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02.06.2017<br />

Harburg-Freudenberger<br />

Maschinenbau GmbH<br />

Relaxed extrusion: A very<br />

important precondition for<br />

high quality treads.<br />

Dr.ir. Gerard Nijman<br />

June 16, 2017<br />

gerard.nijman@hf-group.com<br />

Content<br />

• Tread and sidewall profiles & a typical extrusion line lay out<br />

• Rubber rheology, extrudate swell and profile shrinkage<br />

• How to optimize an extrusion line with respect to rheology?<br />

– Extruder screw design<br />

• Temperature homogeneity<br />

• Feeding conditions<br />

– Balanced flow channels<br />

– Preformer and die-design preconditions<br />

– Relaxed extrusion / shrinkage conveyor design<br />

– Extrusion line control / dancer<br />

• How can HF help you?<br />

• Conclusions and outlook<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

2<br />

1


02.06.2017<br />

Functional tread with 5 different compounds<br />

Cap<br />

Cap<br />

Base 1<br />

Chimney<br />

Base 2<br />

Wing (l+r)<br />

Quintuplex Tread Technology:<br />

Cap : low RR / wet&dry grip compromise<br />

Base 1: low RR<br />

Base 2: low RR & tack cushion<br />

Wing : smooth transition to sidewall<br />

Chimney: conductivity<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

3<br />

Typical extrusion line layout for treads<br />

Quintuplex<br />

Cooling section<br />

Skiver, checkweigher and booking system<br />

Winding units<br />

Cross cutter<br />

& conveyors<br />

Measuring sections<br />

Feeders<br />

Head<br />

Take off and shrinkage<br />

conveyor<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

4<br />

2


Line Speed (m/min)<br />

02.06.2017<br />

Extrusion related problems<br />

• Variation in thickness, linear weight and width of extruded tyre<br />

components<br />

• In line shrinkage, banana shrinkage and “after”shrinkage<br />

• Reduced productivity because of high rework amount and low<br />

booking speed<br />

Typical<br />

customer<br />

request<br />

Objective<br />

How can HF<br />

contribute?<br />

Reducing the Shrinkage in treads in the leaftruck from<br />

Extrusion to Tyre Building<br />

Shrinkage<br />

Present<br />

[mm]<br />

PCR Silica 10 - 12 0 - 2<br />

PCR Carbon black 5 - 6 0 - 2<br />

TBR 5-6 0 - 3<br />

Bias 10-12 0 - 6<br />

Target [mm]<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Example 1:<br />

Result of an extrusion line speed study<br />

35<br />

30<br />

25<br />

Line speed along the line<br />

The jump in speed over the<br />

dancer points to huge<br />

tension in the profile<br />

The line speed increase<br />

may point to a high<br />

dancer load<br />

20<br />

Silica tread extrusion<br />

15<br />

10<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

In order to keep the profile within spec the operator /<br />

technologist needs to stretch the profile. The result is a<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

line speed diagram as shown.<br />

June 16, 2017<br />

6<br />

3


02.06.2017<br />

Example 2:<br />

Analysis of poor capability<br />

Souce: Master Thesis Arnout Oldenburger , University of Twente (2014)<br />

• The diagram shows the meter weight of a particular tread size for PCR<br />

tyres (silica cap compound) produced over > 10 different runs.<br />

• It can be seen clearly that the uniformity between runs has potential to<br />

be improved.<br />

• Customers frequently ask extrusion line manufacturers how to solve<br />

these kind of problems.<br />

‣ The answer is: Understand the rheology of the rubber compounds<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

7<br />

Key questions<br />

• What is the nature of the consistency of rubber compounds and how<br />

does it influence the extrudate dimensions?<br />

• How to plasticize a rubber compound and how to deal with extrudate<br />

swell?<br />

• How can a better understanding of the rheology of a rubber compound<br />

contribute to a better extrusion process?<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion 8<br />

June 16, 2017<br />

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02.06.2017<br />

Rubber essentially is a system with polymer<br />

molecules, fillers and softeners and can be<br />

expressed as micro rheological models with fillers<br />

`<br />

… hindered by fillers<br />

(bound rubber) ….<br />

Reptational<br />

movement of<br />

polymer chains…<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion 9<br />

June 16, 2017<br />

… which can form<br />

(weak) filler filler<br />

networks.<br />

Each compound has its own extrudate swell<br />

behaviour<br />

The extrudate swell factor depends on<br />

• molecular weight (distribution) of the<br />

applied polymers<br />

• type of filler<br />

• filler loading<br />

• existence of a filler filler network<br />

• die land length<br />

• compound temperature<br />

Well silanised silica compounds show a<br />

high extrudate swell, higher than<br />

traditional carbon black compounds<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

10<br />

5


02.06.2017<br />

What happens if s the extrudate is pulled out<br />

of the die?<br />

• Polymers are stretched / oriented during extrusion.<br />

• After leaving the die the polymers are “suddenly” free to move<br />

• They tend to return to their “chaotic” stage (= stage of max entropy) Melt<br />

elasticity<br />

• Extrudate swell may be hindered in case the extrudate is pulled out of the dieopening.<br />

‣ This means profile shrinkage as soon as the tension in the profile is released (at<br />

latest at the tyre building machine)<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

11<br />

The answer is relaxed extrusion:<br />

Picture removed)<br />

Different swell factors across the section<br />

may lead to waviness pulling necessary<br />

Relaxed (l) vs pulled (r) extrusion conditions<br />

The die opening should be designed<br />

such that the extrudate swell behavior<br />

of the compound is “completely”<br />

obeyed.<br />

Tension in the downstream should be<br />

avoided<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

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02.06.2017<br />

Preconditions for a relaxed extrusion<br />

process<br />

1. Thermally homogeneous extrudate proper screw design<br />

2. Balanced flow channels no velocity gradient across the extrusion<br />

head outlet openings<br />

3. No starvation in extruder feeding <strong>optimized</strong> intake behavior and<br />

constant rubber feed strip dimensions<br />

4. Preformer and final die design with front or back relief to reduce<br />

differences in flow resistance across the die opening<br />

5. Optimal settings of the shrinkage conveyor<br />

6. Dancer controllers which does not put an additional load on the profile<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion 13<br />

June 16, 2017<br />

1) Screw design:<br />

Performance Triangle for the Extrusion Process<br />

Output<br />

Operating point<br />

Temperature<br />

Homogeneity<br />

Operating point depends on:<br />

-Product: Material Properties, Back Pressure<br />

-Process Setting: TCU-settings, Pin Configuration, Screw Speed<br />

-Machine: Screw Design, Flow Channel<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

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7


02.06.2017<br />

1) Screw design:<br />

Theoretical backgrounds: homogeneity<br />

Building of a cold core in the screw channel: Reason for insufficient<br />

appearance<br />

v channel<br />

v circular<br />

v rotat.speed<br />

v circular<br />

active flight<br />

melt pool<br />

conveying direction<br />

cold core<br />

(non sheared material)<br />

contact to the barrel<br />

passive flight<br />

The cold core, which is the<br />

result of the shear flow in the<br />

screw channel and the high<br />

gradient in viscous heating,<br />

needs to be distributed into the<br />

„hot melt“ pool, e.g. by pins and<br />

/ or mixing segments in the<br />

screw design<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

15<br />

1) Screw design:<br />

Example: Staggered flights<br />

Improved distributive mixing through pin screw with<br />

staggered and normal flights<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

16<br />

8


02.06.2017<br />

2) Flow channels<br />

in a quintuplex extrusion aggregate<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

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Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

17<br />

2) Flow channels:<br />

Modular Tooling<br />

Single cavity opening<br />

Lateral restrictors for<br />

restricting the width of<br />

the opening<br />

flow divider<br />

humps for<br />

balancing of<br />

the opening<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dual cavity opening<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

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9


02.06.2017<br />

2) Flow channels:<br />

Balancing the flow with CFD technology<br />

Outlet velocity gradient<br />

Flow channel geometry<br />

Pressure lines<br />

• The design of flow channels is<br />

based upon CFD simulations<br />

• During wet commissioning a<br />

fine tuning of the flow balance<br />

is done.<br />

• Even with short flow paths HF<br />

is able to fully balance the flow<br />

• Important precondition for high<br />

process capability is fulfilled<br />

• Therefore compact head design<br />

with low volume flow channels<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved June 16, 2017<br />

Dr. Gerard Nijman: Relaxed Extrusion 19<br />

3) Extruder feeding:<br />

Feeder with recipe based control (loop or balancer)<br />

Dancer control<br />

Feed conveyor<br />

(Intralox or textile belt)<br />

Hold down roller<br />

Chalk marker<br />

Metal detector<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Extrusion Lines from HF<br />

20<br />

10


02.06.2017<br />

3) Extruder feeding<br />

Feed roll<br />

Driven feed roll:<br />

• With hardened surface<br />

• Easily adjustable scraper<br />

out of special bronze<br />

• suitable for liquid<br />

heating/ cooling<br />

• Hinged parallel<br />

to the infeed section<br />

Spiral undercut<br />

An extruder is starved fed when a<br />

additional feed strip would lead to<br />

a higher output.<br />

Starved feeding means pulsation:<br />

quality loss due to (small) feed<br />

strip variations.<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion 21<br />

June 16, 2017<br />

4) Preformer and final die design:<br />

Typical tooling configuration for tread profiles<br />

Back relieved for<br />

better local flow<br />

final die<br />

profile<br />

preformer<br />

flow channel<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

22<br />

11


02.06.2017<br />

5) Settings of the shrinkage conveyor:<br />

Extrudate swell, shrinkage and after shrinkage<br />

• The profile needs to be extruded as tension free as possible. Allow the<br />

profile to swell as much as possible<br />

• The potential max swell can be best obtained with a rectangular die<br />

opening.<br />

• Tension means shrinkage. The less tension in the profile the less<br />

shrinkage can be expected.<br />

• If pulling is necessary to avoid waviness of the profile the final die<br />

needs to be <strong>optimized</strong>, i.e. back / forward relieve<br />

• Remaining tension needs to be fully eliminated by means of the<br />

shrinkage conveyor. No shrinkage over the first dancer<br />

• If a profile is put in the leaf truck with tension after-shrinkage may<br />

occure.<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

5) Settings of the shrinkage conveyor:<br />

Down stream optimization<br />

• The take away conveyor (with take off roll) pulls the profile gently out<br />

of the head<br />

• Profile tension needs to be fully relaxed on the shrinkage conveyor<br />

• The dancer after the shrinkage conveyor is a good indicator of<br />

remaining tension.<br />

• The linear scale shall measure the weight of the final profile.<br />

• Pulling or pushing throughout the downstream shall be avoided. Only<br />

temperature shrinkage is allowed. A good indication is to mark the<br />

tread at the shrinkage conveyor with 500 mm and to follow this 500<br />

mm marking throughout the cooling section.<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

12


Conveyor speed<br />

02.06.2017<br />

5) Settings of the shrinkage conveyor:<br />

The hot section downstream just after the aggregate<br />

Incline conveyer to<br />

cooling section<br />

Meter weight scale<br />

Shrinkage conveyor<br />

(with colour markers)<br />

front edge of<br />

the die<br />

Profile<br />

scanner<br />

Dancer<br />

controller<br />

Take off<br />

conveyor<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

25<br />

5) Settings of the shrinkage conveyor:<br />

Line speed setting (for relaxed extrusion)<br />

• Line speed = winding speed (or speed just before skiver)<br />

• When idle: The line speed is basically the same throughout the line except of<br />

• Take off speed<br />

• Shrinkage conveyor<br />

• The dancer load shall be as low as possible contactless dancers<br />

• Shrinkage setting:<br />

1<br />

3<br />

If the belt speed of linear scale = line<br />

speed of the last shrinkage conveyor<br />

then relaxed extrusion.<br />

2<br />

1: Adjustable shrinkage<br />

2: Mechanical shrinkage<br />

3: NO shrinkage allowed<br />

Along the take off, shrinkage and linear weight conveyor belt<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

26<br />

13


Line speed (m/min)<br />

02.06.2017<br />

6) Dancer controller:<br />

Unit with adjustable load<br />

5<br />

4<br />

6<br />

3<br />

2<br />

1 Counterweight<br />

2 Lifting cylinder<br />

3 Rolling diaphragm<br />

cylinder<br />

4 Toothed rack<br />

5 Swivel arm<br />

6 Dancer roller<br />

KR0I51VS<br />

1<br />

Without rubber the dancer controller should be balanced<br />

by the counterweight.<br />

The recipe based dancer load with profile is given by the<br />

rolling diaphragm cylinder and should be as low as<br />

possible to avoid stretching.<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion 27<br />

June 16, 2017<br />

The result: Extrusion line speed study with<br />

relaxed extrusion conditions<br />

30<br />

25<br />

20<br />

15<br />

10<br />

5<br />

Relaxed<br />

extrusion<br />

Pulled extrusion<br />

0<br />

The cooling line is<br />

between incline and<br />

decline conveyor<br />

After-shrinkage of treads<br />

(silica) from leaf-trucks:<br />

-Pulled extrusion: > 10 mm<br />

-Relaxed extrusion: < 2 mm<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion<br />

June 16, 2017<br />

28<br />

14


02.06.2017<br />

How HF can assist you to achieve the best quality<br />

New projects<br />

• Profile and compound based extrusion line design<br />

• Optimal design of flow channels matching the profiles<br />

• Screw design based on laboratory trials of your compounds<br />

• Training and assistance in running in new profiles<br />

Existing extrusion lines<br />

• Common assessment of the current process:<br />

– Line speed study<br />

– Shrinkage study<br />

– Optimization of line settings<br />

– Training on site with respect to preformer and die-design<br />

• Retrofit projects towards relaxed extrusion (a.o. new screw geometry)<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

Dr. Gerard Nijman: Relaxed Extrusion 29<br />

All rights reserved<br />

Summary & Conclusions<br />

• Tyre component extrusion problems like shrinkage and varying profile<br />

dimensions have their origin in the morphology of rubber compounds.<br />

• Polymer molecules are stretched due to high shear rates in flow<br />

channels, preformers and final die´s. After leaving the die the polymer<br />

molecules strive to come back into their original state, relieving their<br />

stresses.<br />

• In pulled extrusion process this stress relieve is hindered which results<br />

in profile tension.<br />

• By adhering to the rheological nature in die-design the amount of<br />

remaining tension in the profile is minimal Relaxed extrusion<br />

conditions.<br />

• Both extrusion line design and control need to be based on the<br />

principle of avoiding any profile tension<br />

‣ HF can help you improving your processes<br />

© Harburg-Freudenberger Maschinenbau GmbH<br />

All rights reserved<br />

Dr. Gerard Nijman: Relaxed Extrusion 30<br />

June 16, 2017<br />

15

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