third semester - Zakir Hussain College of Engineering & Technology ...
third semester - Zakir Hussain College of Engineering & Technology ...
third semester - Zakir Hussain College of Engineering & Technology ...
You also want an ePaper? Increase the reach of your titles
YUMPU automatically turns print PDFs into web optimized ePapers that Google loves.
CONTENTS<br />
1. INTRODUCTION 2<br />
2. FACULTY PROFILE 6<br />
3. BACHELOR OF TECHNOLOGY (PETROCHEMICAL ENGINEERING) 8<br />
3.1 Curriculum 8<br />
3.2 List <strong>of</strong> Elective Courses 12<br />
3.3 Syllabi <strong>of</strong> Courses<br />
3.3.1 I year B.Tech. (Petrochemical <strong>Engineering</strong>) 13<br />
3.3.2 II year B.Tech. (Petrochemical <strong>Engineering</strong>) 21<br />
3.3.3 III year B.Tech. (Petrochemical <strong>Engineering</strong>) 27<br />
3.3.4 IV year B.Tech. (Petrochemical <strong>Engineering</strong>) 35<br />
4. MASTER OF TECHNOLOGY (PETROLEUM PROCESSING AND 47<br />
PETROCHEMICAL ENGINEERING)<br />
4.1 Curriculum 48<br />
4.2 List <strong>of</strong> Elective Courses 49<br />
4.3 Syllabi <strong>of</strong> Courses<br />
4.3.1 I year M.Tech. (Petroleum Processing and Petrochemical 50<br />
<strong>Engineering</strong>)<br />
4.3.2 II year M.Tech. (Petroleum Processing and Petrochemical 56<br />
<strong>Engineering</strong>)<br />
1
INTRODUCTION<br />
2
The idea <strong>of</strong> establishing an Institute <strong>of</strong> Petroleum <strong>Technology</strong> at Aligarh Muslim University was<br />
conceived following the visit <strong>of</strong> His Highness Sheikh Zaid Bin Sultan Al Nahyan, President <strong>of</strong> UAE who<br />
visited Aligarh Muslim University, Aligarh on Jan 01, 1975. A sum <strong>of</strong> US $ 2 lacs was also contributed<br />
by H.H. Sheikh Zaid for the Institute. In view <strong>of</strong> the above and realizing the importance <strong>of</strong> the job<br />
oriented courses and future demand <strong>of</strong> the country in the area <strong>of</strong> Petroleum Studies, the University<br />
submitted a proposal for the Establishment <strong>of</strong> the Petroleum Institute to the University Grants<br />
Commission, Govt. <strong>of</strong> India, New Delhi. The UGC sanctioned the Establishment <strong>of</strong> the Institute <strong>of</strong><br />
Petroleum Studies & Chemical <strong>Engineering</strong> in 1983 in phased manner, renamed as Department <strong>of</strong><br />
Petroleum Studies. A Grant <strong>of</strong> Rs. 111.45 lacs (N.R) for building, laboratory facilities, books etc and<br />
Rs. 3.52 Lacs (R) per annum for teaching and laboratory supporting staff was provided. The UGC also<br />
sanctioned a one year Post- graduate Diploma in Petroleum Processing for which teaching staff<br />
consisting <strong>of</strong> two posts <strong>of</strong> Pr<strong>of</strong>essor and two posts <strong>of</strong> Reader were also sanctioned for running the<br />
above course. Five Posts <strong>of</strong> Laboratory Supporting Staff were also sanctioned to maintain the proper<br />
laboratories facilities.<br />
The P.G. Diploma in Petroleum Processing course was started with an intake <strong>of</strong> 10 students from the<br />
session 1984-85. Various laboratories relating to testing and determining the characteristics and<br />
properties <strong>of</strong> refinery and petrochemicals products, petroleum and petrochemical processing and<br />
other facilities have also been established from the UGC grant.<br />
The P.G Diploma in Petroleum Processing course sanctioned by UGC was upgraded to full – fledged<br />
M.Sc. <strong>Engineering</strong> in Petroleum Processing from the session 1988-89 to enhance the job<br />
potentialities <strong>of</strong> the post graduate students and to initiate research work in the area <strong>of</strong> Petroleum<br />
Processing and Conversion. A Proposal to start another M.Sc. <strong>Engineering</strong> in Petrochemicals course<br />
was submitted to UGC in 1992. The UGC vide its letter No. F0 5-71 /92 (T-I) dated May 18, 1993<br />
agreed with the above proposal and sanctioned the integration <strong>of</strong> Petrochemicals course with<br />
existing Petroleum Processing course. The M.Sc. <strong>Engineering</strong> in Petrochemicals course was<br />
3
started in the Petroleum Institute from the session 1995-96 with an intake <strong>of</strong> 6 students.<br />
Presently, the following facilities have been created from the grants received from the University<br />
Grants Commission and Sheikh Zaid Donation Fund.<br />
� Crude Evaluation Laboratory<br />
� Petroleum Products Testing Laboratories<br />
� Computer Controlled Process Control laboratory<br />
� Reaction <strong>Engineering</strong> and High Pressure Laboratory<br />
� Polymer Processing Laboratory<br />
� Instrumental and FIA Analysis Laboratory<br />
� Computational Laboratory<br />
� Research Laboratory<br />
� Workshop, Store and Seminar facilities and<br />
� Some Unit operation experimental facilities in the Department <strong>of</strong> Chemical <strong>Engineering</strong><br />
The University Grants Commission also sanctioned two posts <strong>of</strong> lecturer in IX plan and six posts <strong>of</strong><br />
teaching staff (Pr<strong>of</strong>essor = 1, Reader = 2, Lecturer = 3) in X plan. Presently there are 10 sanctioned<br />
teaching posts.<br />
The research facilities in the area <strong>of</strong> Hydrodesulfurization, Heat Transfer Studies to Boiling<br />
Hydrocarbon Liquids and their Mixtures in Vertical tube Thermosiphon Reboiler, Nucleate Boiling <strong>of</strong><br />
Hydrocarbon Mixtures on Smooth and Enhanced Surfaces, Studies on Corrosion & its Control for<br />
Petroleum Industries, Kinetics Studies <strong>of</strong> Hydrogenation and Oxidation Reactions, etc. are also<br />
available.<br />
The Expert Committee appointed by the UGC for the Petroleum Institute has also recommended the<br />
expansion with subsequent starting <strong>of</strong> the courses in Petroleum Refining / Petrochemical <strong>Engineering</strong><br />
and <strong>Technology</strong>, Polymer Science and <strong>Technology</strong>, Plastics and Gas Processing and creation <strong>of</strong><br />
4
esearch facilities in the Petroleum Processing and Conversion, Polymer Science and <strong>Technology</strong>,<br />
Polymer Chemistry, Plastics and Organic Synthetic Fertilizers and Hydrocarcking.<br />
Following the directives <strong>of</strong> the UGC and keeping in view the requirements to develop <strong>of</strong> our own<br />
technologies and become competitive and to meet the ever-increasing demand <strong>of</strong> manpower <strong>of</strong> our<br />
country in the field <strong>of</strong> Petroleum Refining / Petrochemicals / Gas Processing, a Four year Bachelor <strong>of</strong><br />
<strong>Technology</strong> in Petrochemical <strong>Engineering</strong> course was introduced in the Petroleum Institute from the<br />
session 1997-98 with an intake <strong>of</strong> 20 students. The Institute is renamed as Department <strong>of</strong> Petroleum<br />
Studies in Feb 2000. Presently following courses are running in the Department:<br />
� 4 year B.Tech. (Petrochemical <strong>Engineering</strong>) Course with an Intake <strong>of</strong> 25 plus 05 NRI students.<br />
� 2 year M.Tech. (Petroleum Processing & Petrochemical <strong>Engineering</strong>) Course with an Intake <strong>of</strong><br />
16 students<br />
The Department will serve the long felt need <strong>of</strong> deploying young engineers in Petrobased Industries<br />
and will bridge the gap between academic institutions and industrial requirements. Its courses and<br />
curriculum have been so designed as to enable its products to handle / execute the Industrial Jobs<br />
and Research without difficulty. Our Students are serving premier organizations namely, Reliance<br />
Industries limited, Technip KTI, Duncan Fertilizers, Punj Lloyd, Indian Oil Corporation Ltd, Oil and<br />
Natural Gas Corporation Ltd, Hindustan Petroleum Corporation Limited, M I Swaco, Oswal Chemicals<br />
and Fertilizers Limited, Council <strong>of</strong> Scientific & Industrial Research, etc.<br />
5<br />
Chairman<br />
Department <strong>of</strong> Petroleum Studies<br />
Aligarh Muslim University Aligarh
FACULTY PROFILE<br />
6
NAME DESIGNATION ACADEMIC QUALIFICATIONS FIELDS OF SPECIALIZATION / INTEREST<br />
7
Dr. Hamid Ali<br />
Dr. Mohd. Kamil<br />
Mrs. Najam Sardar<br />
Mr. Ashraf Mateen<br />
Ms. Seemi Rafique<br />
Mr. S. J. A. Rizvi<br />
Mr. M. Yusuf Ansari<br />
Pr<strong>of</strong>essor & Chairman<br />
D/o Petroleum Studies &<br />
Dean Faculty <strong>of</strong> Engg. &<br />
Tech.<br />
Pr<strong>of</strong>essor<br />
Associate Pr<strong>of</strong>essor<br />
Assistant Pr<strong>of</strong>essor<br />
Assistant Pr<strong>of</strong>essor<br />
Assistant Pr<strong>of</strong>essor<br />
Assistant Pr<strong>of</strong>essor<br />
�<br />
� B.Tech.(Chemical Engg)<br />
I.I.T. Roorkee, Roorkee<br />
� M.Tech.(Chemical Engg)<br />
� I.I.T. Roorkee, Roorkee<br />
� Ph.D.(Chemical Engg)<br />
� AMU, Aligarh<br />
� B. Tech. (Chemical<br />
Engg)<br />
� M.Tech. (Chemical<br />
Engg)<br />
� Ph.D. (Chemical Engg)<br />
� B. Tech. (Chemical<br />
Engg)<br />
� M. Tech.(Petrochemical<br />
Engg)<br />
� B. Tech. (Chemical Engg)<br />
� M. Tech(Petrochemical<br />
Engg)<br />
� B. Tech. (Chemical<br />
Engg)<br />
� M. Tech.(Petrochemical<br />
Engg)<br />
� B. Tech. (Chemical<br />
Tech)Specialization in<br />
Plastic <strong>Technology</strong><br />
� M. Tech (Polymer Tech)<br />
� B. Tech. (Petrochemical<br />
Engg)<br />
� M. Tech.(Petrochemical<br />
Engg)<br />
COURSE CURRICULUM FOR FIRST YEAR B.TECH. (PETROCHEMICAL ENGINEERING)<br />
8<br />
� Thermal Fluid Sciences and<br />
<strong>Engineering</strong><br />
� Studies on Corrosion Inhibitors in<br />
Petroleum Industry<br />
� Thermal Oxidation <strong>of</strong> Refinery<br />
Sludge<br />
� Thermal Fluid Sciences<br />
� Petroleum Processing<br />
� Modeling & Simulation<br />
� Synthesis and Characterization <strong>of</strong><br />
Shear thicken <strong>of</strong> Fluids.<br />
� Studies on Polymer Surfactant<br />
Interaction<br />
� Studies on Corrosion Inhibitors in<br />
Petroleum Industry<br />
� Modeling & Simulation <strong>of</strong> Refining<br />
Processes<br />
� Petroleum <strong>Engineering</strong><br />
� Heavy Oil Processing<br />
� Process <strong>Engineering</strong> & Design<br />
� Oil & Gas Processing<br />
� Plant Safety<br />
� Alternate Fuels<br />
� Polymer Processing and<br />
� Mould Design<br />
� CAD/CAM<br />
� Industrial Automation<br />
� Separation Processes<br />
� Petrochemical <strong>Technology</strong><br />
� Gas Conversion
Course<br />
Category<br />
Course<br />
No<br />
Course Title<br />
FIRST SEMESTER (Autumn)<br />
Period/Week<br />
L T P<br />
SECOND SEMESTER (Winter)<br />
9<br />
Credits<br />
(Cr)<br />
Course<br />
Work<br />
Marks<br />
Mid<br />
Sem.<br />
Exam<br />
Marks<br />
End<br />
Sem.<br />
Univ.<br />
Exam<br />
Marks<br />
BS APIII Applied Physics 3 1 - 4 15 25 60 100<br />
BS AMIII Applied Mathematics -I 3 1 - 4 15 25 60 100<br />
HM EN101 English 3 1 - 4 15 25 60 100<br />
ESA CEIII Environmental Studies 3 1 - 4 15 25 60 100<br />
ESA MEIII<br />
Mechanics & Strength <strong>of</strong><br />
Material<br />
Total<br />
3 1 - 4 15 25 60 100<br />
BS AP194 Applied Physics Lab 0 1 2 2 60 40 100<br />
ESA ME194 Manufacturing Process Lab<br />
Course<br />
Category<br />
Course<br />
No<br />
0 1 2 2 60 40 100<br />
Total 15 7 4 24 - - -<br />
Course Title<br />
Period/Week<br />
L T P<br />
Credits<br />
(Cr)<br />
Course<br />
Work<br />
Marks<br />
Mid<br />
Sem.<br />
Exam<br />
Marks<br />
End<br />
Sem.<br />
Univ.<br />
Exam<br />
Marks<br />
BS ACIII Applied Chemistry 3 1 - 4 15 25 60 100<br />
BS AM112 Applied Mathematics-II 3 1 - 4 15 25 60 100<br />
ESA ME101 Basic Thermal Sciences 3 1 - 4 15 25 60 100<br />
ESA EEIII<br />
Basic Electrical &<br />
Electronic Engg<br />
Total<br />
3 1 - 4 15 25 60 100<br />
BS AC194 Applied Chemistry Lab 0 1 2 2 60 40 100<br />
ESA CO191<br />
Computer Programming<br />
Lab<br />
0 1 2 2 60 40 100<br />
ESA ME193 <strong>Engineering</strong> Graphics Lab 1 0 2 2 60 40 100<br />
Total 13 06 06 22 - - -
Course<br />
Category<br />
Course<br />
No<br />
COURSE CURRICULUM FOR SECOND YEAR B.TECH. (PETROCHEMICAL ENGINEERING)<br />
Course Title<br />
THIRD SEMESTER (Autumn)<br />
Period/Week<br />
L T P<br />
10<br />
Credits<br />
(Cr)<br />
Course Work<br />
Marks<br />
Mid Sem. Exam<br />
Marks<br />
DC PK-211 Basic Principles <strong>of</strong> Chemical <strong>Engineering</strong> 3 1 - 4 15 25 60 100<br />
DC PK-231 Chemistry <strong>of</strong> Hydrocarbons 3 1 - 4 15 25 60 100<br />
DC PK-232 Fluid Mechanics 3 1 - 4 15 25 60 100<br />
DC PK-214 Reaction Kinetics and Reactor Design 3 1 - 4 15 25 60 100<br />
DC PK-233 Fluid -Particle Operations 3 1 - 4 15 25 60 100<br />
BS AM-241 Higher Mathematics 3 1 - 4 15 25 60 100<br />
ESA ME-294 Machine Drawing and Computer Graphics 1 2 2 60 - 40 100<br />
Total 18 07 02 26 - - -<br />
Course<br />
Category<br />
Course<br />
No<br />
Course Title<br />
FOURTH SEMESTER (Winter)<br />
Period/Week<br />
L T P<br />
Credits<br />
(Cr)<br />
Course Work<br />
Marks<br />
Mid Sem. Exam<br />
Marks<br />
DC PK-221N Chemical <strong>Engineering</strong> Thermodynamics 3 1 - 4 15 25 60 100<br />
DC PK-241<br />
Separation Processes in Hydrocarbon<br />
Industries<br />
3 1 - 4 15 25 60 100<br />
DC PK-242 Process Development and Equipment Design 3 1 - 4 15 25 60 100<br />
DE Departmental Elective-I 3 1 - 4 15 25 60 100<br />
BS AM-242 Applied Numerical Methods 3 1 - 4 15 25 60 100<br />
ESA CH-292 Unit Operations Laboratory-I<br />
- 1 2 2 60 - 40 100<br />
DC PK-293 Petroleum Testing Laboratory - 1 2 2 60 - 40 100<br />
HM EZ-291 Communication Skills Laboratory - 1 2 2 60 - 40 100<br />
Total 15 8 6 26 - - -<br />
End<br />
Sem.<br />
Univ.<br />
Exam<br />
Marks<br />
End<br />
Sem.<br />
Univ.<br />
Exam<br />
Marks<br />
Total<br />
Total
Course<br />
Category<br />
Course<br />
No<br />
COURSE CURRICULUM FOR THIRD YEAR B. TECH. (PETROCHEMICAL ENGINEERING)<br />
Course Title<br />
FIFTH SEMESTER (Autumn)<br />
Period/Week<br />
L T P<br />
11<br />
Credits<br />
(Cr)<br />
Course Work<br />
Marks<br />
Mid Sem. Exam<br />
Marks<br />
DC PK-311N Petroleum Refining Processes 3 1 - 4 15 25 60 100<br />
DC PK-312N Heat Transfer Operations 3 1 - 4 15 25 60 100<br />
DC PK-313N Mass Transfer Operations 3 1 - 4 15 25 60 100<br />
DC PK-331 Refinery <strong>Engineering</strong> Calculations 3 1 4 15 25 60 100<br />
HM ME-340 Economics and Management 3 1 - 4 15 25 60 100<br />
ESA AC-311 <strong>Engineering</strong> Materials 3 1 4 15 25 60 100<br />
DC PK-393 Computer Applications Laboratory - 1 2 2 60 - 40 100<br />
Total 18 7 2 26 - - -<br />
Course<br />
Category<br />
Course<br />
No<br />
Course Title<br />
SIXTH SEMESTER (Winter)<br />
Period/Week<br />
L T P<br />
Credits<br />
(Cr)<br />
Course Work<br />
Marks<br />
Mid Sem.<br />
Exam Marks<br />
DE Departmental Elective – II<br />
3 1 - 4 15 25 60 100<br />
DC PK-342 Petrochemical <strong>Technology</strong> - I 3 1 - 4 15 25 60 100<br />
DC PK-323 Transport Phenomena 3 1 - 4 15 25 60 100<br />
DC PK-343<br />
Health, Safety and Environment in Hydrocarbon<br />
Industries<br />
3 1 - 4 15 25 60 100<br />
DC PK-315N Natural Gas Processing 3 1 - 4 15 25 60 100<br />
ESA CH-393 Unit Operation Laboratory-II - 1 2 2 60 - 40 100<br />
DC PK-394 Reaction Engg. Laboratory - 1 2 2 60 - 40 100<br />
DC PK-395 Process Equipment Design 1 2 2 60 - 40 100<br />
Total 15 8 6 26<br />
End<br />
Sem.<br />
Univ.<br />
Exam<br />
Marks<br />
End<br />
Sem.<br />
Univ.<br />
Exam<br />
Marks<br />
Total<br />
Total
Course<br />
Category<br />
Course<br />
No<br />
COURSE CURRICULUM FOR FOURTH YEAR B.TECH. (PETROCHEMICAL ENGINEERING)<br />
SEVENTH SEMESTER (Autumn)<br />
Period/Week<br />
Course Title<br />
L T P<br />
13<br />
Credits<br />
(Cr)<br />
Course Work<br />
Marks<br />
Mid Sem. Exam<br />
Marks<br />
DC PK-411 Process Dynamics and Control 3 1 - 4 15 25 60 100<br />
DC PK-431 Plant Design & Economics 3 1 - 4 15 25 60 100<br />
DC PK-432 Petrochemical <strong>Technology</strong> – II 3 1 - 4 15 25 60 100<br />
DC PK-433 Polymer Science and <strong>Technology</strong> 3 1 - 4 15 25 60 100<br />
OE ---- Open Elective I 3 1 - 4 15 25 60 100<br />
DC PK-493 Project - 4 - 4 �<br />
30 - - 30<br />
DC PK-481 Seminar - 1 2 2 60 - 40 100<br />
Total 15 9 2 26<br />
�<br />
In complete grade (I) is to be awarded, which will be converted in to regular grades at VIII Semester Level<br />
Course<br />
Category<br />
Course<br />
No<br />
Course Title<br />
EIGHTH SEMSETER (Winter)<br />
Period/Week Credits<br />
L T P (Cr)<br />
DE Departmental Elective III 3<br />
DC PK-422N Process Utilities and Energy Management 3<br />
Course Work<br />
Marks<br />
Mid Sem. Exam<br />
Marks<br />
End<br />
Sem.<br />
Univ.<br />
Exam<br />
Marks<br />
End<br />
Sem.<br />
Univ.<br />
Exam<br />
Marks<br />
Total<br />
Total<br />
1 - 4 15 25 60 100<br />
1 - 4 15 25 60 100<br />
DE Departmental Elective IV 3 1 - 4 15 25 60 100<br />
OE ------ Open Elective II 3 1 - 4 15 25 60 100<br />
DC PK-493 Project - 4 4 40 - 30 70<br />
DC PK-494 Instrumentation and Process Control Laboratory - 1 2 2 60 - 40 100<br />
DC PK-495 Polymer Laboratory - 1 2 2 60 - 40 100<br />
Total 12 10 4 24 100<br />
`<br />
Category Credits Recommended Actual Category Credits Recommended Actual<br />
BS 20-36 28 DC 60-116 106<br />
ESA 20-40 32 DE 16-32 16<br />
HM 10-18 10 OE 8-16 8<br />
NOTE: In order to wind up the old curriculum quickly, there will be a need for alternative courses, filler courses and many other measures. The Dean is authorized to approve alternative<br />
courses, approve filler courses and take such other measures, in consultation with the respective Chairmen, as may be suitable to wind up the old curriculum quickly.
LIST OF ELECTIVES COURSES<br />
DEPARTMENTAL ELECTIVES<br />
Alternate Fuels and Energy Resources<br />
Renewable Energy<br />
Energy Resources and Environment Management<br />
Synthetic Fuels<br />
Heterogeneous Reaction <strong>Engineering</strong><br />
Catalysis<br />
Chemical Reactor Design<br />
Process Instrumentation<br />
Piping and Instrumentation<br />
Instrumentation <strong>Engineering</strong><br />
Fertilizer <strong>Technology</strong><br />
Coal and Gas Conversion <strong>Technology</strong><br />
Selected Topics in Refining and Petrochemicals<br />
OPEN ELECTIVES<br />
Petroleum Refining <strong>Technology</strong><br />
Equilibrium Stage Processes<br />
Plant Safety<br />
Petrochemical <strong>Technology</strong><br />
Bioprocess <strong>Engineering</strong><br />
Modeling and Simulation<br />
Polymer <strong>Technology</strong><br />
Fundamentals <strong>of</strong> Petroleum <strong>Engineering</strong><br />
Introduction to Hydrocarbon <strong>Technology</strong><br />
Polymer Structure Property Relationship<br />
Natural Gas <strong>Technology</strong><br />
Industrial Instrumentation<br />
Waste Management <strong>Technology</strong><br />
Pollution Control Equipment Design<br />
Process Equipment and Piping Design<br />
14
Process Design & Integration<br />
Refinery Equipment Design<br />
Fundamentals <strong>of</strong> Petroleum Prospecting<br />
Oil Recovery Techniques<br />
FIRST YEAR B.TECH. (PETROCHEMICAL ENGINEERING)<br />
15
FIRST & SECOND SEMESTER<br />
AC111 APPLIED CHEMISTRY<br />
UNIT-1: METHODS OF CHEMICAL ANANLYSIS<br />
Qualitative and quantitative analysis, Principle <strong>of</strong> gravimetry and steps involved in gravimetric<br />
analysis, digestion and its importance, favourable conditions for precipitation.<br />
Titration, titrant, analyte, primary and secondary standards. Basic requirements <strong>of</strong> a titrimetric<br />
method, classification <strong>of</strong> titrations (acid-base, oxidation-reduction, precipitation and<br />
chelometric titrations with examples).<br />
Absorption Spectrophotometry : Beer and Lambert’s law (definition and units <strong>of</strong> terms involved.<br />
deviaton from Beer’s Law) Block diagram <strong>of</strong> single bean UV-Visible Spectrophotometer.<br />
Definition <strong>of</strong> chromatography and chromatographic system (stationary and mobile phase),<br />
classification <strong>of</strong> chromatography on the basis <strong>of</strong> physical mode (planar and column<br />
chromatorgrahy) and mechanism (sorption, partition and ion exchange chromatorgrahy).<br />
Calculation <strong>of</strong> RF Value, separation factor, resolution and capacity factor from chromatorgram.<br />
UNIT-II: WATER TRATMENT<br />
Hardness <strong>of</strong> water (units <strong>of</strong> hardness, calculation on hardness, determination by soap and EDTA<br />
methods). Sludge, scale priming and foaming. Boiler corrosion and caustic embrittlement<br />
(causes, defects and prevention). Lime-soda, zeolite and ion exchange processes. Calculations<br />
based on Lim-soda and zeolite proesses. Sedimentation, coagulation and filtration. Disinfection,<br />
requirements <strong>of</strong> a good disinfecting agent and types <strong>of</strong> disinfecting agents, (bleaching powder,<br />
liquid chlorine, ozone, UV radiation and chloramines). Break point chlorination:<br />
UNIT-III FUELS<br />
Classification <strong>of</strong> fuels and characteristics <strong>of</strong> a good fuel, calorific value and its determination by<br />
Boom Calorimeter and Dulong’s formula (Numerical problems). Analysis <strong>of</strong> coal (Proximate<br />
Ultimate analysis) Composition and classification <strong>of</strong> petroleum. Important factions <strong>of</strong> petroleum<br />
and their uses. Synthetic petrol ( Polymerizations and cracking, Fisher Tropsch and Bergius<br />
processes). Advantages and disadvantages <strong>of</strong> gaseous fuels, composition and uses <strong>of</strong> natural<br />
gas, CNG, LPG, Combustion calculations on solid and gaseous fuels.<br />
UNIT-IV LUBRICANTS<br />
Definition and classification <strong>of</strong> lubricants Mechanisms <strong>of</strong> lubrication. Mineral oils, fatty oils,<br />
compounded oils and silicone fluids. Testing <strong>of</strong> liquid lubricants, Viscosity, and index Flash and<br />
Fire points. Cloud, pour and setting Point, Saponification value, Aniline point, Types <strong>of</strong> greases<br />
and conditions for their use. Consistency test, and Drop Point <strong>of</strong> Greases.<br />
UNIT-V CORROSION AND ITS PREVENTION<br />
Definition, significance and classification <strong>of</strong> corrosion. Mechanism <strong>of</strong> oxidation metals, Pilling-<br />
Bedworth rule. Nernst equation, electrochemical and galvanic series. Cathodic and anodic<br />
reactions. Factors affecting corrosion. Corrosion control (design and selection <strong>of</strong> materials,<br />
cathodic protection, metallic coatings, galvanizing and tinning anodized coating). Paints<br />
definition, compositions and the function <strong>of</strong> each component).<br />
UNIT-VI POLYMER<br />
Definition and classification <strong>of</strong> Polymers. Polymerization (addition and condensation),<br />
mechanism <strong>of</strong> free radical addition polymerization.<br />
16
Definition, preparation, properties and uses <strong>of</strong> thermoplastic (PMMA Teflon), and thermosetting<br />
plastics (Bakelite, Polyesters) synthetic fibres (Nylon 66, or lon). Natural rubber and<br />
vulcanization.<br />
BOOKS RECOMMENDED FOR APPLIED CHEMISTRY COURSES (AC-III)<br />
1. Analytical Chemistry by G.D. Christian, John Wiley and Sons, New York.<br />
2. Quantitative Analysis by R.A. Day and A.L. Underwood.<br />
3. A Text Book <strong>of</strong> <strong>Engineering</strong> Chemistry by S.S. Dara. S. Chand & Co., New Delhi (India)<br />
4. <strong>Engineering</strong> Chemistry by B.K. Sharma, Krishna Prakashan Media (P) Ltd., Meerut (India).<br />
5. <strong>Engineering</strong> Chemistry by P.C. Jain, Dhanpat Rai Publishing Company, New Delhi.<br />
AP111 APPLIED PHYSIC<br />
UNIT 1.<br />
Semiconductors Elemental and compound semiconductors, Energy bands, Direct and<br />
indirect semiconductors, Electrons and holes, Effective mass, Intrinsic material, Extrinsic<br />
material, Fermi level Electron and hole concentration at equilibrium, temperature<br />
dependence <strong>of</strong> carrier concentrations, compensation and space charge neutrality,<br />
conductivity and mobility, hall effect in semiconductors<br />
Superconductivity Zero resistivity, Meissner effect, Type I and Type II Superconductors, High<br />
Temperature Superconductors, BCS theory (Qualitative), Josephson effect, SQUIDS.<br />
UNIT II.<br />
Masers and lasers, Basic principle, Einstein coefficients for induced absorption, Spontaneous<br />
Emission and induced emission, Ammonia maser and its applications, Ruby and He-Ne<br />
Lasers, Semiconductor laser, spatial and temporal coherence, characteristics <strong>of</strong> lasers and its<br />
applications based on these characteristics (such as in Industry, Science, Medicine,<br />
Communications, Surveying, Holography, Fusion reactors, Isotope separations etc).<br />
Fibre Optic, Basic principle, Fibre construction and dimensions light Propagation in fibres,<br />
Numerical aperture <strong>of</strong> the fibre, Step index and graded index fibres signal distortion in<br />
optical fibres, Transmission losses, light wave communication in optical fibres, Fibre Optics<br />
in medicine and industry.<br />
UNIT III.<br />
Particles and waves, Mechanism <strong>of</strong> X-ray production (continuous and characteristic X-rays,<br />
Duane-Hunt limit Compton effect, Pair production, Phase and group velocities, Uncertainty<br />
principle.<br />
Quantum Mechanic, Introduction to quantum mechanics wave function, conditions<br />
necessary for physically acceptable wavefunction, Probability density and probability,<br />
Schrodinger equation (Time dependent form and steady state or time independent form),<br />
Eigen values and eigen functions, Expectations values Particle in a box (Infinite potential<br />
well), Tunnel effect.<br />
UNIT IV<br />
Statistical Mechanics, Statistical distributions, Maxell- Boltzman statistics, Molecular<br />
energies in an ideal gas, Quantum statistics, specific heats <strong>of</strong> solids, free electron in a metal<br />
Electron-energy distribution.<br />
Nuclear Physic, Q value and threshold energy <strong>of</strong> nuclear reactions, Cross section <strong>of</strong> nuclear<br />
reaction and reaction rate, Breeder reactors, Fusion reactors, Nuclear detectors (names and<br />
general working principle), gas filled detectors, Scintillation detectors.<br />
Text Books<br />
17
1. Ben G. Streetman, “Solid State Electronic Devices” 5 th edition(2000), Prentice-Hall <strong>of</strong><br />
India Private Limited New Delhi<br />
2. Arthur Beiser, “ Concepts <strong>of</strong> Modern Physics 6 th edition (2003), Mc. Graw Hill Inc.<br />
International Edition.<br />
3. M.R. Wehr, J.A. Richards. Jr. and TW AdairIII, Physics <strong>of</strong> the Atom 4 th editions (1984),<br />
Addison Wesley / Narosa.<br />
4. M.R. Srinivasan, Physics <strong>of</strong> Engineers 1 st Edition (1996), New age International (P)<br />
Limited Publishers.<br />
AM111 MATHEMATIC<br />
UNIT 1.<br />
Rank <strong>of</strong> a matrix with applications to consistency <strong>of</strong> system <strong>of</strong> linera equations, Eigenvalues<br />
and Eigen vectors <strong>of</strong> a matrix, Cayley-Hamilton Theorem.<br />
UNIT 2.<br />
Asymptotes and simple curve tracing. Successive Differentiation, Leibnitz’s Theorem,<br />
Taylor and Maclaurin series with remainder terms.<br />
UNIT 3.<br />
Applications <strong>of</strong> integration to lengths <strong>of</strong> curves, surfaces and volumes <strong>of</strong> solids <strong>of</strong><br />
revolution.<br />
UNIT 4.<br />
Solutin <strong>of</strong> exact differential equations, Linear differential equations <strong>of</strong> second and<br />
higher order with constant coefficients. Homogeneous differential equations.<br />
Simultaneous linear differential equations, Applications to physical problems.<br />
AM112 MATHEMATIC<br />
UNIT 1.<br />
Partial differentiation, Euler’s Theorem, Total differential, small errors, change <strong>of</strong><br />
variables, Jacobians.<br />
UNIT 2.<br />
Taylor series for functions <strong>of</strong> two variables approximate calculations Maxima and<br />
minima <strong>of</strong> functions <strong>of</strong> two variables, lagrange’s multipliers.<br />
UNIT 3.<br />
Double and triple integrals, change <strong>of</strong> variables, change <strong>of</strong> order <strong>of</strong> integration,<br />
Applications <strong>of</strong> areas and volume.<br />
UNIT 4.<br />
General equations <strong>of</strong> second degree, Tracing <strong>of</strong> conics introduction to polar form <strong>of</strong><br />
conics.<br />
UNIT I.<br />
CE111 ENVIRONMENT STUDIES<br />
18
Concepts <strong>of</strong> Ecology, Ecosystem, Energy and nutrient flow in ecosystem, food chain,<br />
Environmental segments. Atmospheric structure, classification <strong>of</strong> Air pollutants, sources<br />
<strong>of</strong> air pollution and their effects on human heath and property. Atmospheric chemistry,<br />
Photochemical Smong, Ozone depletion<br />
UNIT II.<br />
Air Quality and standards, Meteorological phenomena and their influence on Air<br />
Quality, Lapse rates Dispersion <strong>of</strong> Pollutants.<br />
Air Pollution Control Introduction to Particulate and Gaseous pollutant control<br />
UNIT III.<br />
Water Quality Physical, Chemical and Biological parameters water quality standards,<br />
Biochemical (BOD) and Chemical Oxygen Demand (COD). BOD/ COD Calculations.<br />
Environmental Analyses, pH, Alkalinity, Conductivity, Ammmonia, Fluorids, Sulphate,<br />
Chloride. Analysis and measeurement <strong>of</strong> gaseous pollutants.<br />
UNIT IV.<br />
Water purification processes in natural systems, Dissolved Oxygen (DO), Impact <strong>of</strong><br />
wastewater discharge <strong>of</strong> streams, Oxygen Sag curve.<br />
Introduction to Water treatment Technologies, Sedimentation, Coagulation and<br />
Flocculation, Hardness Reduction Filtration and Disinfection.<br />
UNIT V.<br />
Waste water Characteristics, Introduction to wastewater treatment technologies,<br />
Primary Treatment, Screening, Grit Removal, Flow measurement, Flow equalization.<br />
Secondary Treatment. Microbial growth curve, Suspended and attached growth<br />
systems.<br />
UNIT V1.<br />
Solid Waste, Classification, Sources and Characteristics.<br />
Waste Management, Solid Waste Generation, Collection, Processing and Disposal<br />
Methods. Resource Recovery in Waste Management, Biological and Thermal Conversion<br />
Processes.<br />
Note: Unites I and III shall be taught by the Department <strong>of</strong> Applied Chemistry<br />
Units II and VI shall be taught by the Department <strong>of</strong> Chemical <strong>Engineering</strong><br />
Units IV and V shall be taught by the Department <strong>of</strong> Civil <strong>Engineering</strong><br />
Reference Book:<br />
1. Venugopala Rao, P., 2006 Principles <strong>of</strong> Environmental Science and <strong>Engineering</strong>,<br />
Prentice- Hall <strong>of</strong> India Private Limited, New Delhi.<br />
2. Masters, G.M., 1991, Introduction <strong>of</strong> Environmental <strong>Engineering</strong> and Science,<br />
Prentice- Hall International, Inc., Englewood Cliffs, NJ.<br />
3. Peavy, H.S., D.R. Rowe and G. Tchobanglous, 1985 Environmental <strong>Engineering</strong>,<br />
McGraw-Hill Book Company, New York.<br />
4. Henry, J.G. and G.W. Heinke, 1989, Environmental Science and <strong>Engineering</strong>,<br />
Prentice-Hall International, Inc., Englewood Cliffs, NJ.<br />
5. Sawyer, C.N. and P.L. McCarty, 1978, Chemistry for Environmental <strong>Engineering</strong>, 3 rd<br />
Edition, McGraw-Hill Book Company, New York.<br />
19
6. Tchobanoglous, G., H. Theisen and S.Vigil, 1993, Integrated Solid Waste<br />
Management, McGraw-Hill Inc, Singapore.<br />
EN101 ENGLISH<br />
UNIT I<br />
Text. Comprehension Questions, Summary Type as well as short answer type and<br />
questions on Vocabulary for 10 passages <strong>of</strong> the Basic Scientific English by Ewer and<br />
Latorre (Longman). Units are 1,3,4,5,8 & 11 from main book and passages 4,11,13,17<br />
from the supplement.<br />
UNIT II<br />
Comprehension questions, summary or short answer type from the following<br />
supplementary readers:<br />
1. Animal Farm by George Orwell<br />
2. The time machine by HG Wells retold by Margery Gree Macmillan)<br />
UNIT III<br />
Note taking, note making exercises, report and process writings.<br />
UNIT IV<br />
Precis writing<br />
UNIT V<br />
Composition and spoken English.<br />
EE111 BASIC ELECTRICAL AND ELECTRONIC ENGINEERING<br />
PAPT-A<br />
UNIT-I: Circuits and Transformers<br />
Review <strong>of</strong> de circuits and theorems, I-Phase as circuits, superposition theorem,<br />
Thevenin’s norton’s theorem for ac circuits, RLC series & Parallel circuits, 3 phase<br />
balanced ac circuits<br />
Magnetic circuits, magnetization curve, hysteresis & eddy current losses.<br />
Transformer construction, equivalent circuit, calculation <strong>of</strong> losses and efficiency.<br />
UNIT II: Instruction to Electrical <strong>Technology</strong><br />
Fundamentals <strong>of</strong> 3-phase alternators, 3-phase induction motors and 1-phase induction<br />
motors.<br />
Basic elements <strong>of</strong> an instrument, MC & MI instruments, dynamometer wattmeter<br />
energymeter.<br />
Elements <strong>of</strong> power system, layout <strong>of</strong> thermal and hydro plants.<br />
Introduction to renewable energy sources and recent trends in generation.<br />
PART-B<br />
UNIT III: Diode and BJT; Characteristics & Applications<br />
Terminal characteristics <strong>of</strong> diodes, Diode models; Ideal constant voltage and piecewise<br />
linear, load line concept, Diode applications; Rectifiers, logic gates, Zener diode,<br />
operation, characteristics, voltage regulation, Bipolar Junction Transistor; construction,<br />
20
operation configurations, Characteristics <strong>of</strong> common emitter configuration, DC load line<br />
analysis.<br />
UNIT IV : MOSFET and OpAmp; Characteristics & Applications<br />
Introduction to MOSFET; Depletion MOSFET construction & operation, Enhancement<br />
MOSFET construction & operation, Operational Amplifier; equivalent; circuit, ideal<br />
behavior, open loop and closed loop concept concept <strong>of</strong> virtual short, simple OpAmp<br />
applications; Unity gain amplifier, inverting, non-inverting, integrator, differentiator,<br />
subtractor, summer.<br />
TEXT Books<br />
1. Ashfaq Husain, “ Fundamentals <strong>of</strong> Electrical <strong>Engineering</strong> 3 rd edition Dhanpat Rai &<br />
Sons.<br />
2. R. Boylestad & L. Nashelsky, Electronics Devices and Circuits, Prentice Hall, 1995.<br />
Reference Books<br />
1. Hughes, Electrical <strong>Technology</strong> 7 th edition, Addison Wesley<br />
2. A.K. Sawhney, A Course in electrical & Electronic Meas. & Inst. Dhanpat Rai & Sons<br />
3. B.R. Gupta. Generation <strong>of</strong> Electrical Energy, S. Chand.<br />
4. Mathur, Chadda and Kulshrestha, Electronics Devices, Applications and Integrated<br />
Circuits, Umesh Publications.<br />
ME101 BASIC THERMAL SCIENCE<br />
UNIT I<br />
Dimensions and units system boundary types <strong>of</strong> systems and boundaries property cycle<br />
thermodynamic equilibrium and quasi-static process.<br />
Pressure and its measurement, zero’th law <strong>of</strong> thermodynamics, temperature and its<br />
measurement, numerical problems.<br />
UNIT II<br />
Thermodynamic and mechanics definition <strong>of</strong> work. Displacement work and its<br />
expressions engine indicator and indicated work, introduction to 2-stroke and 4stroke<br />
engines, heat, work and heat as energy interactions, Joule’s experiment & mechanical<br />
equivalent <strong>of</strong> heat, firs law <strong>of</strong> thermodynamics for cycle and non cyclic processes.<br />
Definition <strong>of</strong> energy as a property, internal energy, enthalpy, specific heats, first law for<br />
a control volume, steady flow energy Equation (SFEE) and it’s applications, numerical<br />
problems.<br />
UNIT III<br />
Pure substance, different phases <strong>of</strong> pure substance, tow property rule property<br />
diagrams, tables and charts equation <strong>of</strong> state <strong>of</strong> an ideal gas t��, t�p, p�v, and t�v<br />
diagrams, phase boundaries, S-L-V region, CP and TP, dryness fraction and its<br />
measurement using throttling calorimeter, limitations <strong>of</strong> throttling calorimeter,<br />
separating & throttling calorimeter, numerical problems.<br />
UNIT IV<br />
Limitations <strong>of</strong> first law , heat engine heat pump refrigerator, second law <strong>of</strong><br />
thermodynamics-kelvin planck’s and Clausius statements and their equivalence<br />
efficiency <strong>of</strong> heat engine and coefficient <strong>of</strong> performance <strong>of</strong> heat pump and refrigerator,<br />
21
eversible and irreversible processes. Carnot cycle and its efficiency corollaries <strong>of</strong> second<br />
law, the thermodynamic scale. Inequality <strong>of</strong> Clausius, entropy, principle <strong>of</strong> increase <strong>of</strong><br />
entropy, isentropic process, t�s and h�s diagrams (Mollier chart), second law<br />
applications, air standard otto, diesel, dual simple Brayton and steam power cycles<br />
(Rankine cycle) numerical problems.<br />
UNIT V<br />
Modes <strong>of</strong> heat transfer, Fourier’s law <strong>of</strong> steady state heat conduction (one dimensional<br />
conduction), thermal conductivity and its unit, conduction through slab or plane wall,<br />
conduction through composite walls and hollow cylinders, convective heat transfer,<br />
Newton’s law <strong>of</strong> cooling, combine heat transfer, electrical analogy and overall heat<br />
transfer coefficient radiation, black body emissive power emissivity, Kirch<strong>of</strong>f’s law<br />
Stefan Boltzmann’s law. Numerical problems.<br />
Book<br />
1. Thermodynamics, An <strong>Engineering</strong> Approach by yunus A. Cengel and Michael A Boles<br />
2. <strong>Engineering</strong> Thermodynamics by D. B. Spalding and E.H.Cole.<br />
3. <strong>Engineering</strong> Thermodynamics by R. Joel<br />
4. <strong>Engineering</strong> Thermodynamics by P.K.Nag.<br />
5. <strong>Engineering</strong> Heat Transfer by C.P. Gupta and R. Prakash.<br />
ME111 APPLIED MECHANIC<br />
UNIT 1<br />
Fundamental concepts and principles <strong>of</strong> Mechanic, Reduction <strong>of</strong> a system <strong>of</strong> forces to a<br />
force couple system, free body diagrams, equilibrium <strong>of</strong> rigid bodies in 3 Dimensions,<br />
Reactions, loading indeterminacy and solvability. Friction forces and laws <strong>of</strong> dry friction<br />
principle and application <strong>of</strong> virtual work.<br />
UNIT 2<br />
Analysis <strong>of</strong> Multiple particle system application <strong>of</strong> Newton;s laws, linear and angular<br />
momentum, kinetic energy and work energy principle, principle <strong>of</strong> impulse and<br />
momentum to a system <strong>of</strong> particles.<br />
UNIT 3<br />
Translation and rotation about a fixed axis, general plane motion absolute and relative<br />
velocity in plane motion angular momentum <strong>of</strong> rigid body in plane motion. Problems <strong>of</strong><br />
motion <strong>of</strong> rigid bodies and system <strong>of</strong> rigid bodies principle <strong>of</strong> work and energy,<br />
conservation <strong>of</strong> energy for rigid body and a system <strong>of</strong> rigid bodies.<br />
UNIT 4<br />
Analysis <strong>of</strong> stress and strain Mechanical properties analysis <strong>of</strong> simple state <strong>of</strong> stress and<br />
strains, elastic constant, example <strong>of</strong> state <strong>of</strong> tension compression and shear<br />
UNIT 5<br />
22
Bending shear and torsion: Concept <strong>of</strong> bending and shear forces in shear forces in simple<br />
beams, relationship between load, bending moment and shear force. Bending and shear<br />
stresses in simples beams, concept <strong>of</strong> torsion in circular shafts.<br />
Text Books<br />
1. Beer Ferdinand P. and Johnston Jr. E Russel, Vector Mechanics for <strong>Engineering</strong> Statics<br />
and Dynamic Metric edition, Mc Graw Hill, New Delhi.<br />
2. Popov E., <strong>Engineering</strong> Mechanics <strong>of</strong> Solids, PHI, Delhi.<br />
Reference Books<br />
1. Merium, JL, <strong>Engineering</strong> Mechanics (Volume I and II), 3 rd edition, (SI version) John<br />
Wiley and sons, Inc, NT<br />
THIRD SEMESTER<br />
AM- : APPLIED MATHEMATICS III<br />
UNIT I: Vector differentiation, scalar field, gradient <strong>of</strong> a scalar field, vector field, divergence &<br />
curves <strong>of</strong> vector fields, solenoidal angle and irrotational field. Determination <strong>of</strong> potential<br />
function.<br />
UNIT II: Vector integration, line integral, conservation fields, Gauss divergence theorems,<br />
Greens theorem and Stokes theorem.<br />
UNIT III: Laplace’s transformation, shifting theorems, transforms <strong>of</strong> derivatives and integrals.<br />
Differentiation and Integration <strong>of</strong> transforms. Inverse transforms, Application with single and<br />
system <strong>of</strong> linear differential equations.<br />
UNIT IV: Boundary Value Problems, solution <strong>of</strong> 2D laplace equation in Cartesian and polar coordinates,<br />
solution <strong>of</strong> one dimensional diffusion and wave equation by method <strong>of</strong> separation <strong>of</strong><br />
variables.<br />
BOOKS:<br />
1. Prasad, C., “Mathematics for Engineers”, Prasad Mudranalaya, New Delhi, 1985.<br />
PK-214: REACTION KINETICS AND REACTOR DESIGN<br />
23
UNIT I: Rate <strong>of</strong> Reaction , elementary and non-elementary reactions molecularity and order <strong>of</strong><br />
reaction, thermodynamics formulations <strong>of</strong> rates, mechanism <strong>of</strong> reaction, Temperature<br />
dependency from thermodynamics, arrhenius, collision and activated complex theories,<br />
Introduction <strong>of</strong> industrial reactors.<br />
UNIT II: Integral and differential methods for analyzing kinetics data, interpretation <strong>of</strong> constant<br />
volume batch reactor data for zero, first second and <strong>third</strong> order reactions, half life period,<br />
irreversible reactions in parallel and series, auto catalytic reaction, shifting order reactions<br />
enzyme catalyzed and surface catalyzed reactions. Interpretation <strong>of</strong> variable volume batch<br />
reactor data for zero, first and second order reactions.<br />
UNIT III: Design equations for batch, plug flow, back mix, flow and semi batch reactors for<br />
isothermal, adiabatic reactions holding time and space time for flow system Design <strong>of</strong> batch plug<br />
flow and mixed flow reactors for first and second order single reactions. Optimum reactor size<br />
plug flow reactors in series / parallel Equal and different size <strong>of</strong> mixed reactors in series and<br />
finding the best system for a given conversion recycle reactor<br />
UNIT IV: Multiple reactions, independent, parallel and series reactions; mixed reactions,<br />
instantaneous and over all fractional yield, choice <strong>of</strong> reactors for simple and complex reactions<br />
and multiple reactor system; Introduction to thermal stability <strong>of</strong> reactors; temperature and<br />
pressure effects and optimal temperature progression for first order reactions. Introduction to<br />
Residence time Distribution <strong>of</strong> fluid in Vessel.<br />
BOOKS:<br />
1. Levenspiel, O., Chemical Reaction <strong>Engineering</strong>, John Wiley and Sons, New York, 3/e, 1998<br />
2. Fogler, H. S., Elements <strong>of</strong> Chemical Reaction <strong>Engineering</strong>, Prentice Hall, USA 4/e, 2005<br />
3. Smith, J. M., Chemical <strong>Engineering</strong> Kinetics, McGraw Hill Publications, New York, 1981<br />
PK-211: BASIC PRINCIPLES OF CHEMICAL ENGINEERING<br />
UNIT I: Introduction to Chemical <strong>Engineering</strong> and role <strong>of</strong> Chemical Engineer, Units and<br />
dimensions, stoichiometric and composition relationship, application <strong>of</strong><br />
thermodynamics and chemical principles in estimation <strong>of</strong> physical properties, ideal and<br />
real gas laws, critical properties, properties <strong>of</strong> mixtures and solutions, phase equilibria,<br />
vapor pressure<br />
UNIT II: Material balance without and with chemical reactions<br />
UNIT III: Energy balance without and with chemical reactions<br />
UNIT IV: Combined material and energy balance: Psychrometery, unsteady state<br />
material and energy balance, industrial applications.<br />
BOOKS :<br />
1. Felder, R.M. and Rousseau, R.W., “Elementary Principles <strong>of</strong> Chemical Processes”,<br />
Wiley International, New York, 3/e,2004.<br />
2. Himmelblau, D.M., “Basic Principles and Calculations in Chemical <strong>Engineering</strong>”,<br />
Prentice Hall, 7/e, 2004<br />
3. Hougen, O.A., Watson, K.M., and Regatz, R.A., “Chemical Process Principles, Vol.1”,<br />
Wiley International, New York,<br />
24
PK-213: FLUID MECHANICS<br />
Unit-I: Introduction to fluid mechanics, fluid static’s, Pascal’s and Hydrostatic law, manometers.<br />
velocity field, velocity gradient and rate <strong>of</strong> shear. Types <strong>of</strong> fluids, boundary layer concept,<br />
laminar and turbulent flow, boundary layer separation.<br />
Unit-II: Fluid dynamics; continuity equation, Euler equation, bernoullies equation, friction losses<br />
in pipe flow, valves and fittings, k-values, sudden expansion and contraction, pipe flow problems<br />
Unit-III: Transportation <strong>of</strong> fluids; types <strong>of</strong> pumps, centrifugal and positive displacement pumps<br />
compressors, fans, blowers, types <strong>of</strong> valves, pipes and tubes.<br />
Unit-IV: Metering <strong>of</strong> fluids; orifice meter, venturimeter, pitot tube, rotameter, notches, gas flow<br />
meters, coefficient <strong>of</strong> discharge<br />
BOOKS<br />
1. McCabe, W.L., Smith, Julian C. & Harriett, Peter, “Unit Operations <strong>of</strong> Chemical <strong>Engineering</strong>”,<br />
McGraw Hill, New Delhi, 7/e,2005.<br />
2. Kumar, K.L., <strong>Engineering</strong> Fluid Mechanics, Eurasia Publishing House (P) Ltd, New Delhi, 17/e,<br />
2008<br />
3. Bansal, R.K, “A Textbook <strong>of</strong> Fluid Mechanics”, Laxmi Publications(p) LTD, New Delhi, 2008<br />
PK-215: FLUID -PARTICLE OPERATIONS<br />
Unit-I: Particle technology; Particle size and shape , size distribution, equivalent particle<br />
diameter, volume surface mean diameter, determination <strong>of</strong> particle size ,screening, cumulative<br />
and differential plots, efficiency capacity and effectiveness <strong>of</strong> Industrial screens.<br />
Unit-II: Size reduction: crushing and grinding, energy requirement, rittengers law, kicks law,<br />
working <strong>of</strong> different crushers and grinders, power requirement. Close and open grinding.<br />
Storage <strong>of</strong> Solids: characteristics <strong>of</strong> solid masses, bins, silos, hoppers, Janssen’s equation.<br />
Unit-III: Particle dynamics: Drag From immersed body, effect <strong>of</strong> particle shape, wall and<br />
hindered settling, calculation <strong>of</strong> terminal settling velocity in stokes, Transition and Newton<br />
ranges. Particle Separation: sedimentation, elutriation, centrifuges and cyclone separation,<br />
Venturi scrubber, Electro-static precipitator<br />
Unit-IV: Flow Through Packed Beds: Types <strong>of</strong> packing, Characteristic <strong>of</strong> packing, pressure drop in<br />
packed beds, Kozeny-Carman equation, flooding and loading. Fluidization: aggregate and<br />
particulate fluidization, incipient fluidization velocity. Filtration; filter aids, plate and frame filter<br />
press, rotary drum filter.<br />
BOOKS:<br />
1. McCabe, W.L., Smith, Julian C. & Harriett, Peter, “Unit Operations <strong>of</strong> Chemical <strong>Engineering</strong>”,<br />
McGraw Hill, New Delhi, 7/e,2005.<br />
2. Narayanan, C.M., Bhattacharya, B.C., “Mechanical Operations for Chemical Engineers”,<br />
Khanna Publishers, Delhi., 3/e, 2005.<br />
3. Brown G.G., “Unit Operations”, John Wiley and Sons, New York, 1950.<br />
PK-212: CHEMISTRY OF HYDROCARBONS<br />
25
Unit I: origin and formation <strong>of</strong> Petroleum, Reserves and deposits, Indian Petroleum Industry, Composition<br />
<strong>of</strong> crude Oils, ultimate and chemical composition , non-hydrocarbons in petroleum, Asphltenes and<br />
Resins, classification <strong>of</strong> petroleum, evaluation <strong>of</strong> crude oil, Bench mark crudes.<br />
Unit II: characterization <strong>of</strong> crude oils : TBP and ASTM distillation, Classification by chemical composition,<br />
Correlation Index, Density, API gravity, Viscosity, UOP characterization factor, etc. Physical & Thermal<br />
properties <strong>of</strong> petroleum, ASTM, TBP, EFV distillation curves.<br />
Unit III: Distillation: Pretreatment, Electric desalting, atmospheric and vacuum distillation, petroleum<br />
products and their quality control tests.<br />
Unit IV: Value addition <strong>of</strong> petrochemicals from feedstock to consumer end products, chemical reactions<br />
<strong>of</strong> hydrocarbons like Decomposition (Thermal & Catalytic), Halogenations, Isomerization, Hydrogenation,<br />
Alkylation, Nitration, Sulfonation, etc. with chemistry and reaction mechanism.<br />
BOOKS:<br />
1. Speight, J.C.; “The Chemistry and <strong>Technology</strong> <strong>of</strong> Petroleum”, Marcel Dekkar, New York, 3/e1999.<br />
2. Lucas, A.G. (ed.), “Modern Petroleum <strong>Technology</strong>”, Vol. 2, Downstream, John Wiley & Sons<br />
Limited, New York, 6/e, 2000.<br />
3. Simanzhenkov, V. and Idem, R., “Crude oil Chemistry”, Marcel Dekker Inc., New York, 2003.<br />
4. Hobson, G.D., “Modern Petroleum <strong>Technology</strong>” Vol I & II, John Wiley & Sons, New York, 5/e,<br />
1984<br />
5. Rao, B.K.B., “Modern Petroleum Refining Processes”, Oxford & IBH Co. Pvt. Ltd., New Delhi, 4/e,<br />
2002,<br />
6. Prasad, R., “Petroleum Refining <strong>Technology</strong>”, Khanna Publishers, New Delhi, 2000<br />
ME – 290: MACHINE DRAWING AND COMPUTER<br />
GRAPHICS<br />
Drawing <strong>of</strong> following machine parts: threaded fasteners, screw jack, flexible coupling, stuffing box, swivel<br />
bearing, stop valve and some introduction <strong>of</strong> Auto CAD.<br />
FOURTH SEMESTER<br />
AM-: NUMERICAL METHODS AND OPTIMISATION<br />
UNIT I: General iteration method, Newton Raphson method, application <strong>of</strong> Newton Raphson<br />
method, Solution <strong>of</strong> system <strong>of</strong> linear equation by Gauss elimination method and Gauss Siedel<br />
method, Convergence <strong>of</strong> iteration.<br />
UNIT II: Interpolation-Finite difference operator, Central difference operator, backward<br />
difference operator, relation between operators, Newton’s forward Interpolation formula,<br />
Newton’s backward Interpolation formula, Newton’s Interpolation formula for unequal interval,<br />
Lagrange’s Interpolation formula for unequal interval.<br />
UNIT III: Numerical Differentiation- Newton’s divided difference formula; Numerical integration-<br />
Trapezoidal rule, Simpson’s rule, Weedle’s rule; Numerical Solution <strong>of</strong> differential equation-<br />
Solution with Taylor’s series, Euler’s method, modified Euler method, Runge-Kutta method,<br />
Boundary value problems.<br />
26
UNIT IV: Graphical and analytical methods <strong>of</strong> optimization, Numerical search methods, search <strong>of</strong><br />
optimum over single and several design variables, Optimum <strong>of</strong> process systems, linear<br />
programming.<br />
BOOKS :<br />
1. Sastry, S.S., “Introductory Methods <strong>of</strong> Numerical Analysis”, Prentice Hall <strong>of</strong> India Pvt. Ltd.,<br />
2004.<br />
PK – 221: CHEMICAL ENGINEERING THERMODYNAMICS<br />
UNIT I: The scope <strong>of</strong> thermodynamics, dimensions and units, measures <strong>of</strong> amount or size, force,<br />
temperature, pressure, work, energy and heat. The first law <strong>of</strong> thermodynamics and other basic<br />
concepts, Joules’ experiment, internal energy, the first law <strong>of</strong> thermodynamics, energy balance<br />
for closed systems, thermodynamic state and state functions, equilibrium, the phase rule, the<br />
reversible process, constant volume and constant pressure process, enthalpy, heat capacity. The<br />
second law <strong>of</strong> thermodynamics, statements <strong>of</strong> the second law, heat engines, thermodynamic<br />
temperature scales, entropy, entropy changes <strong>of</strong> an ideal gas, mathematical statement <strong>of</strong> the<br />
second law, entropy balance for open systems, calculation <strong>of</strong> ideal work, the <strong>third</strong> law <strong>of</strong><br />
thermodynamics.<br />
UNIT II: Refrigeration and Liquefaction: the Carnot refrigerator, the vapour – compression cycle,<br />
the choice <strong>of</strong> refrigerant, absorption refrigeration, the heat pump, liquefaction process. Vapour-<br />
Liquid Equilibrium: The nature <strong>of</strong> equilibrium, the phase rule-Duchem’s theorem, VLE –<br />
Quantitative behaviour, VLE by modified Raoult’s Law, VLE from k-value correlations.<br />
UNIT III: Solution thermodynamics: theory, fundamental property relation, the chemical<br />
potential and phase equilibria, partial properties, ideal-gas mixtures, fugacity and fugacity<br />
coefficients, pure species, species in solution, generalized correlations for the fugacity<br />
coefficient, the ideal solution, excess properties. Application ; liquid phase properties from VLE<br />
data, models for the excess Gibb’s energy, property changes <strong>of</strong> mixing, heat effects <strong>of</strong> mixing<br />
processes.<br />
UNIT IV: Chemical Reaction Equilibria: The reaction coordinate, application <strong>of</strong> equilibrium<br />
criteria to chemical reactions, the standard Gibbs. Energy change and the equilibrium constant,<br />
effect <strong>of</strong> temperature on the equilibrium constants, relation <strong>of</strong> equilibrium constants to<br />
composition, equilibrium conversions for single reactions, phase rule and Duhem’s theorem for<br />
reacting systems.<br />
BOOKS:<br />
1. Rao, Y.V.C. , “Chemical <strong>Engineering</strong> Thermodynamics”, Universities Press, India 2/e, 2001.<br />
2. Rao, Y.V.C., “Theory and Problems <strong>of</strong> Thermodynamics”, New Age International (P) Ltd, New<br />
Delhi, 2000<br />
3. Smith, J.M., Van Ness, H.C. and Abbott, M.M., “Chemical <strong>Engineering</strong> Thermodynamics”,<br />
Tata McGraw-Hill Publishing, New Delhi, 6/e, 2003.<br />
4. Kyle; B.G., “Chemical and Process Thermodynamics"; Prentice Hall, New York, 3/e, 1999<br />
PK 223 PROCESS DEVELOPMENT AND EQUIPMENT DESIGN<br />
UNIT I: Principles <strong>of</strong> process synthesis: reaction path synthesis, species allocation, separation task<br />
selection, task integration.<br />
27
Unit II: Diagrams for understanding chemical processes: Block Flow Diagram, Process Flow<br />
Diagram, Piping & Instrumentation Diagram. Structure and synthesis <strong>of</strong> process flow diagrams.<br />
Unit III: Chemical product design, tracing chemicals through the process flow diagram,<br />
understanding process conditions.<br />
UnitIV: Introduction to design codes, design <strong>of</strong> cylindrical and spherical shells, design <strong>of</strong> storage<br />
tanks, designs <strong>of</strong> tall vertical vessels, selection and design <strong>of</strong> flanges and supports for<br />
equipment.<br />
BOOKS:<br />
1. Turton, Richard, Bailie, Richard C., Wallace B. Whiting, Shaeiwitz, Joseph A.; “Analysis,<br />
Synthesis and Design <strong>of</strong> Chemical Processes”, Prentice Hall, USA 3/e, 2009.<br />
2. Douglas, J.M., “Conceptual Design <strong>of</strong> Chemical Processes”, McGraw-Hill, 1988<br />
3. Joshi, M.V. and Mahajani, V.V.; Process Equipment Design, 3/e, 1996, MacMillan India<br />
Ltd, New Delhi<br />
4. Bhattacharya, B.C. Introduction to Chemical Equipment Design –Mechanical Aspect,<br />
Chemical <strong>Engineering</strong> Education Development Centre I.I.T Madras.<br />
PK-223: SEPARATION PROCESSES<br />
UNIT-I: Introduction to separation processes, Phase equilibrium thermodynamics, Flash<br />
calculation, Distillation: Flash distillation, Differential distillation & Steam distillation; Binary<br />
distillation, Multi stage tray towers; McCabe & Thiele method, Ponchon & Savarit method,<br />
Continuous contact system (packed towers).<br />
UNIT-II: Multi-component distillation, Adsorption: Adsorption Equilibrium, Fixed bed adsorption<br />
column, Ion exchange method<br />
UNIT-III: Liquid-Liquid Extraction: Extraction Equilibrium, Extractive solvent, Extraction<br />
equipment, Multistage cross current and counter current operations, Liquid-solid leaching<br />
operation.<br />
UNIT-IV: Membrane Separation Processes: Types <strong>of</strong> membrane process, liquid and gas<br />
permeation membrane process, types <strong>of</strong> membrane, Applications<br />
BOOKS:<br />
1. Treybal, Robert E., “Mass Transfer Operations”, McGraw Hill Publications, 3/e, 2003.<br />
2. Geankoplis, Christie J., “Transport Processes and Unit Operations”, Prentice Hall <strong>of</strong> India,<br />
New Delhi, 3/e, 1997.<br />
3. Seader, J.D., Henley, Ernest J., “Separation Process Principles”, John Wiley & Sons, Inc,<br />
1998.<br />
PK-224 A HETEROGENEOUS REACTION ENGINEERING (DE-I)<br />
Unit 1: Catalysts, selecting catalytic agents, properties and characteristics <strong>of</strong> industrial catalysts,<br />
preparation <strong>of</strong> catalysts, catalyst testing, Classification and Kinetics <strong>of</strong> Catalysis.<br />
Unit II: Steps in catalytic reactions, synthesizing a rate law, mechanism and rate limiting steps<br />
design <strong>of</strong> reactors for non catalytic and catalytic reactions, gas-solid reactions. Heterogeneous<br />
Data Analysis for reactor design, catalyst deactivation.<br />
28
Unit III: External Diffusion effects on Heterogeneous Reactions, Diffusion and Reaction in Porous<br />
Catalysts, Effectiveness factors<br />
Unit IV: Reactor modeling with the RTD, zero parameter models, analysis <strong>of</strong> nonideal reactors,<br />
one parameter and two parameter models, testing a model and determining its parameters.<br />
BOOKS:<br />
1. Denbigh, K.G. and Turner, J.C.R., “Chemical Reactor Theory- An Introduction”, ELBS<br />
Publishing House, Cambridge, 2/e, 1981.<br />
2. Fogler, H. S., “Elements <strong>of</strong> Chemical Reaction <strong>Engineering</strong>”, Prentice Hall <strong>of</strong> India Private<br />
Limited, New Delhi, 3/e, 2005.<br />
3. Smith, J.M., “Chemical <strong>Engineering</strong> Kinetics”, McGraw Hill , New York, 3/e, 1981.<br />
4. Holland, C.D., and Anthony, R.G., “Fundamentals <strong>of</strong> Chemical Reaction <strong>Engineering</strong>”,<br />
Prentice Hall, New Jersey, 3/e, 1989.<br />
5. LE Page, J.F., “Applied Heterogeneous Catalysis-Design. Manufacture and Use <strong>of</strong> solid<br />
Catalysts”, Editions Technip..<br />
PK-224B: CATALYSIS (DE I)<br />
Unit I: Introduction <strong>of</strong> catalysis, Properties & chrematistics <strong>of</strong> catalysis<br />
Unit II: Preparation, testing and classification <strong>of</strong> catalysis.<br />
Unit III: Heterogeneous catalysis: Active centers, adsorption phenomena, active, encumbers &<br />
electron notions.<br />
Unit IV: Poisoning & Deactivation <strong>of</strong> Catalysis.<br />
BOOKS:<br />
1. Panchenkou, G.M. and Lebedev, V.P., “Chemical Kinetics & Calalysis, Mir Publishers,<br />
Moscov, 1976.<br />
2. Viswananthan. B., Sivasankar and Ramaswamy, A.V. (ed.), “Catalysis – Principles and<br />
Applications”, Narose Publishing House, New Delhi, 2002.<br />
3. Thomas, J.W. and Thomas, W.U., “Introduction to the Principle <strong>of</strong> Heterogeneous Catalysis,<br />
Academic Press, 1967.<br />
PK-224C CHEMICAL REACTOR DESIGN (DE-I)<br />
UNIT I: Behavior <strong>of</strong> Chemical Reactors: Ideal & Non-Ideal Flow; Classification <strong>of</strong> Reactors:<br />
Isothermal, Ideal batch, CSTR, PFR, Multiple Reactors, Non-isothermal Reactors,<br />
Multiplicity, Non-ideal reactors, Fluid Solid Non-Catalytic reactions, Fluidized Beds.<br />
UNIT II: Introduction to Reactor Design; Detailed Design <strong>of</strong> Batch Reactors.<br />
UNIT III: Flow Reactors; Detailed Design for CSTR; CSTR Design; Single CSTR Battery; CSTR at<br />
Differential Temperature etc.<br />
UNIT IV: Detailed Design for Plug Flow Reactor: Single; Series And Parallel; Mixed Reactor<br />
(Combination); Reactor stability, Design aspects for Non-ideal Reactors.<br />
BOOKS:<br />
1. Octave Levenspiel, “Chemical Reaction <strong>Engineering</strong>”, 3rd Edition, John Wiley &Sons (Asia)Pte Ltd.<br />
29
(1998), ISBN: 978-0-471-25424-9.<br />
2. H. Scott Fogler, “Elements <strong>of</strong> Chemical Reaction <strong>Engineering</strong>” 3rd Edition November,<br />
Prentice Hall <strong>of</strong> India Pvt Ltd (1998).<br />
3. L. D. Schmidt, “The <strong>Engineering</strong> <strong>of</strong> Chemical Reactions”, Oxford Press (1998).<br />
4.J.M. Smith, “Chemical <strong>Engineering</strong> Kinetics”, 2nd, McGraw-Hill (1981).<br />
CH – 292: UNIT OPERATION LAB-I<br />
EXPERIMENTS:<br />
1. To investigate validity <strong>of</strong> Bernoulli’s theorem as applied to flow <strong>of</strong> water in tube <strong>of</strong> varying<br />
cross section<br />
2. To find the efflux time <strong>of</strong> the tank<br />
3. Flow through straight circular tube<br />
4. Capillary flow viscometer<br />
5. Flow through helical tube coils<br />
6. Flow through spiral tubes<br />
7. Pipe flow <strong>of</strong> compressible fluids<br />
8. Flow through annulus<br />
PK-391: PETROLEUM TESTING LABORATORY<br />
Various Experiments related Analysis & Testing <strong>of</strong> Petroleum and Petroleum Products.<br />
FIFTH SEMESTER<br />
PK-311: PETROLEUM REFINING PROCESSES<br />
Unit I: Thermal conversion processes like Visbreaking, Delayed Coking, Fluid coking, Flexicoking,<br />
etc.<br />
Unit II: Catalytic conversion processes - fluid catalytic cracking, RFCC, DCC, Hydrocracking,<br />
Hydrotreating processes, etc.<br />
Unit III: Reforming, hydrogen production, Alkylation, Polymerization, Isomerisation etc.<br />
Unit IV: Evaluation <strong>of</strong> crude for LOBS, Production <strong>of</strong> lubes and waxes.<br />
BOOKS:<br />
1. Speight, J.G. and Ozum, B. “Petroleum Refining Processes”, Marcel Dekker Inc, New York,<br />
2002.<br />
2. Gary, J.H. and Handiwerk, G.E., “Petroleum Refining <strong>Technology</strong> and Economics”, Marcel<br />
Dekker, Inc., New York, 2001.<br />
3. Hobson, G.D., “Modern Petroleum <strong>Technology</strong>” Vol I & II, John Wiley & Sons, New York,<br />
5/e, 1984<br />
30
4. Rao, B.K.B., “Modern Petroleum Refining Processes”, Oxford & IBH Co. Pvt. Ltd., New Delhi,<br />
4/e, 2002,<br />
5. Prasad, R., “Petroleum Refining <strong>Technology</strong>”, Khanna Publishers, New Delhi, 2000<br />
PK-315: NATURAL GAS PROCESSING<br />
Unit I: Natural Gas-origin and occurrence, properties <strong>of</strong> natural gases, phase behavior <strong>of</strong> Natural<br />
Gas systems, vapor liquid equilibrium calculations.<br />
Unit II: Natural gas- liquid separation, separation principles, separation equipment, low<br />
temperature separation.<br />
Unit III: Water-hydrocarbon phase behaviour, measurement <strong>of</strong> water content in Natural gases,<br />
Hydrate formation and prevention <strong>of</strong> hydrates, Gas dehydration- types <strong>of</strong> processes.<br />
Unit IV: Acid gases in natural gas, acid gas treatment, types <strong>of</strong> processes. Natural gas<br />
storage, Natural gas liquids removal, Transportation <strong>of</strong> Natural Gas, LNG chain.<br />
BOOKS:<br />
1. Kumar, S., “Gas Production <strong>Engineering</strong>”, Gulf Publishing Company Book Division, London,<br />
1960.<br />
2. Mokhatab, S., William, A.P. and Speight, J.G., “Handbook <strong>of</strong> Natural Gas Transmission and<br />
Processing”, Gulf Pr<strong>of</strong>essional Publishing, Oxford, 2006.<br />
3. Francis, S.M. and Thompson, R.E., “Oil Field Processing <strong>of</strong> Petroleum, Volume one: Natural<br />
Gas”, Penn Well Books, Penn Well Publishing Company, Oklahoma, 1995.<br />
PK-313: MASS TRANSFER OPERATIONS<br />
UNIT I: General Introduction: Mass transfer operations and its classifications, Diffusion mass<br />
transfer, Mass transfer coefficient, Mass transfer models, Mass transfer with chemical reactions<br />
UNIT II: Gas Absorption Operations: Equilibrium, Choice <strong>of</strong> solvents, co-solvents, co-current and<br />
counter current operations, packed bed and staged columns.<br />
UNIT III: Humidification Operations: Psychrometry, Adiabatic humidification and<br />
dehumidification operations, Packed bed columns, Humidification equipments.<br />
Drying: Fundamentals, drying curves, equipment for drying<br />
UNIT IV: Equipment for Gas-Liquid Operations: Sparged vessels, mechanically agitated vessels.<br />
BOOKS:<br />
1. Treybal, R.E., “Mass Transfer Operations, Mc. Graw Hills, New York, 3/e, 1983<br />
2. Geankoplis, C.J., “Transport Processes and Unit Operations”, Prentice Hall <strong>of</strong> India, New<br />
Delhi, 4/e, 2003.<br />
3. Mc. Cabe, W.L., Smith, J.C., and Harriot, P., “Unit Operations <strong>of</strong> Chemical <strong>Engineering</strong>”, Mc.<br />
Graw Hills, New York, 6/e, 2001<br />
4. Skelland, A.H.P., “Diffusional Mass Transfer”, John Wiley and Sons, New York, 1974<br />
31
PK- 312: HEAT TRANSFER OPERATIONS<br />
UNIT I: Steady State heat conduction in one dimension: heat conduction through plane wall,<br />
composite wall, single layer cylinder, multi layer cylinder, sphere, Fourier’s Law <strong>of</strong> conduction<br />
and thermal conductivity, critical thickness <strong>of</strong> insulation, overall heat transfer coefficients.<br />
Forced Convection: forced convection past planar surface, inside cylindrical pipes and tubes and<br />
in non-circular sections, forced convection for external flow normal to tubes, tube banks.<br />
UNIT II: Heat Transfer by Free Convection: Governing equation for free convection, working<br />
correlations for free convection, analytical solution <strong>of</strong> free convection past vertical plane<br />
surfaces. Heat Transfer in Boiling and Condensing: working correlations <strong>of</strong> film condensation,<br />
dropwise condensation, heat transfer for boiling <strong>of</strong> a liquid, working correlations for pool<br />
boiling, forced convection boiling.<br />
UNIT III: Heat transfer by radiation: basic definition, laws <strong>of</strong> radiation, black body, gray body,<br />
shape factors. Heat Exchangers: Various types, general characteristics, overall heat transfer<br />
coefficient <strong>of</strong> heat exchanger, heat exchanger mean temperature difference, heat exchanger<br />
effectiveness and number <strong>of</strong> transfer units, performance <strong>of</strong> heat exchanger and design <strong>of</strong> heat<br />
exchanger.<br />
UNIT IV: Evaporation and Evaporators: types <strong>of</strong> evaporators, their construction and operation,<br />
evaporator auxiliaries, principles <strong>of</strong> evaporation, single effect evaporator, multiple effect<br />
evaporator, modes <strong>of</strong> feed supply to the evaporator, evaporator selection, effect <strong>of</strong> boiling point<br />
on multiple effect evaporator.<br />
BOOKS<br />
1. Chapman, A.J.,“Heat Transfer”, Mc Millan Publishing Company, New York, 4/e, 1984.<br />
2. Holman, J.P., “Heat Transfer”, Tata McGraw Hill Publishing Company, New Delhi, 9/e, 2009.<br />
AC-: ENGINEERING MATERIALS<br />
UNIT I Introduction to materials – basis <strong>of</strong> materials properties , atomic structure, bonding aggregates <strong>of</strong><br />
atom Iron & Steel : Crystals Structure – brief outlines <strong>of</strong> atomic bonding crystal structure , periodicity in<br />
crystal, different types <strong>of</strong> structures – SC, BCC, FCC and HCP crystals system, crystal lattice unit cell crystal<br />
direction, crystal planes, Miller indices, inter planar spacing , X-ray analysis, Crystals defects –<br />
classifications and impact on the properties <strong>of</strong> engineering materials<br />
UNIT II Phase equilibria – phase rule phase changes in pure Iron, binary systems, solid solution , Eutectic ,<br />
Eutectoid , Peritectic and Peritectoid reactions, General principles <strong>of</strong> heat treatment: Annealing,<br />
normalizing, Hardening, tempering and age hardening.<br />
UNIT III Properties and applications <strong>of</strong> materials <strong>of</strong> construction, factors affecting selection <strong>of</strong> materials,<br />
corrosion <strong>of</strong> materials <strong>of</strong> construction and its control.<br />
UNIT IV.Characterization <strong>of</strong> microstructure using Scanning Electron Microscopy (SEM), Transmission<br />
Electron Microscopy (TEM) and its sample preparation techniques, EDS, Atomic force microscopy (AFM),<br />
Dielectric spectroscopy, Fluorescence spectroscopy.<br />
BOOKS<br />
1. Van Vlack L.H. “Elements <strong>of</strong> Materials Science and <strong>Engineering</strong>” ed 6 th Addison Wesley Inc New York<br />
2. E.d. Dyson R.W “<strong>Engineering</strong> Polymers”, Blackie, New York.<br />
32
3. Smith C.O “The Science <strong>of</strong> <strong>Engineering</strong> Materials <strong>third</strong> edition, Prentice Hall Inc New Jersey.<br />
PK-314: REFINERY ENGINEERING CALCULATIONS<br />
Unit I: Overview <strong>of</strong> Global and Indian Refining Industry, Refinery configurations, ASTM, TBP, EFV<br />
distillation curves, computation <strong>of</strong> the curves Average boiling points. Separation criteria in crude oil<br />
fractionation<br />
Unit II: Atmospheric distillation tower, types <strong>of</strong> refluxes, Watkins method <strong>of</strong> converting crude TBP to<br />
product TBP curves, concept <strong>of</strong> overflash. Energy balance in a topping tower, and calculations involve<br />
estimation <strong>of</strong> top , side, bottom draw tray temperatures. Calculation <strong>of</strong> side steam strippers<br />
Unit III: Vacuum distilation tower, type <strong>of</strong> operations, economic consideration, flash zone & tower base<br />
calculations, flash zone pressure, steam requirements, heat & material balance calculation<br />
Unit IV: Types <strong>of</strong> pipe still heaters, calculations <strong>of</strong> radiant absorption rates, Wilson lobo Hotel equations,<br />
lobo Evans method pipe still design. Heat exchanger in refinery design and operational problems fluid<br />
mechanics and refinery applications use <strong>of</strong> combustion Charts.<br />
BOOKS<br />
1. R.N. Watkin, Petroleum Refinery Distillation, 2/e Gulf Publishing Co, Houstan, Texas, USA, 1981.<br />
2. B.K Bhaskar Rao, Modern Petroleum Refining Processes, 3/e, Oxford & IBH Publishing Co Pvt. Ltd.,<br />
1997.<br />
3. Wayne C. Edmister, Applied Hydrocarbon Thermodynamics, 2/e, Gulf Publishing Co., 1988.<br />
PK-391: COMPUTER APPLICATION LABORATORY<br />
Application <strong>of</strong> s<strong>of</strong>tware/tools related to Chemical/Refinery/Petrochemical processes.<br />
SIXTH SEMESTER<br />
PK-323: TRANSPORT PHENOMENA<br />
UNIT I: General Introduction to Transport Processes: analysis <strong>of</strong> momentum transport process,<br />
principle <strong>of</strong> shell balance, laminar, rectilinear steady flow <strong>of</strong> incompressible fluids in conduits<br />
and thin layer. Flow <strong>of</strong> falling film, flow between parallel plates, flow through circular pipes,<br />
capillary flow viscometer, flow through annular, adjacent flow <strong>of</strong> two immiscible fluids.<br />
UNIT II: Analysis <strong>of</strong> thermal transport processes: Fouriers law <strong>of</strong> heat conduction, steady one<br />
dimensional heat conduction without and with internal heat source, conduction through plane<br />
wall, hollow cylinder, composite wall, multilayer cylinder, overall heat transfer coefficient,<br />
critical thickness <strong>of</strong> insulation, heat conduction with internal electrical/nuclear/viscous and<br />
chemical heat.<br />
33
UNIT III: Analysis <strong>of</strong> species transport processes: Definition <strong>of</strong> concentration, velocity, flux in<br />
multi species system, Fick’s Law <strong>of</strong> diffusion, continuity equation for binary system and<br />
transport <strong>of</strong> species through annulus.<br />
UNIT IV: Macroscopic Analysis <strong>of</strong> momentum, heat and species transport: Macroscopic mass<br />
balance, momentum balance, mechanical energy balance, use <strong>of</strong> macroscopic balance<br />
equations, power requirement for pipeline flow, efflux time <strong>of</strong> tank. Interphase transport <strong>of</strong><br />
momentum/ heat/ species in turbulent flow: definition <strong>of</strong> friction factor, heat transfer<br />
coefficient, binary species transfer coefficient, interphase momentum/ heat/ species transport<br />
in circular tubes.<br />
BOOKS:<br />
1. Bird, R.B., Stewart, W.E., and Lightfoot, E.N., “Transport Phenomena”, John Wiley and Sons,<br />
New Delhi, 2008.<br />
2. Geankoplis, C.J., “Transport Processes and Unit Operations”, Prentice Hall <strong>of</strong> India, New<br />
Delhi, 4/e, 2003.<br />
PK-324: HEALTH, SAFETY AND ENVIRONMENT IN HC INDUSTRIES<br />
Unit I: Introduction, Types <strong>of</strong> hazards, analysis <strong>of</strong> hazards, Major process hazards, Fire hazards,<br />
classification <strong>of</strong> fire, Grades <strong>of</strong> fire hazard, Fire analysis, fire fighting, Different types <strong>of</strong> fire<br />
alarms / detectors & extinguishers, sprinkler, fire fighting services<br />
Unit II: Explosion Hazards in process Industries: Types <strong>of</strong> Explosions, Principles <strong>of</strong> Explosiondetonation<br />
and blast waves-explosion parameters-explosion prevention and protection<br />
Unit III: General discussion on toxicology, Physiological effects <strong>of</strong> various compounds,<br />
Classification <strong>of</strong> hazardous chemicals / conditions, local and systemic and chronic effects<br />
temporary and cumulative effects, Occupational health & safety concepts.<br />
Unit IV: Environmental pollution: Classification and properties <strong>of</strong> air pollutants-Pollution sources<br />
– automobile pollution, dispersion <strong>of</strong> pollutants, control <strong>of</strong> particulate and gaseous air<br />
pollutants. Water pollutants classification, different industrial effluents and their treatment and<br />
disposal – advanced water treatment.<br />
BOOKS:<br />
1. Mannan, S. (ed.), “ Lees’ Loss Prevention in Process Industries: Hazard Identification,<br />
Assessment and Control” Butterworth-Heinemann, 2004.<br />
2. Sanders R.E. “Chemical Process Safety: Learning From Case Histories”, Elsevier India Pvt.<br />
Ltd., 3/e, 2006.<br />
3. Rao, C.S., “Environmental Pollution <strong>Engineering</strong>:, Wiley Eastern Limited, New Delhi, 1992.<br />
4. Mahajan, S.P., “Pollution Control in Process Industries”, Tata McGraw Hill Publishing<br />
Company, New Delhi, 1993.<br />
PK-325: PETROCHEMICAL TECHNOLOGY - I<br />
UNIT I: History and importance <strong>of</strong> Petrochemical industry, growth in India, Classification <strong>of</strong><br />
Petrochemicals, Feedstock <strong>of</strong> the Petrochemicals, Preparation <strong>of</strong> feedstrock from ethane / propane and<br />
naphtha / gas oil cracking, syngas.<br />
34
UNIT II: Petrochemicals from C1, C2, C3, C4, Syngas & aromatics.<br />
UNIT III: Chemistry and technology for the production <strong>of</strong> Methanol formaldehyde, Ethylene oxide , glycol<br />
and Vinyl Chloride<br />
UNIT IV: Chemistry and <strong>Technology</strong> for the Production <strong>of</strong> Acetone, Cumene, Acrylonitrile, Linear alkyl<br />
benzene etc<br />
BOOKS:<br />
1 Waddams, A.L., ‘Chemicals from Petroleum’, 4 th edition, Gulf Publishing Company, London, 1980.<br />
2 Lewis F. Hatch & S Matar, From Hydrocarbon to Petrochemicals<br />
3 Chauvel and B. Lefebvre, Petrochemical Processes 1 & 2; Gulf Publishing Co. Houston, Texas, USA.<br />
4 M. Gopala Rao and Marshall Sitting, Outlines <strong>of</strong> Chemical <strong>Technology</strong>, 3/e, Affiliated East –West Press<br />
Pvt. Ltd, New Delhi.<br />
P321A: ALTERNATE FUELS AND ENERGY RESOURCES (DE - II)<br />
Unit I: Introduction to alternate fuels: the legislation for alternate fuels, the method <strong>of</strong><br />
production, properties and characteristics <strong>of</strong> the different alternate fuels and proper handling<br />
procedures.<br />
Unit II: Gas to Liquids <strong>Technology</strong> Fuels - Introduction to GTL route for cleaner fuels, properties<br />
and characteristics <strong>of</strong> the fuels produced.<br />
Unit III: Gasification technologies, gasification reactions, working <strong>of</strong> different types <strong>of</strong> gasifiers:<br />
moving bed, fluidized bed and entrained bed gasifiers, types <strong>of</strong> processes, fuels from biomass –<br />
thermal, chemical and biochemical conversions.<br />
Unit IV:Coal Liquefaction technologies: Carbonisation and Pyrolysis, Direct Liquefaction, Indirect<br />
Liquefaction<br />
BOOKS:<br />
1. T. N. Veziroglu, Alternative Energy Sources, Vol 5 and 6, McGraw-Hill, 1978.<br />
2. Rao, S. and Parulekar, B.B., “Energy <strong>Technology</strong>”, Khanna Publishers, Delhi.<br />
3. Speight, J.G., “Fuel Science and <strong>Technology</strong> Handbook”, Marcel and Dekker., New York,<br />
1995.<br />
4. Abbasi, S.A. & Abbasi, N., “Renewable Energy Sources and Their Environmental Impact”,<br />
Prentice Hall <strong>of</strong> India, New Delhi, 2002.<br />
PK 321B: RENEWABLE ENERGY (DE - II)<br />
Unit-I: Solar Energy ,Wind Energy ,Ocean Energy and Other Sources:<br />
Unit-II: Biomass resources and their classification; Chemical constituents and physicochemical<br />
characteristics <strong>of</strong> biomass; Biomass conversion processes; Bi<strong>of</strong>uels, Biomass conservation<br />
methods.<br />
Unit-III: Classification <strong>of</strong> wastes and their characteristics; Physical and chemical conversion<br />
processes: Incineration, pelletalization, landfill, and anaerobic digestion.<br />
35
Unit- IV: Fuel Cells ;Thermodynamics and electrochemical principles; Basic design, types,<br />
applications. Hydrogen Energy; Economics <strong>of</strong> hydrogen; Production methods; Biophotolysis:<br />
Hydrogen generation from algae /biological pathways; Storage and transportation; Applications<br />
BOOKS:<br />
1. Kreith, F. and Kreider, J.F., “Principles <strong>of</strong> Solar <strong>Engineering</strong>” , McGraw-Hill, 1978<br />
2. Kreider, J.F. and Kreith, F., “Solar Energy Handbook” McGraw-Hill 1981.<br />
3. T.N. Veziroglu, Alternative Energy Sources, Vol 5 and 6, McGraw-Hill, 1978.<br />
4. Khan, B.H., “Non-conventional Energy Resources”, Tata McGraw Hill, New Delhi, 2008.<br />
5. Sukhatme, S.P., “Solar Energy: Principles <strong>of</strong> Thermal Collection and Storage”, Tata McGraw-<br />
Hill, New Delhi, 1984.<br />
6. Duffie, J. A. and Beckman, W. A., “Solar <strong>Engineering</strong> <strong>of</strong> Thermal Processes”, John Wiley, 3/e,<br />
2006.<br />
7. Sorensen, B., “Renewable Energy”, Academic press, New York, 2/e, 2000.<br />
PK- 321C: ENERGY RESOURCES AND ENVIRONMENT MANAGEMENT(DE-II)<br />
Unit I: Global and Indian energy Scenario, Energy consumption pattern, energy as a factor<br />
limiting growth, need for use <strong>of</strong> new and renewable energy sources, Energy Crisis-Historical<br />
events<br />
Unit II: Non- renewable energy sources - coal, oil, natural gas, and nuclear energy<br />
Unit III: Renewable energy sources – Hydel energy, Solar Energy, tidal energy, biomass energy,<br />
wind energy, etc.<br />
Unit IV: Environmental degradation due to energy production and utilization, Primary and<br />
secondary pollution, air, thermal and water pollution, depletion <strong>of</strong> ozone layer, global warming,<br />
biological damage due to environmental degradation.<br />
BOOKS:<br />
1. Abbasi, S.A. & Abbasi, N., “Renewable Energy Sources and Their Environmental Impact”,<br />
Prentice Hall <strong>of</strong> India, New Delhi, 2002.<br />
2. Sukhatme, S.P., “Solar Energy: Principles <strong>of</strong> Thermal Collection and Storage”, Tata McGraw-<br />
Hill, New Delhi, 1984.<br />
3. Khan, B.H., “Non-conventional Energy Resources”, Tata McGraw Hill, New Delhi, 2008.<br />
4. Rai, G.D., “Non Conventional Energy Sources”, Khanna Publishers, Delhi, 2004.<br />
PK 321D: SYNTHETIC FUELS (DE-II)<br />
Unit-I: Fuels from coal development <strong>of</strong> synfuels, Properties & principles <strong>of</strong> coal conversion,<br />
thermodynamic <strong>of</strong> coal conversion Low, medium & high BTU gas from coal Clean liquid from<br />
coal Pyrolysis, liquefaction, coal & oil processing Environmental issues, CTL.<br />
Unit-II: Liquid fuels from NG, GTL, DME, Methanol, MTBE.<br />
Unit-III: Fuels from Biomass Biomass thermal conversion processes, Biological conversion<br />
processes, Lignocellulosic conversion processes.<br />
Unit-IV: Fuels from oil shales & tar sands, Properties <strong>of</strong> oil shales & tar sand above ground<br />
processes & insitu processes, Constraint in commercial production for oil shales & tar sands.<br />
36
BOOKS:<br />
1. Anderson, L.L. and Tillman, D.A., “Synthetic Fuels from Coal: Overview and Assessment”,<br />
Wiley-Interscience, New York, 1979.<br />
2. Lee, S., Speight, J.G. and Loyalka, S.K., “Handbook <strong>of</strong> Alternative Fuels Technologies”, CRC<br />
Press, 2007.<br />
ME-340: ECONOMICS AND MANAGEMENT<br />
UNIT I: Evolution <strong>of</strong> management, theories <strong>of</strong> management (scientific management, classical<br />
organizational management, Henry Gantt and Gilberth’s theory <strong>of</strong> management, behavorial<br />
approach, management science school), Functions <strong>of</strong> management (forecasting, planning<br />
organizing staffing directing, co-ordinating, controlling, decision making). Ownership-factors<br />
affecting the choice <strong>of</strong> ownerships, types <strong>of</strong> ownerships (individual ownerships, partnership<br />
firms, joint stock companies, co-operative societies, public sector undertakings).<br />
UNIT II: Steps in organizational design (division <strong>of</strong> work, departmentation, hierarchy, coordination),<br />
span <strong>of</strong> control or span <strong>of</strong> management, Garicuna’s theory, approaches to<br />
organizational design, classiscal approach, task technology approach, environmental approach.<br />
Leadership-source <strong>of</strong> power (Reward power, Coercive power, legitimate powers, expert powers,<br />
referent power), theories <strong>of</strong> leadership (trait theories, behavorial theory, situation theory and<br />
contingency approach)<br />
UNIT III: Types <strong>of</strong> behavior (status-meritorial, etc), leadership (democratic, autocratic, lessen<br />
free), motivation. <strong>Engineering</strong> economy (Law <strong>of</strong> supply and demand), Laws <strong>of</strong> diminishing<br />
return, unit cost function, elements <strong>of</strong> cost, overheads, break-even analysis and charts.<br />
UNIT IV: Forecasting and techniques, kinds and types <strong>of</strong> forecasting, methods <strong>of</strong> forecasting,<br />
qualitative methods (consumer survey model, composite sales team method, Delphi method).<br />
Statistical Approach - time series models, components <strong>of</strong> TS models, trend, seasonal variation,<br />
cyclic variation, Random variables, least square method, moving average method, weighted<br />
moving average method, semi-average method, and exponential smoothup. Casual Models –<br />
regression analysis, correlation analysis, standard deviation, Depreciation, cash flow diagrams<br />
and various numerical problems based on it. Present worth method, future worth, annual<br />
worth, ERR worth and ERR worth methods.<br />
BOOKS:<br />
1. Barthwal, R.R., “Industrial Economics”, New Age International Pvt. Ltd., New Delhi, 2/e,<br />
2000.<br />
2. De Garmo, P.E., “<strong>Engineering</strong> Economy”, Printice Hall Inc., New Jersey, 10/e, 1997<br />
3. Stoner, A.F., Freeman, E.R., Gilbert, D.R., Printice Hall Inc., New Jersey, 6/e, 1995<br />
CH – 393: UNIT OPERATION LAB II<br />
EXPERIMENTS<br />
1. Study <strong>of</strong> film and drop wise condensation<br />
2. To determine experimentally the overall heat transfer coefficient at various cold water flow<br />
rate and estimate film heat transfer coefficient on the shell side<br />
3. To study the boiling heat transfer phenomena for pool boiling <strong>of</strong> methylene chloride<br />
37
4. To determine surface heat transfer coefficient for heated vertical cylinder in natural<br />
convection<br />
5. To study convective heat transfer coefficient in an open pan evaporator under laminar and<br />
turbulent flow conditions.etc<br />
PK – 391: REACTION ENGINEERING LABORATORY<br />
Experiments related to reaction engineering such as Residence Time Distribution studies in<br />
CSTR, Studies <strong>of</strong> Plug Flow Reactor, etc.<br />
PK- 392: PROCESS EQUIPMENT DESIGN<br />
Flow sheet, Symbols <strong>of</strong> pipe fittings, valves and process equipment, Sketching and drawing <strong>of</strong><br />
process equipment, General format <strong>of</strong> a design report. Process and Mechanical Design <strong>of</strong><br />
Equipment used in Hydrocarbon Industries, design problems such as fluid transportation,<br />
storage, heat and mass transfer equipment. Preparation <strong>of</strong> process design data sheet.<br />
SEVENTH SEMESTER<br />
PK - 411: PROCESS DYNAMICS AND CONTROL<br />
Unit I: Process Control systems, Basic Concepts in Process Control., Process variables, control<br />
configurations & physical elements <strong>of</strong> a control System, Block diagrams, Dynamic Modeling <strong>of</strong><br />
processes, Linearization <strong>of</strong> Non-linear systems,<br />
Unit II: Response <strong>of</strong> first order system, Response <strong>of</strong> first order system in series (Interacting and<br />
non- interacting systems) , Second order system, Dynamic Response <strong>of</strong> second order system<br />
Transportation<br />
Unit III: Closed loop transfer functions, Modes <strong>of</strong> control action, Classification <strong>of</strong> Controllers,<br />
Transient response <strong>of</strong> some simple control systems. Stability analysis <strong>of</strong> control systems, Root<br />
locus Method, Controller Tuning, Frequency response analysis, Bode diagrams, control system<br />
design by frequency response, Bode stability criterion, Nyquist plots.<br />
Unit IV: Introduction to Advance Control Systems, Control systems with multiple loops, feed<br />
forward and Ratio Control systems. Process Control using Digital Computers, Reconstruction <strong>of</strong><br />
continuous signals from their discrete-time values, conversion <strong>of</strong> continuous to discrete time<br />
models, Z- transforms.<br />
BOOKS:<br />
1. Coughanowr, D. R., “Process Systems Analysis and Control”, McGraw Hill, New York,<br />
1991.<br />
2. Stephanopoulos G., “Chemical Process Control”, Prentice Hall <strong>of</strong> India, 1991.<br />
3. Weber, T.W., “An Introduction to Process Dynamics & Control”, John Wiley & Sons, New<br />
York, 1976.<br />
4. Bequette, B.W., “Process Control-Modeling, Design and Simulation”, Prentice Hall <strong>of</strong><br />
India Pvt. Limited, New Delhi, 2003.<br />
5. Luyben, W.L., “Process Modelling Simulation and Control for Chemical Engineers,<br />
McGraw Hill, New York, 2/e, 1990.<br />
38
6. Seborg, D.E., Edgar, T.E. and Mellichamp, D.A., “Process Dynamics and Control”, Wiley<br />
New York ,1989.<br />
7. Luyben, M.L. & Luyben, W. L., “Essentials <strong>of</strong> Process Control”, McGraw Hill, New York,<br />
1997.<br />
8. Palm, W.J., “Modelling, Analysis and Control <strong>of</strong> Dynamic Systems”, John Wiley and Sons,<br />
New York, 1983.<br />
PK 413: PETROCHEMICAL TECHNOLOGY II<br />
UNIT I: Chemistry and technology for the production <strong>of</strong> Phenol, Maleic anhydride, Phthalic anhydride,<br />
styrene etc.<br />
UNIT II: Chemistry and technology for the production <strong>of</strong> DMT, Terephalic acid, Acrylic acid, Methyl<br />
methacrylate etc<br />
UNIT III: Properties, applications and production technologies <strong>of</strong> the following commodity polymers –<br />
polyethylene, LLDPE, HDPE, polypropylene, polystyrene, PVC.<br />
UNIT IV:Properties, applications and production technologies <strong>of</strong> the following engineering and thermoset<br />
polymers: ABS plastic, nylon-6, polycarbonate, epoxy resin, unsaturated polyester resin, rubber<br />
BOOKS:<br />
1 Waddams, A.L., ‘Chemicals from Petroleum’, 4 th edition, Gulf Publishing Company, London, 1980.<br />
2 Lewis F. Hatch & S Matar, From Hydrocarbon to Petrochemicals<br />
3 B.K. Bhaskara Rao, A Text on Petrochemicals, 2/e, Khanna Publishers, Delhi, 1998.<br />
4 Mall, I.D., “Petrochemical Process <strong>Technology</strong>”, Macmillan India Limited, Delhi, 2007.<br />
5 F.A. Lowenheim and M. K. Moran; Industrial Chemicals, John Wiley & Son<br />
Inc.,USA.<br />
PK 412: PLANT DESIGN AND ECONOMICS<br />
UNIT I: Introduction, Process Design development, General design considerations, Cost and<br />
asset accounting, Cash flow for industrial operations, factors effecting investment and<br />
production cost, capital investments, estimation <strong>of</strong> capital investments, cost indices, cost factors<br />
in capital investment.<br />
Unit-II: Organizations for presenting capital investments, estimates by compartmentalization,<br />
estimation <strong>of</strong> total product <strong>of</strong> cost direction, production costs, fixed charges, plant overhead<br />
costs, financing, Interest and investment cost, type interest, nominal and effective interest<br />
rates, continuous interest, present worth and discount annuities, cost due interest on<br />
investment, source <strong>of</strong> capital.<br />
Unit-III: Taxes and insurances, type <strong>of</strong> taxes: federal income taxes, insurance-types <strong>of</strong> insurance,<br />
self insurance, Depreciation: types <strong>of</strong> depreciation, services life, salvage value, present value,<br />
methods for determining depreciation, single unit and group depreciation.<br />
39
Unit-IV: Pr<strong>of</strong>itability: alternative investments and replacements, pr<strong>of</strong>itability standards,<br />
discounted cash flow, capitalized cost, pay out period ,alternative investments, analysis with<br />
small investments, increments and replacements.<br />
BOOKS<br />
Max S. Peters, Klaus D. Timmerhaus and Ronal E. West, Plant Design and Economics for<br />
Chemical Engineers, 5 th ed. (2002), McGraw-Hill, New York.<br />
PK-414: POLYMER SCIENCE AND TECHNOLOGY<br />
Unit I: Classification <strong>of</strong> polymers, , Linear branched and cross – linked polymers, Molecular<br />
weights <strong>of</strong> polymers, Polydispersity and Mol. Wt. distribution in polymers, Random, alternate,<br />
block and graft co – polymers, polymer characterization techniques,polymer degradation.<br />
Unit II: Kinetics <strong>of</strong> chain & Step polymerization, techniques <strong>of</strong> molecular weight control,<br />
Initiators, Chain transfer agents, Inhibitors. Techniques <strong>of</strong> polymerization Bulk, Solution,<br />
Suspension & Emulsion polymerization.<br />
Unit III: Introduction to polymer rheology, Newtons law <strong>of</strong> viscosity, viscometris plots,<br />
rheometers, rheological models, theory <strong>of</strong> viscoelasticity, Tg, Heat distortion temperature.<br />
Unit IV: Basic concept <strong>of</strong> polymer processing: Compounding methods, Extrusion molding,<br />
Injection molding, Blow molding, Rotational molding. Introduction to fiber reinforced plastics.<br />
BOOKS:<br />
1. Gowariker, V.R., Viswanathan, N.V. and Sreedhar, J., “Polymer Science”, New Age<br />
International (P) Ltd, New Delhi, 1986.<br />
2. Odian, G., “Principles <strong>of</strong> Polymerization”, John Wiley & Sons Inc, New York, 1991.<br />
3. Tager, A., “Physical Chemistry <strong>of</strong> Polymers”, Mir Publishers, Moscow, 1978.<br />
4. Perepechko, I.I., “An Introduction to Polymer Physics”, Mir Publishers, Moscow, 1981.<br />
5. Billmeyer, F. W. “Textbook <strong>of</strong> Polymer Science”, John Wiley & Sons, New York, 1984.<br />
6. Kumar, A., “Fundamentals <strong>of</strong> Polymer <strong>Engineering</strong>”, 2/e, Marcel Dekker, New York, 2003.<br />
PK-491A: PROJECT<br />
Techno-economic feasibility analysis, presentation and report<br />
PK-4 81: PROFESSIONAL COMMUNICATION<br />
Effective technical and pr<strong>of</strong>essional communication that develops skills in Oral presentations, proposal<br />
writing, technical report writing, document design and basic research techniques through online and<br />
library sources. Read, write and evaluate a number <strong>of</strong> short reports, including mechanism and product<br />
descriptions, instructions, abstracts and summaries, project proposals, and progress reports. Business<br />
Communications: principles <strong>of</strong> effective business writing, writing business letters and memos, resume<br />
preparation and job search techniques; understand the principles <strong>of</strong> communication theories and the<br />
40
application <strong>of</strong> those theories in a variety <strong>of</strong> settings. Technical Writing; Technical Communication; Deliver<br />
an oral presentation <strong>of</strong> the findings.<br />
Books:<br />
1. Business correspondence and Report writing by R. C. Sharma and Krishnamohan,Tata<br />
McGrawHill2.<br />
2. Communication skills by B. V. Pathak, Nirali Publications.<br />
PK-492: CAD/SIMULATION LAB<br />
CAD/Simulation <strong>of</strong> Processes related to Chemical/Refinery/Petrochemical processes.<br />
EIGHTH SEMESTER<br />
PK-422: PROCESS UTILITIES AND ENERGY MANAGEMENT IN HC INDUSTRY<br />
Unit-I: Process utilities electricity, air, fuel oil, refrigerant. Classification and application <strong>of</strong><br />
refrigerant. Classification, specification and application <strong>of</strong> fuel oils. Handling and preparation <strong>of</strong><br />
fuel oil. Burner operation and maintenance.<br />
Unit-II: Sources uses, impurities & treatment methods for water, refinery water system. Efficient<br />
generation and utilization <strong>of</strong> steam. High pressure, low pressure and exhaust steams, Steam<br />
traps.<br />
Unit-III: Energy Management approach, Energy Audit, Energy conservation in major equipment<br />
used in refining, petrochemical and fertilizer industries like furnace, boilers, pumps, heat<br />
exchangers, distillation and extraction columns. Introduction to pinch technology.<br />
Unit-IV: Energy conservation equipment like waste heat boiler, recuperator, regenerator, heat<br />
pipe, heat pump, direct contact heat exchanger, economizer, fluidized bed boiler, continuous<br />
furnaces.<br />
BOOKS:<br />
1. Rajan, G. G., “Optimizing Energy Efficiencies in Industry”, Tata McGraw Hill Publishing<br />
Company, New Delhi, 2000.<br />
2. PCRA’s Thermal Booklet Series, Petroleum Conservation Research Association, Sanrakshan<br />
Bhawan, New Delhi<br />
3. Sinnot, R.K. “ Coulson and Richardson’s Chemical <strong>Engineering</strong>, Volume 6 – Chemical Process<br />
Design”, Elsevier, New Delhi, 4/e, 2008.<br />
4. O’Callaghan, P.W., “Energy Management”, McGraw Hill Company, 1993.<br />
PK-421A: PROCESS INSTRUMENTATION (DE-III)<br />
41
Unit I: Introduction to process control and instrumentation. Dynamic and static characteristics<br />
<strong>of</strong> instruments, Sensors for pressure, temperature, flow, level, humidity, viscosity, pH, density<br />
etc.<br />
Unit II: Pressure regulators, safety valves, level regulators, flow control valves such as globe<br />
valve, butterfly valve etc. pneumatic and electrical actuation <strong>of</strong> control valve.<br />
Unit III: Instrument and process equipment symbols, process flow diagram, process<br />
instrumentation diagram, development <strong>of</strong> P&ID for process industry.<br />
Unit IV: Introduction to PLC based instrumentation, Distributed Control System (DCS) system,<br />
and Supervisory Control and Data Acquisition (SCADA).<br />
BOOKS:<br />
1. William C. D., “Fundamental <strong>of</strong> Industrial Instrumentation and Process Control”, McGraw-<br />
Hill, New York, 2005.<br />
2. Eckman, D.P., “Industrial Instrumentation”, CBS Publishers, New Delhi, 2004.<br />
3. Nakra, B.C., Chaudhury, K.K., “Instrumentation Measurements and Analysis”, Tata McGraw-<br />
Hill, 1985.<br />
4. Barney, G.C., “Intelligent Instrumentation”, Prentice Hall <strong>of</strong> India Pvt. Ltd., New Delhi, 1992.<br />
PK-421B PIPING AND INSTRUMENTATION (DE-III)<br />
UNIT I Types <strong>of</strong> flow sheets, Flow sheet Presentation, Flow Sheet Symbols, Process flow<br />
diagram- Synthesis <strong>of</strong> steady state flow sheet - Flow sheeting s<strong>of</strong>tware.<br />
UNIT II P & I D objectives, guide rules, Symbols, Line numbering, Line schedule, P & I D<br />
development, typical stages <strong>of</strong> P & I D.<br />
P & I D for rotating equipment and static pressure vessels, Process vessels, absorber,<br />
evaporator.<br />
UNIT III Control System for Heater, Heat exchangers, reactors, dryers, Distillation column,<br />
Expander.<br />
UNIT IV Applications <strong>of</strong> P & I D in design stage - Construction stage - Commissioning stage -<br />
Operating stage - Revamping stage - Applications <strong>of</strong> P & I D in HAZOPS and Risk<br />
analysis.<br />
BOOKS:<br />
1. Ernest E. Ludwig, “Applied Process Design for Chemical and Petrochemical<br />
Plants”, Vol.-I Gulf Publishing Company, Houston, 1989.<br />
2. Max. S. Peters and K.D.Timmerhaus, “Plant Design and Economics for Chemical<br />
Engineers”, McGraw Hill, Inc., New York, 1991.<br />
3. Anil Kumar,”Chemical Process Synthesis and <strong>Engineering</strong> Design”, Tata McGraw<br />
Hill publishing Company Limited, New Delhi - 1981.<br />
5. A.N. Westerberg, et al., “Process Flowsheeting”, Cambridge University Press, 1979<br />
PK-421C INSTRUMENTATION ENGINEERING<br />
42
UNIT I: Measurements and measurement systems: what is measurement measuring<br />
instruments measurementsystems functional elements and block diagram <strong>of</strong> a measurement<br />
system. Classification <strong>of</strong> measuringinstruments standards calibration <strong>of</strong> measuring instruments.<br />
UNIT II : :Static characteristics specifications <strong>of</strong> instrument static characteristic s order <strong>of</strong> the<br />
instrument systemstandard test signals. Transfer function <strong>of</strong> a measurement system.<br />
UNIT III: Types <strong>of</strong> errors sources <strong>of</strong> errors methods <strong>of</strong> elimination or reduction Statistical<br />
analysis <strong>of</strong> errors selections<strong>of</strong> the instrument.Data presentation systems analog and digital<br />
indicators recorders self balancing or servo recordersmagnetic tape & disc storage systems date<br />
acquisition systems.<br />
UNIT IV: :Introduction control terinalogy open and closed loop control basic elements <strong>of</strong> open<br />
and closed loop controlsystems types <strong>of</strong> control actions.Metrology: standardization and<br />
standardizing organizations international systems <strong>of</strong> units. Toleranceslimits <strong>of</strong> size linear<br />
measurements – calipers – pitch screw gauge – feeler gauges – vernier instruments –dial gauges<br />
angular measurements – vernier and optical level potracters – angle gauges – angle deccer –<br />
spirit level.<br />
BOOKS:<br />
1. Patranabis D – Principles <strong>of</strong> Industrial Instrumentation, TMH publication, N. Delhi, 1976.<br />
2. Liptak B.G (Ed) – Instrument Engineers’ Handbook, Vol I and II and supplement I and II,<br />
Chilton Book Co., Philadelphia, 1972.<br />
3. Jones E B – Instrument <strong>Technology</strong>, Vol. II, Analysis Instruments, Butterworths Scientific<br />
Publication, London<br />
PK-423A: FERTILIZER TECHNOLOGY (DE-IV)<br />
Unit I: Macro- and micro nutrients, fertilizer Grades, Various fertilizers and their demand and<br />
production in India, Bi<strong>of</strong>ertilizers, case studies.<br />
Unit II: Nitrogenous fertilizers , Nitrogen , Hydrogen , Nitric Acid ,Ammonia Synthesis , Urea ,<br />
Sulphuric Acid, Ammonium Sulphate, Ammonium Nitrate , Calcium Ammonium Nitrate.<br />
Unit III: Phosphatic fertilizers, phosphoric acid,, super phosphate , Triple super phosphate,<br />
Mono and diammonium phosphate , Nitro phosphate ,<br />
Unit IV: Potassic fertilizers, Mixed Fertilizers, secondary nutrient fertilizers<br />
BOOKS:<br />
1. Slack, A.V. and James, G.R., “Fertilizers Science and <strong>Technology</strong> Series”, Marcel Dekker Inc.<br />
New York, 1983.<br />
2. Rao, M.G. and Marshall Sittig, “Out lines <strong>of</strong> Chemical <strong>Technology</strong>”, East-West Press, 1996.<br />
3. Pandey G.N. and Shukla, B.D. “A Text Book <strong>of</strong> Chemical <strong>Technology</strong>, Vol I, Vikas. Publishing<br />
House, New Delhi.<br />
PK-423B COAL AND GAS CONVERSION TECHNOLOGY (DE-IV)<br />
UNIT I Origin and Classification <strong>of</strong> Coal, Characterization and Industrial uses, Carbonization Processes,<br />
Chemicals from coal.<br />
UNIT II Theory <strong>of</strong> Gasification reaction, Industrial Gasification <strong>of</strong> Coal with oxygen and steam.<br />
43
UNIT III Important Petrochemicals derived from Natural Gas /Methane syngas,<br />
UNIT IV Conversion <strong>of</strong> Syngas to liquid fuels- Gasoline, Diesel, Olefins, DME, Oxo-alcohols, mixed alcohols,<br />
Polymethylene.<br />
BOOKS<br />
1. F.A Lowenheim and M.KMoran; Industrial Chemicals, John Wiley & Sons Ins. USA.<br />
2. Considine, D.M., Energy <strong>Technology</strong> HandBook, McGraw Hill Book Company, New York.<br />
3. Sarkar S., Fuels and Combustion, Second Edition, Orient Longman Ltd, Kamani Marg, Ballard Estate,<br />
Mumbai-400001<br />
4. Chemical Process Industries, R.N. Shreve and J.A. Brink, Jr. McGraw Hill Book Company, New York<br />
PK 423B: SELECTED TOPICS IN REFINING & PETROCHEMICALS (DE-IV)<br />
UNIT I: Transportation and storage <strong>of</strong> crude oil and petroleum products, Types <strong>of</strong> tanks,<br />
Pressure vessels and underground storage.<br />
UNIT II: Sweetening processes, hydrogen sulphide removal, Sulfur conversion processes, Solvent<br />
Deasphalting, Gasification<br />
UNIT III: Ammonia, Nitric Acid, Ammonium Nitrate, Urea.<br />
UNIT IV: Phosphatic fertilizers, super phosphate, Triple super phosphate, Mono and<br />
diammonium phosphate, Nitro phosphate, Mixed Fertilizers.<br />
BOOKS:<br />
1. Speight, J.G., “The Chemistry & <strong>Technology</strong> <strong>of</strong> Petroleum”, CRC Press, New York, 4/e, 2007.<br />
2. Speight, J.G. and Ozum, B. “Petroleum Refining Processes”, Marcel Dekker Inc, New York,<br />
2002.<br />
3. Gary, J.H. and Handiwerk, G.E., “Petroleum Refining <strong>Technology</strong> and Economics”, Marcel<br />
Dekker, Inc., New York, 2001.<br />
4. Hobson, G.D., “Modern Petroleum <strong>Technology</strong>” Vol I & II, John Wiley & Sons, New York,<br />
5/e, 1984<br />
5. Chauvel, A. and Lefebvre, G., “Petrochemical Processes”, Gulf Publishing Company,<br />
Houston, 1989.<br />
6. Matar, S., “Chemistry <strong>of</strong> Petrochemical Processes”, Gulf Publishing Company, Houston, 2/e,<br />
2000<br />
7. Waddams, A.L., “Chemicals from Petroleum”, Gulf Publishing Company, London, 4/e, 1980.<br />
8. Mall, I.D., “Petrochemical Process <strong>Technology</strong>”, Macmillan India Limited, Delhi, 2007.<br />
9. Meyers, R.A. (ed.), “Handbook <strong>of</strong> Petrochemicals Production Processes”, McGraw Hill, New<br />
York, 2005.<br />
PK-491B: PROJECT<br />
Techno-economic feasibility analysis, presentation and report.<br />
44
PK – 494: INSTRUMENTATION AND PROCESS CONTROL LABORATORY<br />
Experiments related to Process instrumentation and control .<br />
PK-493: POLYMER LABORATORY<br />
Experiments related to polymer Science and <strong>Technology</strong> .<br />
OPEN ELECTIVES<br />
PK – : POLYMER STRUCTURE PROPERTY RELATIONSHIP<br />
UNIT I Linear, branched, cross linked and other polymer structures, Homochain and heterochain<br />
polymers, random, alternate, block and graft copolymers. Pressure volume temperature (PVT)<br />
relationship. Prediction <strong>of</strong> polymer properties.<br />
UNIT II Mechanical and Rheological properties - Stress-strain relationship in polymer.<br />
Introduction to modulus, tensile strength, yield strength, percentage elongation, toughness,<br />
creep, fatigue and stress relaxation. Effect <strong>of</strong> additives on mechanical properties <strong>of</strong> polymers.<br />
Flow Behaviour <strong>of</strong> non – Newtonian fluids. Rheological models like power law, truncated power<br />
law, Bird – Carreau model etc. Effect <strong>of</strong> structure on viscometeric plot (shear rate vs. true<br />
viscosity).<br />
Introduction to Rheometers.<br />
UNIT III Thermal and Chemical Properties – Transition temperature in polymers, glass transition<br />
(Tg), melt transition (Tm), relationship between Tg and Tm. Heat Deflection Temperature (HDT)<br />
and its significance. Thermal characterization techniques like DSC, TGA, etc. Effect <strong>of</strong> polymer<br />
structure on thermal properties <strong>of</strong> polymer. Cohesive energy, cohesive energy density, solubility<br />
parameter, Prediction <strong>of</strong> solubility parameter -Effect <strong>of</strong> polymer structure on solubility <strong>of</strong><br />
polymer. Influence <strong>of</strong> structure in prediction <strong>of</strong> flame retardancy, water<br />
repellency.<br />
UNIT IV Electrical properties - Effect <strong>of</strong> polymer structure on dielectric constant, power factor,<br />
dissipation factor, and loss factor - effect <strong>of</strong> frequency <strong>of</strong> voltage and temperature on dielectric<br />
properties. Effect <strong>of</strong> additives on electrical properties <strong>of</strong> polymers<br />
BOOKS:<br />
1. Norbert M. Bikales, “Mechanical Properties <strong>of</strong> Polymers” Encyclopedia Reprints, Wiley<br />
Interscience, New York , ISBN: 0-471-07234-6.<br />
2. Johan J. Aklonis, William J. Macknights, M. Shen, “Introduction to Polymer<br />
Viscoelasticity” Wiley Interscience, New York , ISBN: 0-471-01860-0.<br />
3. W. Van Krevelen And P.J. H<strong>of</strong>tyzen, "Properties Of Polymer , 3rd Edition Elsevier<br />
Scientific PublishingCompany Amsterdam - Oxford - Newyork. 1990.<br />
4. D.A. Seanor, ed., Electrical properties <strong>of</strong> polymers, Acadamic press, Newyork, 1982.<br />
45
PK -: BIO PROCESS ENGINEERING<br />
Unit I: Introduction to Bioprocesses, outline <strong>of</strong> an integrated bioprocess and the various<br />
(upstream and down stream) unit operations involved in bioprocesses, generalized process flow<br />
sheets.<br />
Unit II: Fermentation Processes and Microbial growth ;General requirements <strong>of</strong> fermentation<br />
processes, Basic design and construction <strong>of</strong> fermentor and ancillaries, solid-substrate, slurry<br />
fermentation and its applications, behaviour <strong>of</strong> microbes in different reactors (air lift,<br />
fluidized,batch, continuous fed batch condition)<br />
Unit III: Bioreactors;Introduction to bioreactors; Batch and Fed-batch bioreactors, Continuous<br />
bioreactors; Immobilized cells; Bioreactor operation; Sterilization; Aeration; Sensors;<br />
Instrumentation; Culture-specific design aspects: plant/mammalian cell culture reactors.<br />
Unit IV: Bioseparations andindsstrial processes;Biomass removal; Biomass disruption;<br />
Membrane-based techniques; Extraction; Adsorption and Chromatography<br />
BOOKS:<br />
1. Biochemical <strong>Engineering</strong> Fundamentals Bailey and Ollis, McGraw Hill (2 nd Ed.), 1986.<br />
2. Bioprocess <strong>Engineering</strong>, Shule and Kargi, Prentice Hall, 1992.<br />
3. Stanbury, P. F., Whitaker, A., & Hall, S. J., (1998), Principles <strong>of</strong> fermentation<br />
PK : MODELLING AND SIMULATION<br />
Unit I: Fundamentals <strong>of</strong> Modelling, classification <strong>of</strong> models, determination <strong>of</strong> the process model,<br />
typical mathematical forms <strong>of</strong> models, component balance, energy balance, equation <strong>of</strong> motion<br />
and transport equations.<br />
Unit II: Process models examples <strong>of</strong> importance, modeling <strong>of</strong> Reactors, Distillation columns,<br />
furnaces, heat exchangers etc. Linearization <strong>of</strong> non-linear models.<br />
Unit III: Simulation <strong>of</strong> systems: Scope <strong>of</strong> process simulator, flowsheeting and specification<br />
problem, optimization problem, synthesis problem, steps for steady state simulation,<br />
flowsheeting decomposition and equation ordering.<br />
Unit IV: Simulation strategies, process simulator Process simulation with s<strong>of</strong>tware’s, Integrated<br />
computer aided design,<br />
BOOKS:<br />
1. W. F. Ramivez, computational Methods for Process Simulation, 2 nd ed., Butter worth’s 1997.<br />
2. K.M. Hangos & I.T. Cameras, Process Modulating & Model Analysis, Academic Process, 2009.<br />
3. Process Modelling and Simulation, R.W.Gaikwad and Dhirendra, Central Techno Publications,<br />
Nagpur, First Edition, 2003.<br />
4. Bird, R-P, Stewart, W.E, and light foot, E.N., Transport Pheromona, John Wiley & Sons, 1994.<br />
5. Westerberg. A.W., etal, Process flow sheeting, canbridge university Process, 1990,<br />
PK-: WASTE MANAGEMENT TECHNOLOGY<br />
46
Unit I: Sources, Classification and Composition <strong>of</strong> solid, liquid and gaseous wastes Hazardous<br />
and non-hazardous wastes, special waste materials<br />
Unit II: Waste Collection, Storage and Transport, Waste Disposal, Waste Processing Techniques.<br />
Unit III: Management <strong>of</strong> wastes, minimization, reuse and recycling Waste utilization and<br />
materials recovery<br />
Unit IV: Treatment <strong>of</strong> wastes; biological treatment, composting, anaerobic digestion,<br />
combustion, incineration<br />
BOOKS:<br />
1. Peavy, H.S., Rowe, D.R., and Techbanoglous, G., “Environmental <strong>Engineering</strong>”, McGraw Hill<br />
Books Company, 1985.<br />
2. Corbitt, R.A., “Standard Handbook <strong>of</strong> Environmental <strong>Engineering</strong>”; McGraw Hill, New York,<br />
1989.<br />
3. Martin, M. (ed), “Bio-conservation <strong>of</strong> Waste Materials to Industrial Products”; Elsevier,<br />
Amsterdam, 1991.<br />
4. Kharbanda, O.P. and Stellworthy, E.A., “Waste Management-Towards a Sustainable<br />
Society”, Gower Pub. Company, 1990.<br />
5. Mortensen, E., “Introduction to Solid Waste”, Lecture Notes to Graduate Diploma in<br />
Environmental <strong>Engineering</strong>, University <strong>College</strong>, Ireland, 1990-1993.<br />
6. Zirm, K.L., “The Management <strong>of</strong> Hazardous Substances in the Environment”, Routledge,<br />
New York, 1990.<br />
7. Somasekhar, R.K. and Mariyengar (ed.), “Solid Waste Management- Current Status and<br />
Stratagies for Future”, Allied Publishers, Mumbai, 2002.<br />
PK-: POLLUTION CONTROL EQUIPMENT DESIGN<br />
UNIT I: Introduction to air quality standards, effects <strong>of</strong> air pollution at regional and global scales,<br />
industrial air pollution sources, air quality parameters.<br />
UNIT II: Introduction to water quality standards, effects <strong>of</strong> air pollution at regional and global<br />
scales, industrial water pollution sources, water quality parameters.<br />
UNIT III: Design <strong>of</strong> selected gaseous and particulate pollutants control equipment such as<br />
Cyclones, Wet Scrubbers, Electrostatic Precipitators, incinerators, etc. Control <strong>of</strong> motor vehicle<br />
emissions, noise pollution and control.<br />
UNIT IV: Classification <strong>of</strong> wastewater treatment processes, Design <strong>of</strong> selected wastewater<br />
treatment equipment such as settling tank, trickling bed filter, etc.<br />
BOOKS:<br />
1. Nicholas, P.C. “Handbook <strong>of</strong> Air Pollution Prevention and Control”, Butterworth Heineman,<br />
N&P limited 2002.<br />
2. Schiftner, K.C., “Air Pollution Control Equipment Selection Guide”, Lewis Press, New York,<br />
2002.<br />
3. Peavy, H. S., Rowe, D.R., Tchobanoglous, G., “Environmental <strong>Engineering</strong>”, McGraw Hill.<br />
4. Louis T., “Air Pollution Control Equipment Calculations”, John Wiley and Sons, New Jersey,<br />
2008<br />
47
PK-: PROCESS EQUIPMENT AND PIPING DESIGN<br />
Unit I: Classification, selection, design and specification <strong>of</strong> selected process equipment like<br />
drums and tanks, mixers and agitators, etc.<br />
Unit II: Introduction to pressure vessel design, elementary idea <strong>of</strong> theories <strong>of</strong> failure <strong>of</strong> vessel<br />
under pressure, introduction to national and international design codes and their scopes, Design<br />
<strong>of</strong> cylindrical and spherical shells, design <strong>of</strong> storage tanks.<br />
Unit III: Introduction to high pressure vessel design, design <strong>of</strong> tall vertical vessels. Selection and<br />
design <strong>of</strong> flanges and support for vessels and piping, selection and design <strong>of</strong> heads and closures.<br />
Unit IV: Piping design, classification <strong>of</strong> pipes and tubes, important fittings and valves and their<br />
uses, color codes for pipelines, selection <strong>of</strong> optimum pipe size, schedule number, piping layout.<br />
BOOKS:<br />
1. Joshi, M.V. and Mahajani, V.V.; Process Equipment Design, , MacMillan India Ltd, New Delhi,<br />
3/e, 1996<br />
2. Sinnot, R. K., “Coulson and Richardson’s Chemical <strong>Engineering</strong>, Volume 6 – Chemical Process<br />
Design”, Elsevier, New Delhi, 2008.<br />
3. Brownell, L.L. and Young, E.H., “Process Equipment Design: Vessel Design”, John Wiley and<br />
Sons, New Delhi,<br />
4. Bhattacharya, B.C., “Introduction to Chemical Equipment Design – Mechanical Aspect”, CBS<br />
Publishers, New Delhi, 2009.<br />
5. IS 2825 – 1969, code for unfired pressure vessels, Indian Standards Institution, New Delhi.<br />
PK-: PROCESS DESIGN AND INTEGRATION<br />
Unit I: Background Concepts: Hierarchy <strong>of</strong> process design and integration, Onion Model,<br />
approaches to process design and integration. Role <strong>of</strong> process economics, capital costs for new<br />
design and retr<strong>of</strong>its, operating costs, criteria for economic evaluation.<br />
Unit II: Reaction Process Design: Choice <strong>of</strong> reactors, reactor conditions, reactor configuration.<br />
Unit III: Separation Process Design: choice <strong>of</strong> separation technology, operating conditions and<br />
configurations.<br />
Reaction, Separation and Recycle systems for Batch and continuous process.<br />
Unit IV: Heat Exchanger Networks: Basic elements <strong>of</strong> Pinch <strong>Technology</strong> – Grid diagram,<br />
composite curves, problem table algorithm. Targeting <strong>of</strong> Heat Exchange Networks, HEN Design.<br />
BOOKS:<br />
1. Smith, R. “Chemical Process: Design and Integration”, John Wiley and Sons, 2005.<br />
2. Kemp I. C., “Pinch Analysis and Process Integration: A user Guide on Process Integration for<br />
the Efficient Use <strong>of</strong> Energy”, Butterworth-Heinemann, 2/e, 2007<br />
3. El Halwagi M. M., “Process Integration”, Academic Press, 7/e, 2006.<br />
48
PK-: REFINERY EQUIPMENT DESIGN<br />
Unit I: ASTM, TBP EFV distillation curves, average boiling points, thermo-physical properties <strong>of</strong><br />
hydrocarbon, Review <strong>of</strong> refinery operations<br />
Unit II: Separation criteria in crude oil, atmospheric distillation column: refluxes, over flash;<br />
Energy and material balance calculations, estimation <strong>of</strong> top, side, bottom draw tray<br />
temperatures, topping tower design procedure.<br />
Unit III: Vacuum atmosphere tower, type <strong>of</strong> operations, economic consideration, flash zone &<br />
tower base calculations, flash zone pressure, steam requirements, heat & material balance<br />
calculation<br />
Unit IV: Types <strong>of</strong> pipe still heaters, thermal efficiency and component <strong>of</strong> furnaces, calculations<br />
<strong>of</strong> radiant absorption rates, Wilson lobo Hotel equations, lobo Evans method pipe still design.<br />
BOOKS:<br />
1. Watkins, R.N., “Petroleum Refinery Distillation”, Gulf Publishing Company, Houstan, 2/e,<br />
1981.<br />
2. Rao, B.K.B., “Modern Petroleum Refining Processes”, Oxford & IBH Co. Pvt. Ltd., New Delhi,<br />
4/e, 2002,<br />
3. Edmister, W. C., “Applied Hydrocarbon Thermodynamics”, Gulf Publishing Company,<br />
Houstan, 2/e, 1988.<br />
4. Trambouze, P., “Petroleum Refining - Material and Equipment” Part 4, Editions Technip,<br />
Paris, 2000.<br />
PK-: INTRODUCTION TO PETROLEUM ENGINEERING<br />
UNIT I: Global/Indian petroleum and petrochemical industry. Origin and occurrence <strong>of</strong> oil & gas.<br />
Migration and accumulation <strong>of</strong> oil and gas. Source, reservoir and cap rocks, Petroleum Traps,<br />
physical properties <strong>of</strong> oil bearing rocks.<br />
UNIT II: Oil & gas exploration methods, direct oil finding methods, geological and geophysical<br />
methods.<br />
UNIT III: Introduction to drilling operations, drilling equipment – drilling rigs and drill string,<br />
drilling fluids and mud testing, mud circulation and treating equipment, etc.<br />
UNIT IV : Production principles, types <strong>of</strong> reservoir drives, primary oil recovery, secondary oil<br />
recovery, enhanced oil recovery methods.<br />
BOOKS:<br />
1. Dawe, R.A. (ed.), “Modern Petroleum <strong>Technology</strong>”, Volume 1, John Wiley & Sons Limited,<br />
New York, 6/e, 2000<br />
2. Nontechnical Guide to Petroleum Geology, Exploration, Drilling and Production, Penn Well<br />
Corporation, Oklahoma, USA, 2/e, 2001<br />
49
3. Mian, M.A., “Petroleum Processing Handbook for Practicing Engineer”, Penn Well<br />
Corporation, Oklahoma, USA, 1992<br />
4. Deshpande, B.G., “The world <strong>of</strong> Petroleum”, Wiley Eastern Industry<br />
PK-: FUNDAMENTALS OF PETROLEUM PROSPECTING<br />
UNIT-I: Introduction, Historical Review, Prospecting for oil, seismic reflection method, seismic<br />
waves & seismic pulses,<br />
UNIT-II: The composition <strong>of</strong> reflection, seismic noise, data acquisition & data processing,<br />
Interpretation <strong>of</strong> seismic sections,<br />
UNIT-III: Direct indication <strong>of</strong> petroleum, earths magnetic field, air borne instruments,<br />
production <strong>of</strong> magnetic maps & interpretation, filtering methods.<br />
UNIT-IV: Gravity meters, Gravity reductions, Rock densities & interpretation, well logging, Bore<br />
hole conditions, Resistivity logs, Radioactivity logs, and other logs.<br />
BOOKS:<br />
1. Dawe, R.A. (ed.), “Modern Petroleum <strong>Technology</strong>”, Volume 1, John Wiley & Sons Limited,<br />
New York, 6/e, 2000<br />
2. Nontechnical Guide to Petroleum Geology, Exploration, Drilling and Production, Penn Well<br />
Corporation, Oklahoma, USA, 2/e, 2001<br />
3. The Petroleum Industry-A Nontechnical Guide, Charles F. Conaway, Penn Well Corporation,<br />
Oklahoma, USA.<br />
4. Production <strong>of</strong> Oil & Gas, F. Abdulin , Mir Publishers, Moscow<br />
5. Mian, M.A., “Petroleum Processing Handbook for Practicing Engineer”, Penn Well<br />
Corporation, Oklahoma, USA, 1992<br />
6. The world <strong>of</strong> Petroleum , B.G, Despande , Wiley Eastern Industry<br />
PK-: OIL RECOVERY TECHNIQUES<br />
Unit-I: Recovery <strong>of</strong> Hydrocarbons, exploration, drilling, well completion, well Products & product quality.<br />
Unit-II: Primary Recovery (Natural Methods): Dissolved gas drive, gas cap drive, water drive gravity drive<br />
& general considerations.<br />
Unit-III: Secondary Recovery Methods: Influence <strong>of</strong> Interfacial tension, oil recovery using gas or water<br />
injection, etc.<br />
Unit-IV: Enhanced oil Recovery methods (Tertiary Methods): Effect <strong>of</strong> Research Heterogeneity type on oil<br />
recovery, Chemical Methods, Miscible Methods, Thermal Methods, Mining Methods, Microbial Enhanced<br />
Oil Recovery, etc.<br />
BOOKS:<br />
1. Dawe, R.A. (ed.), “Modern Petroleum <strong>Technology</strong>”, Volume 1, John Wiley & Sons Limited,<br />
New York, 6/e, 2000<br />
2. Speight, J.C.; “The Chemistry and <strong>Technology</strong> <strong>of</strong> Petroleum”, Marcel Dekkar, New York,<br />
3/e1999.<br />
3. . Hobson, G.D, Pohl, W., Modern Petroleum <strong>Technology</strong> (Part I &II), John Wiley & Sons, N.Y.,<br />
1986.<br />
4. Nontechnical Guide to Petroleum Geology, Exploration, Drilling and Production, Penn Well<br />
Corporation, Oklahoma, USA., 2/e, 2001<br />
50
5. The Petroleum Industry-A Nontechnical Guide, Charles F. Conaway, Penn Well Corporation,<br />
Oklahoma, USA.<br />
6. Production <strong>of</strong> Oil & Gas, F. Abdulin , Mir Publishers, Moscow<br />
7. Mian, M.A., “Petroleum Processing Handbook for Practicing Engineer”, Penn Well<br />
Corporation, Oklahoma, USA, 1992<br />
8. The world <strong>of</strong> Petroleum , B.G, Despande , Wiley Eastern Industry<br />
MASTER OF TECHNOLOGY<br />
(PETROLEUM PROCESSING & PETROCHEMICAL ENGINEERING)<br />
51
COURSE CURRICULUM FOR M.TECH. (PETROLEUM PROCESSING & PETROCHEMICAL ENGINEERING)<br />
Session 2011-12<br />
Contact period per week<br />
Marks<br />
Course<br />
Lecture Practical General<br />
Course Mid-Sem End-Sem Total<br />
No.<br />
Semester - 1<br />
Course Title<br />
L P G Credits Work Exam Exam<br />
AM641 Advance Mathematics 3 0 1 4 15 25 60 100<br />
PK601 Fluid Flow and Heat Transfer 3 0 1 4 15 25 60 100<br />
PK602 Petroleum Processing 3 0 1 4 15 25 60 100<br />
PK603 Distillation and Extraction 3 0 1 4 15 25 60 100<br />
PK611 Elective -I 3 0 1 4 15 25 60 100<br />
PK-612 Elective -II 3 0 1 4 15 25 60 100<br />
Total 12 0 4 24<br />
Semester - 2<br />
PK604 Process Dynamics and Control 3 0 1 4 15 25 60 100<br />
PK605 Reactor Analysis and Design 3 0 1 4 15 25 60 100<br />
PK606 Petrochemical Processes 3 0 1 4 15 25 60 100<br />
PK607 Polymer and Composites 3 0 1 4 15 25 60 100<br />
PK608 Gas Processing 3 0 1 4 15 25 60 100<br />
PK690 Petroleum Testing Laboratory 0 4 0 4 60 40 100<br />
Total 15 4 5 24<br />
Semester - 3<br />
PK731 Elective –III 3 0 1 4 15 25 60 100<br />
PK780P General Seminar 0 0 2 2 60 40 100<br />
PK791P Lab/Project 0 3 0 3 60 40 100<br />
PK781P Preliminary Dissertation Seminar 0 0 3 3 60 40 100<br />
Total 0 3 5 12<br />
Semester -4<br />
PK782P Final Dissertation Seminar 0 0 0 2 60 40 100<br />
PK798P Dissertation 0 0 3 10 60 40 100<br />
Total 0 0 3 12<br />
Grand Total 72<br />
53
List <strong>of</strong> Electives : Comprising <strong>of</strong> Elective –I (PK-611), Elective II (PK-612) and Elective - III (PK-731)<br />
Modeling & Simulation <strong>of</strong> Separation Processes 3 0 1 4 15 25 60 100<br />
Alternate Fuels 3 0 1 4 15 25 60 100<br />
Materials <strong>of</strong> Construction in Petroleum & Petrochemical Plants 3 0 1 4 15 25 60 100<br />
Petroleum <strong>Engineering</strong> 3 0 1 4 15 25 60 100<br />
Reservoir <strong>Engineering</strong> 3 0 1 4 15 25 60 100<br />
Process Modelling and Simulation 3 0 1 4 15 25 60 100<br />
Process Optimization 3 0 1 4 15 25 60 100<br />
Air Pollution and Control 3 0 1 4 15 25 60 100<br />
Environmental Pollution and Impact Analysis 3 0 1 4 15 25 60 100<br />
Environmental Chemistry 3 0 1 4 15 25 60 100<br />
Ecology and Environmental Microbiology 3 0 1 4 15 25 60 100<br />
Petroleum Refinery <strong>Engineering</strong> 3 0 1 4 15 25 60 100<br />
Selected Topics in Petroleum Processing 3 0 1 4 15 25 60 100<br />
Solids and Industrial Waste Management 3 0 1 4 15 25 60 100<br />
Project <strong>Engineering</strong> <strong>of</strong> Petroleum and Petrochemical Plants 3 0 1 4 15 25 60 100<br />
Rheology and Testing <strong>of</strong> Polymers 3 0 1 4 15 25 60 100<br />
Multiphase Reactors 3 0 1 4 15 25 60 100<br />
Thermodynamics <strong>of</strong> Fluids and Fluid Mixture 3 0 1 4 15 25 60 100<br />
Mixing and Fluid Agitation 3 0 1 4 15 25 60 100<br />
Advanced Mass Transfer 3 0 1 4 15 25 60 100<br />
Coal Conversion Processes 3 0 1 4 15 25 60 100<br />
Heterogeneous Catalysis 3 0 1 4 15 25 60 100<br />
Novel Separation Process in Hydrocarbon Industries 3 0 1 4 15 25 60 100<br />
Safety and Hazard Assessment <strong>of</strong> Hydrocarbon Plants 3 0 1 4 15 25 60 100<br />
Colloid and Interface Science and <strong>Technology</strong> 3 0 1 4 15 25 60 100<br />
Bio-Chemical <strong>Engineering</strong> and Bio –<strong>Technology</strong>. 3 0 1 4 15 25 60 100<br />
54
FIRST YEAR<br />
M.TECH. (PETROLEUM PROCESSING & PETROCHEMICAL ENGINEERING)<br />
56
FIRST SEMESTER<br />
AM – 641: ADVANCE MATHEMATICS<br />
Vector space matrix solution <strong>of</strong> ODE (IVP), partial differential equations. Sturm<br />
louiville theory, separation <strong>of</strong> variables, Greens function, transform techniques, non<br />
– linear equation, continuous methods, bifurcation and Chaos Runge Kutta,<br />
multistep methods, Gears algorithm, Finite difference, finite elements, shooting<br />
methods.<br />
BOOKS<br />
1. Sastry, S.S., “Introductory Methods <strong>of</strong> Numerical Analysis”, Prentice Hall <strong>of</strong> india<br />
Pvt. Ltd., 1983.<br />
PK – 601: FLUID FLOW AND HEAT TRANSFER<br />
Fluid flow phenomena, Equation <strong>of</strong> continuity and continuity and momentum<br />
transfer, Navier Stroke’s equation and its solution to practical situation. Boundary<br />
layer theory, Von – Karmann theorem <strong>of</strong> integral momentum, Universal velocity<br />
pr<strong>of</strong>ile. Turbulent boundary layer, Non – Newtonian Fluid Flow. Flow <strong>of</strong> two – phase<br />
gas – liquid mixture in pipes two phase two flow model and governing equations,<br />
flow transition pressure drop calculation.<br />
Forced Convection heat transfer, Introduction to compact heat exchanger employing<br />
extended surfaces, heat transfer by conduction, heat transfer to solids in packed and<br />
moving / fluidized beds. Heat transfer to boiling liquids, Pinch <strong>Technology</strong> and its<br />
application, concepts <strong>of</strong> energy conservation and its application in process<br />
equipment.<br />
BOOKS<br />
1. F.A. Holland, Fluid Flow, Chemical Publishing Company, New York.<br />
2. D. Butterworth & G.F. Hewitt, Two – phase Flow and Heat Transfer, oxford<br />
university Press, London<br />
PK – 602: PETROLEUM PROCESSING<br />
Origin, occurrence, exploration, drilling & Production <strong>of</strong> Oil/ Gas Evaluation <strong>of</strong> oil,<br />
Petroleum refining in India, Refinery tests and crude distillation column, catalytic<br />
reforming for Gasoline upgrading and for aromatic production.<br />
BOOKS<br />
1. Speight, J.C.; The Chemistry and <strong>Technology</strong> <strong>of</strong> Petroleum, Marcel Dekkar, New<br />
York, 1991.<br />
2. Ram Prasad , Petroleum Refining <strong>Technology</strong> , Khanna Publishers , Delhi 2000<br />
57
3. Rao, B.K.B; Modern Petroleum Refining Processes, 4/e, 2002, Oxford and IBH<br />
Company Pvt. Ltd.<br />
4. G.D. Hobson, W. Pohl, Modern Petroleum <strong>Technology</strong> (Part I &II), John Wiley &<br />
Sons, N.Y., 1986.<br />
PK – 603 DISTILLATION AND EXTRACTION<br />
Thermodynamic equilibrium diagrams for binary and ternary system, analytical and<br />
graphical methods <strong>of</strong> calculation in distillation and extraction design <strong>of</strong> extractors<br />
key components bubble points and dew point, stage and extraction examples from<br />
petroleum refining, Azeotropic and extractive distillation.<br />
BOOKS<br />
1. Henley E.L., J.D. Seeder, Equilibrium – Stage separation operation in chemical<br />
engineering, John Wiley<br />
2. King C.J. Separation Process, TMH New Delhi (1962)<br />
PK – 611: ELECTIVE – I<br />
Modeling and Simulation <strong>of</strong> Separation Processes<br />
Thermodynamics <strong>of</strong> separation Processes: Property Calculation from various models.<br />
Single equilibrium stage and flash separation calculation. Modeling and separation<br />
cascades. Modeling <strong>of</strong> batch distillation. Advanced topics in Multicomponent staged<br />
separation processes such as distillation, absorption, extraction etc. Approximate<br />
(Shortcut) methods, rigorous methods, Rate based models for distillation, enhanced<br />
distillation and supercritical extraction modeling <strong>of</strong> membrane separation.<br />
BOOKS<br />
1. Smith B.D. Design <strong>of</strong> Equilibrium Stage Processes, McGraw Hill Book company,<br />
New York (1985)<br />
2. Holland C.D. and A.I. Liapis Computer Methods For Solving Dynamic Separation<br />
Problems, McGraw Hill Book company, New York (1983)<br />
3. Seader, J.D. and E.J. Henley, Separation Processes Principles, John Wiley and Sons<br />
Inc. New York (1983)<br />
Air Pollution and Control<br />
Classification and sources <strong>of</strong> air pollutants principle <strong>of</strong> meteorology and diffusion <strong>of</strong><br />
pollutants. Theory and description <strong>of</strong> control devices and their applications.<br />
BOOKS<br />
1. Peavy, H. S., Rowe, D.R., Tchobanoglous, G., “Environmental <strong>Engineering</strong>”,<br />
McGraw Hill.<br />
58
Environmental Pollution & Impact Analysis<br />
Dispersal <strong>of</strong> pollutants in environment and their effects principles <strong>of</strong> toxicology, air<br />
water quality criteria, standards framework for environmental assessment prediction<br />
and assessment <strong>of</strong> impact or air, water noise and biological environment,<br />
socioeconomic environment method <strong>of</strong> impact analysis.<br />
BOOKS<br />
1. M.N. Rao and HVN Rao Air Pollution Tata McGraw Hill Publication Co, Ltd. New<br />
Delhi<br />
2. L.Hodges Environment Population (Halt) and Winston Inc. New York 1973.<br />
3. S.H. Stroke and S.L. Seager, Environment Chemistry Air and Water Pollution<br />
(Scott Foresman & Co. New York)<br />
Reservoir Fluid Properties<br />
Study <strong>of</strong> the phase behavior <strong>of</strong> hydrocarbon system as related to petroleum and gas<br />
recovery. Ideal and real gas behavior, single and Multicomponent two – phase<br />
systems properties <strong>of</strong> reservoirs fluids under various conditions and pressure and<br />
temperature. Laboratory tests on reservoir fluids.<br />
BOOKS<br />
1. Modern Petroleum <strong>Technology</strong> , edited by Richard A. Dawe , Volume 1 , sixth<br />
edition , John Wiley & Sons Limited , New York<br />
2. Production <strong>of</strong> Oil & Gas, F. Abdulin , Mir Publishers, Moscow<br />
3. Petroleum Processing handbook for Practicing Engineer, M.A Mian<br />
Petroleum <strong>Engineering</strong><br />
Overview <strong>of</strong> petroleum engineering including geological and geophysical aspects.<br />
Presentation <strong>of</strong> the various stages <strong>of</strong> development <strong>of</strong> a petroleum reservoir including<br />
exploration drilling reservoir rock & fluid production and processing highlight <strong>of</strong> the<br />
petroleum industries.<br />
BOOKS<br />
1. Nontechnical Guide to Petroleum Geology, Exploration, Drilling and Production,<br />
2/e, 2001, Penn Well Corporation, Oklahoma, USA.<br />
2. The Petroleum Industry-A Nontechnical Guide, Charles F. Conaway, Penn Well<br />
Corporation, Oklahoma, USA.<br />
3. Modern Petroleum <strong>Technology</strong> , edited by Richard A. Dawe , Volume 1 , sixth<br />
edition , John Wiley & Sons Limited , New York<br />
59
Process Modeling and Simulation<br />
Model building and process analysis, model based on transport phenomena<br />
principles. Classification <strong>of</strong> transport phenomena models. Population balance model,<br />
simulation <strong>of</strong> steady state material and heat balance, process equipments.<br />
Simulation techniques for integrated Hydrocarbon plant.<br />
SECOND SEMESTER<br />
PK – 604 PROCESS DYNAMICS & CONTROL<br />
Development <strong>of</strong> dynamic models for physical system. Analysis <strong>of</strong> Pumped<br />
parameters system using transfer function and state models response <strong>of</strong> multistage<br />
process. Analysis <strong>of</strong> industrial system response <strong>of</strong> thermal and mass transfer<br />
methods with and without diffusion using exact and transfer system methods<br />
Classical control methods for linear system stability and optimum controller setting.<br />
Multiline loop multivariable feed forward, time optional and direct digital process<br />
control. Introduction <strong>of</strong> computer control <strong>of</strong> petroleum and chemical process<br />
industries.<br />
BOOKS<br />
1. J.M. Douglas, Process Dynamics and control Vol – I Analysis <strong>of</strong> Dynamic system<br />
Vol - II Control System Synthesis, Prentice Hall (1972)<br />
2. Donald R. Coughnowr and L.B. Koppel, Process System Anaysis and control,<br />
McGraw Hill<br />
3. W.L. Luyben Process Modeling, Simulation and control for Chemical Engineers,<br />
McGraw Hill Book Co. (1993)<br />
4. John & Fredly, Dynamic Behavior <strong>of</strong> Process, Prentice Hall<br />
PK-605 REACTOR ANALYSIS AND DESIGN<br />
RTD <strong>of</strong> ideal reactors, models for nonideal flow influence <strong>of</strong> RTD and micromixing<br />
on conversion, correlation for axial dispersion in continuous reactors. Rate <strong>of</strong> heat <strong>of</strong><br />
Chemical<br />
Reactors with or without external heat exchange. Role <strong>of</strong> mass transfer in chemical<br />
reactors,<br />
external and internal pellet mass and heat transfer, estimation <strong>of</strong> effectiveness factor,<br />
catalyst deactivation.<br />
BOOKS<br />
60
1. J.M. Thomas and W.J. Thomas, Introduction to the Principles <strong>of</strong> Heterogeneous<br />
Catalyst, Academic Press (1976).<br />
2. J.M. Smith, Kinetics for Chemical Engineers, McGraw Hill 1981.<br />
3. Kramer H. and Westertrap, Elements <strong>of</strong> Chemical Reactor Design and Analysis<br />
4. Danbigh, K.C. and Turnar, J.CR Chemical Reactor Theory, University Press,<br />
Cambridge<br />
PK-606 PETROCHEMICAL PROCESSES<br />
Petrochemical Industry overview, feedstocks, Production <strong>of</strong> olefins, Petrochemicals<br />
from C1, C2, C3, C4 and cyclic hydrocarbon with unit processes involved.<br />
Petrochemical from the processes namely alkylation, dealkylation, disproportionation,<br />
carboxylation, Hydration, dehydration, hydrolysis, esterification, desertification, oxidation,<br />
hydr<strong>of</strong>ormylation, isomerization synthesis, LAB detergent. Chemicals from coal F & T<br />
process.<br />
BOOKS<br />
1. Groogins, Unit Process in Organic Synthesis McGraw Hill Book Company, New York.<br />
2. Hatch L.F. and Matar Sarri From Hydrocarbons to Petrochemicals, Gulf Publishing Co.,<br />
Houston, London.<br />
3. Channel, A & Lefebvre G. Petrochemical Process, Vol. I & II, Gulf Publishing Co.,<br />
Houston, London.<br />
PK-607 POLYMERS AND COMPOSITES<br />
Definitions structure and classification <strong>of</strong> polymers methods <strong>of</strong> polymerizaion<br />
manufacturing<br />
methods properties and application technology <strong>of</strong> rubber and elastomers adhesive and<br />
sealants<br />
manufacture <strong>of</strong> films rods pipes and fibres.<br />
Definition structure, classification and characteristics <strong>of</strong> composites, raw materials-fibers<br />
resin,<br />
fibers and additives, pellets molding compounds, performs and textiles and perpetrates.<br />
Processing methods <strong>of</strong> thermoset and thermoplastic matrix composites structure property<br />
relations design consideration testing and quality control <strong>of</strong> composites.<br />
PK-608 GAS PROCESSING<br />
Gas processing: Gas and liquid separation, separation equipment, type <strong>of</strong> separators, separation<br />
principles, separator design, stage separation, low temperature separation, and gas cleaning.<br />
Dehydration processing <strong>of</strong> gas- water system: water content <strong>of</strong> natural gas, gas hydrates, absorption<br />
dehydration, adsorption, dehydration and dehydration by expansion, refrigeration. Desulfurization<br />
processing: removal processes, solid bed sweetening processes and physical and chemical absorption<br />
processes.<br />
61
BOOKS<br />
1. Gas Production <strong>Engineering</strong>, Sanjay Kumar, Gulf Publishing Company Book<br />
Division, London.<br />
2. Natural Gas <strong>Engineering</strong> Production & Storage, Donald L. Katz, Robert L. Lee, Mc.<br />
Graw Hill International Edition, New York.<br />
3. Francis, S.M. and Thompson, R.E., “Oil Field Processing <strong>of</strong> Petroleum, Volume<br />
one: Natural Gas”, Penn Well Books, Penn Well Publishing Company, Oklahoma.<br />
PK – 609 PETROLEUM TESTING LABORATORY<br />
Lab experiments covering the important test for distillation (ASTM/ IP. TBP) sulpher<br />
content, FIA analysis etc. these experiments will includes (a) Distillation <strong>of</strong> crude oils<br />
& characteristics <strong>of</strong> products (b) Test methods for petroleum products (c)<br />
Significance and interpretation <strong>of</strong> data and (d) Correlation & Prediction & Prediction<br />
<strong>of</strong> Properties.<br />
62
SECOND YEAR<br />
M.TECH. (PETROLEUM PROCESSING & PETROCHEMICAL ENGINEERING)<br />
63
THIRD SEMESTER<br />
PK-721: ELECTIVE-II<br />
Petroleum Refinery <strong>Engineering</strong><br />
An overview to petroleum refining industry in India., distillation fractions and their<br />
quality control Thermal Conversion processes, Thermal cracking, Visbreaking delayed<br />
& flexicoking. Catalytic conversion processes, catalytic cracking, FCC,<br />
catalytic reforming, Hydrocarcking, Hydrodesulphurization, Reside upgradation. etc.<br />
BOOKS<br />
1. Modern Petroleum <strong>Technology</strong>: G.D Hobson by. Who (Part I& II)<br />
2. Petroleum reining <strong>Technology</strong> & Economics, J.H. Garry, G.E Handiwork, Marcel &<br />
Dekker Inc. New York.<br />
Selected Topics in Petroleum Processing<br />
Treating Processes, Sweetening Processes Sulfur removal Process, Evaluation <strong>of</strong><br />
crude for lube base stocks Processes for deasphaltization, solvent extraction<br />
Dewaxing and refining <strong>of</strong> lube oil stocks. Quality improvement <strong>of</strong> lubricants with<br />
additive agents Manufacturing <strong>of</strong> specialty products bitumen and waxes<br />
Hydr<strong>of</strong>inishing <strong>of</strong> lube-base stocks Tests for finished lube oils grease and bitumen oil<br />
movement storage and safety requirements equipments refining effluents and their<br />
treatment, statutory regulation in Petroleum refining practice.<br />
BOOKS<br />
1. W.L. Nelson Petroleum Refining <strong>Engineering</strong>. 4th edition McGraw Hill(1961)<br />
2. G.d. Hobson and D.R. Pehl Modern Petroleum technology<br />
3. W.A. Gruse and D.R. Stevens Chemical <strong>Technology</strong> <strong>of</strong> Petroleum<br />
4. R.J. Hengetback, Petroleum Processing Primcipal and Application McGarw Hill<br />
5. V.A.Kalichesky amd K.A. kobe Petroleum Refining with Chemiclas Amsterdam<br />
Elsevier (1956)<br />
6. E.A. Evens London Lubricating and oils Champment and Hall (1963)<br />
Solid and Industrial Waste Management<br />
Quantity and characteristics if solid wastes concept <strong>of</strong> solid and hazardous waste<br />
management theory and application <strong>of</strong> unit operations unique to treatment<br />
reclamation and disposal <strong>of</strong> such wasters case studies<br />
Project <strong>Engineering</strong> <strong>of</strong> Petroleum & Petrochemical Plants<br />
64
Scope <strong>of</strong> project engineering project management plants techno-economical<br />
feasibility report, process refineries, Petrochemical Plants. Preliminary data for<br />
construction projects financial planning in project engineering problems in<br />
commercialization <strong>of</strong> Process developed by indigenous R&D evaluation and<br />
estimated material and energy balance equipment cost estimate waste study flow<br />
diagram Plot Plans Planning and Scheduling the project.<br />
Rheology and Testing <strong>of</strong> Polymers<br />
Analysis and characterization <strong>of</strong> the flow <strong>of</strong> non-Newtonian fluids, Rheology<br />
measurements on polymers and their interpretation viscoelasyiccoelastic material<br />
analysis <strong>of</strong> experimental data on and characterization <strong>of</strong> viscoelastics material.<br />
Mechanical, thermal electrical and optical properties <strong>of</strong> polymers and their<br />
evaluations.<br />
Multiphase Reactors<br />
Gas-liquid-solid catalytic and non-catalytic reacting systems Interaction <strong>of</strong> Physical<br />
and chemical inter-and interparticle transport Development <strong>of</strong> Kinetic models.<br />
Isothermal systems Stability criteria. Flow Modeling Hydrodynamic, deterministic<br />
and stochastic description. Evaluation <strong>of</strong> Model parameters. Interfacial area Bubble/<br />
Drop breakup, distributions, coalescence and dynamics.<br />
Mixing and Fluid Agitation<br />
Basic concepts <strong>of</strong> fluid mixing Impeller characteristics power correlation Pumping<br />
capacity <strong>of</strong> impeller Mixing in agitated vessel scale up and operating characteristics<br />
<strong>of</strong> liquid mixing system Heal and Mass transfer in agitated vessels Mixing Chemical<br />
reactions.<br />
Advanced Mass Transfer<br />
Molecular transport properties steady state diffusion Diffusitives in solids liquids<br />
gasses and electrolytes. Interphase mass transfer mechanism multicomponent<br />
system Ordinary diffusion in multicomponent system Convective Mass Transfer, in<br />
Laminar<br />
flow Turbulent Flow. Hatta and Dankwerts models.<br />
BOOKS<br />
1. Hanley E.L.J.D. Seader, Equilibrium Stage Separable Separations in Chemical<br />
Equilibrium John Wiley and Sons New York (1981).<br />
2. Holland, C.D. Fundamentals <strong>of</strong> Multicomponent Distillations McGraw Hill Book<br />
Company New York (1981).<br />
3. Watking R.N. Petroleum refinery Distillations and Publishing Company Houston<br />
(1979).<br />
65
4. King C.J. Separation Processes TMH New Delhi (1982), S. Skelland A.H.P.<br />
Diffusional Mass transfer New York McGraw hill Book Company (1974).<br />
Coal Conversion Process<br />
Origin and Classification <strong>of</strong> Coal, Characteristics and industrial uses, Carbonization<br />
Processes Coke areas by Product recovery systems liquid fuels from coal and tar.<br />
Theory <strong>of</strong> Gasification reaction, Industrial gasification <strong>of</strong> Coal with oxygen and<br />
steam.<br />
BOOKS<br />
1. Considine, D.M. Energy <strong>Technology</strong> Hand Book/ McGraw Hill Book Company,<br />
New York.<br />
2. Sarkar S. Fuels and Combustion Second edition Orient Longman Ltd. Kamani<br />
Marg Ballard Estate, Mumbai-400001<br />
3. Lowenhien, F.A. and Moran, M.K. Industrial Chemicals, John Willey and Sons,<br />
New Delhi.<br />
Heterogeneous Catalysts<br />
Review <strong>of</strong> Chemical kinetics, Homogeneous acid catalysts heterogenic catalysts<br />
Physical and chemical, surface area pore size and determination, reaction rates and<br />
selected diffusion in catalysts polymerization in emulsions selection preparation and<br />
evaporation <strong>of</strong> catalysts.<br />
BOOKS<br />
1. J.W. Thomas and W.J. Thomas Introduction to the principles <strong>of</strong> heterogeneous<br />
catalysts academic Press 1967.<br />
2. C.N. sattereed and T.I. Sherwood The role <strong>of</strong> diffusion in catalysts Addition<br />
Wesley 1963.<br />
Safety & Hazard Assessment <strong>of</strong> Hydrocarbon Plants<br />
industrial Safety & Loss trends, Loss Prevention, Major Hazards, legislation law,<br />
Technologies for hazard identification & assessment. Safety aspect <strong>of</strong> combustion,<br />
self heating, flame propagation, limits <strong>of</strong> flammability, Explosion, detonation &<br />
deflagation, toxic materials, dosage, acute & Chromic effects, Threshold limits,<br />
Instrumentation and Safety devices for temperature, flow, level composition and<br />
pressure, plant layout, fabrication & Inspection, Operability Steady, Hazard analysis,<br />
Safety effectiveness, Personal safety.<br />
BOOKS<br />
1. Frank P. Less, Loss Prevention in the process industry, Butter worth Heinmann.<br />
2. Roy E. A Saders, Chemical Process Safety learning from case History, butter worth<br />
Heinamann.<br />
66
3. Klctz, Trevor A, Critical Aspects <strong>of</strong> Safety & Loss Prevention, Butter worth London<br />
& Boston.<br />
Colloid and Interface Science and <strong>Technology</strong><br />
Capillarity, interfacial thermodynamics surfactants stability <strong>of</strong> multiphase systems<br />
foam, emulsion multiphase reactors wetting and adhesion catalyst sintering/<br />
redispersion stability and coagulation <strong>of</strong> colloids nucleation and growth colloids in<br />
Chemical engineering in separation processes, bio science.<br />
Biochemical <strong>Engineering</strong> and Biotechnology<br />
Computer application for instrumentation and control for on-line data acquisition<br />
and calculation <strong>of</strong> instantaneous mass and energy balance r-DNA manipulation and<br />
cell fusion approaches for hybridomas, dynamics <strong>of</strong> mixed culture and unstable<br />
recombinant microbial strains plant and animal tissue culture lines and bio<br />
transformation.<br />
PK-612 / CE - 625 Air Pollution & Control<br />
Classification and sources <strong>of</strong> air pollutants, Principles <strong>of</strong> meteorology and diffusion <strong>of</strong> pollutants,<br />
Dispersion models, Theory and description <strong>of</strong> control devices and their applications, Sources and<br />
effects <strong>of</strong> noise pollution. Kinetics <strong>of</strong> noise, Measurement and control <strong>of</strong> noise pollution.<br />
PK-612 / CE - 622 Environmental Chemistry<br />
Units <strong>of</strong> measurement, Chemical Kinetics, Acid base Chemistry, Solubility Concepts, Oxidationreduction<br />
reactions, Chemical equilibria, Organic chemistry, Aquatic chemistry Atmospheric<br />
chemistry, Pesticides, Surfactants and their biodegradability, Laboratory practice for determination <strong>of</strong><br />
ions and solids.<br />
PK-612 / CE - 623 Ecology and Environmental Microbiology<br />
Principles <strong>of</strong> ecology, Food chain, Trophic levels, Ecosystems, Biochemistry <strong>of</strong> natural compounds,<br />
Classification <strong>of</strong> microorganisms, Growth pattern <strong>of</strong> microorganisms, Biochemical reaction,<br />
Microbiology <strong>of</strong> aerobic and anaerobic processes, Biochemical pathways, Metabolism, Energy<br />
concepts, Pathogenic diseases, Basic microbiology <strong>of</strong> water, air and soil, Application <strong>of</strong> microbiology<br />
for pollution control, Laboratory Practice.<br />
THIRD SEMESTER<br />
PK731 : Elective- III<br />
PK780P : General Seminar<br />
67
PK791P : Lab/ Project<br />
PK781P : Preliminary Dissertation Seminar<br />
FOURTH SEMESTER<br />
PK782P : Final Dissertation Seminar<br />
PK798P : Dissertation<br />
2. Job Prospects Appendix –II<br />
S.No Name Details<br />
1. GAURAV JAIN Earlier in Reliance Industries / Kothari Infosys<br />
2. RAGHVENDRA SINGH PunjLoyd, K.S.A<br />
3. NITIU MAHEHAWARI Lecturer, BITS Pilani, Presently working in K.S.A<br />
4. MD. FARAZ AHMAD USA<br />
5. S.M. TARIQ ANWAR Earlier in Germany<br />
6. MOHD. JALAL SAEED Earlier in Sclumberger, Presently in Kuwait Oil Company<br />
7. PARUL GUPTA Working in U.S.A<br />
8. DILASHAD AHMAD Saudi ARAMCO, K.S.A<br />
9. RAKESH KUMAR SHARMA Works Manager, Ordinance Factory, Govt. <strong>of</strong> India<br />
10 MOHD. DANISH Radicon Gulf Consultant, K.S.A<br />
11. FAHIM ULLAH Earlier in Lurgi India, Presently with SABIC, KSA<br />
12. MOHAMMAD FAIZAN SAIPEM, India<br />
13 RAJ KUMAR TCS, Gurgaon<br />
14 SUMIT GUPTA SAP labs India Pvt. Limited<br />
15 MONIKA GOYAL Reliance Industries<br />
16 ZAID BIN KHALID Earlier in Reliance Industries, now in Gulf Country<br />
17 MOHD YUSUF ANSARI Assistant Pr<strong>of</strong>essor, AMU, Aligarh<br />
18 TABISH MAQBOOL Ph.D. (Michigan University), working in USA<br />
19 SAIMA MUNAWWAR Ph.D (Ireland), working in Dubai<br />
20 ABU. MOKHTARUL HASSAN Ph.D. (Michigan University), working in USA<br />
21 SHABIH UL HASAN Pursuing Ph.D. (IIT Bombay)<br />
22 SAMIDHA MITTAL DRDO (AGNI Project), Delhi<br />
23 MISS PREENA RAJORIA Reliance Industries<br />
24 ARAFAT ANWAR Reliance Industries<br />
25 MOHD RIZWAN Earlier in ONGC, Presently not known<br />
26 MOHD KAFEEL Lecturer, Engg, <strong>College</strong>, Meerut<br />
27 Pushkar Varshney Indian Oil Corporation Limited, Delhi<br />
28 Md. Faiyazur Rahman Valdel E & C Noida.<br />
29 Rohan Sharma Pursuing Ph.D (Temple University) USA<br />
30 Faheem Moohammad Khan PunjLoyd, India, Noida<br />
31 Satyendra Pratap Singh Infosys Gurgaon (Haryana)<br />
32 Shoeb Ahmad Lurgi India, Delhi<br />
33 Farid Ul Qadra Indian Oil Corporation Limited, Vadodara<br />
34 Utkarsh Maheshwari Lecturer, BITS, Pilani,<br />
35 Abhishek Gupta IIT Guwhati, Assam<br />
68
36 Muzzamil <strong>Hussain</strong> Politecnico di Milano, Como, Italy<br />
37 Wahid Ali Lecturer, Banasthali University, Rajasthan<br />
38 Faisal Abdullah Wipro Ltd. (WCCLG), Himachal Pradesh<br />
39 Mohd. Shariq Khan Pursuing Ph.D (Yeungnam University), South Korea<br />
40 Mustakim Ali Falcor Engg & Contraction Serv, ABU Dhabi<br />
41 Priyam Varshney IFFCO, Aonla, Bareily<br />
42 Ankit Varshney TCS, New Delhi<br />
43 Hakeem Abrar Ahmad Pursuing Ph.D. (Delft University <strong>of</strong> Tech.), Netherland<br />
44 Prashant Balyan GS E & C (LG. Haryana<br />
45 Shahid Kalam Samsung Heavy Industries, South Korea<br />
46 Mudassir Hasan Bahwaan Engg. Co., LLC, UAE<br />
47 Nehaluddin Khan Tradewell Group, KSA<br />
48 Mohammad Adnan Ajmal Indo Gulf Fertilizers Ltd, India<br />
49 Ibrar Ahmad Khan Reliance Industries Ltd.<br />
50 Saleem Akhtar Farooqui Scientist C, Indian Institute <strong>of</strong> Petroleum, Dehradun<br />
51 Rahul Singh ICICI Bank, India<br />
52 Tauseef Ahmad Indian Oil Corporation Limited, Barauni.<br />
53 Ms. Mehar Nosh Hafizee Earlier in UOP, Presently in IOCL<br />
54 Saad Ahmad Siddiqui Reda, Al Khobar KSA<br />
55 Nikhil Kumar Reliance Industries Ltd, Presently Pursuing Ph.D<br />
(Australia)<br />
56 Rahul Sirohi Pursuing Ph.D. (RGPIT Raibarelli)<br />
57 Mohammad Anas Ghayas Reda, Al Khobar KSA<br />
58 Mubashshir Arif Pursuing M.Tech (IIT Gawhati)<br />
59 Mohd Haseeb Khan TATA Chemical Gujarat, India<br />
60 Ali Shoeb Moon Yeungnam Univesity, Daegu, South Korea<br />
61 Syed Sahil Abbas Rizvi British Petroleum, Gurgaon<br />
62 Tafizur Rehman Indian Oil Corporation Ltd, R & D Centre, Faridabad<br />
63 Saima Hamid Pursuing M.Tech (TERI University), New Delhi<br />
64 Aashti Hamid Pursuing M.Tech (NCL, Pune) & will join as Scientist<br />
65 Amit Saxena Pursuing Ph.D (ISM Dhanbad)<br />
66 Shivanjali Sharma Pursuing Ph.D (ISM Dhanbad)<br />
67 Mohit Varshney Accenture, Chennai<br />
68 Shahid Amin KBC, Mumbai / (Earlier worked in KSA)<br />
69 Rajneesh Sirohi Lurgi India, Delhi<br />
70 Tarun Kumar Earlier in Duncan Fertilizers, Presently in Reliance<br />
Industries<br />
71 Syed Shariq Ali Earlier in Chambal Fertilizers, now in KSA Kota<br />
72 Md Junaid Ansari Earlier in Larsen & Toubro, Mumbai now in KSA<br />
73 Imarn Ali Khan SABIC, KSA<br />
74 Haris Kamal Shell, Holland<br />
75 Tauseef Zia Earlier in Vedanta as Head (Environment Section)<br />
76 Ahsan Munir Earlier in South Korea, Presently in Denmark<br />
77 Aslam Parveez Oil & Gas Company, Kuwait<br />
78 Nafees Ahmad Lecturer, KFUM, KSA<br />
79 Anuj Saxena Punj Lyod, Noida<br />
80 Md Faiyazur Rehman GS Engg. & Construction Pvt. Ltd.<br />
69