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4026 Synthesis of 2-chloro-2-methylpropane (tert-butyl ... - kriemhild

4026 Synthesis of 2-chloro-2-methylpropane (tert-butyl ... - kriemhild

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NOP http://www.oc-praktikum.de<br />

13 C NMR spectrum <strong>of</strong> the crude product (75.5 MHz, CDCl3)<br />

13 C NMR spectrum <strong>of</strong> the pure product (75.5 MHz, CDCl3)<br />

δ (ppm) Assignment<br />

67.25 C-CH 3<br />

34.43 CH 3<br />

76.5-77.5 solvent<br />

Cl<br />

The 13 C NMR-spectrum <strong>of</strong> the crude product shows at 31.3 ppm the signal for the methylgroups <strong>of</strong> <strong>tert</strong>-butanol.<br />

6<br />

March 2006

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