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poly bis-gma/ha based hybrid composite materials - Scientific Bulletin

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82 Maria Ficai, Ecaterina Andronescu, Anton Ficai, Georgeta Voicu, Bogdan Ştefan Vasile<br />

DTA, uV<br />

DTA, uA<br />

a)<br />

b)<br />

250<br />

200<br />

150<br />

100<br />

50<br />

0<br />

-50<br />

200<br />

150<br />

100<br />

50<br />

0<br />

-50<br />

DTA (uV)<br />

TGA, (%)<br />

DrTGA (mg/sec)<br />

200 400 600 800<br />

86<br />

1000<br />

t, 0 C<br />

DTA (uV)<br />

TGA (%)<br />

DrTGA (mg/sec)<br />

200 400 600 800<br />

86<br />

1000<br />

TGA, DrTGA<br />

% mg/<br />

100 0.0005<br />

0 C<br />

98<br />

96<br />

94<br />

92<br />

90<br />

88<br />

98<br />

96<br />

94<br />

92<br />

90<br />

88<br />

0.0000<br />

-0.0005<br />

-0.0010<br />

-0.0015<br />

-0.0020<br />

-0.0025<br />

-0.0030<br />

-0.0035<br />

TGA DrTGA<br />

% mg/<br />

100 0.0005<br />

0 C<br />

0.0000<br />

-0.0005<br />

-0.0010<br />

-0.0015<br />

-0.0020<br />

-0.0025<br />

-0.0030<br />

t, 0 C<br />

Fig. 6. Complex thermal be<strong>ha</strong>viour of <strong>poly</strong> Bis-GMA/HA <strong>composite</strong> <strong>materials</strong> obtained by a)<br />

chemical and b) thermal <strong>poly</strong>merization

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