Microflow Disc Reactors

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Continuous flow microwave reactor

• microwave synthesizer (Emrys TM Optimizer)

• MCF wound around teflon microwave insert

• 2 cylindrical MCF connectors

• length: 4 m inside microwave cavity (+ 2x 20 cm leads)

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Continuous flow microwave reactor • microwave synthesizer (Emrys TM Optimizer) • MCF wound around teflon microwave insert • 2 cylindrical MCF connectors • length: 4 m inside microwave cavity (+ 2x 20 cm leads) 12

Continuous flow microwave reactor F F F + H N NH 2 Cl - EtOH F F F H NC N N H CN µ-wave 75°C F F F N H 2 CN N N EtO CN Cl Cl H CN Pyrazole Reaction conditions: Q = 0.1 – 0.2 ml/min solvent: MeOH τ = 15 - 30 min T = 60 - 75 °C 15 min / 60 °C 39.67 % conv. 15 min / 75 °C 64.46 % conv. 30 min / 75 °C ~100 % conv. 13

Page 1 and 2: Micro Flow Disc Reactors for contin
Page 3 and 4: Microcapillary flow disc (MFD) •
Page 5 and 6: Kilogram-scale reactor 8 flow discs
Page 7 and 8: Conclusions Variable, low cost, con
Page 9 and 10: Microcapillary Reactors (MCRs) 9
Page 11: Microcapillary flow disc (MFD) •

Microflow Disc Reactors

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