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Appendix C: - University of Illinois at Chicago

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<strong>Illinois</strong> St<strong>at</strong>e W<strong>at</strong>er Survey - W<strong>at</strong>ershed Science Section<br />

VC SOP No. I<br />

Origin<strong>at</strong>ion D<strong>at</strong>e: 2/02<br />

Version: 1.2, 5/4/2004. Page 6<strong>of</strong>6<br />

STANDARD OPERATING PROCEDURE FOR THE COLLECTION OF SEDIMENT CORES<br />

USING THE ROSSFELDER P-3C VIBROCORE<br />

Requirements for the transport<strong>at</strong>ion and storage Of Collected cores will<br />

vary depending on the intended uses or analyses. The cores as collected<br />

are capped, labeled and sealed. There is limited chance for reordering <strong>of</strong><br />

the core str<strong>at</strong>igraphy when the core tube has been properly cut and<br />

capped so there i's no requirement th<strong>at</strong> the core remain upright. In<br />

addition, while being transported on the bo<strong>at</strong> the core tubes are placed<br />

within storage tubes constructed <strong>of</strong> schedule 40 PVC equipped with end<br />

caps. Since the tubes are completely enclosed there is no chance for<br />

distortion <strong>of</strong> the core due to flexing <strong>of</strong> the sample. When core retrieval is<br />

<strong>at</strong> or near 1 00%, core sample weights can approach 100 lbs. Care should<br />

be taken when handling samples to avoid injury and to avoid any flexing<br />

<strong>of</strong> the core sample to minimize any disturbance to the sample. Since<br />

cores commonly approach 10 feet in length, a vehicle capable <strong>of</strong><br />

transporting this size m<strong>at</strong>erial must be available.<br />

Core samples by the n<strong>at</strong>ure <strong>of</strong> the collection technique limit exposure <strong>of</strong><br />

the sample to <strong>at</strong>mospheric oxygen and possible oxid<strong>at</strong>ion <strong>of</strong> selected<br />

chemical constituents. If temper<strong>at</strong>ure is an important consider<strong>at</strong>ion thenr<br />

it may become necessary for samples to be immedi<strong>at</strong>ely transported to a<br />

cold storage facility or sub-sampling may be required on site with<br />

appropri<strong>at</strong>e storage <strong>of</strong> sub-samples. It is important th<strong>at</strong> the plan <strong>of</strong> study<br />

for chemical analysis be clearly defined as constituents have specific<br />

requirements for holding times, temper<strong>at</strong>ure and m<strong>at</strong>erial in which the<br />

sample is stored. Requirements for the storage and manipul<strong>at</strong>ion <strong>of</strong><br />

sediment samples can be found in such reference m<strong>at</strong>erials as United<br />

St<strong>at</strong>es Environmental Protection Agency document EPA-823-B3-0l1-002<br />

and the 2000 ASTM Standards on Environmental Sampling, Vol. 11.05.<br />

UNITED ANALTIMCAL SERVICES, INC.<br />

Page 31

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