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Fine Coal Recovery From The Ömerler Washery Tailings And Plant ...

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<strong>Fine</strong> <strong>Coal</strong> <strong>Recovery</strong> <strong>From</strong> <strong>The</strong> <strong>Ömerler</strong> <strong>Washery</strong> <strong>Tailings</strong> <strong>And</strong> <strong>Plant</strong> Applications<br />

Ayşe Erdem, Akan Gülmez, Oğuz Altun, Selami Toprak<br />

General Directorate Of Mineral Research <strong>And</strong> Exploration (MTA), Ankara, Turkey.<br />

Zeki Olgun, Ahmet Gitmez<br />

General Directorate of Turkish <strong>Coal</strong> Enterprises (TKI), Ankara, Turkey.<br />

ABSTRACT: In this study, approximately 3 tons of coal sample taken from thickener entrance was<br />

prepared by mineral processing techniques and cleaned by gravity methods. <strong>The</strong> samples were classified<br />

to 5 size fractions by wet screening. <strong>The</strong> size fractions of +1mm and -1 +0.500 mm were chosen for direct<br />

consumption or cleaning by spirals. <strong>The</strong> studies by Multi Gravity Separator (MGS) were carried out with<br />

the -0.500 +0.280 mm and -0.280 +0.020 mm size fractions where the -0.020 mm fraction does not used<br />

in the experiments. <strong>The</strong> clean coal fractions of +1 mm and -1 +0.500 mm obtained by classification were<br />

subjected to lower calorific value (LCV), ash and total sulphur analyses. <strong>The</strong> results were 4168-4946<br />

kcal/kg (on dry basis), 31.01-38.54 % ash and 4-4.27 % total sulphur content respectively. <strong>The</strong> results of<br />

the clean coal concentrated by MGS experiments in -0.500 +0.280 mm fraction was found 5918 kcal/kg<br />

LCV, 19.82 % ash content and 80.47 % combustible recovery. <strong>The</strong> results for the -0.280 +0.020mm<br />

fraction were 6004 kcal/kg LCV, 19.19 % ash content, 80.47 % combustible recovery respectively. With<br />

reference to the above experimental results, pre-economic evaluation studies were completed and decided<br />

to construct an additional unit to the plant. Capacity of the constructed unit is 75.000 t/y which<br />

corresponds $ 2.600.000 income in a year. General Directorate of Turkish <strong>Coal</strong> Enterprises concluded to<br />

apply this project to the other coal washing plants in the country due to the successful results of this study<br />

and laboratory studies has been going on by MTA currently<br />

INTRODUCTION<br />

Turkish <strong>Coal</strong> Enterprises (TKI) is the largest public organization in Turkey. One of its regional<br />

institutions is Western Lignite Establishment (GLI) locating at Tavşanlı Town of Kütahya Province.<br />

6.1 million tons of run of mine of coal has been produced at GLI. More than 45 % of these are consumed<br />

to produce electrical energy at nearby thermal power plants. <strong>The</strong> remaining (55 %) is washed at <strong>The</strong><br />

Washeries of Tunçbilek and <strong>Ömerler</strong>.<br />

Both <strong>The</strong> Washeries of Tunçbilek and <strong>Ömerler</strong> are sub-units of GLI. <strong>The</strong> former plant was in service<br />

in 1952 and the latter one was in service in the year of 1994. <strong>Ömerler</strong> <strong>Washery</strong> being a public<br />

organization has been in service with 600 tons per hour of capacity in the year of 1994 after completing<br />

its performance tests in 1993.<br />

<strong>The</strong> tailings of these two plants are accumulated at the ponds containing plenty amounts of fine coal<br />

particles.<br />

EXPERIMENTAL<br />

Equipment and Method<br />

<strong>The</strong> laboratory type C 900 MGS was used in the experimental work. (MGS Application Guide 1991,<br />

Chan et al. 1991). 25 % solid concentration (by weight) was prepared and fed to the MGS by using a<br />

peristaltic pump to obtain a continuous run. <strong>The</strong> mixture was agitated mechanically during the<br />

experiment. <strong>The</strong> MGS variables were adjusted at the required levels as per the experimental design. <strong>The</strong><br />

feed slurry was then fed to the MGS feed vessel at the required flow rate while the MGS was in operation.<br />

Samples from the concentrate and tailings streams were collected at steady state conditions, which were<br />

achieved after about 5 min of processing. Heavy product, which was collected through front launder,


eferred to as tailings, and light product, which was collected through back launder, referred to as<br />

concentrate. <strong>The</strong> samples were filtered, dried, and analysed for ash, sulphur and LCV.<br />

Sample<br />

Approximately 3 tons of samples were taken from entrance of TKI-GLI-<strong>Ömerler</strong> <strong>Washery</strong> tailing<br />

thickener. <strong>The</strong> samples were mixed and obtained a homogenously composite sample.<br />

<strong>The</strong> slurry sample was then wet sieved into four size fractions; +0.500; -0.500 +0.280; -0.280 +0.020<br />

and -0.020 mm. <strong>The</strong> sieve analysis, ash, total sulphur, LCV and combustible recovery of fractions are<br />

given in Table 1. <strong>The</strong> +0,500 mm fraction was not used in experimental studies because of that fraction<br />

be able to directly selling or available (cleanable) at spirals; –0.500 +0.280 and –0.280 +0.020 mm<br />

fractions were cleaned by MGS. Preliminary experiments revealed that –0.020 mm fraction was not<br />

effectively cleaned by physical methods and therefore was not used in the experimental work.<br />

Table 1. <strong>The</strong> sieve analysis of the composite sample on dry basis<br />

Particle Size, Weight Grade (%)<br />

mm<br />

(%)<br />

Ash S LCV, kcal/kg<br />

+1 1.56 31.01 4.00 4946<br />

-1 +0.500 5.11 38.54 4.27 4168<br />

-0.500 +0.280 7.90 34.69 3.60 4435<br />

-0.280 +0.150 4.76 34.45 3.11 4544<br />

-0.150 +0.100 3.49 35.82 3.03 4402<br />

-0.100 +0.055 5.24 42.10 2.69 3878<br />

-0.055 +0.038 2.33 47.70 2.28 3279<br />

-0.038 +0.020 2.69 54.44 1.99 2868<br />

-0.020 66.94 77.92 0.76 707<br />

Feed 100.00 65.02 1.57 1840<br />

<strong>The</strong> general studies of abovementioned work to determine both physical and chemical properties of<br />

output of coal washing plant, one can summarize;<br />

<strong>The</strong>re is a significant density difference between coal and gangue,<br />

About 6.67 % of sample has an over 0.500 mm. particle size,<br />

<strong>The</strong> coal particle size is average 10 microns in the -20 microns sized slurry fraction having 66.94 %<br />

weight of the sample and 707 kcal /kg. of LCV,<br />

<strong>The</strong> LCV of sample vary from 3868 to 4946 kcal /kg. at over 20 microns particle sized sieve fractions,<br />

<strong>The</strong> MGS experiments reveal that the prepared sample has 7.90 % by weight at -0.500 +0.280 mm.<br />

and 18.51 % by weight at -0.280 +0.020 mm. sieve fractions<br />

<strong>The</strong> Russell branded wet -sieve system is employed for preparation of different sized fractions of<br />

sample.<br />

<strong>The</strong> fractions of samples used in the experiments of MGS are both the fractions of -0.500 +0.280 mm.<br />

and -0.280 +0.020 mm. But, the fraction of -0.020 mm. is removed as slurry without any treatment.<br />

Experiments<br />

MGS Experiments at -0.500 +0.280 Fraction<br />

Wash water flow rate, drum speed and tilt of the drum were tested to determine optimum conditions of<br />

separation. Shake frequency and shake amplitude of the MGS were predetermined and set as 4 cps and 10<br />

mm, respectively. Results are illustrated in graphs in terms of ash content and combustible recovery in the


concentrate fraction. <strong>The</strong> results for coarse (-0.500 +0.280 mm) fraction are given in Table 2 and Figure<br />

1.<br />

Table 2. Optimum values for -0.500 +0.280 particle size<br />

TILT<br />

DEGREES º<br />

CONCENTRATE (%)<br />

Weight Dry Ash Sulphur Combustible <strong>Recovery</strong> LCV<br />

kcal/kg<br />

0 67.37 21.28 1.82 84.11 5892<br />

1 69.51 19.82 1.19 85.24 5918<br />

2 78.13 25.63 1.19 90.64 5450<br />

Concentrate,%<br />

100<br />

80<br />

60<br />

40<br />

20<br />

0<br />

0 1 2 3 4<br />

Tilt of Drum, º<br />

Figure 1. Optimum values graph of tilt degrees for -0.500 +0.280 mm particle size<br />

<strong>The</strong> effect of wash water was studied at three different flow rates, i.e. 1, 2 and 3 l/min and drum speed<br />

and tilt of drum were adjusted as 240, 260 and 280 rpm and 0, 1 and 2�, respectively.<br />

When Washing water and speed of drum are examined, one can say that the increasing of washing<br />

water causes the picking up of ash content and decreasing of LCV.<br />

<strong>The</strong> stratification of sample in the MGS takes place from surface to inward that decreasing of the<br />

density. <strong>The</strong> particles having less density on upper part of the strata are transported to the back exit of the<br />

device due to the effects of washing water. But, the denser particles sitting inside of drum are drifted to<br />

the front exit by scrapers. Here, the denser particles have the same revolution direction with the drum.<br />

<strong>The</strong> scraper’s revolution speed is more than the particle’s speed, however. <strong>The</strong> more the washing water<br />

means the more the drifted light material toward the back exit. Relatively, that makes an increase of ash,<br />

too.<br />

<strong>The</strong> increasing of the tilt of the drum causes the increase of amount of concentrate. But, the<br />

transportation by scrapers becomes difficult.<br />

By the operation principle of the MGS, the dense material is taken from the front exit. <strong>The</strong> light<br />

material is taken back front, however.<br />

Weight<br />

Dry Ash<br />

Total Sulphur<br />

Combustible<br />

<strong>Recovery</strong>


MGS Experiments at -0.280 +0.020 Fraction<br />

<strong>The</strong> effect of drum speed, wash water amount, tilt of drum, shake amplitude and shake frequency<br />

parameters studied on this size fraction, respectively. Operation conditions are also specified at<br />

experiments. <strong>The</strong> results are given in Table 3 and Figure 2, respectively.<br />

<strong>The</strong> -0.280 +0.020 mm size fraction which is used in experiments, 18.51 % of the material constitute.<br />

Table 3. Optimum values for -0,280 +0,020 particle size<br />

TILT<br />

DEGREES º<br />

CONCENTRATE (%)<br />

Weight Dry Ash Sulphur Combustible <strong>Recovery</strong> LCV<br />

kcal/kg<br />

0 59.17 19.19 1.63 80.47 6004<br />

1 64.12 21.37 1.19 84.67 5877<br />

2 66.10 22.89 1.19 87.22 5696<br />

Figure 2. Optimum values graph of tilt degrees for -0.280 +0.020 mm particle size<br />

Installation of Industrial <strong>Plant</strong><br />

Concentrate,%<br />

100<br />

80<br />

60<br />

40<br />

20<br />

0<br />

0 1 2 3 4<br />

Tilt of Drum, º<br />

A protocol was signed within the scope of projects carried out jointly between TKI and MTA. By this<br />

protocol, a pilot plant will be established in Tunçbilek <strong>Ömerler</strong> <strong>Washery</strong> whose condition for this purpose<br />

considering appropriate by TKI<br />

<strong>The</strong> plant was supposed to be found nearby outside the washing plant. <strong>The</strong> samples were taken to<br />

conduct mineral processing studies at MTA. <strong>The</strong> technological studies on these samples reveal that fine<br />

coal can be recovered economically and technically.<br />

<strong>The</strong> four alternative methods were presented to the General Directorate of TKI after the result of prefeasibility<br />

studies. By the lights of these technical data, a pilot plant was established at a chosen place at<br />

Tunçbilek <strong>Ömerler</strong> <strong>Washery</strong>. (Table 4)<br />

Weight<br />

Dry Ash<br />

Total Sulphur<br />

Combustible<br />

<strong>Recovery</strong>


Table 4. <strong>The</strong> Alternative Economical Assessment of the <strong>Tailings</strong> of <strong>Ömerler</strong> <strong>Washery</strong><br />

ALTERNATIVES CLASSIFICATION ALTERNATIVE MGS ALTERNATIVE<br />

1-Selling to Power <strong>Plant</strong><br />

Investment ($) 444.583 1.192.811<br />

Running Costs ($/y) 243.731 282.985<br />

Running Incomes ($/y) 4.039.845 3.476.411<br />

Net Present Value ($) 22.230.026 17.996.548<br />

Rate of Return (%) 672 213<br />

2-Selling to Cement Factory<br />

Investment ($) 444.583 1.587.356<br />

Running Costs ($/y) 243.731 282.985<br />

Running Incomes ($/y) 6.633.572 5.708.393<br />

Net Present Value ($) 37.696.849 31.306.225<br />

Rate of Return (%) 1127 360<br />

As a result of evaluations of alternative methods, TKI decided to invest in additional units. To observe<br />

the applicability of this work, the first alternative was accepted. By this first alternative, the additional<br />

unit could provide only classification of fine coal that is saleable to power plants.<br />

RESULTS AND DISCUSSIONS<br />

a. <strong>The</strong> experiments were executed by a C 902 type semi-pilot MGS. <strong>The</strong> optimum laboratory<br />

conditions were determined using drum speed, washing water flow rate, slope of drum as parameters. <strong>The</strong><br />

studies show that purposed plant can produce TKI demanded market products of coal having the various<br />

LCV.<br />

b. When it was evaluated, the lowest value of result is obtained at the -0.500 +0.280 mm. particle<br />

sized product recovered by 98.56 % combustible recovery with 4750 kcal /kg. LCV and having 33.09 %<br />

dry- ash content.<br />

<strong>The</strong> upper value of the result was obtained at 85.24 % of combustible recovery at the same particle<br />

size having 5918 kcal /kg. of LCV and 19.82 % dry –ash content.<br />

c. As for the -0.280 +0.020 mm. sieve fraction, the minimum value of result was obtained at the<br />

product recovered by 91.68 % combustible recovery with 5380 kcal /kg. LCV and having 26.68 % dry-<br />

ash content.<br />

<strong>The</strong> maximum value of the result was reached at 80.47 % of combustible recovery at the same particle<br />

size having 6004 kcal /kg. of LCV and 19.19 % dry –ash content.<br />

d. <strong>The</strong> obtained this quality fine coal can be present to either blending it with the coal having a low<br />

specific calorie to feed the power plants or marketing it to the industrial plants who use fine coal.<br />

e. By the light of studies conducted by Mineral Processing Division of MTA, TKI invested in the<br />

Directorate of GLI of <strong>The</strong> <strong>Washery</strong> of Tunçbilek-<strong>Ömerler</strong> to evaluate of this work economically. As<br />

mentioned above, the first alternative was realized and the plant has been established.<br />

f. As soon as possible the pilot plant had been setup, the industrial scale plant was built and installed<br />

by the date of November, 2009. Since then, the saleable fine coal has been produced at the plant.<br />

g. <strong>The</strong> cost of the investment was regained in two weeks of operations of the plant. It was<br />

determined that the <strong>Washery</strong> of Tunçbilek-<strong>Ömerler</strong> can recover 75.000 tons of fine coal valuing $<br />

2.600.000. This fine coal can market to EÜAŞ (<strong>The</strong> Electrical Production Cooperation).<br />

h. In the year 2011, a new project is initiated to execute same studies on the other washing plants by<br />

jointly TKI and MTA. By the scope of this project, the team of experts have already examined concerning<br />

coal washing plants and decided to be taken enough amount of samples;<br />

� <strong>From</strong> the thickener entrance of Dereköy of Ege Lignite Establishment,<br />

� <strong>From</strong> the thickener output of the <strong>Washery</strong> of Directorate of Seyitömer Lignite Establishment.


REFERENCES<br />

Burt, O.R. 1984. Gravity concentration technology, Elsevier science publishers B.V, Amsterdam. <strong>The</strong><br />

Netherlands, 603 p.<br />

Chan, B.S.K., Mozley, R.H. & Childs, G.J.C. 1991. <strong>The</strong> MGS-A mine scale machine UK, Richard<br />

Mozley ltd.<br />

Erdem, A., Olgun, Z., Gülmez, A., Koca, S. & Öteyaka, B. 2008. Beneficiation of lignites by means of<br />

shaking table, MGS and flotation, Project report 4, Project No. 106G056 (Turkish), MTA, Ankara.<br />

MGS Application Guide. 1991. How to get the best from your C 900 MGS. UK, Richard Mozley ltd.<br />

Kirnarsky, A. & Sbitnev, M. 1998. Development of spiral separation technology for coal slimes<br />

treatment. Proceedings of the fifth international symposium on environmental issues and waste<br />

management in energy and mineral production, Ankara. Turkey, pp.659-662.<br />

Erdem A, Gülmez A ve Altun O. 2010. Beneficiation of lignites by means of shaking table, MGS and<br />

flotation, Project report, Proje No, 106G056 (Turkish), TÜBİTAK, Ankara<br />

www.tki.gov.tr/ activity report (Turkish), 2010.<br />

*This Project supported by TÜBİTAK.

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