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A Portable NIR and Mid IR Spectrometer with No Moving Parts, No ...

A Portable NIR and Mid IR Spectrometer with No Moving Parts, No ...

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InfraSpec Variable Filter Array<br />

(VFA) <strong>IR</strong> <strong>Spectrometer</strong>:<br />

Alcohol Analyzer<br />

Wilks Enterprise, Inc.<br />

www.Wilks<strong>IR</strong>.com<br />

info@Wilks<strong>IR</strong>.com


InfraSpec Variable Filter Array<br />

(VFA) <strong>IR</strong> <strong>Spectrometer</strong>:<br />

A <strong>Portable</strong> <strong>Mid</strong>-<strong>IR</strong> <strong>Spectrometer</strong>


Ideal for<br />

laboratory, field <strong>and</strong> on-site analysis


<strong>Mid</strong> Infrared Measurement of<br />

Alcohol<br />

• Infrared absorbance is directly<br />

proportional concentration<br />

• Alcohol has a characteristic <strong>and</strong> well-<br />

delineated absorption b<strong>and</strong> in the mid<br />

infrared region


Infrared Spectra of Alcohol<br />

0.15<br />

Absorbance<br />

0.10<br />

0.05<br />

'28.5% alcohol 3_Abs'<br />

'38% alcohol 2_Abs'<br />

'47.5% alcohol 2_Abs'<br />

'57% alcohol 3_Abs'<br />

'66.5% alcohol 2_Abs'<br />

0.00<br />

9.5<br />

10.0<br />

Wavelength (µm)<br />

10.5<br />

11.0


Peak Area Measurement: 9.5-9.8 9.8 microns<br />

0.15<br />

Absorbance<br />

0.10<br />

0.05<br />

0.00<br />

9.5<br />

9.6<br />

9.7<br />

Wavelength (µm)<br />

9.8<br />

9.9


Wine calibration<br />

Area of Region<br />

0.02<br />

0.018<br />

0.016<br />

0.014<br />

y = -2E-05x 2 + 0.0012x + 0.0032<br />

R 2 = 0.9997<br />

0.012<br />

11 13 15 17 19 21<br />

Concentration %


Internal calibration allows for<br />

quantitative analysis


Operator introduces sample to<br />

<strong>Spectrometer</strong>


Operator Selects “Run Sample”


Quantitative Measurement <strong>with</strong> a Numeric<br />

Readout<br />

Concentration:<br />

13.6%<br />

Alcohol


Exposed ATR crystal<br />

makes sample presentation <strong>and</strong><br />

cleaning quick <strong>and</strong> easy


Two new developments<br />

• Detector arrays<br />

• Linear variable filters (LVFs(<br />

LVFs)


Two new developments<br />

• Detector arrays<br />

• Linear variable filters (LVFs(<br />

LVFs)<br />

Allow for<br />

filter based infrared spectrometers<br />

capable of measuring a spectral range


Linear Variable Filter (LVF)<br />

Wavelength Range for Alcohol analysis:<br />

9-11 microns (1100-910 cm -1 )


Schematic of the<br />

InfraSpec ATR Sample Stage


• <strong>No</strong> moving parts<br />

Advantages:


Advantages:<br />

• <strong>No</strong> moving parts<br />

• <strong>No</strong> exposed optical path


Advantages:<br />

• <strong>No</strong> moving parts<br />

• <strong>No</strong> exposed optical path<br />

• Rugged <strong>and</strong> compact


Advantages:<br />

• <strong>No</strong> moving parts<br />

• <strong>No</strong> exposed optical path<br />

• Rugged <strong>and</strong> compact<br />

• <strong>Portable</strong>


Advantages:<br />

• <strong>No</strong> moving parts<br />

• <strong>No</strong> exposed optical path<br />

• Rugged <strong>and</strong> compact<br />

• <strong>Portable</strong><br />

• Easy to use


Advantages:<br />

• <strong>No</strong> moving parts<br />

• <strong>No</strong> exposed optical path<br />

• Rugged <strong>and</strong> compact<br />

• <strong>Portable</strong><br />

• Easy to use<br />

• Relatively low cost


InfraSpec Variable Filter Array<br />

(VFA) <strong>IR</strong> <strong>Spectrometer</strong>:<br />

Alcohol Analyzer<br />

Wilks Enterprise, Inc.<br />

140 Water Street<br />

South <strong>No</strong>rwalk, CT 06854<br />

· Tel 203 855 9136<br />

· Fax 203 838 9868<br />

Visit our Web Site –<br />

www.Wilks<strong>IR</strong>.com<br />

info@Wilks<strong>IR</strong>.com

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