chromatographic determination of glycoalkaloids in eggplant

More documents

Recommendations

Info

We approve the thesis of Neslihan TEK Date of Signature ........................................ 12 October 2006 Asst. Prof. Dr. Ritchie C. EANES Supervisor Department of Chemistry zmir Institute of Technology ........................................ 12 October 2006 Assoc. Prof. Dr. Durmu ÖZDEM R Department of Chemistry zmir Institute of Technology ........................................ 12 October 2006 Assoc. Prof. Dr. Sami DO ANLAR Department of Biology zmir Institute of Technology ........................................ 12 October 2006 Assoc. Prof. Dr. Ahmet E. ERO LU Head of Department zmir Institute of Technology ......................................................... Assoc. Prof. Dr. Semahat ÖZDEM R Head of the Graduate School
ACKNOWLEDGEMENT I would like to express my sincerest gratitude to my supervisor, Assist. Prof. Ritchie Eanes for his support, advise and patience during my thesis. Without his generous donation of his time and encouragement this thesis would not have been completed. I would also like to thank Assoc. Prof. Durmu Özdemir and Assoc. Prof. Sami Do anlar for serving as my research committee members. Also, special thanks to Gülay Haznedar and Murat Erdo an for their time and expertise to help during HPLC and GC- MS analysis. 103T139). I am pleased to acknowledge TUBITAK for its financial support (Project No. Thanks to my friends in IYTE, principally to Esra Altay and Demet Erdo an for their company and for sharing hard and happy moments. Most importantly, I would like to thank my familiy for their support, understanding and love all these years.
Page 1: CHROMATOGRAPHIC DETERMINATION OF GL
Page 5 and 6: ÖZET PATLICANDA GL KOALKALO DLER N
Page 7 and 8: 3.1.2. Derivatization and SPME ....
Page 9 and 10: Figure 2.21. Calibration plot for s
Page 11 and 12: 1.1. Eggplant CHAPTER 1 INTRODUCTIO
Page 13 and 14: 1.2. Plant Secondary Metabolites Pl
Page 15 and 16: Phenolic compounds (Group 2) are a
Page 17 and 18: Table 1.4. (cont.) SGA a Sugar Moie
Page 19 and 20: Solasonine and solamargine are the
Page 21 and 22: The toxicity of several GAs was tes
Page 23 and 24: Furthermore, solasodine present in
Page 25 and 26: Pest-related stress following folia
Page 27 and 28: in potato materials. Even though GC
Page 29 and 30: hydrophobicity. Hydrophilic compoun
Page 31 and 32: (TEAP)) for the determination of gl
Page 33 and 34: est mobile phase system, eluting re
Page 35 and 36: Mobile phase: B=ACN A=TEAP (25 mM)
Page 37 and 38: separation of SGAs was observed wit
Page 39 and 40: Mobile phase: B=ACN A=TEAP (25 mM)
Page 41 and 42: Mobile phase: B= ACN A= AH 2P (100
Page 43 and 44: Mobile phase: A= AH 2P (100 mM) Fig
Page 45 and 46: separated under all conditions disc
Page 47 and 48: Peak Area Solanidine 3 2,5 2 1,5 1
Page 49 and 50: Peak Area Solanidine 2500000 200000
Page 51 and 52: CHAPTER 3 GAS CHROMATOGRAPHY MASS S
Page 53 and 54:
SPME is not an exhaustive extractio
Page 55 and 56:
Fiber coating Film thickness (µm)
Page 57 and 58:
aglycones with a tomatidine type st
Page 59 and 60:
(a) (b) (c) Figure 3.2. Schematic o
Page 61 and 62:
Figure 3.3. Total ion GC-MS chromat
Page 63 and 64:
added extraction step for 30 min. I
Page 65 and 66:
Figure 3.9 Mass spectrum of e in fi
Page 67 and 68:
Figure 3.12. Mass spectrum of solan
Page 69 and 70:
the range of 4-230 mg/L for solanid
Page 71 and 72:
Cheng, L., Tsai, T., Wang, J., Lin,
Page 73 and 74:
Kodamatani, H., Saito, K., Niina, N
Page 75 and 76:
Sinden, S., Sanford, L. and Deahl,
Page 77 and 78:
Taiz, L. and Zeiger E. 2002. Plant
Page 79 and 80:
Mobile phase: B=ACN A=TEAP Figure A
Page 81 and 82:
Mobile phase: B=ACN A= AH 2P (100 m
Page 83 and 84:
Mobile phase: B=ACN A=TEAP (25 mM)
Page 85 and 86:
Mobile phase: A=TEAP (25mM) Figure
show all

chromatographic determination of glycoalkaloids in eggplant

You also want an ePaper? Increase the reach of your titles

Delete template?

Save as template?