Dynamic Nuclei Polarization
Dynamic Nuclei Polarization
Dynamic Nuclei Polarization
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Dissolution Procedure<br />
➣<br />
➣<br />
➣<br />
DNP-insert replaced by<br />
‘dissolution’ insert<br />
Dissolution of the solid material<br />
by water<br />
(some bar at ~ 150°C)<br />
Dissolution exit directly connected<br />
with the infusion apparatus<br />
H 2 O (150°C, 12 bar)<br />
dissolved sample<br />
+ 4 He-Gas →<br />
infusion apparatus<br />
NMR coils<br />
target material<br />
~ 1ml