range of accessories offering:<br />

• fully automated digestion with user interface adapting to<br />

actual product configuration<br />

• convenient, safe and flexible operation<br />

• GLP-support through two way PC communication<br />

• economy of chemicals, energy, labour, space and time<br />

• efficient fume containment through optional exhaust<br />

• efficient fume removal through optional scrubber<br />

The systems, with extensive application support, are compatible<br />

with Kjeltec Distilling Units.<br />

General Description:<br />

The products <strong>de</strong>scribed in this brochure can be combined to<br />

match individual needs, from units capable of handling just a<br />

few samples a day up to fully automated systems for high sample<br />

throughput. Three configurations; Auto Lift, Auto Rack,<br />

and Basic; are available for either 250 ml or 100 ml digestion<br />

tubes; which must be specified when or<strong>de</strong>ring; <strong>de</strong>pendant on<br />

the application required.<br />

A Digestion System is based on a Digestion Unit and tube<br />

rack with capacity for either eight or twenty tubes. For most<br />

Kjeldahl digestions straight 250 ml tubes are recommen<strong>de</strong>d.<br />

To comply with GLP and Health & Safety requirements we<br />

recommend that all Digestion Units are used with an Exhaust<br />

Manifold or Reflux Head, and are located in a fume cupboard.<br />

An optional Scrubber Unit creates a fully integrated system.<br />

Dedicated Analytical Solutions<br />

Tecator Digestion Systems<br />

Auto Lift versions, with exhaust docking facility, allow fully<br />

automated unatten<strong>de</strong>d operation contributing to safety and convenience<br />

by eliminating handling of hot chemicals and saving<br />

valuable bench space. Auto Rack versions allow automated<br />

digestions but require manual placement of Tube Rack and<br />

Exhaust Manifold which are stored above the Digestion Unit<br />

in a similar position to the Auto Lift. All Auto mo<strong>de</strong>ls have an<br />

integrated programmer which precisely controls temperature(s)<br />

and timing together with connected components. The analysis<br />

cycle is clearly monitored on the graphical display. Auto mo<strong>de</strong>ls<br />

can be connected to a PC for data logging and downloading<br />

of standard, and user <strong>de</strong>fined, applications. The programmer<br />

has various password protected access levels to prevent unauthorised<br />

modification and comply with accreditation procedures.<br />

Basic versions have built in, user <strong>de</strong>finable, temperature<br />

and time control clearly viewed on the display.<br />

Auto Rack versions can be upgra<strong>de</strong>d to Auto Lift systems to<br />

spread the investment across fiscal periods.<br />

The Basic version can be fitted with a rack system at any<br />

time to save valuable bench space.<br />

Various accessories are available to make routine analysis<br />

safe and simple. They inclu<strong>de</strong> a range of test tubes, tube racks,<br />

retainer plates for washing, fume removal systems, boiling<br />

rods and catalyst tablets.<br />

Digestion system products and accessories are <strong>de</strong>scribed in<br />

more <strong>de</strong>tail on the following pages.


All Digestion Systems are based on one of the “four” Digestion Units for either 250 ml or 100 ml tubes*.<br />

* Tube volume to be specified when or<strong>de</strong>ring your digestion unit.<br />

Digestion Units<br />

The Digestion Units are insulated to minimise heat transfer to<br />

the surroundings and allow fast, even heating, thus giving good<br />

working conditions as well as saving energy. They are <strong>de</strong>signed<br />

for batches of either eight or twenty test tubes with three different<br />

levels of control.<br />

The Auto versions have an integrated all activity controller,<br />

that adapts to the actual product configuration and is programmable<br />

using the software supplied. When a Lift or Scrubber<br />

Unit is connected they are controlled by the selected application<br />

program, which is stored in the Digestion Unit memory, allowing<br />

fully unatten<strong>de</strong>d operation.<br />

The Basic versions have a built in, user <strong>de</strong>finable, time and<br />

temperature controller and display.<br />

Software for Auto Lift and Auto Rack systems<br />

There are two se<strong>para</strong>te software systems in Auto versions. The<br />

embed<strong>de</strong>d software controls all necessary functions of the digestion<br />

system on a routine basis. The PC Application software,<br />

<strong>de</strong>livered on CD, is system management software which enables<br />

<strong>de</strong>fault values to be modified according to the needs of the authorised<br />

user. To process different type of samples a wi<strong>de</strong> range<br />

of Tecator applications can be downloa<strong>de</strong>d from the database<br />

inclu<strong>de</strong>d on the CD. Up to 254 Applications can be stored in the<br />

digestion unit at any one time, of which half can be standard<br />

Tecator format and half can be user <strong>de</strong>fined. Each application<br />

can control up to 23 steps including all Temperature; ramp and<br />

time; Lift and Scrubber steps.<br />

The software supports Good Laboratory Practice (GLP)<br />

routines and accreditation procedures. Data for date, time,<br />

temperature, application used, operator, batch number, and ID<br />

number are constantly logged. The 32 most recent Data Logs<br />

can be stored in the Digestion Unit. All this information can be<br />

transferred to a PC for archiving and generation of up to seven<br />

different reports. Original Tecator Applications cannot be<br />

changed. They can be adapted and saved as different files or the<br />

user can <strong>de</strong>sign their own applications. To prevent unauthorised<br />

changes, and comply with GLP routines, the software is password<br />

protected at different authority levels.<br />

Audible alerts<br />

Audible ‘’ready’’ or ‘’cycle over’’ alerts advise the user when the<br />

digestion application is completed<br />

Audible ‘’alarm’’ alerts advise the user when errors/interruptions<br />

occur within the running application program<br />

Alerts can be adjusted High, Low or Off.<br />

Power failure or interruption of power supply<br />

In the event of power failure the digestion unit operation is automatically<br />

handled in the safest way. If the failure or interruption<br />

occurs at any time up to or during preheating, before digestion<br />

has started, the cycle will continue when power is restored. Following<br />

a power failure or interruption, after the digestion cycle<br />

has started, the unit stops heating immediately and the Lift goes<br />

to the cooling position with exhaust in place, upon restoration of<br />

power. This complies with GLP and Health & Safety routines.<br />

These interruptions will be recor<strong>de</strong>d in the data logging function.<br />

Communication with PC<br />

The PC Application software has two way communication<br />

with the Digestion Unit via the serial RS232 cable supplied as<br />

standard. Alternatively communication can be achieved through<br />

Bluetooth TDK blu2i modules, or equivalent, available from your<br />

computer supplier.<br />

Language versions<br />

The software is available in the following languages:-<br />

Chinese (simplified), Dutch, English, French, German, Italian,<br />

Japanese, Korean, Polish, Russian, Spanish, and Swedish. Other<br />

languages can be accommodated in co-operation with your local<br />

supplier.<br />

Auto Lift Systems<br />

Auto Lift systems facilitate highly automated procedures,<br />

eliminating heavy and risky handling of hot chemicals. Valuable<br />

bench space is saved, as the Tube Rack and Exhaust Manifold are<br />

positioned above the Digestion Unit.<br />

A Tube Rack with 8 or 20 tubes is placed in the Lift. The application<br />

selected then fully controls the entire process. The Exhaust<br />

Manifold docks automatically with the Tube Rack as they<br />

move down into the preheated Digestion Unit; and the Scrubber<br />

Unit, if connected, starts.<br />

The scrubber capacity is automatically adjusted during the<br />

cycle to contain fumes and minimise acid losses. When the<br />

digestion is completed the combined Tube Rack and Exhaust<br />

Manifold move to the cooling position with the Scrubber Unit<br />

still running until no further fumes are evolved. An adjustable<br />

audible signal in the Digestion Unit indicates “cycle over”.<br />

To avoid any spillage a drip tray, supplied with the Exhaust<br />

Manifold, is inserted un<strong>de</strong>rneath the Exhaust Manifold when it is<br />

se<strong>para</strong>ted from the Tube Rack after cooling.


The Lift eliminates heavy handling. The Rack System saves space.<br />

Auto Rack Systems<br />

When an Auto Rack system is used in place of an Auto Lift<br />

system the typical procedure is as with the Auto Lift system with<br />

the exception that the combining/se<strong>para</strong>ting of Tube Rack and<br />

Exhaust Manifold and the movement to the cooling position is<br />

performed manually when the signal is heard. The application<br />

selected controls all other functions as with the Auto Lift system.<br />

Basic Systems<br />

The temperature and time for the digestion are selected on the<br />

front panel. All other procedures, including operation of a connected<br />

scrubber, are then performed by the operator once the<br />

digestion unit has reached the selected temperature.<br />

Fume Removal and Containment Systems<br />

Exhaust Manifolds<br />

Many digestion applications, e.g. Kjeldahl, produce fumes that<br />

are unpleasant and corrosive. Exhaust Manifolds <strong>de</strong>signed for<br />

each Digestion Unit facilitate fume removal and containment and<br />

are strongly recommen<strong>de</strong>d for use with all digestion procedures.<br />

The cost of replacement of a fume cupboard which has been<br />

corro<strong>de</strong>d by inefficient fume handling is very much greater than<br />

the relatively low cost of an approved exhaust. Whilst many users<br />

choose to operate integrated systems in the open laboratory, we<br />

strongly recommend the use of both exhaust systems and fume<br />

cupboards for these operations. This is simply Good Laboratory<br />

Practice (GLP) and avoids conflict with local Health & Safety<br />

(H&S) requirements.<br />

The Exhaust Manifolds should be connected to the water aspirator<br />

supplied, or to a suitable Scrubber Unit.<br />

Scrubber Unit<br />

Where water is a scarce or expensive commodity, or simply when<br />

a higher level of automation is <strong>de</strong>sired, the water aspirator should<br />

be replaced with an efficient Scrubber Unit. Exhaust Manifolds<br />

and Scrubber Units which require an external water source are<br />

subject to variation in vacuum efficiency due to fluctuations in<br />

local water pressure.<br />

The compact bench top Tecator Scrubber Unit is self contained<br />

and is therefore unaffected by water supply issues. During<br />

digestion moist, acidic fumes from the connected exhaust are<br />

drawn through the Scrubber Unit. Acid vapours are first con<strong>de</strong>nsed<br />

and diluted in a large acid trap. Any residual fumes are<br />

collected, washed and neutralised before passing through a second<br />

small acid trap which protects the vacuum pump in the event<br />

that the scrubbing agents are exhausted. The cleaned air is then<br />

There is an Exhaust for each Digestion Unit.<br />

The Scrubber neutralizes the corrosive fumes.


There are Reflux Heads for 250 ml Digestion Units.<br />

Select the correct tube for your application.<br />

Kjeltabs, salt and catalyst in tablet form.<br />

vented via a tubing outlet. In the interest of GLP and H&S this<br />

venting tube should be directed into a fume cupboard. When the<br />

Scrubber Unit is connected to an Auto Lift or Auto Rack system<br />

the program will fully control the function including switching<br />

from high to low aspiration settings.<br />

Reflux Heads<br />

When a digestion unit is used for reflux chemistries, such as<br />

Chemical Oxygen Demand (COD), a Reflux Head connected to a<br />

suitable cold water supply should be used in place of the Exhaust<br />

Manifold. Tecator Reflux Heads are conveniently mounted in<br />

handling racks which match the tube rack in the Digestion Unit.<br />

The ball jointed con<strong>de</strong>nsers are <strong>de</strong>signed for use with ball jointed<br />

digestion tubes. The Reflux Heads are compatible with Auto Lift,<br />

Auto Rack and Basic systems.<br />

Digestion Tubes<br />

To suit different applications and manual/automatic handling<br />

systems, tubes for the Digestion Units are available in two sizes<br />

(250 ml and 100 ml) and three shapes. Straight si<strong>de</strong>d tubes<br />

are recommen<strong>de</strong>d for the majority of digestion applications.<br />

Volumetric tubes with a constriction at the neck are recommen<strong>de</strong>d<br />

for applications where the digestate requires dilution to<br />

a fixed volume before analyses such as FIA, SFA, and AA etc.<br />

Ball jointed tubes, available in 250 ml size only, are required for<br />

reflux chemistries using the reflux con<strong>de</strong>nser heads. The larger<br />

250 ml straight si<strong>de</strong>d tubes are recommen<strong>de</strong>d for Kjeldahl, as<br />

they can hold samples of wi<strong>de</strong>ly varying sizes. Samples of heterogeneous<br />

material often need to be fairly large to ensure that<br />

they are representative. There is no lower limit of sample size in<br />

the 250 ml tubes; they simply allow greater flexibility for most<br />

type of samples.<br />

The 100 ml straight si<strong>de</strong>d tubes can be used where the material<br />

is homogeneous and small samples are fully representative or<br />

where they are specified by the approved method.<br />

Kjeltabs<br />

A salt, to increase the boiling point, and a catalyst, to increase<br />

the speed of reaction, are used for Kjeldahl digestions. As a convenient<br />

way to obtain the correct dosage, FOSS supplies Kjeltabs<br />

– tablets containing Potassium Sulphate and a catalyst (Copper,<br />

Selenium, or Copper/Titanium). Digestion time may <strong>de</strong>pend on<br />

the catalyst used. Historically Mercury has been used as the most<br />

efficient catalyst. Today it has been replaced largely by Copper,<br />

or other metals, due to safety and environmental consi<strong>de</strong>rations.<br />

Kjeltabs are supplied in two sizes; 3.5 g and 1.5 g. One or more<br />

tablets are combined with the acid to obtain an optimal salt/acid<br />

ratio. The smaller 1.5 g size is <strong>de</strong>signed for the 100 ml tubes.


Or<strong>de</strong>ring information:*<br />

Digestion Units:<br />

All mo<strong>de</strong>ls are <strong>de</strong>livered with a Tube Rack with integrated<br />

heat shields. They should always be combined with a matching<br />

Exhaust Manifold or Reflux Head and Test Tubes – 100 or 250<br />

ml volume.<br />

For Kjeldahl digestions the 2501-001 Scrubber Unit should<br />

always be consi<strong>de</strong>red for safe and efficient neutralisation of<br />

corrosive gases. This replaces the water aspirator, supplied as<br />

standard.<br />

Auto Lift mo<strong>de</strong>ls, complete with 2515-001 Lift and integrated<br />

controller for fully automatic control of digestion applications,<br />

including the operation of the Lift and a 2501-001 Scrubber<br />

Unit (optional extra). The digestion unit can be connected to<br />

PC for application updates, traceability and logging purposes.<br />

NOTE. An appropriate exhaust manifold or reflux head<br />

MUST be ad<strong>de</strong>d for an automatic system.<br />

Auto Rack mo<strong>de</strong>ls, complete with 2515-011 Rack and<br />

integrated controller for full control of digestion applications,<br />

including the operation of a 2501-001 Scrubber (optional extra).<br />

The digestion unit can be connected to PC for application<br />

updates, traceability and logging purposes.<br />

Can be upgra<strong>de</strong>d to an Auto Lift system by addition of the<br />

2515-001 Lift.<br />

NOTE. An appropriate exhaust manifold or reflux head<br />

MUST be ad<strong>de</strong>d for an automatic system.<br />

Basic mo<strong>de</strong>ls, with built in electronics for control of temperature<br />

and time only.<br />

Can not be upgra<strong>de</strong>d to Auto mo<strong>de</strong>ls but are compatible with<br />

2515-011 Rack.<br />

Tecator Auto Digestion Units<br />

Auto mo<strong>de</strong>ls with integrated all activity controller and graphical<br />

display.<br />

Versions for 250 ml tubes<br />

2508-001 Tecator Digestion Unit 8 – Auto Lift system,<br />

250 ml tubes, 230 V 50-60 Hz<br />

2508-002 Same as above but for 110 V 50-60 Hz<br />

2508-011 Tecator Digestion Unit 8 – Auto Rack system,<br />

250 ml tubes, 230 V 50-60 Hz<br />

2508-012 Same as above but for 110 V 50-60 Hz<br />

2520-001 Tecator Digestion Unit 20 – Auto Lift system,<br />

250 ml tubes, 230 V 50-60 Hz<br />

2520-011 Tecator Digestion Unit 20 – Auto Rack system,<br />

250 ml tubes, 230 V 50-60 Hz<br />

Versions for 100 ml tubes<br />

2508-006 Tecator Digestion Unit 8 – Auto Lift system,<br />

100 ml tubes, 230 V 50-60 Hz<br />

2508-007 Same as above but for 110 V 50-60 Hz<br />

2508-016 Tecator Digestion Unit 8 – Auto Rack system,<br />

100 ml tubes, 230 V 50-60 Hz<br />

2508-017 Same as above but for 110 V 50-60 Hz<br />

2520-006 Tecator Digestion Unit 20 – Auto Lift system,<br />

100 ml tubes, 230 V 50-60 Hz<br />

2520-016 Tecator Digestion Unit 20 – Auto Rack system,<br />

100 ml tubes, 230 V 50-60 Hz<br />

Tecator Digestion Units<br />

Basic mo<strong>de</strong>ls with built in electronics for control of temperature<br />

and time.<br />

Versions for 250 ml tubes<br />

2508-051 Tecator Digestion Unit 8 – Basic, 250 ml tubes,<br />

230 V 50-60 Hz<br />

2508-052 Same as above but for 110 V 50-60 Hz<br />

2520-051 Tecator Digestion Unit 20 – Basic 250 ml tubes,<br />

230 V 50-60 Hz<br />

Versions for 100 ml tubes<br />

2508-056 Tecator Digestion Unit 8 – Basic, 100 ml tubes,<br />

230 V 50-60 Hz<br />

2508-057 Same as above but for 110 V 50-60 Hz<br />

2520-056 Tecator Digestion Unit 20 – Basic 100 ml tubes,<br />

230 V 50-60 Hz<br />

Fume Removal & Containment Systems<br />

2508-020 Exhaust Manifold for Digestion Units 2508, if 250<br />

ml tubes are used.<br />

Complete with Water Aspirator and Drip Tray.<br />

2508-021 Exhaust Manifold for Digestion Units 2508, if 100<br />

ml tubes are used.<br />

Complete with Water Aspirator and Drip Tray.<br />

2520-020 Exhaust Manifold for Digestion Units 2520, if 250<br />

ml tubes are used.<br />

Complete with Water Aspirator and Drip Tray.<br />

2520-021 Exhaust Manifold for Digestion Units 2520, if 100<br />

ml tubes are used.<br />

Complete with Water Aspirator and Drip Tray.<br />

2501-001 Scrubber Unit 110/230 V 50-60 Hz.<br />

For neutralization of fumes in acid digestions. It<br />

can be combined with any of the Exhaust Manifolds.<br />

Up to 100 samples without changing of<br />

reagent. Fully automatic operation when connected<br />

to an Auto Digestion Unit.<br />

Lift & Rack Systems<br />

2515-001 LIFT for the AUTO version of Digestion Unit<br />

2508 and 2520.<br />

The Application run in the Digestion Unit fully<br />

controls the LIFT.<br />

The Lift can only be connected to Auto version<br />

Digestion Unit.<br />

2515-011 RACK System for all versions of Digestion Unit<br />

2508 and 2520 without LIFT.<br />

Enables manual positioning of components in a<br />

similar way as the Auto Lift.<br />

Reflux con<strong>de</strong>nsers<br />

2508-030 Reflux Head COD Digestion Unit 2508.<br />

Water-cooled Con<strong>de</strong>nsers for 8x250 ml tubes.<br />

2520-030 Reflux Head COD Digestion Unit 2520.<br />

Water-cooled Con<strong>de</strong>nsers for 20x250 ml tubes.<br />

10000254 Reflux Con<strong>de</strong>nser, Air Cooled.<br />

700 mm. With ground joint for 250 ml tubes.


Cont. Or<strong>de</strong>ring information:*<br />

Handling Systems<br />

Digestion Units are <strong>de</strong>livered complete with one Tube Rack.<br />

It may be found convenient to or<strong>de</strong>r extra so that all tubes<br />

normally in use in the laboratory are placed in a rack.<br />

All Tube Racks fit the Kjeltec 2460 Sampler.<br />

10013896 Tube Rack for 8 Digestion Tubes 250 ml.<br />

10013981 Tube Rack for 8 Digestion Tubes 100 ml.<br />

10013895 Tube Rack for 20 Digestion Tubes 250 ml.<br />

10013982 Tube Rack for 20 Digestion Tubes 100 ml.<br />

10014006 Retainer Plate for Washing; Digestor 2520, 250 ml<br />

Tubes.<br />

10014007 Retainer Plate for Washing; Digestor 2520, 100 ml<br />

Tubes.<br />

10000460 Boiling Rod<br />

To avoid bumping when digesting large volumes of water.<br />

10000897 Handling Device for Digestion Tube<br />

10007117 Dispenser 2-10 ml, 1000 ml Bottle<br />

10007118 Dispenser 10-30 ml, 2000 ml Bottle<br />

Test tubes<br />

Straight mo<strong>de</strong>l Test Tubes, often used for Kjeldahl <strong>de</strong>termination.<br />

10014311 Digestion Tubes Straight 100 ml 8/pkg<br />

10014312 Digestion Tubes Straight 100 ml 20/pkg<br />

10014278 Digestion Tubes Straight 250 ml 8/pkg<br />

10000158 Digestion Tubes Straight 250 ml 20/pkg<br />

With constriction and volume mark, used in applications where<br />

the digest is diluted to volume and an aliquot is taken for<br />

analysis.<br />

10014313 Digestion Tubes With Mark 100 ml 8/pkg<br />

10014314 Digestion Tubes With Mark 100 ml 20/pkg<br />

10014315 Digestion Tubes With Mark 250 ml 8/pkg<br />

10000157 Digestion Tubes With Mark 250 ml 20/pkg<br />

With ground joint for air-cooled Reflux Con<strong>de</strong>nsers.<br />

10014316 Digestion Tubes - Ground Joint 250 ml 8/pkg<br />

10000159 Digestion Tubes - Ground Joint 250 ml 20/pkg<br />

With ball joint for water-cooled Reflux Con<strong>de</strong>nsers.<br />

10014317 Digestion Tubes - Ball Joint 250 ml 8/pkg<br />

10000611 Digestion Tubes - Ball Joint 250 ml 20/pkg<br />

Kjeltabs:<br />

Most types are <strong>de</strong>livered in boxes of 1000.<br />

15270001 Selenium, Tablets with 1.5 g K 2 SO 4 + 7.5 mg Se.<br />

15270002 Selenium, Tablets with 5 g K 2 SO 4 + 5 mg Se.<br />

15270003 Selenium, Tablets with 3.5 g K 2 SO 4 + 3.5 mg Se.<br />

15270056 Selenium, Tablets with 1 g Na 2 SO 4 + 0.05 g Se.<br />

15270010 Copper/Titanium, Tablets with 5 g K 2 SO 4 + 0.15 g<br />

CuSO 4 .5H 2 O + 0.15 g TiO 2 .<br />

15270020 Copper/Titanium, Tablets with 3.5 g K 2 SO 4 +<br />

0.105 g CuSO 4 .5H 2 O + 0.105 g TiO 2 .<br />

15270018 Copper, Tablets with 3.5 g K 2 SO 4 + 0.4 g<br />

CuSO 4 .5H 2 O.<br />

15270034 Copper, Tablets with 1.5 g K 2 SO 4 + 0.15 g<br />

CuSO 4 .5H 2 O.<br />

15270057 Copper, Tablets with 4.5 g K 2 SO 4 + 0.5 g<br />

CuSO 4 .5H 2 O.<br />

Other types are available upon request


Installation requirements:<br />

Digestion Unit 2508 Auto<br />

Power Supply: 200 - 240 V or 100 - 115 V,<br />

50 - 60 Hz<br />

Power consumption: 1100 W<br />

Water supply: See Exhaust Manifolds. If<br />

Scrubber connected - None<br />

Weight: 10 kg<br />

Dimensions, W × D × H: 300 × 500 × 697 mm (incl. Rack<br />

system)<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Exhaust system and Fume hood<br />

Recommen<strong>de</strong>d bench space: 1 m, or 0.4 m if a Lift or Racking<br />

System is used<br />

Digestion Unit 2508 Basic<br />

Power Supply: 200 - 240 V or 100 - 115 V,<br />

50 - 60 Hz<br />

Power consumption: 1100 W<br />

Water supply: See Exhaust Manifolds. If<br />

Scrubber connected - None<br />

Weight: 10 kg<br />

Dimensions, W × D × H: 300 × 390 × 140 mm<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Exhaust system and Fume hood<br />

Recommen<strong>de</strong>d bench space: 1 m, or 0.4 m if a Racking System<br />

is used<br />

Digestion Unit 2520 Auto<br />

Power Supply: 200 - 240 V, 50 - 60 Hz<br />

Power consumption: 2300 W<br />

Water supply: See Exhaust Manifolds. If<br />

Scrubber connected - None<br />

Weight: 18 kg<br />

Dimensions, W × D × H: 300 × 660 × 697 mm (incl. Rack<br />

system)<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Exhaust system and Fume hood<br />

Recommen<strong>de</strong>d bench space: 1 m, or 0.4 m if a Lift or Rack<br />

System is used<br />

Digestion Unit 2520 Basic<br />

Power Supply: 200 - 240 V, 50 - 60 Hz<br />

Power consumption: 2300 W<br />

Water supply: See Exhaust Manifolds. If<br />

Scrubber connected - None<br />

Weight: 18 kg<br />

Dimensions, W × D × H: 300 × 550 × 140 mm<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Exhaust system and Fume hood<br />

Recommen<strong>de</strong>d bench space: 1 m, or 0.4 m if a Rack System is<br />

used<br />

Scrubber<br />

Power Supply: 100 to 240 V, 50 - 60 Hz, Self<br />

selecting<br />

Power consumption: 50 W<br />

Water supply: No<br />

Weight: 19 kg<br />

Dimensions, W × D × H: 335 × 485 × 395 mm<br />

Ambient temperature: max 40°C<br />

Ventilation requirement: Outlet tubing preferably into sink<br />

in fume hood<br />

Recommen<strong>de</strong>d bench space: 0.6 m<br />

Exhaust 2508<br />

Water supply: 3 - 5 l/min for 5 minutes, then<br />

1 l/min<br />

Exhaust 2520<br />

Water supply: 10 - 12 l/min for 5 minutes, then<br />

3 - 5 l/min<br />

Lift<br />

Power Supply: None. Powered from the Digestion<br />

Unit Auto<br />

Power consumption: 10 W<br />

Weight: 7 kg<br />

Dimensions, W × D × H: 300 × 550 × 697 mm (Mounted<br />

on Digestion Unit)<br />

Ambient temperature: max 40�C<br />

Ventilation requirement: No<br />

Recommen<strong>de</strong>d bench space: 0 m. Lift is mounted on the<br />

Digestion Unit


Performance data:<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

2508 Auto 2508 Basic 2520 Auto 2520 Basic<br />

Temperature range Ambient - 440°C 100 - 440°C Ambient - 440°C 100 - 440°C<br />

Temperature setting<br />

repeatability<br />

1°C 1°C 1°C 1°C<br />

Temperature readout Digital Digital Digital Digital<br />

Heater indication LED LED LED LED<br />

Heater warning Text in display Text in display Text in display Text in display<br />

Over temperature<br />

protection<br />

Temperature stability at<br />

100°C<br />

Temperature stability at<br />

400°C<br />

Heating time 20 to<br />

400°C at 230 V<br />

Yes Yes Yes Yes<br />

± 2°C ± 5°C ± 2°C ± 5°C<br />

± 1°C ± 2°C ± 1°C ± 2°C<br />

~35 min ~35 min ~40 min ~40 min<br />

Time setting per step 1 - 999 min 1 - 1199 min 1 - 999 min 1 - 1199 min<br />

Ramp control (Rate of<br />

heating)<br />

Digestion applications<br />

memory<br />

Digestion steps per<br />

application<br />

Yes No Yes No<br />

Up to 254 No Up to 254 No<br />

Up to 23 1, Manual control Up to 23 1, Manual control<br />

Lift connection Yes, full control No Yes, full control No<br />

Scrubber Yes, full control Yes, man control Yes, full control Yes, man control<br />

Tubes / batch 8 8 20 20<br />

Typical sample capacity<br />

Tube size 250 ml 250 ml 250 ml 250 ml<br />

Sample size* solids up to 5 g up to 5 g up to 5 g up to 5 g<br />

Sample size* liquids up to 15 ml up to 15 ml up to 15 ml up to 15 ml<br />

Tube size 100 ml 100 ml 100 ml 100 ml<br />

Sample size* solids up to 1 g up to 1 g up to 1 g up to 1 g<br />

Sample size* liquids up to 3 ml up to 3 ml up to 3 ml up to 3 ml<br />

*Note: Larger samples require special procedures. Please see the relevant Application Notes or consult our Customer Service Laboratory.<br />

P/N 9999 0720E, Issue 1 GB, May 2005


High capacity laboratory Shaking Water Bath for precise and reproducible control of<br />

chemical and biochemical reactions, e.g. incubations, fermentations, extractions, dialyses,<br />

diffusions, etc.<br />

Benefits<br />

• High incubation capacity<br />

• Protection against overheating<br />

• Digital read out of actual temperature<br />

• Flexible shaking capacity<br />

• Easy to combine with the FOSS Analytical 1023<br />

Filtration Module<br />

• Circulating water for temperature stability<br />

Description<br />

The FOSS Analytical Shaking Water Bath is <strong>de</strong>signed<br />

for accurate temperature control and continuous<br />

mixing of liquids and suspensions.<br />

A series of exchangeable flask trays provi<strong>de</strong> high<br />

incubation capacity for a wi<strong>de</strong> range of sample<br />

sizes.<br />

The specially <strong>de</strong>veloped container system makes<br />

the Shaking Water Bath particularly useful in combination<br />

with the FOSS Analytical 1023 Filtration<br />

Module for rapid filtration of incubated solutions as<br />

e.g. in dietary fibre <strong>de</strong>termination.<br />

Dedicated Analytical Solutions<br />

Shaking Water Bath 1024<br />

The Shaking Water Bath is an electronically<br />

controlled thermostatic bath with a mechanically<br />

driven shaking trolley. It inclu<strong>de</strong>s a transparent<br />

lid to ensure temperature stability and minimize<br />

evaporation loss. The water tank is <strong>de</strong>signed to<br />

minimize splashing.<br />

A digital display gives the actual water temperature.<br />

A cut out <strong>de</strong>vice prevents overheating due<br />

to low water level or thermostat malfunction. The<br />

speed and stroke length of the shaking trolley are<br />

continuously adjustable to ensure a<strong>de</strong>quate mixing<br />

in a broad range of applications.<br />

The Shaking Water Bath has a constant flow of<br />

circulating water. This ensures temperature stability<br />

also when the shaking trolley is not in use.


System <strong>de</strong>scription:<br />

The FOSS Analytical Shaking Water Bath comprises:<br />

• Shaking Water Bath 1024, 230V, equipped with a shaking<br />

trolley, facilities for manual and automatic temperature<br />

setting, temperature control and a transparent hinged lid.<br />

The interior of the water bath is ma<strong>de</strong> of polished stainless<br />

steel. Flask tray are avilable as accessories (see below).<br />

• Shaking Water Bath 1024, 115V. As above.<br />

A special flask tray and a container system combines the<br />

FOSS Analytical Shaking Water Bath with the FOSS Analytical<br />

1023 Filtration Module for incubation followed by<br />

filtration of suspensions, e.g. in dietary fibre <strong>de</strong>termination.<br />

Performance data:<br />

Max. water volume: 20 litres<br />

Overall dimensions (L×W×D): 89×37×32 cm<br />

Weight: 24 kg<br />

Power supply: 115-230 V ±10%, 50/60 Hz<br />

Power consumption: 1500W/230 V (800W/115V)<br />

Maximum flask immersion: 65 mm<br />

Temperature range: Ambient to 80ºC<br />

Temperature stability: ±0.1ºC<br />

Shaking speed: 10-150 strokes/minute<br />

Stroke length: 0-50 mm<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Choose from the following accessories:<br />

Standard tray for Erlenmeyer flasks:<br />

holds 33 × 50 ml flasks<br />

holds 22 × 100 ml flasks<br />

holds 12 × 250 ml flasks<br />

holds 8 × 500 ml flasks<br />

Special flaks tray, holds 12 × 600 ml 1000 2081 Incubation<br />

Flasks<br />

Incubation Flasks (set of 6)<br />

P/N 9999 0704E, Issue 1 GB, Dec 2004


The SoxCap 2047 is a simple solution for total fat analysis prior to solvent extraction<br />

using the Soxtec Systems.<br />

Features and benefits<br />

• No sample transfer in combination with batch handling tools<br />

improves measurement precision and speeds up analysis<br />

• Low system investment cost<br />

• For operator safety and convenience acid fumes are automatically<br />

removed<br />

• Fast filtration and washing of samples thanks to SoxCap<br />

capsule* <strong>de</strong>sign<br />

• Minimum use of Celite**<br />

• No contact with hot acid during hydrolysis, filtration or<br />

washing. The entire analysis takes place in a closed vessel<br />

• Compact system requiring minimum bench space<br />

Dedicated Analytical Solutions<br />

SoxCap 2047<br />

Hydrolysis Unit<br />

System <strong>de</strong>scription<br />

The SoxCap 2047 features a new technique combining superior<br />

performance with low investment. It offers a solution<br />

for hydrolysis of food and feed samples, in accordance with<br />

recognized methods, prior to solvent extraction.<br />

The SoxCap system performs hydrolysis, filtration and<br />

washing without any sample transfer, with minimum manual<br />

handling using batch handling tools. The system does not<br />

require to be placed in a fume hood, as it has a built in fume removal<br />

system. After hydrolysis, filtration and washing is done<br />

insi<strong>de</strong> the beaker within minutes, ensuring no contact with the<br />

hot hydrolysis solution.<br />

The sample is weighed into a SoxCap glass capsule fitted<br />

with a disposable filter. After hydrolysis the glass capsule is<br />

simply turned upsi<strong>de</strong> down, a cellulose thimble is fitted on top<br />

and the capsule is placed in the Soxtec Avanti for the solvent<br />

extraction step.<br />

The patented technique is based on the SoxCap capsule’s<br />

ability to hold the fat present in the sample during hydrolysis<br />

and release it during solvent extraction.<br />

* patent pending<br />

** only with liquid samples and very fine particle size samples


System <strong>de</strong>scription:<br />

• SoxCap 2047, 230 V, 50-60 Hz comprising:*<br />

Ceramic Hot Plate 2022, Con<strong>de</strong>nser hol<strong>de</strong>r with valve<br />

plate, Con<strong>de</strong>nser, Hydrolysis Beaker, Beaker, Boiling<br />

Stand, Capsule Tray (set of 2), Drying Stand, Glass Capsules<br />

(2 sets of 6), Filters (set of 100), Thimbles (set of 25),<br />

Adapters (set of 6), Cotton, Water Aspirator, User Manual<br />

• SoxCap 2047, 115 V, 50-60 Hz. As above.<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Hydrolysis in a SoxCap 2047 Microwave drying Solvent extraction<br />

in a Soxtec System<br />

Performance data:<br />

Sample size: 0,5 - 3 g<br />

Hydrolysis time: 60 min<br />

Measuring range: 0,1 - 100 % fat<br />

Capacity per batch: 6 samples simultaneously<br />

Capacity per day: Up to 36 analyses<br />

Accessories:<br />

Filters, set of 100<br />

Cellulose Thimbles 28 × 22 mm, set of 25<br />

Hydrolysis Beaker<br />

Beaker, Low<br />

Con<strong>de</strong>nser<br />

Con<strong>de</strong>nser Hol<strong>de</strong>r<br />

Boiling Stand<br />

Drying Stand<br />

Capsule Tray<br />

Adapters, set of 6<br />

Glass Capsules, set of 6<br />

Cotton, <strong>de</strong>fatted<br />

Installation requirements:<br />

Equipment Power supply Power consumption Dimensions Weight Water supply<br />

w × d × h<br />

2022 Hot Plate 230 V, 50 - 60 Hz 500 W 19 × 30 × 11 cm 2,5 kg 2 taps nee<strong>de</strong>d: 0,4 l/min<br />

115 V, 50 - 60 Hz Tap water for vacuum pump<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

P/N 9999 0311E, Issue 1 GB, Dec 2004


Solvent extraction system for fast, safe <strong>de</strong>termination of soluble material in food, feed,<br />

soil, polymers, textiles, paper, pulp, etc.<br />

Features and benefits<br />

• Only ~10 ml of solvent used per sample with the<br />

recovery system<br />

• Se<strong>para</strong>te timer functions for each extraction step<br />

make programming and procedure conveniently<br />

repeatable<br />

• Accessories for batch handling improve laboratory<br />

efficiency<br />

• Official approvals AOAC 991.36 (meat), AOAC<br />

2003.05, 2003.06 (feed), SCAN-CM 49:93 (paper/pulp),<br />

EPA method 3541 (PAH in soil)<br />

System <strong>de</strong>scription<br />

The Soxtec 2043 is <strong>de</strong>signed for rapid, safe and<br />

economic extraction of solid and semisolid materials.<br />

This has been achieved by applying a patented<br />

version of the Soxhlet extraction technique. It is<br />

<strong>de</strong>signed for maximum user convenience through<br />

batch handling of six samples at a time.<br />

Dedicated Analytical Solutions<br />

Soxtec 2043<br />

Fat Extraction System<br />

The Soxtec 2043 is CE approved according to the<br />

LVD and EMC Directives. It consists of an Extraction<br />

Unit and a Control Unit. The extraction unit<br />

must be installed in a well ventilated fume hood<br />

(air flow 0,5 m/s). The sample to be analyzed is<br />

weighed into thimbles and inserted in the Extraction<br />

Unit. The cups are heated by the electrical<br />

heating plate. The 3-step extraction procedure<br />

consists of boiling, rinsing and recovery.<br />

The system is flexible and suitable for a wi<strong>de</strong> variety<br />

of applications in the food, feed, environmental<br />

and industrial segments. It is <strong>de</strong>signed to work<br />

with all common solvents used for solvent extraction<br />

(we do not recommend the use of Diethyl ether<br />

due to the explosion risk when handling it.) Typical<br />

solvent recovery is 80%, only ~10 ml solvent<br />

is used per sample. Sample pre<strong>para</strong>tion prior to<br />

GC/HPLC work is also possible using a specially<br />

<strong>de</strong>signed seal. The repeatability is equal to traditional<br />

technique (1% rel. or better).


System <strong>de</strong>scription<br />

Soxtec 2043 comprises:<br />

• Soxtec 2043, 230 V<br />

1 ea Soxtec 2043 Extraction Unit<br />

1 ea Soxtec 2046 Control Unit<br />

1 ea Food/Agri routine accessories kit comprising:<br />

Extraction cups (1 set of 6), cup hol<strong>de</strong>r, thimbles (set of<br />

25), thimble adaptors, thimble stand, seals in viton and<br />

butyl, Manual and Application Note AN 301.<br />

• Soxtec 2043, 115 V. As above.<br />

In addition, we recommend:<br />

Cellulose thimbles, ∅ 26mm (set of 25)<br />

Cellulose thimbles, ∅ 26mm (set of 25) for sample pre<strong>para</strong>tion<br />

Thimble handler<br />

Thimble support<br />

Hol<strong>de</strong>r for thimble support<br />

Performance data:<br />

Thimble size: 26 × 60 mm. Approx. 25 ml<br />

Solvent volume: 40 ml<br />

Extraction time: typically 40 to 60 min, <strong>de</strong>pending on application<br />

Capacity per batch: 6 samples<br />

Capacity per day: 30-36 samples<br />

Measuring range: 0.1-100% fat<br />

Accuracy: According to official approvals<br />

Repeatability: ± 1% rel. or better at 5-100% fat<br />

Heating up time: from 20°C to 280°C in 7-9 min (230 V)<br />

Installation requirements:<br />

Equipment Power supply Power consumption Dimensions Weight Water supply Ventilation<br />

w × d × h<br />

Extraction Unit - - 57 × 35 × 58 30 kg 2 l/min Fume hood min.<br />

airflow 0,5 m/s<br />

(inter locked)<br />

Control Unit 230 V, 50-60 Hz 1 250 W 28 × 23 × 19 3 kg - -<br />

115 V, 50-60 Hz<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Accessories:<br />

Cup hol<strong>de</strong>r<br />

Thimble stand<br />

Extraction cups (set of 6), aluminium<br />

Extraction cups (set of 6), glass<br />

Seals for con<strong>de</strong>nsers, viton (set of 6)<br />

Seals for con<strong>de</strong>nsers, butyl (set of 6)<br />

1090 Cemotec sample mill (food, feed prior to moisture<br />

analysis)<br />

1093 Cyclotec sample mill (food, feed general applications)<br />

2094 Homogenizer, blen<strong>de</strong>r type<br />

1095 Knifetec (water cooled for high fat and high fibre)<br />

P/N 9999 0312E, Issue 1 GB, Dec 2004


Solvent extraction system for fast, safe <strong>de</strong>termination of soluble material in food, feed,<br />

soil, polymers, textiles, paper, pulp, etc.<br />

Features and benefits<br />

• Only ~15 ml of solvent used per sample with the<br />

recovery system<br />

• Se<strong>para</strong>te timer functions for each extraction step<br />

make programming and procedure conveniently<br />

repeatable<br />

• Accessories for batch handling improve laboratory<br />

efficiency<br />

• Official approvals AOAC 991.36 (meat), AOAC<br />

2003.05, 2003.06 (feed), SCAN- CM 49:93 (paper<br />

/ pulp), EPA method 3541 (PAH in soil)<br />

• Large thimble size, 65 ml, extends application<br />

range<br />

System <strong>de</strong>scription<br />

The Soxtec 2045 is <strong>de</strong>signed for rapid, safe and<br />

economic extraction of solid and semisolid materials.<br />

This has been achieved by applying a patented<br />

version of the Soxhlet extraction technique.<br />

The Soxtec System 2045 is an electrically heated<br />

solvent extraction system which is CE approved ac-<br />

Dedicated Analytical Solutions<br />

Soxtec 2045<br />

Fat Extraction System<br />

cording to the LVD and EMC Directives. It consists<br />

of an Extraction Unit and a Control Unit where the<br />

extraction unit must be installed in a well ventilated<br />

fume hood (air flow 0,5 m/s). It is <strong>de</strong>signed for user<br />

convenience through handling of two samples at<br />

a time. The sample to be analyzed is weighed into<br />

thimbles and inserted in the Extraction Unit. After<br />

the 3-step extraction procedure consisting of boiling,<br />

rinsing and recovery, the extractable matter is<br />

collected in the cup.<br />

The system is flexible and suitable for a wi<strong>de</strong> variety<br />

of applications in the food, feed, environmental<br />

and industrial segments. It is <strong>de</strong>signed to work<br />

with all common solvents used for solvent extraction<br />

(we do not recommend the use of Diethyl ether<br />

due to the explosion risk when handling it). Typical<br />

solvent recovery is 75%, only ~15 ml solvent<br />

is used per sample. Sample pre<strong>para</strong>tion prior to<br />

GC/HPLC work is also possible using a specially<br />

<strong>de</strong>signed seal. The repeatability is equal to traditional<br />

technique (1% rel. or better).


System <strong>de</strong>scription<br />

Soxtec 2045 comprises:<br />

• Soxtec 2045, 230 V complete with<br />

1 ea 2045 Extraction Unit<br />

1 ea 2046 Control Unit<br />

1 ea Food/Agri routine accessories kit comprising:<br />

Extraction cups (1 set of 2), cup hol<strong>de</strong>r, thimbles (set of<br />

25), thimble adapters (1 set of 6), thimble stand, seals in<br />

viton and butyl, Manual and Application Note AN 301.<br />

• Soxtec 2045, 115 V. As above.<br />

In addition, we recommend:<br />

Cellulose thimbles, ∅ 33mm (set of 25) single thickness<br />

Cellulose thimbles, ∅ 33mm (set of 25) double thickness<br />

Cellulose thimbles, ∅ 26mm (set of 25) double thickness<br />

Thimble adapter, ∅ 33mm (set of 6)<br />

Thimble adapter, ∅ 26mm (set of 6)<br />

Performance data:<br />

Thimble size: 33 × 80 mm, 65 ml<br />

0.5 to 15 g <strong>de</strong>pending on sample<br />

Solvent volume: 60 ml<br />

Extraction time: typically 40 to 60 min, <strong>de</strong>pending on application<br />

Capacity per batch: 2 samples<br />

Capacity per day: 10-12 samples<br />

Measuring range: 0.1-100% fat<br />

Accuracy: According to official approvals<br />

Repeatability: ± 1% rel. or better at 5-100% fat<br />

Heating up time: from 20 to 285°C in 10 min (230V)<br />

Installation requirements:<br />

Equipment Power supply Power consumption Dimensions Weight Water supply Ventilation<br />

w × d × h<br />

Extraction Unit - - 34 × 27 × 58 18 kg 1-2 l/min Fume hood min.<br />

airflow 0,5 m/s<br />

(inter locked).<br />

Control Unit 230 V, 50-60 Hz 600 W 28 × 23 × 19 3 kg - -<br />

115 V, 50-60 Hz<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Accessories:<br />

Cup hol<strong>de</strong>r<br />

Thimble stand<br />

Extraction cups (set of 2), aluminium<br />

Extraction cups (set of 2), glass<br />

Seals for con<strong>de</strong>nsers, viton (set of 2)<br />

Seals for con<strong>de</strong>nsers, butyl (set of 2)<br />

1090 Cemotec sample mill (food, feed prior to moisture<br />

analysis)<br />

1093 Cyclotec sample mill (food, feed general applications)<br />

2094 Homogenizer, blen<strong>de</strong>r type<br />

1095 Knifetec (water cooled for high fat and high fibre)<br />

For total fat <strong>de</strong>termination, used in conjunction with Soxtec Extraction Systems we recommend:<br />

SoxCap 2047 comprises:<br />

• SoxCap 2047, 230 V, complete system for integrated boiling and filtration of samples and all accessories nee<strong>de</strong>d for acid<br />

hydrolysis of food and feed samples<br />

•<br />

SoxCap 2047, 115 V. As above.<br />

P/N 9999 0310E, Issue 1 GB, Dec 2004


Soxtec 2050 Auto Fat Extraction System - the fully automated solvent extraction<br />

system for safe <strong>de</strong>termination of soluble material in food, feed, soil, polymers, textiles,<br />

paper pulp, etc.<br />

Features and benefits<br />

•<br />

•<br />

•<br />

•<br />

•<br />

•<br />

Fully automatic for unatten<strong>de</strong>d operation<br />

Accessories for batch handling offer operator<br />

convenience<br />

Closed solvent addition limits operator’s exposure<br />

to solvent<br />

Cooling water control reduces water costs<br />

Automatic shutdown enables overnight operation<br />

Official approvals; AOAC 991.36 (meat), AOAC<br />

2003.05, 2003.06 (feed), SCAN-CM 49:93 (paper<br />

pulp), EPA No 3541 (soil)<br />

System <strong>de</strong>scription<br />

The Soxtec 2050 System represents the new<br />

generation of automated Soxhlet extraction. It is<br />

<strong>de</strong>signed for maximum user convenience with full<br />

automation for unatten<strong>de</strong>d operation and minimum<br />

system handling.<br />

This has been achieved by applying a new patented<br />

version of the Soxhlet extraction technique<br />

Dedicated Analytical Solutions<br />

Soxtec 2050<br />

Auto Fat Extraction System<br />

combined with integral solvent handling. The<br />

system consists of an Extraction Unit, a Control<br />

Unit and a Drive Unit. The sample to be analysed is<br />

weighed into thimbles and inserted into the extraction<br />

unit. Solvent is ad<strong>de</strong>d to the extraction cups in<br />

a closed system. The cups are heated by the electric<br />

heating plate. The 4-step extraction consists of boiling,<br />

rinsing, solvent recovery and pre-drying.<br />

The system is flexible and suitable for a broad<br />

range of applications in the food, feed, environmental<br />

and industrial segments. It is <strong>de</strong>signed to work<br />

with all common solvents used for solvent extraction<br />

(we do not recommend the use of Diethyl ether<br />

due to the explosion risk when handling it). Typical<br />

solvent recovery is 80%, only 16 ml solvent is used<br />

per sample. Sample pre<strong>para</strong>tion prior to GC/HPLC<br />

work is also suitable; ask for our special accessories.<br />

The repeatability is equal to traditional technique.


System <strong>de</strong>scription:<br />

Soxtec 2050 comprises:<br />

• Soxtec 2050, 230V complete with<br />

1 ea Soxtec 2050 Extraction Unit<br />

1 ea Soxtec 2050 Control Unit<br />

1 ea Soxtec 2050 Drive Unit<br />

1 ea Food/Agri Routine Accessories kit comprising:<br />

Extraction cups (3 sets of 6), Cup hol<strong>de</strong>r, Thimble support,<br />

Thimble hol<strong>de</strong>r, Thimbles (set of 25), Thimble adaptors<br />

(2 sets of 6), Thimble handler, Tong for extraction cups,<br />

Thimble stand (2 sets of 6), Cup stand, seals of viton<br />

and butyl, Solvent addition tube, Solvent emptying tube,<br />

Manual and Application Note AN 301.<br />

• Soxtec 2050, 115V. As above.<br />

In addition, we recommend:<br />

Cellulose thimble, ∅ 33mm (set of 25)<br />

Cellulose thimble, ∅ 33mm (set of 25) Single thickness<br />

For total fat <strong>de</strong>termination, used in conjunction with Soxtec<br />

Extraction Systems we recommend:<br />

SoxCap 2047 comprises:<br />

• SoxCap 2047, 230 V, complete system for integrated boiling and filtration<br />

of samples and all accessories nee<strong>de</strong>d for acid hydrolysis of food and feed<br />

samples<br />

• SoxCap 2047, 115 V. As above.<br />

Performance data:<br />

Thimble size: 33 × 80 mm, 65 ml<br />

0.5 to 15 g <strong>de</strong>pending on sample<br />

Solvent volume: 70-90 ml<br />

Extraction time: typically 40 to 60 min, <strong>de</strong>pending on application<br />

Capacity per batch: 6 samples<br />

Capacity per day: 42 samples<br />

Measuring range: 0.1-100% fat<br />

Accuracy: According to official approvals<br />

Repeatability: ± 1% rel. or better (5-100% fat)<br />

Heating up time: from 20 to 280°C in 7-9 min (230V)<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Accessories:<br />

Extraction Cups (set of 6), aluminium<br />

Extraction Cups (set of 6), glass<br />

Seals for con<strong>de</strong>nsers, viton (set of 6)<br />

Seals for con<strong>de</strong>nsers, butyl (set of 6)<br />

Con<strong>de</strong>nser sealing ring of teflon<br />

Solvent dispenser<br />

1090 Cemotec sample mill (food, feed prior to<br />

moisture analysis)<br />

1093 Cyclotec sample mill (food, feed general<br />

applications)<br />

2094 Homogenizer, blen<strong>de</strong>r type<br />

2096 Homogenizer, blen<strong>de</strong>r type<br />

1095 Knifetec (water cooled for high fat and high fibre)<br />

Closed solvent addition limits operator’s<br />

exposure to solvents.<br />

Installation requirements:<br />

Equipment Power supply Power consumption Dimensions Weight Water supply Ventilation<br />

w × d × h<br />

Extraction Unit - - 60 × 38 × 58 30 kg 2 l/min. Fume hood min.<br />

airflow 0,5 m/s<br />

(inter locked)<br />

Control Unit 230V, 50-60 Hz 1550 W 31 × 24 × 16 3 kg - -<br />

115V, 50-60 Hz<br />

Drive Unit 230V, 50-60 Hz 40 W 40 × 28 × 12 8 kg - -<br />

115V, 50-60 Hz<br />

P/N 9999 0306E, Issue 1 GB, Dec 2004


Soxtec 2055 Fat Extraction System - the new generation of manual solvent extraction<br />

systems for safe <strong>de</strong>termination of soluble material in food, feed, soil, polymers, textiles,<br />

paper, pulp, etc.<br />

Features and benefits<br />

• Se<strong>para</strong>te timer functions for each extraction step<br />

make programming and procedure conveniently<br />

repeatable<br />

• One handle moves all samples simultaneously<br />

• Accessories for batch handling offer operator<br />

convenience<br />

• Closed solvent addition limits operator’s exposure<br />

to solvents<br />

• Official approvals AOAC 991.36 (meat), AOAC<br />

2003.05, 2003.06 (feed), SCAN-CM 49:93 (paper/<br />

pulp), EPA method 3541 (PAH in soil)<br />

System <strong>de</strong>scription<br />

The Soxtec 2055 System represents the new<br />

generation of manual Soxhlet extraction systems. It<br />

is <strong>de</strong>signed for maximum user convenience through<br />

batch handling of six samples at a time, giving a<br />

minimum of system handling.<br />

This has been achieved by applying a new patented<br />

version of the Soxhlet extraction technique<br />

Dedicated Analytical Solutions<br />

Soxtec 2055<br />

Fat Extraction System<br />

combined with integral solvent handling. The<br />

system consists of an Extraction Unit and a Control<br />

Unit. The sample to be analyzed is weighed into<br />

thimbles and inserted in the Extraction Unit. The<br />

solvent is ad<strong>de</strong>d in a closed system. The cups are<br />

heated by the electrical heating plate. The 4-step<br />

extraction procedure consists of boiling, rinsing,<br />

recovery and pre-drying.<br />

The system is flexible and suitable for a wi<strong>de</strong> variety<br />

of applications in the food, feed, environmental<br />

and industrial segments. It is <strong>de</strong>signed to work<br />

with all common solvents used for solvent extraction<br />

(we do not recommend the use of Diethyl ether<br />

due to the explosion risk when handling it). Typical<br />

solvent recovery is 80%, only 16 ml solvent is used<br />

per sample. Sample pre<strong>para</strong>tion prior to GC/HPLC<br />

work is also possible using a specially <strong>de</strong>signed<br />

seal. The repeatability is equal to traditional technique<br />

(1% rel. or better).


System <strong>de</strong>scription<br />

Soxtec 2055 comprises:<br />

• Soxtec 2055, 230V Complete with<br />

1 ea Soxtec 2055 Extraction Unit<br />

1 ea Soxtec 2055 Control Unit<br />

1 ea Food/Agri routine accessories kit comprising:<br />

Extraction cups (3 sets of 6), cup hol<strong>de</strong>r, thimble support,<br />

thimble hol<strong>de</strong>r, thimbles (set of 25), thimble adaptors,<br />

thimble handler, tongs for extraction cups, thimble stand,<br />

cup stand, seals in viton and butyl, solvent addition tube,<br />

solvent emptying tube, Manual and Application Notes.<br />

• Soxtec 2055, 115V. As above.<br />

In addition, we recommend:<br />

Cellulose thimbles, ∅ 33mm (set of 25)<br />

Cellulose thimbles, ∅ 33mm (set of 25) single thickness<br />

For total fat <strong>de</strong>termination, used in conjunction with Soxtec<br />

Extraction Systems we recommend:<br />

SoxCap 2047 comprises:<br />

• SoxCap 2047, 230 V, complete system for integrated boiling and filtration<br />

of samples and all accessories nee<strong>de</strong>d for acid hydrolysis of food and feed<br />

samples<br />

• SoxCap 2047, 115 V. As above.<br />

Performance data:<br />

Thimble size: 33 × 80 mm, 65 ml<br />

0.5 to 15 g <strong>de</strong>pending on sample<br />

Solvent volume: 70-90 ml<br />

Extraction time: typically 40 to 60 min, <strong>de</strong>pending on application<br />

Capacity per batch: 6 samples<br />

Capacity per day: 36 samples<br />

Measuring range: 0.1-100% fat<br />

Accuracy: According to official approvals<br />

Repeatability: ± 1% rel. or better (5-100% fat)<br />

Heating up time: from 20 to 280°C in 7-9 min (230V)<br />

Installation requirements:<br />

Equipment Power supply Power consumption Dimensions Weight Water supply Ventilation<br />

w × d × h<br />

Extraction Unit - - 60 × 38 × 58 30 kg 2 l/min. Fume hood min.<br />

airflow 0,5 m/s<br />

(inter locked)<br />

Control Unit 230V, 50-60 Hz 1550 W 31 × 24 × 16 3 kg - -<br />

115V, 50-60 Hz<br />

* Or<strong>de</strong>ring information: See se<strong>para</strong>te price-list<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Accessories:<br />

Extraction cups (set of 6), aluminium<br />

Extraction cups (set of 6), glass<br />

Seals for con<strong>de</strong>nsers, viton (set of 6)<br />

Seals for con<strong>de</strong>nsers, butyl (set of 6)<br />

Seals for con<strong>de</strong>nsers, RESEL (set of 6)<br />

1090 Cemotec sample mill (food, feed prior to moisture<br />

analysis)<br />

1093 Cyclotec sample mill (food, feed general applications)<br />

2094 Homogenizer, blen<strong>de</strong>r type<br />

1095 Knifetec (water cooled for high fat and high fibre)<br />

Closed solvent addition limits operator’s<br />

exposure to solvents.<br />

P/N 9999 0308E, Issue 1 GB, Dec 2004


A Soxtec for every need<br />

Dedicated Analytical Solutions


Just load, start and walk away<br />

For 30 years, FOSS has <strong>de</strong>veloped and supplied instruments with<br />

a mission: to always make routine analysis simpler.<br />

A great step forward<br />

As early as 1975, we revolutionised solvent extraction<br />

by introducing Edward Randall’s patented two-stage<br />

technique for boiling and rinsing. Six years later, FOSS<br />

launched an improved system, Soxtec , based on Tecator <br />

technology, that also handled solvent recovery.<br />

Soxtec 2050 is the next great step forward in solvent<br />

extraction. A solvent extractor that needs practically no<br />

handling by lab personnel. A fully automatic Soxhlet<br />

analyzer that is the fastest on the market, using less<br />

solvent and less water.


Four automatic steps<br />

1 2 3 4<br />

Boiling<br />

Rapid solubilisation in<br />

boiling solvent.<br />

Rinsing<br />

Efficient removal of<br />

remaining soluble matter.<br />

Fully automated, unatten<strong>de</strong>d operation<br />

The Soxtec 2050 utilizes a new, patented four-step solvent<br />

extraction technique. It performs boiling, rinsing<br />

and solvent recovery.<br />

In its fourth step, the sample cup lifts off the hot plate,<br />

utilizing residual heat to pre-dry while eliminating<br />

boil-dry risk. The entire process is a fully automatic,<br />

unatten<strong>de</strong>d operation.<br />

You just load, start and walk away. Soxtec 2050 will<br />

even shut down automatically when finished.<br />

Because it frees operators from routine tasks, Soxtec<br />

2050 helps to improve the laboratory’s productivity.<br />

And it’s very quiet – an additional bonus for the laboratory<br />

working environment.<br />

Recovery<br />

Automatic collection of<br />

distilled solvent for re-use.<br />

Pre-drying<br />

Elimination of boil-dry<br />

risk.<br />

Application flexibility<br />

Soxtec systems are <strong>de</strong>veloped for maximum application<br />

flexibility.<br />

Users can easily <strong>de</strong>sign and optimise their own applications<br />

for accurate, safe <strong>de</strong>termination of soluble<br />

matter within the food, feed, environmental and<br />

industrial sectors.<br />

Soxtec can handle larger sample volumes (a standard<br />

33×80 mm thimble), and its higher temperature range<br />

even enables effective use of high-boiling point solvents,<br />

such as toluene and xylene.<br />

Furthermore, the glass/Teflon solvent interface makes<br />

it possible to run metal-sensitive applications.


Built for the purpose<br />

Safety is important<br />

Minimal manual handling assures safety in the process.<br />

When the sample has been loa<strong>de</strong>d, the solvent is ad<strong>de</strong>d<br />

in a closed, secure system. The solvent dispenser, automatic<br />

solvent recovery and built-in fume hood limit<br />

solvent vapour to a minimum, thus ensuring a safe<br />

working environment.<br />

Safety has always been important to us, the only electrical<br />

part in the Extraction unit, the hot plate, is spark<br />

proof. The double temperature sensors ensure that the<br />

set temperature is kept and that the ignition point is<br />

never reach for any solvent.<br />

Soxtec 2050 guarantees a safe working environment<br />

– the entire analysis takes place in a closed,<br />

secure system. It is <strong>de</strong>signed and built to surpass<br />

strict European safety standards.<br />

There is simply no safer solvent extraction system<br />

available.<br />

Operating convenience<br />

Soxtec 2050’s automation improves efficiency.<br />

Overall laboratory efficiency is further improved by the<br />

purpose-<strong>de</strong>veloped handling tools <strong>de</strong>livered with the<br />

Soxtec system. The tools for simple batch-wise sample<br />

handling save time, simplify usage and minimize risk of<br />

operator error. There is no longer any need for manual<br />

handling of thimbles or hot extraction cups.<br />

Soxtec 2050 and 2055 are operated through the Control Unit,<br />

with simple logic commands and a full graphical interface.


The fastest on the market<br />

Typically five times faster than the classical Soxhlet technique, Soxtec Systems are the fastest<br />

Soxhlet extractors on the market. With Soxtec 2050 you can extract as many as seven batches per<br />

day, with absolutely no loss in precision or accuracy. The Soxtec systems follow officially approved<br />

methods for fat in feed (AOAC), meat (AOAC), PCB (EPA) and paper pulp (SCAN).<br />

Dramatically reduced extraction times Soxhlet Soxtec<br />

Analyte Extraction time Extraction time<br />

Fat in feed 2 h to 16 h 1 h<br />

Fat in food (eg. meat, cereals) 2 h to 16 h 1 h<br />

PCB, PAH & Pestici<strong>de</strong>s in soil 17 h 2 h<br />

Oil & Grease in water 4 h 45 min<br />

Extractable Matter in polymers & rubber 2 h to 48 h 1 h to 5 h<br />

Extractable Matter in paper & pulp 2 h to 48 h 1 h to 5 h<br />

Extractable Matter in explosives & propellants 16 h 1 h<br />

Hydrocarbons in petroleum rock 24 h 2 h<br />

Finishing Oil on textile & synthetic fibres 2 h 30 min<br />

Anti-Caking Coating on fertilisers 3 h to 4 h 1 h<br />

Detergent in <strong>de</strong>tergent pow<strong>de</strong>r 5 h 1 h<br />

Fat in leather 5 h 1 h


A profitable solution<br />

Soxtec extractors range in capacity and function from the<br />

small Soxtec 2045 to the fully automatic Soxtec 2050.<br />

All Soxtec mo<strong>de</strong>ls fully utilise our batch handling concept to<br />

make sample processing as easy and safe as possible.<br />

Whatever your Soxhlet extraction need is, we can offer you<br />

the right solution.<br />

Total fat analysis<br />

The SoxCap 2047 is an integral part of the Soxtec<br />

systems. It offers total fat analysis in accordance with<br />

recognized methods. The SoxCap system performs<br />

hydrolysis, filtration and washing without any sample<br />

transfer. This patented technique offers high throughput<br />

together with minimum manual handling using batch<br />

handling tools.<br />

Save time and money<br />

Soxtec 2050 shortens the analysis time, increasing<br />

throughput to up to seven extractions per day. Furthermore,<br />

the automatic shutdown function enables<br />

overnight operation*. Its automatic operation frees<br />

operators from time-consuming routine tasks, thereby<br />

increasing laboratory efficiency.<br />

Most users prefer aluminium extraction cups –only environmental<br />

applications require glass cups. Aluminium<br />

cups are unbreakable, and they offer rapid heat transfer,<br />

which in turn shortens heating and drying times. The<br />

low weight of the aluminium cups also makes it possible<br />

to use a standard 120 g capacity balance.<br />

Soxtec systems utilizes environmentally sound technology.<br />

Compared to classical Soxhlet, the Soxtec systems<br />

uses a significantly lower solvent volume.<br />

No other Soxhlet extractor uses solvents so efficiently.<br />

Typically, thanks to solvent recovery,<br />

16 ml of solvent is used per sample – so costs for<br />

solvent purchase and disposal can be kept to a<br />

minimum. Built-in water control minimizes water<br />

consumption.<br />

*Subject to local regulation<br />

With Soxtec 2050, you make the most<br />

of your laboratory – day and night!


Soxtec Systems<br />

Solvent extraction systems for safe <strong>de</strong>termination of soluble matter in food, feed, soil, polymers, textiles,<br />

paper pulp, and more. Whatever your Soxhlet extraction needs, we can offer the right solution.<br />

Soxtec Soxtec Soxtec Soxtec SoxCap<br />

2045 2043 2055 2050 2047<br />

Sample Positions 2 6 6 6 6<br />

Capacity,<br />

samples per day<br />

12 36 36 42 36<br />

Solvent Volume per sample 50–70 ml 40-50 ml 70–90 ml 70–90 ml –<br />

Solvent Recovery 80% 80% 80% 80%, automatic –<br />

Closed Solvent Addition No No Yes Yes –<br />

Programmable Yes Yes Yes Yes No<br />

Fully Automated No No No Yes No<br />

Overnight Operation No No No Yes No<br />

Batch Handling Yes Yes Yes Yes Yes<br />

Extraction Cups Glass & Aluminium Glass & Aluminium Glass & Aluminium Glass & Aluminium –<br />

Thimbles Cellulose, Glass Cellulose, Glass Cellulose, Glass Cellulose, Glass Cellulose<br />

Thimble Diameter 26, 33, 45 26 26, 33 26, 33 30<br />

Thimble Volume 120 ml 30 ml 65 ml 65 ml 50 ml<br />

Heating Remotely Remotely Remotely Remotely Electric<br />

controlled electric controlled electric controlled electric controlled electric<br />

Temperature Range 0–285ºC 0–285ºC 0–285ºC 0–285ºC –<br />

Overtemperature<br />

Protection<br />

145, 210 & 330ºC 145, 210 & 330ºC 145, 210 & 330ºC 145, 210 & 330ºC –<br />

Power Consumption 1500 W 1500 W 1550 W 1590 W 500 W<br />

Water Consumption 2 l/min 2 l/min 2 l/min 2 l/min 0,4 l/min<br />

Water Saving System No No No Yes No<br />

Dimensions, cm 34×27×58 51×32×58 60×38×58 60×38×58 19×30×11<br />

Accuracy +/- 1% relative +/- 1% relative +/- 1% relative +/- 1% relative +/- 1% relative<br />

In the interest of product <strong>de</strong>velopment we reserve the right to alter specifications without prior notice.


About FOSS<br />

FOSS provi<strong>de</strong>s <strong>de</strong>dicated analytical solutions that<br />

ensure optimal production of food, agricultural, pharmaceutical<br />

and chemical products. FOSS solutions<br />

analyse and control your products during production<br />

– helping you to optimise both quality and profit.<br />

FOSS is unique in offering a range of <strong>de</strong>dicated solutions<br />

based on both indirect and reference methods.<br />

FOSS solutions provi<strong>de</strong> analysis and control throughout<br />

the production process, from raw material to finished<br />

product and from routine analysis to at-line and in-line<br />

process control.<br />

FOSS is a privately-owned company employing over<br />

1100 worldwi<strong>de</strong>. FOSS has manufacturing and research<br />

and <strong>de</strong>velopment facilities in Denmark, Swe<strong>de</strong>n and<br />

the USA.<br />

Solutions are sold and supported through FOSS sales<br />

and service companies in 21 countries and by more<br />

than 75 <strong>de</strong>dicated distributors.<br />

Please visit www.foss.dk.<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

P/N 99990307, Issue 2 GB, April 2006


The SoxCap 2047 is a simple solution for total fat analysis prior to solvent extraction<br />

using the Soxtec Systems.<br />

Features and benefits<br />

• No sample transfer in combination with batch handling tools<br />

improves measurement precision and speeds up analysis<br />

• Low system investment cost<br />

• For operator safety and convenience acid fumes are automatically<br />

removed<br />

• Fast filtration and washing of samples thanks to SoxCap<br />

capsule* <strong>de</strong>sign<br />

• Minimum use of Celite**<br />

• No contact with hot acid during hydrolysis, filtration or<br />

washing. The entire analysis takes place in a closed vessel<br />

• Compact system requiring minimum bench space<br />

Dedicated Analytical Solutions<br />

SoxCap 2047<br />

Hydrolysis Unit<br />

System <strong>de</strong>scription<br />

The SoxCap 2047 features a new technique combining superior<br />

performance with low investment. It offers a solution<br />

for hydrolysis of food and feed samples, in accordance with<br />

recognized methods, prior to solvent extraction.<br />

The SoxCap system performs hydrolysis, filtration and<br />

washing without any sample transfer, with minimum manual<br />

handling using batch handling tools. The system does not<br />

require to be placed in a fume hood, as it has a built in fume removal<br />

system. After hydrolysis, filtration and washing is done<br />

insi<strong>de</strong> the beaker within minutes, ensuring no contact with the<br />

hot hydrolysis solution.<br />

The sample is weighed into a SoxCap glass capsule fitted<br />

with a disposable filter. After hydrolysis the glass capsule is<br />

simply turned upsi<strong>de</strong> down, a cellulose thimble is fitted on top<br />

and the capsule is placed in the Soxtec for the solvent extraction<br />

step.<br />

The patented technique is based on the SoxCap capsule’s<br />

ability to hold the fat present in the sample during hydrolysis<br />

and release it during solvent extraction.<br />

* patent pending<br />

** only with liquid samples and very fine particle size samples


System <strong>de</strong>scription:<br />

20470001 SoxCap 2047, 230 V, 50-60 Hz comprising:*<br />

Ceramic Hot Plate 2022, Con<strong>de</strong>nser hol<strong>de</strong>r with<br />

valve plate, Con<strong>de</strong>nser, Hydrolysis Beaker,<br />

Beaker, Boiling Stand, Capsule Tray (set of 2),<br />

Drying Stand, Glass Capsules (2 sets of 6),<br />

Filters (set of 100), Thimbles (set of 25),<br />

Adapters (set of 6), Cotton, Water Aspirator,<br />

User Manual<br />

20470002 SoxCap 2047, 115 V, 50-60 Hz. As above.<br />

20470003 SoxCap 2047 mini , 230 V, 50-60 Hz comprising:*<br />

Ceramic Hot Plate 2022, Con<strong>de</strong>nser hol<strong>de</strong>r with<br />

valve plate, Con<strong>de</strong>nser, Hydrolysis Beaker,<br />

Beaker, Boiling Stand, Capsule Tray (set of 2),<br />

Drying Stand, Glass Capsules mini (2 sets of 6),<br />

Filters (set of 100), Thimbles (set of 25),<br />

Adapters (set of 6), Cotton, Water Aspirator,<br />

User Manual<br />

20470004 SoxCap 2047 mini , 115 V, 50-60 Hz. As above.<br />

FOSS Analytical<br />

69, Slangerupga<strong>de</strong><br />

DK-3400 Hilleroed<br />

Denmark<br />

Tel.: +45 7010 3370<br />

Fax: +45 7010 3371<br />

info@foss.dk<br />

www.foss.dk<br />

Hydrolysis in a SoxCap 2047 Microwave drying Solvent extraction<br />

in a Soxtec System<br />

Performance data:<br />

Sample size: 0,5 - 3 g<br />

Hydrolysis time: 60 min<br />

Measuring range: 0,1 - 100 % fat<br />

Capacity per batch: 6 samples simultaneously<br />

Capacity per day: Up to 30 analyses<br />

Accessories:<br />

10012381 Filters, set of 100<br />

15220053 Cellulose Thimbles 28 × 22 mm, set of 25<br />

10012233 Hydrolysis Beaker<br />

10011595 Beaker, Low<br />

10013849 Con<strong>de</strong>nser<br />

10013840 Con<strong>de</strong>nser with drip tray assembly<br />

10012227 Boiling Stand<br />

10012229 Drying Stand<br />

10012230 Capsule Tray<br />

10012379 Adapters, set of 6<br />

10012378 Glass Capsules, set of 6<br />

15290009 Cotton, <strong>de</strong>fatted<br />

60022802 Glass Capsules mini , set of 6<br />

Installation requirements:<br />

Equipment Power supply Power consumption Dimensions Weight Water supply<br />

w × d × h<br />

2022 Hot Plate 230 V, 50 - 60 Hz 500 W 19 × 30 × 11 cm 2,5 kg 2 taps nee<strong>de</strong>d: 0,4 l/min<br />

115 V, 50 - 60 Hz Tap water for vacuum pump<br />

*Or<strong>de</strong>ring information: Use the above specified Cat. Nos. together with the text.<br />

P/N 9999 0311, Issue 2 GB, Feb 2007

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