02.10.2015 Views

Dynamic Nuclei Polarization

Dynamic Nuclei Polarization

Dynamic Nuclei Polarization

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Dissolution Procedure<br />

➣<br />

➣<br />

➣<br />

DNP-insert replaced by<br />

‘dissolution’ insert<br />

Dissolution of the solid material<br />

by water<br />

(some bar at ~ 150°C)<br />

Dissolution exit directly connected<br />

with the infusion apparatus<br />

H 2 O (150°C, 12 bar)<br />

dissolved sample<br />

+ 4 He-Gas →<br />

infusion apparatus<br />

NMR coils<br />

target material<br />

~ 1ml

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