D1-S2-P2-A-Rheologically-optimized
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02.06.2017<br />
Harburg-Freudenberger<br />
Maschinenbau GmbH<br />
Relaxed extrusion: A very<br />
important precondition for<br />
high quality treads.<br />
Dr.ir. Gerard Nijman<br />
June 16, 2017<br />
gerard.nijman@hf-group.com<br />
Content<br />
• Tread and sidewall profiles & a typical extrusion line lay out<br />
• Rubber rheology, extrudate swell and profile shrinkage<br />
• How to optimize an extrusion line with respect to rheology?<br />
– Extruder screw design<br />
• Temperature homogeneity<br />
• Feeding conditions<br />
– Balanced flow channels<br />
– Preformer and die-design preconditions<br />
– Relaxed extrusion / shrinkage conveyor design<br />
– Extrusion line control / dancer<br />
• How can HF help you?<br />
• Conclusions and outlook<br />
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All rights reserved<br />
Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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1
02.06.2017<br />
Functional tread with 5 different compounds<br />
Cap<br />
Cap<br />
Base 1<br />
Chimney<br />
Base 2<br />
Wing (l+r)<br />
Quintuplex Tread Technology:<br />
Cap : low RR / wet&dry grip compromise<br />
Base 1: low RR<br />
Base 2: low RR & tack cushion<br />
Wing : smooth transition to sidewall<br />
Chimney: conductivity<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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Typical extrusion line layout for treads<br />
Quintuplex<br />
Cooling section<br />
Skiver, checkweigher and booking system<br />
Winding units<br />
Cross cutter<br />
& conveyors<br />
Measuring sections<br />
Feeders<br />
Head<br />
Take off and shrinkage<br />
conveyor<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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Line Speed (m/min)<br />
02.06.2017<br />
Extrusion related problems<br />
• Variation in thickness, linear weight and width of extruded tyre<br />
components<br />
• In line shrinkage, banana shrinkage and “after”shrinkage<br />
• Reduced productivity because of high rework amount and low<br />
booking speed<br />
Typical<br />
customer<br />
request<br />
Objective<br />
How can HF<br />
contribute?<br />
Reducing the Shrinkage in treads in the leaftruck from<br />
Extrusion to Tyre Building<br />
Shrinkage<br />
Present<br />
[mm]<br />
PCR Silica 10 - 12 0 - 2<br />
PCR Carbon black 5 - 6 0 - 2<br />
TBR 5-6 0 - 3<br />
Bias 10-12 0 - 6<br />
Target [mm]<br />
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Example 1:<br />
Result of an extrusion line speed study<br />
35<br />
30<br />
25<br />
Line speed along the line<br />
The jump in speed over the<br />
dancer points to huge<br />
tension in the profile<br />
The line speed increase<br />
may point to a high<br />
dancer load<br />
20<br />
Silica tread extrusion<br />
15<br />
10<br />
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In order to keep the profile within spec the operator /<br />
technologist needs to stretch the profile. The result is a<br />
Dr. Gerard Nijman: Relaxed Extrusion<br />
line speed diagram as shown.<br />
June 16, 2017<br />
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Example 2:<br />
Analysis of poor capability<br />
Souce: Master Thesis Arnout Oldenburger , University of Twente (2014)<br />
• The diagram shows the meter weight of a particular tread size for PCR<br />
tyres (silica cap compound) produced over > 10 different runs.<br />
• It can be seen clearly that the uniformity between runs has potential to<br />
be improved.<br />
• Customers frequently ask extrusion line manufacturers how to solve<br />
these kind of problems.<br />
‣ The answer is: Understand the rheology of the rubber compounds<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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Key questions<br />
• What is the nature of the consistency of rubber compounds and how<br />
does it influence the extrudate dimensions?<br />
• How to plasticize a rubber compound and how to deal with extrudate<br />
swell?<br />
• How can a better understanding of the rheology of a rubber compound<br />
contribute to a better extrusion process?<br />
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Dr. Gerard Nijman: Relaxed Extrusion 8<br />
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Rubber essentially is a system with polymer<br />
molecules, fillers and softeners and can be<br />
expressed as micro rheological models with fillers<br />
`<br />
… hindered by fillers<br />
(bound rubber) ….<br />
Reptational<br />
movement of<br />
polymer chains…<br />
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Dr. Gerard Nijman: Relaxed Extrusion 9<br />
June 16, 2017<br />
… which can form<br />
(weak) filler filler<br />
networks.<br />
Each compound has its own extrudate swell<br />
behaviour<br />
The extrudate swell factor depends on<br />
• molecular weight (distribution) of the<br />
applied polymers<br />
• type of filler<br />
• filler loading<br />
• existence of a filler filler network<br />
• die land length<br />
• compound temperature<br />
Well silanised silica compounds show a<br />
high extrudate swell, higher than<br />
traditional carbon black compounds<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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What happens if s the extrudate is pulled out<br />
of the die?<br />
• Polymers are stretched / oriented during extrusion.<br />
• After leaving the die the polymers are “suddenly” free to move<br />
• They tend to return to their “chaotic” stage (= stage of max entropy) Melt<br />
elasticity<br />
• Extrudate swell may be hindered in case the extrudate is pulled out of the dieopening.<br />
‣ This means profile shrinkage as soon as the tension in the profile is released (at<br />
latest at the tyre building machine)<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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The answer is relaxed extrusion:<br />
Picture removed)<br />
Different swell factors across the section<br />
may lead to waviness pulling necessary<br />
Relaxed (l) vs pulled (r) extrusion conditions<br />
The die opening should be designed<br />
such that the extrudate swell behavior<br />
of the compound is “completely”<br />
obeyed.<br />
Tension in the downstream should be<br />
avoided<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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Preconditions for a relaxed extrusion<br />
process<br />
1. Thermally homogeneous extrudate proper screw design<br />
2. Balanced flow channels no velocity gradient across the extrusion<br />
head outlet openings<br />
3. No starvation in extruder feeding <strong>optimized</strong> intake behavior and<br />
constant rubber feed strip dimensions<br />
4. Preformer and final die design with front or back relief to reduce<br />
differences in flow resistance across the die opening<br />
5. Optimal settings of the shrinkage conveyor<br />
6. Dancer controllers which does not put an additional load on the profile<br />
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Dr. Gerard Nijman: Relaxed Extrusion 13<br />
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1) Screw design:<br />
Performance Triangle for the Extrusion Process<br />
Output<br />
Operating point<br />
Temperature<br />
Homogeneity<br />
Operating point depends on:<br />
-Product: Material Properties, Back Pressure<br />
-Process Setting: TCU-settings, Pin Configuration, Screw Speed<br />
-Machine: Screw Design, Flow Channel<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
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1) Screw design:<br />
Theoretical backgrounds: homogeneity<br />
Building of a cold core in the screw channel: Reason for insufficient<br />
appearance<br />
v channel<br />
v circular<br />
v rotat.speed<br />
v circular<br />
active flight<br />
melt pool<br />
conveying direction<br />
cold core<br />
(non sheared material)<br />
contact to the barrel<br />
passive flight<br />
The cold core, which is the<br />
result of the shear flow in the<br />
screw channel and the high<br />
gradient in viscous heating,<br />
needs to be distributed into the<br />
„hot melt“ pool, e.g. by pins and<br />
/ or mixing segments in the<br />
screw design<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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1) Screw design:<br />
Example: Staggered flights<br />
Improved distributive mixing through pin screw with<br />
staggered and normal flights<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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02.06.2017<br />
2) Flow channels<br />
in a quintuplex extrusion aggregate<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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2) Flow channels:<br />
Modular Tooling<br />
Single cavity opening<br />
Lateral restrictors for<br />
restricting the width of<br />
the opening<br />
flow divider<br />
humps for<br />
balancing of<br />
the opening<br />
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Dual cavity opening<br />
Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
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2) Flow channels:<br />
Balancing the flow with CFD technology<br />
Outlet velocity gradient<br />
Flow channel geometry<br />
Pressure lines<br />
• The design of flow channels is<br />
based upon CFD simulations<br />
• During wet commissioning a<br />
fine tuning of the flow balance<br />
is done.<br />
• Even with short flow paths HF<br />
is able to fully balance the flow<br />
• Important precondition for high<br />
process capability is fulfilled<br />
• Therefore compact head design<br />
with low volume flow channels<br />
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Dr. Gerard Nijman: Relaxed Extrusion 19<br />
3) Extruder feeding:<br />
Feeder with recipe based control (loop or balancer)<br />
Dancer control<br />
Feed conveyor<br />
(Intralox or textile belt)<br />
Hold down roller<br />
Chalk marker<br />
Metal detector<br />
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Extrusion Lines from HF<br />
20<br />
10
02.06.2017<br />
3) Extruder feeding<br />
Feed roll<br />
Driven feed roll:<br />
• With hardened surface<br />
• Easily adjustable scraper<br />
out of special bronze<br />
• suitable for liquid<br />
heating/ cooling<br />
• Hinged parallel<br />
to the infeed section<br />
Spiral undercut<br />
An extruder is starved fed when a<br />
additional feed strip would lead to<br />
a higher output.<br />
Starved feeding means pulsation:<br />
quality loss due to (small) feed<br />
strip variations.<br />
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Dr. Gerard Nijman: Relaxed Extrusion 21<br />
June 16, 2017<br />
4) Preformer and final die design:<br />
Typical tooling configuration for tread profiles<br />
Back relieved for<br />
better local flow<br />
final die<br />
profile<br />
preformer<br />
flow channel<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
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5) Settings of the shrinkage conveyor:<br />
Extrudate swell, shrinkage and after shrinkage<br />
• The profile needs to be extruded as tension free as possible. Allow the<br />
profile to swell as much as possible<br />
• The potential max swell can be best obtained with a rectangular die<br />
opening.<br />
• Tension means shrinkage. The less tension in the profile the less<br />
shrinkage can be expected.<br />
• If pulling is necessary to avoid waviness of the profile the final die<br />
needs to be <strong>optimized</strong>, i.e. back / forward relieve<br />
• Remaining tension needs to be fully eliminated by means of the<br />
shrinkage conveyor. No shrinkage over the first dancer<br />
• If a profile is put in the leaf truck with tension after-shrinkage may<br />
occure.<br />
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5) Settings of the shrinkage conveyor:<br />
Down stream optimization<br />
• The take away conveyor (with take off roll) pulls the profile gently out<br />
of the head<br />
• Profile tension needs to be fully relaxed on the shrinkage conveyor<br />
• The dancer after the shrinkage conveyor is a good indicator of<br />
remaining tension.<br />
• The linear scale shall measure the weight of the final profile.<br />
• Pulling or pushing throughout the downstream shall be avoided. Only<br />
temperature shrinkage is allowed. A good indication is to mark the<br />
tread at the shrinkage conveyor with 500 mm and to follow this 500<br />
mm marking throughout the cooling section.<br />
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12
Conveyor speed<br />
02.06.2017<br />
5) Settings of the shrinkage conveyor:<br />
The hot section downstream just after the aggregate<br />
Incline conveyer to<br />
cooling section<br />
Meter weight scale<br />
Shrinkage conveyor<br />
(with colour markers)<br />
front edge of<br />
the die<br />
Profile<br />
scanner<br />
Dancer<br />
controller<br />
Take off<br />
conveyor<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
25<br />
5) Settings of the shrinkage conveyor:<br />
Line speed setting (for relaxed extrusion)<br />
• Line speed = winding speed (or speed just before skiver)<br />
• When idle: The line speed is basically the same throughout the line except of<br />
• Take off speed<br />
• Shrinkage conveyor<br />
• The dancer load shall be as low as possible contactless dancers<br />
• Shrinkage setting:<br />
1<br />
3<br />
If the belt speed of linear scale = line<br />
speed of the last shrinkage conveyor<br />
then relaxed extrusion.<br />
2<br />
1: Adjustable shrinkage<br />
2: Mechanical shrinkage<br />
3: NO shrinkage allowed<br />
Along the take off, shrinkage and linear weight conveyor belt<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
26<br />
13
Line speed (m/min)<br />
02.06.2017<br />
6) Dancer controller:<br />
Unit with adjustable load<br />
5<br />
4<br />
6<br />
3<br />
2<br />
1 Counterweight<br />
2 Lifting cylinder<br />
3 Rolling diaphragm<br />
cylinder<br />
4 Toothed rack<br />
5 Swivel arm<br />
6 Dancer roller<br />
KR0I51VS<br />
1<br />
Without rubber the dancer controller should be balanced<br />
by the counterweight.<br />
The recipe based dancer load with profile is given by the<br />
rolling diaphragm cylinder and should be as low as<br />
possible to avoid stretching.<br />
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Dr. Gerard Nijman: Relaxed Extrusion 27<br />
June 16, 2017<br />
The result: Extrusion line speed study with<br />
relaxed extrusion conditions<br />
30<br />
25<br />
20<br />
15<br />
10<br />
5<br />
Relaxed<br />
extrusion<br />
Pulled extrusion<br />
0<br />
The cooling line is<br />
between incline and<br />
decline conveyor<br />
After-shrinkage of treads<br />
(silica) from leaf-trucks:<br />
-Pulled extrusion: > 10 mm<br />
-Relaxed extrusion: < 2 mm<br />
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Dr. Gerard Nijman: Relaxed Extrusion<br />
June 16, 2017<br />
28<br />
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How HF can assist you to achieve the best quality<br />
New projects<br />
• Profile and compound based extrusion line design<br />
• Optimal design of flow channels matching the profiles<br />
• Screw design based on laboratory trials of your compounds<br />
• Training and assistance in running in new profiles<br />
Existing extrusion lines<br />
• Common assessment of the current process:<br />
– Line speed study<br />
– Shrinkage study<br />
– Optimization of line settings<br />
– Training on site with respect to preformer and die-design<br />
• Retrofit projects towards relaxed extrusion (a.o. new screw geometry)<br />
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Dr. Gerard Nijman: Relaxed Extrusion 29<br />
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Summary & Conclusions<br />
• Tyre component extrusion problems like shrinkage and varying profile<br />
dimensions have their origin in the morphology of rubber compounds.<br />
• Polymer molecules are stretched due to high shear rates in flow<br />
channels, preformers and final die´s. After leaving the die the polymer<br />
molecules strive to come back into their original state, relieving their<br />
stresses.<br />
• In pulled extrusion process this stress relieve is hindered which results<br />
in profile tension.<br />
• By adhering to the rheological nature in die-design the amount of<br />
remaining tension in the profile is minimal Relaxed extrusion<br />
conditions.<br />
• Both extrusion line design and control need to be based on the<br />
principle of avoiding any profile tension<br />
‣ HF can help you improving your processes<br />
© Harburg-Freudenberger Maschinenbau GmbH<br />
All rights reserved<br />
Dr. Gerard Nijman: Relaxed Extrusion 30<br />
June 16, 2017<br />
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