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In-Tube SPME–LC–MS of Herbicides in Water 381 2. Schantz, S. L. and Widholm, J. J. (2001) Cognitive effects of endocrine-disrupting chemicals in animals. Environ. Health Perspect. 109, 1197–1206. 3. Waissmann, W. (2002) Health surveillance and endocrine disruptors. Cad. Saude. Publ. 18, 511–517. 4. van der Hoff, G. R. and van Zoonen, P. (1999) Trace analysis of pesticides by gas chromatography. J. Chromatogr. A 843, 301–322. 5. Karcher, A. and El Rassi, Z. (1999) Capillary electrophoresis and electrochromatography of pesticides and metabolites. Electrophoresis 20, 3280–3296. 6. D’Ascenzo, G., Curini, R., Gentili, A., Bruno, F., Marchese, S., and Perret, D. (2000) Determination of herbicides in water using HPLC–MS techniques. Adv. Chromatogr. 40, 567–598. 7. Hogendoorn, E. and van Zoonen, P. (2000) Recent and future developments of liquid chromatography in pesticide trace analysis. J. Chromatogr. A 892, 435–453. 8. Sabik, H., Jeannot, R., and Rondeau, B. (2000) Multiresidue methods using solid-phase extraction techniques for monitoring priority pesticides, including triazines and degradation products, in ground and surface waters. J. Chromatogr. A 885, 217–236. 9. Wells, M. J. and Yu, L. Z. (2000) Solid-phase extraction of acidic herbicides. J. Chromatogr. A 885, 237–250. 10. Pico, Y., Font, G., Molto, J. C., and Manes, J. (2000) Solid-phase extraction of quaternary ammonium herbicides. J. Chromatogr. A 885, 251–271. 11. Lee, N. A. and Kennedy, I. R. (2001) Environmental monitoring of pesticides by immunoanalytical techniques: validation, current status, and future perspectives. J. AOAC Int. 84, 1393–1406. 12. Beltran, J., Lopez, F. J., and Hernandez, F. (2000) Solid-phase microextraction in pesticide residue analysis. J. Chromatogr. A 885, 389–404. 13. Krutz, L. J., Senseman, S. A., and Sciumbato, A. S. (2003) Solid-phase microextraction for herbicide determination in environmental samples. J. Chromatogr. A 999, 103–121. 14. Arthur, C. L. and Pawliszyn, J. (1990) Solid-phase microextraction with thermal desorption using fused silica optical fibers. Anal. Chem. 62, 2145–2148. 15. Kataoka, H., Lord, H. L., and Pawliszyn, J. (2000) Applications of solid-phase microextraction in food analysis. J. Chromatogr. A 880, 35–62. 16. Lord, H. and Pawliszyn, J. (2000) Evolution of solid-phase microextraction technology. J. Chromatogr. A 885, 153–193. 17. Alpendurada, M. de F. (2000) Solid-phase microextraction: a promising technique for sample preparation in environmental analysis. J. Chromatogr. A 889, 3–14. 18. Pawliszyn, J. (2001) Solid-phase microextraction. Adv. Exp. Med. Biol. 488, 73–87. 19. Buldini, P. L., Ricci, L., and Sharma, J. L. (2002) Recent applications of sample preparation techniques in food analysis. J. Chromatogr. A 975, 47–70. 20. Zambonin, C. G. (2003) Coupling solid-phase microextraction to liquid chromatography. A review. Anal. Bioanal. Chem. 375, 73–80. 21. Eisert, R. and Pawliszyn, J. (1997) Automated in-tube solid-phase microextraction coupled to high-performance liquid chromatography. Anal. Chem. 69, 3140–3147. 22. Kataoka, H. (2002) Automated sample preparation using in-tube solid-phase microextraction and its application—a review. Anal. Bioanal. Chem. 373, 31–45. 23. Gou, Y., Tragas, C., Lord, H. L., and Pawliszyn, J. (2000) On-line coupling of in-tube solid-phase microextraction (SPME) to HPLC for analysis of carbamates in water samples: comparison of two commercially available autosamplers. J. Microcol. Sep. 12, 125–134. 24. Gou, Y. and Pawliszyn, J. (2000) In-tube solid-phase microextraction coupled to capillary LC for carbamate analysis in water samples. Anal. Chem. 72, 2774–2779.
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TM METHODS IN BIOTECHNOLOGY � 19
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M E T H O D S I N B I O T E C H N O
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© 2006 Humana Press Inc. 999 River
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vi Preface candidates for a relevan
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viii Contents 9 Analysis of Pentach
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x Contents 30 On-Line Admicelle-Bas
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xii Contributors JANE C. CHUANG •
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xiv Contributors JOHN PATSIAS • A
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4 Martínez Vidal et al. excellent
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6 Martínez Vidal et al. Table 1 MS
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8 Martínez Vidal et al. 7. Check t
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F2 10 Martínez Vidal et al. where
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12 Martínez Vidal et al. 11. Inter
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14 Martínez Vidal et al. 11. Kohlm
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Pyrethroids in Blood Plasma and Uri
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19 Fig. 1. Metabolism of the pyreth
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36 Barr et al. Because the metaboli
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38 Table 1 Pesticides Included in t
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40 Barr et al. 4. Spike the first p
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42 Table 3 High-Resolution Mass Spe
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44 Table 3 High-Resolution Mass Spe
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46 Barr et al. 4. Griffin, P., Maso
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OCPs in Human Fluids by SPDE and GC
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62 Barr et al. exposures (2). For c
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64 Table 1 The Target Analytes, Abb
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66 Fig. 1. Structures of target ana
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68 Barr et al. Table 3 Pesticides a
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70 Barr et al. 3.2.3.2. NATIVE STAN
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72 Barr et al. 8. Inject each sampl
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74 Barr et al. Table 5 Optimized Pr
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76 Barr et al. 3.7.4. Intra- and In
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78 Barr et al. 11. Hill, R. H., Jr.
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80 Fustinoni et al. Fig. 1. Molecul
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82 Fustinoni et al. Develop the che
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84 Fustinoni et al. the ETU and ETU
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86 Fustinoni et al. 3.3. Biological
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88 Fustinoni et al. of pesticides s
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2,4-D and MCPA in Human Urine 91 7
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2,4-D and MCPA in Human Urine 93 4.
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2,4-D and MCPA in Human Urine 95 Ta
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2,4-D and MCPA in Human Urine 101 F
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2,4-D and MCPA in Human Urine 103 6
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106 Jardim, Pozzebon, and Queiroz S
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108 Jardim, Pozzebon, and Queiroz 3
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110 Jardim, Pozzebon, and Queiroz A
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112 Zhang been widely used to detec
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114 Zhang 3. Maintain the ion sourc
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116 Zhang Fig. 1. Mass ion chromato
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118 Zhang 15. Crespin, M. A., Galle
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120 Knopp The search for alternativ
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122 Knopp 4. Dissolve 40 mg BSA in
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124 Knopp Fig. 2. Scheme of tracer
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126 Knopp Fig. 3. Flow chart of the
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128 Knopp Fig. 4. Phenoxyalcanoic a
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130 Knopp 18. No or only minimal sa
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HTS-IS-ELISA for Biomonitoring Chlo
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150 van Hemmen, van der Jagt, and B
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166 Glass the collector and the mom
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168 Glass 3.2.1. Selection of Appli
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170 Glass Fig. 2. A field layout fo
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172 Glass questions that may arise
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174 Glass 3.5.3. Labeling of Media
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176 Glass Again, this can be relate
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Determination of Insecticides in In
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185 Fig. 3. Total ion current (TIC)
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187 Fig. 5. TIC chromatogram (y-axi
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Exposure to Malathion and Metabolit
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208 Araque et al. tive xenoestrogen
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210 Araque et al. 3. Methods The me
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212 Araque et al. values of 0.1 to
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214 Araque et al. estradiol and tra
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Internal Quality Criteria 219 17 Qu
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Internal Quality Criteria 221 instr
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223 Fig. 1. Basic components of the
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Internal Quality Criteria 225 Fig.
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Internal Quality Criteria 227 Resul
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Internal Quality Criteria 229 5. Th
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Pesticide Analysis by ELISA 231 18
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Pesticide Analysis by ELISA 233 4.
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QuEChERS Approach for Pesticides 23
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253 Table 2 Conditions for the GC-M
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264 Di Muccio et al. 1. Introductio
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266 Di Muccio et al. Fig. 1. Assemb
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268 Di Muccio et al. Table 1 Mean (
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270 Di Muccio et al. evaporator. In
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Pesticide Analysis by LPGC-MS/MS 27
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286 Barker shorten turnaround time,
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288 Barker 9. The extract is placed
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290 Barker The mobile phase composi
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292 Barker phase solid support surf
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294 Barker 8. Fernandez, M., Pico,
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296 Barker 43. Pico, Y., Molto, J.
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298 Picó ultraviolet absorbance, i
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300 Picó 3. Attach the conditioned
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302 Picó Fig. 2. EDA-only vs conve
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304 Picó Fig. 3. CE-MS/ESI electro
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306 Picó Fig 4. CE-MS/ESI electrop
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308 Picó tration. The optimum samp
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Residues in Grain and Dried Foodstu
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320 Papadopoulou-Mourkidou, Papadak
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326 Table 4 Method Validation Data:
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Molecular Imprinted Solid-Phase Ext
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Molecular Imprinted Solid-Phase Ext
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436 Papadopoulou-Mourkidou, Patsias
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438 Fig. 1. Simplified flow diagram
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Analysis of Organotins by GC-HRMS 4
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457 Table 1 Calibration Curves for
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459 Table 4 Summary of Positive Ion
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Triazine in Water 467 34 Determinat
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Triazine in Water 469 with various
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Triazine in Water 471 Fig. 1. A chr
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Triazine in Water 473 Fig. 2. LC/AP
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475 Table 3 General Conditions Used
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Triazine in Water 477 (>60%) except
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Triazine in Water 479 13. Koskinen,
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482 Rodríguez-Mozaz, López de Ald
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Index 491 Index Adipose tissue anal
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Index 493 high-throughput screening
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Index 495 Food analysis, see Atrazi
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Index 497 HPLC, see High-performanc
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Index 499 quality control, 98 recov
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Index 501 Pyrethroids, air sampling
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Index 503 Uncertainty, estimation,
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