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TECHNICAL FLAGS FOR MANUAL INTEGRATION Manual quan modifications or integrations are performed routinely to improve the data quality for a variety of technical reasons. Documentation of these modifications should be clear and concise. The following "flags" are used to indicate the technical reasons for quan modifications: RFW 21-21-035/Aa/93 YLI^ MP - Missed Peak: manually added peak not found by automatic quan program. PA - Peak Assignment: quan report was changed to re flect correct peak assignment. RI Routine Integration: routine integrations are performed for some analytes that are consistently integrated improperly by the automatic integration programs. Examples are the dichlorobenzene isomers on the VOA packed column and benzo(b)fluoranthene/benzo(k) flu oranthene which are poorly resolved on the BNA column. SP - Split Peak: the automatic integration improperly split the peak; a manual integration was performed to get the correct area. CB - Coelution/Background: peak was manually integrated to eliminate contribution from coeluting compounds, background signal, or other interference. PI - Proper Integration: a peak with poor or inconsistent integration (e.g., excessive tail) was properly integrated manually.
Lionville Laboratory, Inc. Semivolatiles by GC/MS, Special List Report Date: 06/12/03 11:133 RFW Batch Number 030SL329 Client: TNUBANFORD F03-006 82194 Work Order: 11343606001 Page: la Q. Cust ID: B16W79 B16W80 B16W80 B16W80 B16W81 B16W82 Sample RFW#: 001 002 002 MS 002 MSD 003 004 Information Matrix: SOIL SOIL SOIL SOIL SOIL SOIL D.F.: 1.00 1.00 1.00 1.00 1.00 1.00 Units: UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG Nitrobenzene-d5 67 t 75 % 73 w 73 k 78 71 g Surrogate 2-Fluorobiphenyl 64 & 72 & 70 %, 71 t 72 t 71 Recovery Terphenyl-d14 82 k 94 t 87 P6 88 w 98 !k 93 %; Phenol-d5 68 k 76 %; 73 t 74 g 78 t 74 %; 2-Fluorophenol 59 t 67 % 66 k 67 67 t 63 !k 2,4,6-Tribromophenol 63 W 69 t 72 %; 70 %r 60 k 67 %; Phenol 360 U 350 U 67 71 350 U 350 U bis(2-Chloroethyl)ether 360 U 350 U 350 U 350 U 350 U 350 U 2-Chlorophenol 360 U 350 U 63 k 65 w 350 U 350 U 1,3-Dichlorobenzene 360 U 350 U 350 U 350 U 350 U 350 U 1,4-Dichlorobenzene 360 U 350 U 66 t 66 %, 350 U 350 U 1,2-Dichlorobenzene 360 U 350 U 350 U 350 U 350 U 350 U 2-Methylphenol 360 U 350 U 350 U 350 U 350 U 350 U 2,2 1 -oxybis(1-Chloropropa ne) 360 U 350 U 350 U 350 U 350 U 350 U 3- and/or 4-Methylphenol 360 U 350 U 350 U 350 U 350 U 350 U N-Nitroso-di-n-propylamine 360 U 350 U 67 %, 67 t 350 U 350 U Hexachloroethane 360 U 350 U 350 U 350 U 350 U 350 U Nitrobenzene 360 U 350 U 350 U 350 U 350 U 350 U Isophorone 360 U 350 U 350 U 350 U 350 U 350 U 2-Nitrophenol 360 U 350 U 350 U 350 U 350 U 350 U 2,4-Dimethylphenol 360 U 350 U 350 U 350 U 350 U 350 U bis(2-Chloroethoxy)methane 360 U 350 U 350 U 350 U 350 U 350 U 2,4-Dichlorophenol 360 U 350 U 350 U 350 U 350 U 350 U 1,2,4-Trichlorobenzene 360 U 350 U 67 1; 66 %; 350 U 350 U Naphthalene 360 U 350 U 350 U 350 U 350 U 350 U 4-Chloroaniline 360 U 350 U 350 U 350 U 350 U 350 U Hexachlorobutadiene 360 U 350 U 350 U 350 U 350 U 350 U 4-Chloro-3-methylphenol 360 U 350 U 67 k 67 t 350 U 350 U 2-Methylnaphthalene 360 U 350 U 350 U 350 U 350 U 350 U Hexachlorocyclopentadiene 360 U 350 U 350 U 350 U 350 U 350 U 2,4,6-Trichlorophenol 360 U 350 U 350 U 350 U 350 U 350 U 2,4,5-Trichlorophenol 890 U 870 U 870 U 870 U 870 U 880 U *= outside of EPA CLP QC limits.
Page 1 and 2: 24 June 2003 Mr. Steve Trent Fluor
Page 3 and 4: Client: TNU-HANFORD B03-006 W.O.#:
Page 5 and 6: ABBREVIATIONS BS = BSD = MS = MSD =
Page 7 and 8: RFW Batch Number: 0305L329 Lionvill
Page 9 and 10: Lionville Laboratory, Inc. Volatile
Page 11 and 12: Lionville Laborato ry Use Only Cust
Page 13 and 14: FR-Central Plateau 00-PW-2/200-PW-4
Page 15 and 16: FH-Central Plateau Project CHAIN OF
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Page 19 and 20: I LIONTVILLE LABORATORY INCORPORATE
Page 21 and 22: Client: TNU-HANFORD F03-006 W.O.#:
Page 23: ABBREVIATIONS BS = nl 1 MS = MSD =
Page 27 and 28: RFW Batch Number: 030SL329 Client:
Page 29 and 30: RFW Batch Number • 0305L329 Clien
Page 31 and 32: 1F SEMIVOLATILE ORGANICS ANALYSIS D
Page 33 and 34: IF CLIENT SAMPLE NO SEMIVOLATILE OR
Page 35 and 36: 1F SEMIVOLATILE ORGANICS ANALYSIS D
Page 37 and 38: 1F CLIENT SAMPLE NO. SEMIVOLATILE O
Page 45 and 46: l M-Central Plateau P roject CHAIN
Page 47 and 48: Lionville Laboratory, Inc. HBGX ANA
Page 49 and 50: Lionville Laborato ry Sample Discre
Page 51 and 52: ^3 vLl GLOSSARY OF HERBICIDE DATA P
Page 53 and 54: Lionville Laborato ry Use Only Cust
Page 55 and 56: F11-Central Plateau Project CHAIN O
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Page 63 and 64: Client: TNU-HANFORD F03-006 LVL #:
Page 65 and 66: (1(,yIVIMLpyy(„Q,MI- DATA QUA EMM
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M-Central Plateau Project CHAIN OF
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DATE RECEIVED: 05/02/03 Lionville L
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Lionville Laborato ry Sample Discre
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P D ^CIHHUICtSIdIMN^- GLOSSARY OFPE
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Lionville Laborato ry Use Only X51-
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C FR-Central Plateau Project CHAIN
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FR-Central Plateau Project CHAIN OF
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FI3-Central Plateau Project CHAIN O
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LIONVILLE LABORATORY INCORPORATED S
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Analytical Repo rt Client: TNiJ-HAN
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QLVMU1 GLOSSARY OF GASOLINE RANGE O
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Lionville Laboratory, Inc. GAS RANG
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FH-Central Plateau Project CHAIN OF
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Lionville Laboratory, Inc. DRO ANAL
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Laboratory Sample Discrepancy Repor
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,DvI GLOSSARY OF DIESEL RANGE ORGAN
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Lionville Laborato ry Use Only i51-
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F11-Central Plateau Project CHAIN O
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Client: TNU-HANFORD F03-006 LVL #:
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OLVMLIM DATA QUALIFIERS GLOSSARY OF
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Lionville Laboratory, Inc. GC SCAN
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FE-Central Plateau Project CHAIN OF
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FU-Central Plateau Project CHAIN OF
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Lionville Laboratory, Inc. 8015 ANA
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Lionville Laborato ry Sample Discre
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0LVI M, GLOSSARY OF GC SCAN DATA P
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Lionville Laborato ry Use Only •5
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C F11-Central Plateau Project CHAIN
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Lionville Laboratory, Inc. INORGANI
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Client: TNU-HANFORD F03-006 W.O.#:
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METALS METHOD GLOSSARY The followin
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CLIENT: TNUHANPORD FO3-006 H2194 WO
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CLIENT: TNUHANPORD F03-006 H2194 WO
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CLIENT: TNUHANPORD P03-006 H2194 WO
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Lionville Laborato ry Use Only Cust
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FE-Central Plateau Project CHAIN OF
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IENT: I chase Order/Project: A LION
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Client: TNU-HANFORD F03-006 H2194 L
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Lionville Laborato ry Incorporated
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CLIENT: TNUNANPORD P03-006 H2194 WO
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CLIENT: TNVHANPORD P03-006 H3194 WO
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I^ESERLINE SRVICS E E June 17. 2003
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Eberline Services W.O. No. R3-06-01
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EBERLINE SERVICES/RICHMOND SAMPLE D
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SDG 7507 Contact Melissa C. Ma..i:
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SDG 7507 Contact Melissa C. Mannton
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=SDG7507 EBERLINE SERVICES/RICHMOND
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7507-008 SDG 7507 Contact Melissa C
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SDG 7507 Contact Melissa C. Manion
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7507-001 EBERLINE SERVICES/RICHMOND
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EBE RLIN E SE RVIC ES /RICHMOND SAM
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Test TH Matrix SOLID SDG 7507 Conta
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Test 1 Matrix SOLID SDG 7507 Contac
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Test NI L Matrix SOLID SDG 7507 Con
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SDG 7507 EBERLINE SERVICES/RICHMOND
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EBERLINE SERVI CES /RI CHMOND SAMPL
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EBE RLIK E SE RVI CES / RI C HM O N
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