Oilfield nanoparticles: Synthesis, characterization and application.

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X-Ray Diffraction: Zn-Phn600Zn-DTPMP XRD spectrumIntensity (counts40020031.6845.556.575.400 20 40 60 80 1002 thetaX-ray diffraction indicated of the microcrystalline structureof fabricated Zn-Phn particles
Fourier transform infrared spectroscopyAbsorbance0.60.50.40.30.20.10-0.1-0.2-0.3996109014601660FT-IRCa-Phn-A1 (surf)Ca-Phn A2 (No surf)Ca-Phn-B2 (70C, w/ surf)Ca-Phn C2( w/ surf)0 1000 2000 3000 4000 5000Wave number(cm-1)• 1660 cm‐1: surfact adsorbed hydroxyl group;• 1460 cm‐1: C‐H bending in –CH2‐ groups;• 1090 cm‐1: phosphonate P‐O‐Metal;• 996cm‐1: P‐C stretching vibration
Page 4: Why nano?• Nanoparticles is able
Page 7 and 8: Previous work of Dr. Heather Shiple
Page 9 and 10: Background information: Surfactant
Page 11 and 12: Synthesis route for nanoparticles:S
Page 13 and 14: Synthesis schematicSyringePumpVaria
Page 15: X-Ray Diffraction: Ca-Phn800Ca-DTPM
Page 19 and 20: Scanning electron microscopeCa‐DT
Page 21 and 22: Transmission electron microscopyZn-
Page 23 and 24: Slurry Stability: Ca-DTPMPw/o TTAB
Page 25 and 26: AgendaSynthesis andprevious workcha
Page 27 and 28: Mechanisms of particle collisionSed
Page 29 and 30: M-Phn Breakthrough in porous media1
Page 31 and 32: Nanoparticle Return setup:• Retur
Page 33 and 34: 10000Nano-particle return curve:Ca-
Page 35 and 36: 1000Nano-particle return curve:Zn-P
Page 37 and 38: Conclusions• A simple and economi

Oilfield nanoparticles: Synthesis, characterization and application.

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