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EXPERIMENT # UO1<br />

DOUBLE EFFECT EVAPORATOR<br />

OBJECTIVE:<br />

The objective of this <strong>experiment</strong> is to study the performance of a <strong>double</strong> <strong>effect</strong><br />

<strong>evaporator</strong>. Mass and energy balances will be carried out to determine steam<br />

economy and heat transfer coefficients.<br />

INTRODUCTION<br />

Evaporation is a process whereby a solution consisting of a volatile solvent and<br />

a non-volatile solute is concentrated by vaporizing the solvent. Common types<br />

of <strong>evaporator</strong>s used in the industry include i.) forced circulation <strong>evaporator</strong>s,<br />

ii.) natural circulation <strong>evaporator</strong>s (thermosiphon), iii.) falling film<br />

<strong>evaporator</strong>s, and iv.) rising film <strong>evaporator</strong>s. Drying differs from evaporation<br />

in that the product in this case is solid.<br />

In many industrial applications, water is used as the solvent while steam is<br />

utilized as heating medium for the vaporization process. In such cases, given<br />

efficient heat exchange, one kilogram of water may be evaporated per kilogram<br />

of steam condensed.<br />

To improve steam economy, multiple <strong>evaporator</strong>s are used. The basic<br />

principle involved is to utilize steam generated in one <strong>effect</strong> as the source of<br />

heat for the subsequent <strong>evaporator</strong>. In this way, multiple <strong>effect</strong> <strong>evaporator</strong>s<br />

have the capacity to significantly reduce steam consumption.<br />

THEORETICAL BACKGROUND<br />

Steam economy, which is defined as the mass of water vapor generated per<br />

mass of steam is the process parameter most significant in evaluating the<br />

performance of multiple <strong>effect</strong> <strong>evaporator</strong>s (Equation 1). The other important<br />

parameter upon which both the evaporation and condensation process depend<br />

is the heat transfer coefficient (Equation 2).<br />

Steam Economy :<br />

m<br />

m<br />

v<br />

E = (1)<br />

s<br />

Heat Transfer Rate: q = UAΔT (2)<br />

UO1-1


ΔT for both <strong>effect</strong>s should be considered. For U 1 , ΔT=T s – T 1 , and for U 2 ,<br />

ΔT=T 1 – T 2 .<br />

MASS AND ENERGY BALANCES<br />

Assuming that the stream entering the <strong>effect</strong> is saturated and that the<br />

condensate resulting from the steam is not sub cooled, then the total heat<br />

transfer in the <strong>effect</strong> is obtained as :<br />

q = m s .λ s<br />

-(3)<br />

The heat given up by the condensing steam is absorbed by the process fluid and<br />

used for partial vaporization. From mass and enthalpy balance,<br />

q = ( m − m ) H + m H − m H<br />

-(4)<br />

f p v p p f f<br />

Values of enthalpies at the <strong>experiment</strong>al conditions of temperature and pressure<br />

should be obtained from literature. The flow rates of various streams are<br />

determined from <strong>experiment</strong>al data.<br />

PROCESS DESCRIPTION AND EXPERIMENTAL PROGRAM<br />

The <strong>double</strong> <strong>effect</strong> <strong>evaporator</strong> unit is shown schematically in Figure 1.The two<br />

<strong>effect</strong>s are initially filled to desired operating levels. Steam is supplied to the<br />

first <strong>effect</strong> where heat transfer takes place causing partial evaporation of water<br />

in the <strong>effect</strong>. The vapor generated is then supplied to the second <strong>effect</strong> where it<br />

is used to vaporize some of the liquid water in the <strong>evaporator</strong>. Vapor produced<br />

in the second <strong>effect</strong> is subsequently condensed and collected in the receiving<br />

tank.<br />

The entire <strong>experiment</strong>al unit is to be operated at steady state for analysis. At<br />

steady state, process parameters such as pressures, temperatures, mass flow<br />

rates and tank level are measured and recorded as shown in the log sheet. The<br />

measurements are repeated three times at regular intervals for reproducibility.<br />

UO1-2


P2<br />

m v1<br />

P4<br />

m v2<br />

T3<br />

P5<br />

T1<br />

FIRST<br />

EFFECT<br />

CYCLONE<br />

I<br />

T2<br />

SECOND<br />

EFFECT<br />

CYCLONE<br />

II<br />

CONDENSER<br />

T4<br />

C3<br />

Steam<br />

P1<br />

P3<br />

CONDENSATE<br />

TANK<br />

T5<br />

Feed Water F1<br />

m p1<br />

m p2<br />

C1<br />

FIGURE 1 : DOUBLE EFFECT EVAPORATOR<br />

C2<br />

UO1-3<br />

Data:<br />

Condensate Tank Diameter D = 50 cm<br />

Evaporator Heat A = 0.51m 2<br />

Transfer Area<br />

C : Condensate<br />

P : Pressure Indicator<br />

T : Temperature Indicator


EXPERIMENTAL PROCEDURE<br />

1. Start the unit and let it reach steady state (to be done with the help of<br />

technician).<br />

2. After the unit reaches steady state, record the temperature and pressure at<br />

various points as shown in the log sheet.<br />

3. Measure the flow rate of condensate from the first <strong>effect</strong> by collecting a<br />

quantity of the condensate in a given time.<br />

4. Repeat steps (3) for the second <strong>effect</strong>.<br />

5. Measure the flow rate of the condensate flowing into the receiving tank by<br />

monitoring the rise in the level in the tank.<br />

6. Repeat steps (3) to (5) two more times.<br />

7. Shut down the unit. (To be done with the help of technician).<br />

DATA ANALYSIS<br />

The following items must be covered in the data analysis and the analysis sheet<br />

filled in accordingly:<br />

1) Tabulate all enthalpies used in analysis from literature.<br />

2) Carry out a mass and energy balance for the two <strong>effect</strong>s.<br />

3) Determine the steam economy of the process.<br />

4) Determine the overall heat transfer coefficients for thde two <strong>effect</strong>s.<br />

Notations:<br />

A Surface area of heat transfer , m 2<br />

E<br />

Steam Economy<br />

Hv, Hf , Hp Enthalpies of the vapor, the feed and the product, W/m 2 .K<br />

m f , m p , m s mass flow rate of the feed, product and steam supplied<br />

kg/hr<br />

m v1<br />

mass flow rate of vapor from first <strong>effect</strong>, (= C2) kg/hr<br />

m v2<br />

mass flow rate of vapor from second <strong>effect</strong>, (= C2) kg/hr<br />

q heat transfer rate, W.<br />

T p<br />

temperature of the process fluid, K<br />

T s<br />

temperature of the steam supplied, K<br />

U overall heat transfer coefficient, W/m 2 .K<br />

λ<br />

Latent heat of vaporization, J/kg<br />

UO1-4


References:<br />

1.) Kern, D. Q., Process Heat Transfer, McGraw Hill, (1965)<br />

2.) Perry, R.H. and Chilton, C.H., "Chemical Engineers' Handbook", 5th<br />

Edition, McGraw-Hill Book Company NY, chap 20 (1973).<br />

3.) Thompson, E.V., and Ceckler, W.H., "Introduction to Chemical<br />

Engineering.", McGraw-Hill Book Company, NY, chap.17 (1977).<br />

UO1-5


TABLE 1. LOG SHEET FOR EXPERIMENT UO1<br />

Date :<br />

Name of students: 1)<br />

2)<br />

3)<br />

Signature of Instructor:<br />

Tag Description Units Set 1 Set 2 Set 3<br />

PI-1 Fresh steam pressure Psig<br />

PI-2 Vap. pr. in the 1 st <strong>effect</strong> "<br />

PI-3 Steam pr. in the 2nd <strong>effect</strong> "<br />

PI-4 Vapor pr. in the 2nd <strong>effect</strong> In. Hg<br />

PI-5 Shell side pr. in the cond. "<br />

TI-1 Vap temp in the 1st <strong>effect</strong> oF<br />

TI-2 Vap temp in the 2nd <strong>effect</strong> "<br />

TI-3 Vap temp at cond. Inlet "<br />

TI-4 Temp at condenser outlet "<br />

TI-5 Feed temperature "<br />

FI-1 Feed flow rate LPM<br />

Weight of cond (1st <strong>effect</strong>)<br />

Flow time (1st <strong>effect</strong>)<br />

Weight of cond (2nd <strong>effect</strong>)<br />

Flow time (2nd <strong>effect</strong>)<br />

kg<br />

min.<br />

kg<br />

min.<br />

LI-3 Rise in tank level cm<br />

Diameter of Tank cm 50<br />

Total Time<br />

Weight of empty bucket<br />

Weight of empty bucket<br />

with condensate<br />

min.<br />

kg<br />

kg<br />

UO1-6


TABLE 2. ENTHALPY TABULATION<br />

Temperature Pressure Enthalpy Ref.<br />

T1 P2 H v1 =<br />

" " H p1 =<br />

T5 1 atm. H f1 =<br />

T2 P4 H v2 =<br />

" " H p2 =<br />

T sat P1 λ1 =<br />

T sat P3 λ2 =<br />

TABLE 3. CALCULATION SUMMARY<br />

(Details to be shown elsewhere)<br />

Parameter Value Units<br />

Feed flow rate to 1st <strong>effect</strong><br />

kg/h<br />

Vapor flow rate from 1st <strong>effect</strong> "<br />

Condensate flow rate from 1st <strong>effect</strong> "<br />

Steam Economy of 1st <strong>effect</strong><br />

Vapor flow rate from 2nd <strong>effect</strong><br />

kg/h<br />

Condensate flow rate from 2nd <strong>effect</strong> "<br />

Steam Economy of 2nd <strong>effect</strong><br />

Heat transfer area of H01,H02 0.51 m2<br />

Overall heat transfer coefficient of 1st <strong>effect</strong><br />

W/m2.K<br />

Overall heat transfer coefficient of 2nd <strong>effect</strong> "<br />

Overall Steam Economy of process<br />

UO1-7


UO1-8

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