IRMS catalogue innards.qxd - Spectra 2000 Srl

Ordering InformationWe are happy to accept orders by any ofthe following methods:Phone: +44 (0)1837 54446Fax: +44 (0)1837 54544E-mail: info@microanalysis.co.ukMail: Elemental Microanalysis Ltd1 Hameldown RoadOkehampton Business ParkOkehamptonDevon EX20 1UBUnited KingdomWe can invoice you in Sterling, Euro or USDollar and accept Visa, Mastercard andAmerican Express, account facilities are readilyavailable for regular customers, please enquire.Shipping worldwideWe regularly ship directly to customers in allparts of the world. Local dealers are availablein many countries: contact us for details.Available locally from:

ContentsElementalMicroanalysisOther literature availablefrom Elemental MicroanalysisIn addition to this catalogue a range of othercatalogues and product sheets are available:CataloguesWe publish catalogues covering thefollowing areas of elemental analysis:• Organic Elemental (CHN/O/S)• Nitrogen/Protein• Inorganic• Carbon/Sulphur• IRMS24567IntroductionConfiguration GuideEurovector EA-3028HT/EuroPyrHekatech HT-OThermoFinnigan TC/EAThermoFinnigan TC/EA Modified Lower FittingConsumables and KitsEuropa9Europa Glassware and O-ringsProduct sheetsProduct sheets are available for everyinstrument we support. These cover allthe common day-to-day items requiredto run your instrument. These sheets arelaminated to help them survive in thelab environment.101112GC Combustion/PyrolysisEquilibration Reagents and SundriesIsotope Reference MaterialsNafion Dryers ®Preparation System Vials and SealsFaxback formContract analysis serviceWe also offer a contract analysis servicefor a variety of (mainly) organic compounds.Full details are in this brochure.This additional brochure contains extraconfigurations and products that arespecific to CF and EA-IRMS applications.All other consumables and productssuch as reagents, capsules, glassware etcthat can be used in both EA and EA-IRMSapplications can be found in our mainOrganic Elemental CHN/O/S catalogue.ContentsAll literature is available using the ‘fax-back’form on the rear cover of this catalogue orcan be downloaded from our website.1

ElementalMicroanalysisIntroductionAbout the CompanyElemental Microanalysis grew from smallbeginnings almost 30 years ago as amicro-analytical laboratory to its current formas a leading manufacturer and supplier ofconsumables, supplies and other productsfor Elemental Analysers. We operate fromour purpose-built factory and laboratorycomplex in Devon UK.You learn a lot in 30 years - a lot about yourproducts - how to make them and how to usethem, a lot about your customers and theirneeds. We have been developing, refining andusing products for elemental analysis since1976 and have a unique in-depth knowledgeof instruments from all manufacturers.These days we offer the world’s largest rangeof products for elemental analysers sendingour products to customers across the globe.We take great care with the quality of ourproducts. The vast majority are manufacturedin-house by our trained technicians within ourISO 9001:2000 accredited quality system. Butwe don’t just make the products - we use themevery day in our own analytical laboratory givingus constant feedback on their performance.We do not compromise on quality and don’texpect you to either. Our total satisfactionguarantee backs up our commitment to ourproduct quality.‘Price is what you pay, value is what you get’.As the leading independent supplier of elementalanalysis consumables you can achieve substantialsavings in comparison to the prices charged bythe original supplier of your instrument. But weknow that you need more from a supplier thansimply low prices. You need to buy with theconfidence that your analysis will not becompromised by poor quality consumablesand the knowledge that your supplier has allthe resources to provide the full range of supportthat you expect.We will always treat our customers with honestyand integrity. If we do make a mistake we don’ttry to hide it - we recognise it and put it right.We won’t sell you short measure and we won’tmislead you in any way. Our business is builton long-term relationships as our customers willtestify - many have been with us for more than20 years.Introduction2

ElementalMicroanalysisConfiguration GuideEA-IRMS AnalysisNote: See CHNOS catalogue for other EA configurations

OXYGENKey12345678Product Qty Eurovector no Cat noO-ring for ceramic reactor E13538 E1506Ceramic Outer, 17mm E12507 C1102Glassy Carbon Tube E12529 C7004Nickelised Carbon 20mm E10145 B1182Glassy Carbon Chips 120mm E10521 C7003Quartz Wool 20mm E10514 B1017Quartz Wool 20mm E10514 B1017O-ring, 17mm,bottom quick fit E13539 E1507High TemperaturePyrolysisEurovector EA-3028HT/EuroPyrHYDROGENKey11234567Product Qty Eurovector no Cat noO-ring for ceramic reactor E13538 E1506Ceramic Outer, 17mm E12507 C1102Glassy Carbon Tube E12529 C7004Glassy Carbon Chips 140mm E10521 C7003Quartz Wool 20mm E10514 B1017Quartz Wool 20mm E10514 B1017O-ring, 17mm,bottom quick fit E13539 E150723High TemperaturePyrolysis4567H IN LIQUIDS USING CHROME CATALYSTKey2112345Product Qty Eurovector no Cat noO-ring, 18mm E13536 E1504Modified Quartz Reactor E12512 C1056Chrome Catalyst(Max-Chrome) 90mm E10103 B1450Quartz Wool 10mm E10514 B1017O-ring, 6mmbottom quick fit E13540 E1508GC COLUMNS3123456784Product Eurovector no Cat noGC Column, 1m Stainless Steel E11520 E3001GC Column, 1.5m Stainless Steel E11521 E300954

Key123456Product Qty Hekatech no Cat noCeramic Reactor HE 468110 C1103Glassy Carbon Tube HE 46860100 C7004Nickelised Carbon 10mm HE 33823800 B1182Glassy Carbon Chips 135mm HE 33823850 C7003Nickel Wool 5mm HE 3382500 B1007GC Column, 1m Stainless Steel HE 26007900 E30011234567LIQUID SAMPLESKeySOLID SAMPLESKey12345678Product Qty ThermoF. no Cat noO-ring, Viton 1121120 E6053Graphite Tube 1132080 C7011Ceramic Tube 1121320 C1101Glassy Carbon Reactor 1121310 C7001Glassy Carbon Chips 1117400 C7002Glassy Carbon Chips 1117400 C7002Quartz Wool 20mm 1087770 B1017GC Column 0.6m 1/4 Stainless Steel 1121030 E303512345HEKATECH HT-OHigh TemperaturePyrolysis6Hekatech HT-O112345678910Product Qty ThermoF. no Cat noO-ring, Viton 1121120 E6053Graphite Tube 1121351 C7010Ceramic Tube 1121320 C1101Glassy Carbon Reactor 1121310 C7001Graphite Crucible 1117332 C7012Glassy Carbon Chips 1117400 C7002Silver Wool 5mm 1117430 B1119Glassy Carbon Chips 1117400 C7002Quartz Wool 20mm 1087770 B1017GC Column 0.6m 1/4 Stainless Steel 1121030 E303520mm23270mm 270mm4High TemperaturePyrolysis5High TemperaturePyrolysis68107897ThermoFinnigan TC/EA5

ThermoFinnigan TC/EAModified Lower FittingTC/EA SparesProduct Thermo No. Cat no.Replacement TC/EA Furnace Element 35450010 E4406Furnace Repair*E4407*Furnace repair - a faulty furnace may be may sent to Elemental Microanalysisfor examination with a new element and/or thermocouple fitted if required.Modified Lower Fitting for Improved Analysis of WatersThe adapter channels the helium flow up between the ceramic outer anddown through the centre of the glassy carbon tube ensuring all watervapour is swept down into the reactive zone. Use of this fitting requiresa different length glassy carbon inner from standard (see below).ProductPart no.AdapterE4405O-ring E6054 (pack of 2)Glassy carbon tube 12 x 9 x 453 C7007ElementalMicroanalysisConsumables and KitsGlassy Carbon ChipsC7003Product Pack Cat.no.Glassy carbon tube 12 x 7 x 356 1 C7001Glassy carbon tube 12 x 9 x 453 for use with E4405 1 C7007Glassy carbon tube 12 x 7 x 450(one end closed with 2mm central hole) 1 C7005Glassy carbon tube 12 x 9 x 400 1 C7004Glassy carbon chips (splinter powder) 3-4mm 25g C7002Glassy carbon chips (splinter powder) 2-3mm 25g C7003Graphite Crucible C7012Graphite crucible 4.5 x 3.5 x 30mm 1 C7012Nickel Wool B1007Quartz wool (very pure, very fine) 5g B1017Quartz wool (very pure, very fine) 10g B1208Quartz wool (very pure, very fine) 50g B1102Nickel wool 2g B1007Silver wool 10g B1119GlassyCarbonTubeChrome catalyst (fine powder) 100g B1450Chrome catalyst (fine powder) 25g B1451Consumables and Kits6Nickelised Carbon 30% Ni, granular 0.3-0.85mm 5g B1086Nickelised Carbon 40% Ni, granular 0.3-0.85mm 5g B1087Nickelised Carbon 50% Ni, granular 0.3-0.85mm 5g B1181Nickelised Carbon 30% Ni, granular 0.85-1.7mm 5g B1088Nickelised Carbon 40% Ni, granular 0.85-1.7mm 5g B1106Nickelised Carbon 50% Ni, granular 0.85-1.7mm 5g B1182Spares Kits for IsoPrime ElementalAnalyser ModulesProduct OEM Cat.no.EA-CN 1000 analysis kit 6063056 X3250EA-O and/or H for solid samples(High temperature) 1000 analyses 6062979 X3251EA-Sulphur 1000 analysis kit 6062974 X3252EA-Hydrogen kit for liquid samples(low temperature) 6062977 X3253EA-Oxygen kit for liquid samples 6062978 X3254(High temperature)NickelisedCarbonB1181

1 1228A B39435363 37N DETERMINATIONKey12345678910111213141516Product Qty Europa no Cat noO-Ring, Upper Reaction Tube - E1004Reaction Tube, clear C1001012 C1040Quartz Wool 5mm C1001016 B1208Chromium Oxide 110mm C1001004 B1004Copper Oxide Wires 40mm C1001007 B1002Silver Wool 20mm C1001018 B1119O-ring, Lower Reaction Tube E1005550 E1420Quartz Chips 100mm C1001017 B1008Copper Wires 320mm C1001006 B1015O-Ring, Scrubber Adaptor - E1421Scrubber Tube E1002687 C1063Quartz Wool 10mm C1001016 B1208Magnesium Perchlorate C1001008 B1101Carbosorb, 6-12 mesh C1001001 B1041Carbosorb, 12-24 mesh C1001002 B1042C & N Separation Column E1004907 E3031ABPrepacked Reaction Tube (includes C1050 liner)Transparent X1200Translucent X1201Prepacked Reduction Tube, transparent X1203Prepacked Reduction Tube, translucent X120410111112121413151612121 1228A B34935363377N & C DETERMINATION S DETERMINATIONKeyKey1011121314123456789Product Qty Europa no Cat noO-Ring, Upper Reaction Tube - E1004Reaction Tube, clear C1001012 C1040Quartz Wool 5mm C1001016 B1208Chromium Oxide 110mm C1001004 B1004Copper Oxide Wires 40mm C1001007 B1002Silver Wool 20mm C1001018 B1119O-ring, Lower Reaction Tube E1005550 E1420Quartz Chips 100mm C1001017 B1008Copper Wires 320mm C1001006 B1015O-Ring, Scrubber Adaptor - E1421Scrubber Tube E1002687 C1063Quartz Wool 10mm C1001016 B1208Magnesium Perchlorate C1001008 B1101C & N Separation Column E1004907 E303112A12345678Product Qty Europa no Cat noO-ring, upper E1005551 E1004Reaction Tube C1001012 C1040Quartz Wool 5mm C1001016 B1208Tungstic Oxide on Zirconia 90mm - B1082Copper Wires, high purity 80mm C1001042 B1035Quartz Chips 10mm C1001017 B1008O-ring, lower E1005550 E1420GC Column for S - E3032Prepacked Reaction/Reduction TubeTransparent X1205Translucent X1206ABPrepacked Reaction Tube (includes C1050 liner)Transparent X1200Translucent X1201Prepacked Reduction Tube, transparent X1203Prepacked Reduction Tube, translucent X1204A101131241338751463127Europa7

789109O PYROLYSISKey12345678910111213Product Qty Europa no Cat noO-Ring, upper - E1004Combustion Tube C1001012 C104050% Nickelised Carbon 10mm - B1182Glassy Carbon Chips 2-3mm 180mm C1001071 C7003Quartz Wool 5mm C1001016 B1208O-Ring, lower E1005550 E1420O-ring, scrubber tube - E1421Scrubber Tube E1002687 C1063Quartz Wool 10mm C1001016 B1208Magnesium Perchlorate C1001008 B1101Carbosorb 6-12 mesh C1001001 B1041Carbosorb 12-24 mesh C1001002 B1042GC separation column C1001070 E3030APrepacked Oxygen Pyrolysis TubeTransparent X1207Translucent X120889111213912A34567898EuropaH PYROLYSISKey101112123456789Product Qty Europa no Cat noO-ring, upper - E1004Combustion Tube C1001012 C1040Glassy Carbon Chips 2-3mm 190mm C1001071 C7003Quartz Wool 5mm C1001016 B1208O-ring, lower E1005550 E1420O-ring, scrubber tube - E1421Scrubber Tube E1002687 C1063Quartz Wool 10mm C1001016 B1208Magnesium Perchlorate C1001008 B1101Carbosorb 6-12 mesh C1001001 B1041Carbosorb 12-24 mesh C1001002 B1042GC separation column C1001070 E3030APrepacked Hydrogen Pyrolysis TubeTransparent X1209Translucent X1210781011128121589A B31043593637 7EUROPA ROBOPREP CNKey10111213141516123456789Product Qty Europa no Cat noO-ring upper - E1004Reaction tube C1001012 C1040Quartz wool 5mm C1001016 B1208Chromium oxide 110mm C1001004 B1004Copper oxide wires 40mm C1001007 B1002Silver wool 20mm C1001018 B1119O-ring lower E1005550 E1420Reduction tube C1001014 C1030Quartz wool 10mm C1001016 B1208Copper wires C1001006 B1015Scrubber tube C1001015 C1032Magnesium perchlorate C1001008 B1101Carbosorb 6-12 mesh C1001001 B1180Carbosorb 12-24 mesh C1001002 B1042O-ring, scrubber tube - E1421GC separation column - E3033ABPrepacked Reaction Tube (includes C1050 liner)Transparent X1200Translucent X1201Prepacked Reduction Tube X120215 1511 11991312161499812A3456

Europa O-ringsGlassware and O-ringsElementalMicroanalysisEuropa GlasswareProduct Pack OEM Cat noO-ring Viton 10 E1001O-ring Nitrile 10 E1004Seal Viton Chamfered Square Profile 5 E1042O-ring 1 E1005669 E1420O-ring 1 E1002684 E1421Description Pack OEM Cat no.Reduction Tube 1 C1001014 C1030Scrubber 1 C1001015 C1032Reaction/Reduction Tube, transparent 1 C1001012 C1040Reaction/Reduction Tube, translucent 1 C1001013 C1041Reaction/Reduction Tube, transparent, heavy wall 1 - C1039Sleeve insert 180mm (Open both ends) 1 C1001048 C1050Scrubber 1 E1002687 C1063Sleeve insert 220mm (Open both ends) 1 C1094Sleeve insert 220mm (Closed one end) 1 C2030O-rings shown actual sizeE1001Pre-packed tubes for this instrument are available -please see configuration guide for details.C1041C1040C1039E1004C1030E1042E1420E1421C1063C1032C1094C2030C1050Glassware and O-rings - Europa9

ElementalMicroanalysisGC Combustion/PyrolysisCeramicTubeFurnace Reaction TubesCeramicLength OD ID Cat no Application630mm 6mm 0.7mm C1110 GVI600mm 3mm 0.5mm C1111 Thermo/GVI400mm 1.6mm 0.8mm C1112 Europa/PDZ300mm 1.55mm 0.6mm C1077 Europa/ThermoQuartz TubeC1076QuartzLength OD ID Cat no Application630mm 6mm 0.7mm C1115 GVI220mm 6mm 1.0mm C1075 Europa/PDZ300mm 6mm 1.0mm C1076 EuropaGC Combustion/Pyrolysis / Equilibration Reagents and SundriesNote: quartz and ceramic tubes can be supplied in different lengths.Please contact us with your requirements.Packing MaterialsProduct Pack size Cat noCopper Oxide Wires 1% Pt 1%NiO 5g B1149Copper Oxide Wires 3% Pt 1%NiO 5g B1151Copper Wire 0.125mm diameter 10m D9101Platinum Wire 0.125mm diameter 1m D9100Nickel Wire 0.125mm diameter 10m D9102Copper Granules, fine 0.05-0.2mm 100g B1108Prepacked GC Reaction TubesLength OD ID Material Packing Cat no600mm 3mm 0.5mm Ceramic Cu and Pt wires X1500400mm 1.6mm 0.8mm Ceramic Cu wires X1501400mm 1.6mm 0.8mm Ceramic Cu and Pt wires X1502400mm 1.6mm 0.8mm Ceramic Ni wires X1503630mm 6mm 0.7mm Quartz Copper Oxide wires1% Pt, 1% NiO X1504Note: many combinations of wire types, numbers of strands etc. are possible.Please contact us with your Prepacked GC Reaction Tube requirements.Equilibration Reagents and SundriesProduct Pack Cat noPlatinum Catalysts sticks for HD equilibration 50 sticks B14525% Pt on Alumina -325 mesh powder 10g B1453Tapered glass inserts 1000 E280010

Isotope Reference MaterialsElementalMicroanalysisIsotope Reference Materials from Elemental Microanalysis aretraceable to primary standards issued by IAEA Vienna.These materials are supplied with Certificates of Analysis.Values shown are indicative and may vary slightlyfrom batch to batch.Actual values shown on certificate.Reference Materials (RM)Cat no Standard Pack %C ∂C 13 %N ∂N 15 %S ∂S 34B2151 Sediment 5g 6.5 -26 0.5 +4 0.9 +4B2153 Soil 5g 1.5 -27 0.15 +7 0.03 +5B2155 Protein (Casein) 5g 47 -27 14 +6 0.9 +6B2157 Wheat Flour 5g 40 -27 1.5 +3 0.1 -1B2159 Sorghum Flour 5g 42 -14 1.5 +2 0.1 +10Uncertified Working Reference MaterialsCat no Standard Pack ∂C 13 ∂N 15B2172 Olive Oil 5g -28.5 -B2174 Urea 5g -45 -0.8Nafion Dryers ®ANafion ® water removal dryers can be supplied as complete units or replacement inner elements.Dryers and elements are supplied with 0.05” OD, 0.04” ID Nafion ® tubing.Dimensions1/8"Product1/8"14"Stainless steel body, 1/8” end fittings (A)Stainless steel body, 1/16” end fittings (A)Fluoropolymer body, 1/8” end fittings (A)Polypropylene body, 1/8” end fittings (A)Complete DryerCat noE2810E2811E2812E2813Replacement Inner ElementsProductElements, 12” long, 0.05” OD tubing, flanged end piecesPolypropylene endsCat noE28201/8"AIsotope Reference Materials / Nafion Dryers ®Nafion ® is a registered trademark of E.I. DuPontFluoropolymer endsStainless steel endsE2821E282211

ElementalMicroanalysisPreparation System Vials and SealsDescription4.5ml Borosilicate Vial - round bottomed, 46 x 15.5mmPack of 1000Non-evacuated, unlabelled, seal + white capEvacuated, unlabelled, seal + white capNon-evacuated, labelled, seal + white capEvacuated, labelled, seal + white capPart NoE2830E2831E2832E28335.9ml Soda Glass Vial - flat bottomed, 55 x 15.5mmPack of 1000Non-evacuated, unlabelled, seal + white capEvacuated, unlabelled, seal + white capNon-evacuated, labelled, seal + white capEvacuated, labelled, seal + white capE2840E2841E2842E284312ml Soda Glass Vial - flat bottomed, 101 x 15.5mmPack of 1000Non-evacuated, unlabelled, seal + white capEvacuated, unlabelled, seal + white capNon-evacuated, labelled, seal + white capEvacuated, labelled, seal + white capE2850E2851E2852E285312ml Borosilicate Vial - round bottomed, 101 x 15.5mmPack of 1000Non-evacuated, unlabelled, seal + white capEvacuated, unlabelled, seal + white capNon-evacuated, labelled, seal + white capEvacuated, labelled, seal + white capE2860E2861E2862E286312ml Soda Glass Vial - flat bottomed, 101 x 15.5mmSilicone coated for C 13 Breath Testing, Pack of 1000Non-evacuated, unlabelled, seal + white capEvacuated, unlabelled, seal + white capNon-evacuated, labelled, seal + white capEvacuated, labelled, seal + white capE2870E2871E2872E2873Preparation System Vials and Seals12ml Borosilicate Vial - round bottomed, 104 x 15.5mmPack of 1000The new thread profile on this Exetainer ® gives a very tightscrew fit, and is designed to avoid any cap movement whensamples are heated - eg. on a GasBench.Non-evacuated, unlabelled, seal + white capEvacuated, unlabelled, seal + white capNon-evacuated, labelled, seal + white capEvacuated, labelled, seal + white capCaps are available in a variety of colours, also replacement capsand seals - please enquire for details.Exetainer ® is a registered trademark of Labco Ltd.E2880E2881E2882E288312

LITERATURE REQUEST FAXBACK FORMFor full details of all the products we supply for yourinstrument please copy this page and fax it back to us.+44 (0)1837 54544 or your local dealer:Please tick to request the relevant literature.Micro/CHN(OS) InstrumentsThermoFinnigan Flash EA1112 CHNOSThermoFinnigan Flash EA1112 NC/SThermoFinnigan (Carlo Erba/Fison) EA1110ThermoFinnigan (Carlo Erba/Fison) EA1108ThermoFinnigan (Carlo Erba/Fison) EA1106ThermoFinnigan (Carlo Erba/Fison) EA1102/1104ThermoFinnigan (Carlo Erba/Fison) NA2500 N/NC/NCSThermoFinnigan (Carlo Erba/Fison) NA1500 (Series 1&2)CataloguesCHNOSInorganicCarbon/SulphurNitrogen/ProteinContract Analysis ServicePerkin Elmer 2400Perkin Elmer 240 Series ABCPerkin Elmer 440Perkin Elmer 2410Exeter Analytical (CEC) CE440Exeter Analytical (CEC) 240Europa RoboprepEuropa AncaEuropa IntegraElementar (Foss Heraeus) Vario ELElementar (Foss Heraeus) CHN RapidNameOrganisationAddressEuroVector EA3000Leco ® CHN-900Leco ® CHN-932Leco ® CHN-1000Leco ® CHN-2000Leco ® CHN-600Leco ® CHN-800Leco ® Truspec CHN/CNTelCostech ECS 4010FaxE-mail“the centre of excellence in elemental analysis”Elemental Microanalysis Ltd • Hameldown Road • Okehampton Business Park • Exeter Road • Okehampton • Devon EX20 1UB • United KingdomTel: +44 (0)1837 54446 • Fax: +44 (0)1837 54544 • E-mail: info@microanalysis.co.uk • Website: www.microanalysis.co.ukCompany Registration No: 1281028 • VAT No: 217 5194 65

Elemental Microanalysis LtdHameldown RoadOkehampton Business ParkExeter RoadOkehamptonDevon EX20 1UBUnited KingdomTel: +44 (0)1837 54446Fax: +44 (0)1837 54544E-mail: info@microanalysis.co.ukwww.microanalysis.co.uk