M.Sc Chemistry - Skymount Distance Education

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UNIT – VProperties of Commercial Polymers : Polyethylene, polyvinyl chlorides,polyesters, phenolic resins, epoxy resins and silicone polymers. Functional polymers –Fire retarding polymers and electrically conducting polymers. Biomedical polymers –contact lens, dental polymers, artificial heart, kidney, skin and blood cells.
MSCH/S/230Paper – 3SPECTROSCOPYUNIT – IUV and IR Spectroscopy : Ultraviolet – visible spectroscopy – types of electronictransitions – chromophores and auxochroms – factors influencing position and intensityof absorption bands – absorption spectra of dienes, ployenes and α , β – unsaturedcarbony 1 compounds – woodward – fieser rules.IR Spectroscopy – vinrational frequencies and factors affecting them –identification of functional groups – intra and inter molecular hydrogen bonding – fingerprint reion – far IT region – metal ligand stretching vibrations.UNIT – II1 H NMR Spectra : Nuclear spin – magnetic moments of a nucles – nuclear spinenergy levels in the presence of magnetic fields, basic principles of NMR experiments –CW and FT NMR – 1 H NMR chemical shift and coupling constants – factors influencingproton chemical shifts and vicinal proton – proton coupling constants.UNIT – III13 C NMR and Two dimensional NMR Spectroscopy :13 C NMR – prtotondecoupled and off-resonance – 13 C NMR spectra – factors affecting 13 C chemical shifts –13 C NMR spectra of simple organic molecules – use of INEPT and DEPT methods inassigning 13 C signals. Basic principles of two dimensional NMR spectroscopy –HOMOCOSY, HETCOSY, NOESY.UNIT – IVPrinciples – Measurement techniques (EI, CI, FD FAB, SIMS) – Presentation ofspectra data – molecular ions – isotope ions – fragment ions of odd and even electrontypes – rearrangement ions – factors affecting fragmentation patterns – Mc.Laffertyrearrangement.UNIT – VIdentification of organic compounds using UV, IR, NMR spectroscopy and massspectrometry – problems.
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M.Sc Chemistry - Skymount Distance Education

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