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UNITED STATES DEPARTMENT OF THE INTERIOR
GEOLOGICAL SURVEY
A LISTING AND STATISTICAL SUMMARY OF ANALYTICAL RESULTS
FOR PEBBLES, STREAM SEDIMENTS, AND HEAVY-MINERAL CONCENTRATES
FROM STREAM SEDIMENTS, PETERSRURG AREA, SOUTHEAST ALASKA
John B. Cathrall, Gordon W. Day, James D. Hoffman,
and Steven K. McDanal
Open-File Report 83-420-A
1983
please return to
MLNERRLS LIBRARY
A.D.G,G.S.
This report is the first publication belonging to the series of geochemical maps (having
the same Dpen-File Report number) concerning the Pttersburg area, southeast Alaska.
This report is preliminary and has not been reviewed for conformity with U.S. Geolo~ical
Survey editorial standards and stratigraphic nomenclature. Any use of trade names is for
dcscriptivc purposes only and does not imply constitute endorsement by the U.S.G.S.

CONTENTS
Page
Introduction ............................................................. 1
!lethods .................................................................. 1
Sampling and sample preparation methods ................................ 1
Analytical methods .................................................... 2
Statistical method ..................................................... 2
Media selection ............................................................ 3
Explanation for table 1 .................................................. 4
Explanation for tkble 2 ..................................................... 5
Explanation for tables 3 and 4 ............................................. 6
Explanation for table 5 ................................................... S
References cited ....................................................... 10
ILLUSTRATIONS
Plate 1.-;>lap showing localities for pebbles. stream sediments. and
heavy-mineral concentrate from stream-sediment samples.
Petersburg study area. Alaska .............................. ,., ....
TABLES
Table l.--Statistical summary of analytical results .............................. I1
2.-Enrichment above crustal abundance statistical summary ............... 15
3.-Analytical results for 1. 449 stream-sediment samples .................. 19
4.-Analytical results for 442 pebble samples ........................ ..,... 131
5.-Analytical results for 1. 430 heavy-mineral concentrate samples ........ -171

INTRODUCTION
A geochemical reconnaissance study was undertaken in the Petersburg area of
southeast Alaska, during the summers of 1978-1982, to aid in the evaluation of its
mineral potential. The study area includes the Pctcrsburg quadrangle, the western edge
of the Bradfield Canal quadrangle, the southwest edge of the Sumdum quadrangle, the
southeast edge of the Sitka quadrangle, and the east edge of the Port Alexander
quadrangle as shown on plate 1. In this report, these units will be referred to as the "he
Petersburg study arca.n For this study, 1,430 heavy-mineral concentrates from stream
sediments, 1,449 stream sediments, and 442 pebble samples from streams were
collected. Sample localities, analytical results, enrichment, and statistical data are
presented in this report. Sample localities are shown on plate 1. Statistical and
enrichment data derived from the analytical results arc shown in tables 1 and 2.
Analytical results for stream sediments, pebbles, and heavy-mineral concentrates from
stream sediments are shown in tables 3, 4, and 5.
METHODS
Sampling and Sample Preparation
Heavy-mirtral concentrates from strtam $ediments, stream sediments, and pebbles
fram streams wtre collected from the active parts of the stream channel.
Stream-sediment samples consisted of coarse- to fine-grained sediment that were
wet-sieved through a 2-mm stainless steel screen at the sample site; the screened
fraction was placed in metal-free cloth bags. Sample weights ranged from 150 to 251) g.
The samples were then air dried and screened by shaking through an 80-mesh stainltss-
steel sieve. The minus-80-mesh fractions were plactd in 0.12-L metal-free cardboard
containers and subsequently analyzed.
Heavy-mineral concentrates from stream-sediment samples consisted of several
scoops of coarse- to fine-grained sediment that were wet-sieved through a 2-mm
stainless-steel screen at the sample site. This sieved fraction was wet panned at the
sample site to reduce the percentages of light minerals in the sample. The panned
heavy-mineral concentrates from stream sediments were placed in metal-free paper
envelopes. The samples were then air-dried and further prepared by shaking through a
35-mesh stainless-steel sieve, the minus-35-mesh fraction was retained. In the
laboratory, the minus-35-mesh fraction was separated with bromoform into two
fractions: a light-mineral fraction having a specific gravity of 2.R5 or less and a hcavy-
mineral fraction having a specific gravity greater than 2.$5. The light-mineral fraction
was discarded. Magnetite and other magnetic minerals were removed from the heavy-
mineral fraction by use of a hand magnet and a Frantz lsodynarnic magnetic separator at
a setting of 0.2 amperes. The magnetic fraction was saved, but not analyzed. The
remaining heavy-mineral fraction was again run through the Frantz lsodynamic magnetic
separator at a setting of 0.6 amperes. The fraction that was nonmagnetic at this higher
setting contained primarily zircon, apatite, and sulfides; it was labeled C-3 and was
retained for spectrographic analysis. The intermediate fraction having magnetic
susceptibility between 0.2 and 0.6 amperes was not analyzed.
Pebbles from streams were collccttd from the strtam channel. Although alttrtd
and mineralized pebbles were looked for, few showed visible indication of alteration or
mineralization. Several pebbles wtre collccttd from the stream channel and plactd in
metal-fret cloth bags. All pebbles were crushed in a Chipmunk crusher to approximately

Analytical methods
The procedures used in analyzing stream sediments and pebble samples werc
identical. A six-step, DC-arc, semiquantitative emission spectrographic method was
used for the determination of Fe, Mg, Ca, Ti, Mn, Ag, AS, Au, B, Ba, Be, Bi, Cd, Co, Cr,
Cu, La, Mo, Nb, Ni, Pb, Sb, Sc, Sn, Sr, V, W, Y, Zn, Zr, and fh (Grimes and Marranzino,
1968). Atomic-absorption specfrophotometry was used to determine Cu, Pb, Zn, and Au
(Ward and others, 1969); colorimetry was used to determine W (Quinn and Brooks, 1972)
and fh (Palkalnes, 1972); selective ion electrode method was used to determine fluorine
(Hopkins, 1977); fluorornetric method was used to determine uranium (Centanni and
others, 1956); and neutron activation, delayed neutron counting, was used for U and Th
(M illard, 1976).
The C-3 fraction of the heavy-mineral concentrates from stream sediments was
analyzed by a six-step, DC-arc, semiquantitative emission spectrographic method
generally following that described by Grimes and M arranzino (1 968) for the analysis of
geologic material. fhcir method was modified in the following way to eliminate the
spectral interferences caused by high concentrations of iron, titanium, and zirconium.
Five milligrams of prepared sample was mixed with 20 rng of pure graphite powder and 5
mg of pure Arkansas quartz; the mixture was packed into a preformed graphite electrode
6.35 mm in diameter, and was burned in a DC-arc for 736 seconds using a 1.5-m
Wadsworth-mount grating spectrograph. As a result, the lower limits of determination
for the elements analyzed for this type of sample art all raised two reporting values
above the normal lower limit values of those values listed by Grimes and Marranzino
(1968). Spectrographic standards werc prepared in the same manner. Spectra were
recorded on 35-rnm SA-1 film in groups of 23 samples per film (that is each film includes
analytical spectra results for 22 field samples and one reference standard sample). The
rcferenct standard sample is included with each set of field samplcs to monitor the
quality of the analyses from film to film; however, the analysis for these reference
samples have bctn omitted from tables 3-5. Thirty-one elements were determined (Fe,
Mg, Ca, Ti, M n, Ag, As, Au, 8, Ba, Be, Bi, Cd, Co, Cr, Cu, La, M o, Nb, Ni, Pb, Sb, Sc, Sn,
Sr, V, W, Y, Zn, Zr, and Th).
The observed spectra from the stream sediment, and C-3 fraction samples were
compared visually to standard sptctra using a 20X comparator. The spectrographic
analytical values are reported as the approximate geometric midpoints 0.1 5, 0.2, 0.3, 0.5,
0.7, and 1.0 (or approximate powers of ten of these ralucs) of concentration ranges whose
respective boundaries are 0.1 2, 0.1 8, 0.26, 0.38, 0.56, 0.83, and 1.2 (or appropriate powers
of ten of these values).
The precision of a reported value is approximately plus or minus one reporting
value at 83 percent confidence and two reporting values at 96 percent confidence
(M otooka and Grimes, 1976).
The analyses were done by G. D. Day, S. 1. Sutlcy, J. D. Hoffman, B. F. Arbogast,
R. B. Vaughn, H. T. Y illard, Jr., and B. A. Ktattn,
Statistical methods
All data listed in tables 3, 4, and 5 were entered in the U.S. Geological Survey
computer data storage system entitled RASS (Rock Analyses Storage System), and
retrieved and analyzed by S. K. McDanal, W. 5. Speckman, C. M. Y cDougal, and j. D.
Hoffman, using the U.S. Geological Survey STATPAC program library (VanTrump and
M icsch, 1977).
A statistical summary of the analytical results for various sample media data are
presented in table 1, and an enrichment above crustal abundance statistical summary is
presented in table 2.

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C
M EDlA SELECTION
Stream sediments were chosen as the primary sample media because of the large
rite of the area that influcncer each sample.
Three sample media from the stream sediment were chosen to afford maximum
coverage of the major gcochcmical components of a drainage basin. They are (1) the
mtdiurn to fint fraction (-80 mesh) of the active sediment in the bed load of the stream,
(2) the heavy minerals incorporated in the bed load of the stream, and (3) pebbles
incorporated in the bed load of the stream channel.
The first of these sample media provides a typical geochemical cross section of the
transported components of the drainage basin. Its chemical composition is controlled
predominantly by the major geologic units of the drainage basin and to a Itsser extent by
scavenging materials such as amorphous iron-manganese oxides, clays, and organic
matter. Minor components of the drainage basin, such as a deposit of potentially
economic minerals, are usually reflected in this sample medium, but the influence is
often small because of dilution by the Iarge bulk of barren material derived from the
major components of the basin.
The second sample medium, in essence a subsample of the first, is used to enhance
the influence of minor components such as ore-telated minerals and to eliminate the
enhancing affect caused by organic material, clays, and in some instances the iron and
manganese hydrous oxides, which art commonly in this medium but are not very
magnetic. Most of the sediment in this medium is composed of minerals such as quartz,
feldspar, and clay, which art of low specific gravity and of little or no interest in the
search for mineralization. By contrast, many of the elements of a mineral deposit are
transporfed as components of minerals that are of a high specific gravity and can
therefore be concentrated by a simple gravity separation, usually in a gold pan. Ore
minerals that have the distressing properitcs of softness (hardness 3.5-4), cleavage, and
brittleness, such as galena, sphalerite, cerurrite, malachite, and cuprite arc also
concentrated.
The stream sediments contain at least 90 percent light minerals and panning raises
the relative amounts of heavy minerals by 10 to 1,000 times. If a 5 kg. sample is panned
to 100 gr., this is a concentration ratio of 50 to 1. If further separation processes in the
laboratory reduce this 100-g. sample to 100 mg., there is a total concentration ratio
occurs of 50,000 to 1 (that is 1 part per billion becomes 50 parts per million-if no losses
occur). The concentration processes (panning and laboratory separations) raise the
relative content of ore and ore-related
spectrographic analysis.
elements so that they can be detected by
The heavy-mineral concentrates were split into three fractions on the basis of the
magnetic susceptibility of the minerals. The logi; for this separation and for the choice
of the least magnetic of these as the highest priority for analysis follow from the logic in
choosing a heavy-mineral concentrate in the first place. Many of the ore metals will
substitute readily for iron or magnesium in common rock-forming silicate minerals.
These minerals are abundant but are, in themselves, not of economic importance as they
contribute mainly to the wbackground"metal content. Less abundant minerals in which
the economic metals are major components are the ore minerals. Though some of the
ore minerals are somewhat magnetic, the majority are not. By contrast, the majority of
the iron and magnesium silicate mincrals art magnetic when passed through an
electromagnetic separator. Thc magnetic separation, therefore, allows further reduction
of the inttrference from variations in the quantity or composition of non-orc+tlated
minerals and, hence, accentuates variation in the conttnt of ore and ore-related
elements resulting from variations in abundance of the ore minerals.
The analytical results indicate a higher contrast of element conttnt in the heavymineral
separates, as compared to the fint to mtdiurn fraction of the stream sediment.
The use of heavy-mineral concentrates fro-n stream sediments for reconnaissance
geochemical evaluation of the Petcrsburg arta, a logistically difficult and large arta, has

decided advantages over the use of the fine to medium fraction of the stream
sediments. These advantages are (1) a much lower sample density is sufficient to obtain
meaningful results; (2) the problem of hard to evaluate scattered spot anomalies is
largely eliminated; (3) optical mineralogy studies can be made to determine minerals of
possible economic interest and the presence of cconomic minerals can be used as ore
guides rather than that of metal percentages; (4) some minerals (example: cassiterite,
fluorite, and wolframitc) may be observed because they are resistant to physical and
chemical weathering and are transported primarily in stream sediment as mineral grains,
and not as ions absorbed on clays or contained in organic matter as are base metals
derived from sulfides; (5) some clement values (As, Sb, Cd, W, Sn, Mo, Bi, and Th) in the
fine to medium fraction of the stream sediments are frequently close to or below the
detection limit for spectrographic and chemical analysis. In the heavy-mineral
concentrate, these elements arc concentrated and therefore easily determined and, thus,
the contrast between mineralization and unmineralized areas is increased, and anomalies
are enhanced by removing major rock-forming minerals unrelated to mineralizing
processes and concentrating those minerals related to mineralizing process; (6)
elimination of the organic matter variable that may be present in one drainage basin and
not in the other; (7) separates arc independent of the diluting effects caused by seasonal
variations in sediment transport, and the concentration is nundiluting"the stream
sediment relative to heavy minerals, thus, the use of concentrates minimizes sampling
errors by minimizing (reducing but not eliminating) variable dilutions resulting from
hydraulic sorting during sedimentation as well as from related seasonal stream effects;
(8) the analytical composition of a concentrate may also indicate specific minerals. For
example, the barium content in a stream-sediment sample is predominantly the sum of
barium in the mineral barite plus barium substituted in feldspars, clay minerals, and
possibly other minerals, whereas the barium in a concentrate sample is essentially all in
barite.
Pebbles from streams were colltcted from the stream channel. Although altered
and mineralized pebbles were looked for, few showed visible indicarions of alteration or
mineralization. These pebbles were considered to be weathered, stream worn, and
represtnative of outcrop from the drainage basin. These pebbles provide information on
chemical signatures in rock that have not been or may have been affected by alteration
or mineralization,
Explanation for Table 1
The data listed in table 1 are a statistical summary of the analytical results for
stream sediments, nonmagnetic fraction of heavy-mineral concentrates from stream
stdimcnts, stream pebbles, and rock.
The procedures used in analyzing the various sample media and their references are
given in the text under analytical methods.
Values for Fe, M g, Ca, and Ti are reported in percent, all other eltmenrs values are
reported in parts per million.
The lower and upper limits of determination for analyses for the various methods of
analyses are given in the text under explanation for tables 3, 4, and 5.
A qualified population is one in which the tlerncnt concentrations are coded with N,
L, or G; N = not detected at limit of determination; L = detected but below limit of
determination; G = greater than upper limit of derermination; n = the corn bincd total of
N, L, G, and the number of values. Leaders (A) = no data or insufficient data.
The sample type column is coded as f~llow~:
SS -Stream sediment
C-3 -Nonmagnetic fraction of heavy-mineral concentrate from stream
sediments.
Peb -Stream-sediment pebbles
Rx -Rock.

The method of analyses column is coded as follows:
S -Semiquantitative spectrographic analysts
AA -Atomic absorption analyses
CM -Colorim ttric analyses
51 -Selective ion electrode analyses
AC -Neutron activation, delayed neutron counting, analyses
lnst -Fluoromctric analyses.
Explanation for Table 2
Table 2 gives the enrichment above rock crustal abundance (Krauskopf, 1967) for
selected percentiles of the chalcophile, siderophile, and lithophile eltmcnts in the
Petersburg study area, Alaska. Enrichment above rock crustal abundance was
determined by dividing average crustal abundance taken from Krauskopf (1967) and
dividing that into the actual concentration values computed for stlccted percentiles.
Tht element column heading is coded as follows:
S-F t -5tmiquantitative spectrographic analyses of iron
AA-Zn -Atomic absorption analyses of zinc
CM-W -Colorimetric analyses of tungsttn
A C-U -Neutron activation, delayed neutron counting, analysts of uranium
S I-F -Selccrivc ion electrode analysts of fluorine
U-lnst. -Fluorometric analysis of uranium.
The crustal abundance column heading values for Fe, hl g, Ca, and Ti are reported in
percent, all other values are in parts per million.
Tht sample-type column heading is coded as follows:
S S -Stream sediment
C -3 -Nonmagnetic fraction of heavy-mineral
sedim ents
concentrate from stream
Peb -Strean-sediment pebbles
RX -Rock.
Leaders -(-) equals no data or insufficient data.

Explanation for Tables 3 and 4
The data listed in tables 3 and 4 include analytical results of the stream-sediment
and pebble samples collected by the U.S. Geological Survey for the Pttersburg study
area, Alaska. The data are arranged according to the subquadrangles into which the
1:250,000 scale Petersburg, Sumdum, Sitka, Port Alexander, and Rradficld Canal 1
quadrangles art divided (pi. 1). Column 1 contains the sample number keyed to plate 1,
The latitude and longitude in degrees, minutes, and seconds arc shown in column 2 and
3, The remaining columns lists the elements for which data are available.
The clement column heading is coded as follows:
S-Ft% -Semiquantitative spectrographic analyses of iron in percent
1
S-MN -Semiquantitative spectrographic analyses of manganese in pprn
(parts per million).
AA-Zn -...Atomic absorption analyses of zinc in ppm (parts per million)
Cm-W -Colorimetric analyses of tungsten in ppm (parts per million)
AC-U -Neutron activation, delayed neutron counting, analyses of uranium in
pprn (parts per million).
-
51-F
U-lnst
-Specific Ion Electrode analyses of fluorine in pprn (parts per million)
-Fluorometric analyses of uranium in ppm (parts per million).
Other row codes arc:
N =not detected
- =no data available
<
>
=detected, but below lower limit of determination, or below value shown.
=greater than upper limit of determination, or greater than value shown
Because of the formating used in the computer program that produced tables 3
and 4, some of the elements listed in thtse tables (Fe, Y g, Co, Ti, Ag, and Be) carry one
or more nonsignificant zeros to the right of the significant digits. The analyst did not
determine thtse elcmtnts to the accuracy suggested by the extra zeros.

The lower and upper limits of determination for se miquantitative emission
spectrographic analyses for stream sediments, stream pebbles, and rocks arc as follows:
Lower detection Upper dejection
Element limit lim~t
Iron (Fe)
M agnesiom (M g)
Calcium (Ca)
Titanium (Ti)
M anganesc (M n)
Silver (Ag)
Arsenic (As)
Gold (Au)
Boron (0)
Barium (Ba)
Beryllium (Re)
Bismuth (Bi)
Cadmium (Cd)
Cobalt (Co)
Chromium (Cr)
Copptr (Cu)
Lanthanum (La)
M olybdenurn (Ma)
Niobium (Nb)
Nickel (Ni)
Lead (Pb)
Antimony (Sb)
Scandium (Sc)
Tin (Sn)
Strontium (Sr)
Vanadium (V)
Tungsten (W)
Yttrium (Y)
Zinc (Zn)
Zirconium (Zr)
Thorium (Th)
20 %
10
2 0
1
5,000 ppm
5,000
10,000
500
2,000
5,000
I ,oon
1,000
500
2,000
5,000
20,000
1,000
2,000
2,000
5,000
20,000
7 0,000
100
1,000
5,000
10,000
10,000
2,000
10,000
1,000
2,000
The detection limits for atomic absorption analyses are as follows:
Copper (Cu) 5 -
Lead (P b) 5 -
Zinc (Zn) 5 -
told (Au) 0.05 -
The detection limits for colorimetric analysis arc as follows:
Tungsten (W) 1 P Pn -
Thorium (Th) 1 PPm -
The dertction limits for neutron activation, delayed neutron counting are as
follows:
Uranium (U) -1 PPm -
Thorium (Th) .t pp!n -
Tht dttection limits for specific ion electrode analyses are as follows:
Fluorine (F) 100 ppm -
The limits for fluorornetric analyses are as follows:
Uranium (U) *2 PPm -

Analytical results of stream sediments begin on p. and the analytical results of
pebbles begin on p. .
Explanation for Table 5
The data listed in table 5 include analytical results of the C-3 fraction of the
heavy-mineral concentrates from stream-sediment samples collected by the U.S.
Geological Survey in the ~tttrsbur~ study area, Alaska.
The data arc arranged according to the subquadrangles into which the 1:250,000
scale Petersburg, Sumdum, Sitka, Port Alexander, and gradfield Canal quadrangles are
divided. Column 1 contains the sample number keyed to plate 1. The latitude and
longitude in degrees, minutes, and seconds are shown in column 2 and 3.
columns list the clcrntnts for which data are available.
The clement column heading is coded as follows:
The rtmaining
S-Fe% -Semiquantitative spectrographic analyses of iron in percent.
S-Mn -5trniquantitative
(parts per million)
spectrographic analyses of manganese in pprn
Other row codes are:
N =not detected
- =no data available
< =detected, but below the limit of determination, or below value shown
> =greater than upper limit of determination, or greater than value shown
Because of the formating used in thc computer program that produced table 5,
somt of the elements listed in this table (Fc, Mg, Co, Ti, Ag, and Be) carry one or more
nonsignificant zeros to the right of the significant digits. The analyst did not determine
these elcments to the accuracy suggested by the extra zeros.

The lower and upper limits of determination for semiquantitative emission
spectrographic analysts for heavy-mineral concentrates from stream sediments arc as
follows:
Lower detection Upper detection
Element limit limit
Iron (Fe)
M agnesium (M g)
Calcium (Ca)
Titanium (Ti)
Manganese (M n)
Silver (Ag)
Arsenic (As)
Gold (Au)
Boron (B)
Barium (Ba)
Beryllium (Be)
Bismuth (Bi)
Cadmium (Cd)
Cobalt (Co)
Chromium (Cr)
Copper (Cu)
Lanthanum (La)
Molybdenum (M o)
Niobium (Nb)
Nickel (Ni)
Lead (Pb)
Antimony (Sb)
Scandium (SC)
Tin (Sn)
Strontium (Sr)
Vanadium (V)
Tungsten (W)
Yttrium (Y)
Zinc (Zn)
Zirconium (Zr)
Thorium (Th)
2
10,000 ppm
10,000
20,000
1,000
5,000
10,000
2,000
2,000
1,000
5,000
10,000
50,000
2,000
5,000
5,000
10,000
50,001)
20,000
200
2,000
10,000
20,000
20,000
5,000
20,000
2,000
5,000
Analytical results of the C-3 fraction of heavy-mineral concentrates from stream
sediments begin on p. .

REFERENCES CITED
Centanni, F. A., Ross, A. M., and DcScsa, M. A., 1956, Fluorometric Determinations of
Uranium: Analytical Chemistry, v. 28, p. 7 657,
Grimes, D. J., and Marranzino, A. P., 1968, Direct-current arc and alternating-current
spark emission spectrographic field methods for the semiquantitative analysis of
geologic materials: U.S. t;tological Survey Circular 591, 6 p.
Hopkins, D. M., 1977, An improved ion-selective tltCtf0d~ method for the rapid
determination of fluorine in rocks and soils: U.S. Geological Survey journal of
Research, v. 5, no. 5, p. 589-593.
Kraushopf, K. B., 1967, Introduction to gtochtmistry: McCraw-Hill Publishing Co., New
York.
Millard, H. T., Jr., 1976, Determination of uranium and thorium in USGS standard rocks
by delayed neutron techniques: U.S. Geological Survey Professional Paper 840,
p. 67-65.
Motooka, J. M., and Grimes, O. J., 1976, Analytical precision of one-sixth order
semiquantitative spectrographic analysis: U.S. Gcological Survey Circular 738,
25 p.
Palkalnes, R., 1972, lntcrfertnce of titanium in the determination of thorium in rocks
with arscnro Ill: Ana!ytica Chirnica Acta, v. 58, p. 5.
Quinn, B. F., and Brooks, R. R., 1972, The rapid determination of tungsten in soils,
stream sediments, rocks, and vegetation: Anatytica Chimica Acta, v. 58, p. 301.
VanTrump, George, jr., and Miesch, A. T., 1977, The U.S. Geological Survey RAS+
STATPAC system for management and statistical reduction of geochemical data:
Computers and Gcosciences, v. 3, p. 475488.
Ward, F. N., Nakagawa, H. M., Harms, T. F., and VanSickle, G. H., 196Q, Atomic-
absorption methods of analysis useful in geochemical exploration: U.S. Geological
Survey Bulletin '1289, 45 p.

[See paqe 9 for caplanat ton. Tahle pages run from /I to 14 3
nata based on the
qua 1 1 fled II~IOU~ ,I t ton Data based on the unq~~alllled population Percentile dlstrlbution based on n samples anrgyz14
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Method
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analysts Element type H 1 G valuer valuer mean devfat ton mean devtatlon 25th 50th 15th 80th 9Mh 95th 97.5 9'1th
SS 0 0 0 1449 .I - 10
C- 3 0 3 0 1427 .i?5 - 10
Peb 0 2 0 440 -02 - 10
Rx 2 30 6 6951 -02 - ln
5 5 0 0 43 1406 50 - 5000
t-3 o 0 0 1430 50 - ~nnno
Peb 1 0 0 441 10 - 5000
RX 5 o 39 6931 3 - 5nnn
S 5 R 107 0 1334 10-100
C-3 7 174 t 1240 20 - 5000
Peb 6 201 0 235 I0 -150
Rx 4D? 2563 0 4005 7 - 2000
55 0 0 2 1447 50 - 5000
C- 3 6 2 97 1325 30 - ln0OO
Peb 7 3 t 431 20 - 5000
Ax IR1 59 31 669~ 20 - 5no0
5 S 199 289 0 961 I -10
C- 3 646 tl O 776 2-200
Peb 320 1 o 121 I - ln
Rx 1881 853 O 4235 I - 500
- -
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m -

Table 2.--Enrichment above rock crustal abundance for selected percentiles of the
chalcophile, siderophile, and l ithophi le elements in the Petersburg area, southeast Alaska
[See page 5 for explanation. Table pages run from 15 to /8 ]
El ement Crustal Sample Percenti 1 es
Element class abundance1 type 25th 50th 75th 80th 90th 95th 97.5 9gh
S S 0.63 0.95 1.5 1.7 2.1 2.5 2.9 3.:
Fe------ Si derophi 1 e 5.6 C- 3 -38 .71 1.1 1.2 1.4 2.1 3 4.3
Peb .48 .57 .66 .71 -91 1.1 1.4 1.8
Ex -41 .67 1.0 1.1 1.6 2 2.4 3.2
- SS .48 .78 1.2 1.4 1.8 2.2 2.6 3.3
Mg------ Li thophil e 2.3 C-3 .39 .61 .87 .96 1.7 2.2 2.7 4.5
Peb .25 .33 .46 .50 .91 1 1,13 1.6
Rx .36 .69 1.0 1.2 1.7 2.3 3.0 4.1
SS .27 -51 .95 1.09 1.5 1.9 2.2 2.8
Ca------ Li thophi 1 e 4.1 C-3 1.3 1.8 2.6 2.8 5.1 6.1 9.4 11.9
Peb .20 .32 .4 9 -54 .71 .90 1.4 2.7
Rx -20 .48 1.0 1.1 2.2 3.7 5.4 - -
e .
A+---- Chal cophi 1 e
As------ Chal cophi 1 e 1.8
ku------ Siderophi 1 e

Table 2.--Conti nued
El anent Crustal Sample
Element class abundance1 type
Percenti 1 es
25th 50th 75th 80th 90th 95th 97.5 99th
S S -- - - - - - - -- - - -- * -
Bi ------ Chal cophi 1 e -17 . C-3 -- - -- -- -- - - -- - -
Peb -- - - -- -- -- -- -- - -
R% -- -- - - *- -- - - -- - -
S S -- -- - - *- -
- -- - - - -
Cd------ Chal cophi 1 e .2 C-3 -- - - - *- -- -- 669 1011
Co------ Siderophi 1 e 25
Cr------ Li thophil e 100
CU------ Chal cophi 1 e 55
I La------ Lithophi 1 e 25
KO------ Siderophile 1.5
~b------ Lithophile 20
Ni------ Siderophi le 75
Pb------ Chal cophi 1 e 1.2.5
Sb------ Chal cophi 1 e -2
SS .68 -91 1.2 1.3 1.5 1.7 2 2.2
C- 3 -- -- -9 1 1.4 2 2.7 3.9
Peb -- -37 .56 .6 -7 1 1.4 1.9
Rx -23 -63 1.1 1.2 1.6 2.0 2.2 3.0
S S
C-3
Peb
Rx
ss
C-3
Peb
Rx
$5
C-3
Peb
Rx
SS
C-3
Peb
Rx
SS
C- 3
Peb
Rx
SS
C- 3
Peb
Rx
SS
C- 3
Peb
Rx
S S
C-3
Peb
Rx

Tab1 e 2.--Conti nued
El ement Crus' tal Sampl e
abund ancel type
Percenti 1 es
25th 50th 75th 80th 90th 95th 97.5 99th
Sc------
Sn------
Li thophi 1 e
Si derophi 1 e
22
2
'
SS
C-3
Peb
Rx
S S
C-3
.66
--
- -
-32
*-
- -
.90
-81
--
-67
--
--
1.2
1.2
-34
1.1
* -
--
1.3
1.4
-36
1.2
- *
--
1.6
1.7
.52
1.5
- -
14.2
1.7
2.4
.71
1.9
*-
34.4
2 2.3
3.5 7.1
-91 1.5
2.2 2.5
-- - -
141.1 359.4
-
I Peb - - * - - - - - * * -- - - - -
i
S S
Sr------ Li thophi 1 e 375 C- 3
Peb
Rx
S S
I
j
V------- Li thophi 1 e 135 C-3
Peb
Rx
i
1 W------ Lithophi 1 e 1.5
s s
C-3
Peb
Rx
------ I @ .
Rx - -- - -- * * -- - 7.4
S S -65 .8d 1.2 1.3 ;. 6 2 2,: Z.2
Li thophi 1 e 33 C- 3 4.8 10.8 21.2 26.1 35.5 44.2 44.8 53.5
Peb -- - -. -60 -69 .97 1.2 1.6 - -
I RX .45 .69 1.0 1.1 1.5 1.9 2.3 3.2
SS - - -- - - -- - - - - -- 5.8
: Zn------ Chalcophile 70 C-3 - - -- - - -- 14.9 44.8 79.3 182.5
Peb - - -- - - -- - - - - 4 14.7
3 RX -- -- -* - * - - - - - 10.1
S S .51 .67 1.1 1.3 1.7 2.4 3.4 5.1
i Zr------ Lithophile 165 C- 3 11.3 -- -- - - - - - - -- - -
I Peb -30 .46 .69 .79 1.3 1.7 3.2 4.3
Rx .33 .55 .87 1.0 1.3 1.8 2.5 3.8
Au------ Siderophi l e

Tab1 e 2.--Corrti nued
Element Crustal Sarnpl
Percenti 1 es
e
Element class abundance1 type 25th 50th 75th 80th 90th 95th 97.5 99th
S S .66 1.1 1.6 1-7 2 2.9 4 6.2
Pb------ Chal cophil e 12.5 C-3 -- -- ..- ..- - - -- -- - -
Peb -- .67 1.1 1.3 1.7 2 3.1 5.3
Rx .36 -84 1.2 1.4 1.8 2.1 3.2 15.5
Zn------ Chal cophll e 70
S 5 .71 1 1.4 1.5 1.7 2.3 3.2 5.6
C-3 -- - * - - -- -- -- - - - 1
Peb
Rx
S S
C- 3
Peb
Rx
.44
.48
- .
- -
- -
--
.73
.81
*
-- -
--
- -
1.2
1.1
--
- -
--
--
1.3
1.3
--
-*
--
1.8
1.6
--
--
- -
--
3
2.0
1.3
- -
- -
.93
5.9
3.0
2.1
- -
1.5
1.6
14.8
10.1
3.7
- -
2.7
2.4.
~h------ Li thophi 1 e 9.6
S S
C-3
Peb
"24
- -
- -
.32
- .
- -
.51
- -
--
.60 - -
--
1.2
--
- -
1.9
--
--
2.5
- -
--
3.3
- ..,
-*
F - - - - - - - LS thophile 625
SS
C- 3
Peb
.40
..-
- -
.51 - -
--
--
- -
--
--
--
--
- -
- -
--
- -
--
--
--
*-
--
--
- -
n------ Lithophile 9.6 C- 3 - . - - - - -- - - - - . - --
Peb - - - - - - - - - * - -- --
S S .78 1 1.4 1.6 2.1 2.8 3.8 5.7
A:-U---- Li thophile 2.7 C- 3 - . - - - - -- - - - - -- - -
Peb - - - - - - -- - - - - - - *-

Table 3.--Analytical results for 1,449 stream-sediment samples, Petersburg
study area, southeast Alaska.
[See page 6 for explanation. Table pages run from 20 to 1301

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Tab1 e 4.--Analytical results for 442 stream-sediment pebble sampl es,
Petersburg study area, southeast Alaska.
[See page 6 for explanation. Table pages run from 132 to 1701 C

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Tab1 e 5 .--Analytical results for 1,430 nonmagnetic fraction (C-3) of heavy-
mi neral concentrates from stream sediments, Peters burg study
area, southeast Alaska.
[See page 8 for exp7anation. Table pages run from 172 to 2811

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F~ m--.-w ~ F - * : N -- - rrvlwr r.n W 5 - h - F C Q C W W hmVC- -hhCV!
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L? ----- -,--PC- C C C G ~ cvvnn rr t C S C t CZC-u udu-7~ r-hhhk
CCCCC COOOC fr-7- 7--7- -r COCCC OCCCC CCCOC CCCCC
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o~aoo 00a00 cccco COOOD QO
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WrCINNN P J - N N W Nh' -NNNh. --.
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COO-o ooccc G ~ C O C DCCOC
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E oooco O ~ C O O COOGO on00 . oooco OCCoa oocuc uzouo
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~ A P u b h b hmm-b Oaht-0 L h m h NhWshh NP-hbN hOh-Ul hWbWfU
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mmmmrr. mmvr~rn .........
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a OY,CCO OComO ooaoo CCtO ~ O ~ OCCOC* C coooo CGPCO
a *.-OOE horn m ov,m"-s- 'Okmu3 -0mmrn -c*"-s- OCON.0 .n*OOC .
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occoo ooerc cncoo oocc CCCOC cccco cooco cccoo
E OOOCQ 050CO OOCOC OCCO G000C Dt3CC CGSCC C2CCC
a o*ooo acomc ooooa moot COOOC OCCCG 000C4 DODOC
a
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OCOOC Or300C OCOOC -wC=OO 0COC)O 0000C OOCOO C
E OOQOW 0tm00 00003 0 0 0 3 m O ~ C O C ommum COGOO o
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E O N ~ N N Nmlvmh iLNWrUh NhmNN 0hbW.O mONhV? rnN-NO N
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