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HP 5890 Series I and Series II Reference Manual (05890 ... - Ipes.us

HP 5890 Series I and Series II Reference Manual (05890 ... - Ipes.us

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Temperature Control<br />

Oven temperature calibration<br />

The <strong>HP</strong> <strong>5890</strong> provides the means to (if necessary) reset oven temperature<br />

monitoring so the displayed ACTUAL value accurately represents the<br />

correct temperature.<br />

Oven temperature calibration requires entering the difference (delta)<br />

value (in �C) between an independently measured temperature value<br />

vers<strong>us</strong> the corresponding displayed oven temperature value:<br />

Correction Value =<br />

Measured Temperature (�C) - Displayed Temperature (�C)<br />

For example, if actual measured oven temperature were found to be<br />

148.73�C, while the corresponding displayed value was 150.00, the<br />

calibration difference value to be entered would be -1.27.<br />

Setting the oven calibration value<br />

An oven temperature calibration measurement should be made at a<br />

temperature in the middle of the range of interest. Allow ample time (up<br />

to 1/2•hour)for thermal equilibration at the selected temperature; no<br />

drift should be observed. The temperature•sensingprobe should be placed<br />

in the region of the oven occupied by the column(s).<br />

1. Through the keyboard, select CALIB AND TEST mode, function 1:<br />

CLEAR .<br />

1 ENTER<br />

CALIB is displayed, followed by two values: the observed oven<br />

temperature (to 0.01�C), <strong>and</strong> the current difference (delta)<br />

calibration value.<br />

Note: Record the displayed calibration delta value! If problems are<br />

encountered in recalibration, the value may be reentered.<br />

2. Assuming no drift in temperature, the new difference (delta) value is<br />

then entered by pressing appropriate number keys, followed by ENTER :<br />

appropriate value ENTER<br />

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