Analytical Methodology for Herbicide Orange. Volume II - Special ...

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UnclassifiedJtCUHITY CLASSIFICATION OF THIS PAOtfHTian D«l» B
PREFACEThe research and development described in this report were performed inhouseby the Gaseous lonizat r .on and Excitation Processes Group of theChemistry Research Laboratory, Aerospace Research Laboratories (AFSC),Wright Patterson AFB, Ohio.' This work was funded by Air Force LogisticsCommand, Assistant Deputy Chief of Staff/Distribution, Mr. Karl Merrill.Dr. Billy E. Welch, Special Assistant for Environmental Quality, Officeof the Secretary of the Air Force, had overall cognizance for thiseffort which was undertaken to provide analytical chemistry support ofUSAF efforts to dispose of excess herbicide stocks in accordance withEnvironmental Protection Agency guidelines. The in-house work forcewas augmented during these studies via Contract No. F33615-73-C-4099 withSystems Research Laboratories, Inc., Dayton, Ohio 45440. These studieswere performed under Project 7023, Task 702306, Work Unit 70230614,"Advanced Mass Spectrometric Analytical and Diagnostic Techniques forMaterials and Research Applications."The ARL principal investigator ir. these studies was Dr. Thomas 0. Tiernan,ARL (LJ), Wright Patterson AFB, Ohio 45433.
Page 1 and 2: Item I Number 04848 D NotScann8dAut
Page 4 and 5: A D - A 011 5 y 8ANALYTICAL METHODO
Page 7: UnclassifiedSECURITY CLASSIFICATION
Page 11 and 12: LIST OF TABLESTABLEPAGEIIIIIIIVVVIV
Page 14 and 15: SECTION IINTRODUCTIONCommercial her
Page 16 and 17: SECTION IIEXPERIMENTALSAMPLING PROC
Page 18 and 19: TABLE IIDENTIFICATION DATA ON HERBI
Page 20: 59 Hercutes 14I900 1800 2700TIME, S
Page 23 and 24: m—is900t1800 2700TME.SecFigure 5.
Page 25 and 26: 251 Dow 10s900 1800 2700TIME.SecFig
Page 27 and 28: o CL OO900 1800TIME, SecFigure 9.Ch
Page 29 and 30: 263 MONSANTO 6BOO27QOTOE.SECFigure
Page 31 and 32: TABLE IIICOMPARISON OF ANALYSES OF
Page 33 and 34: TABLE VCOMPARISON OF DUPLICATE SAMP
Page 35 and 36: TABLE VIICOMPARISON OF DUPLICATE SA
Page 37 and 38: TABLE VIIISUMMARY OF ANALYSES OF HE
Page 39 and 40: TABLE VIII (Continued)RetentionTime
Page 41 and 42: 11) Analysis Sequence Group 6 (Mons
Page 43: 19. R. Baughman and M. Meselson, Ad

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