Crystal Engineering on Organic Pigments

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Pigment Yellow 14: Synchrotr<strong>on</strong> data and Rietveld refinement Intensität (Counts) Diff. experimental calculated NSLS Brookhaven�� = 1.149 Å Refinement of individual x, y, z, and B iso for all atoms (except H) was possible R p = 8.53 %, R wp = 12.87 %, R F 2 =17.60%, � 2 = 3.3
Pigment Yellow 13 and 14 Planar molecules Layer packings [M.U. Schmidt, R.E. Dinnebier, H. Kalkhof, J. Phys. Chem. B 111 (2007), 9722-9732] P.Y.13: P1, Z = 2 a = 8.3691(1) Å b = 8.7650(2) Å c = 12.8167(3) Å � = 112.054(1)º � = 92.920(2)º � = 105.691(1)ºP P.Y.14: P1, Z = 2 a = 8.21420(6) Å b = 9.33011(5) Å c = 11.78471(8) Å � = 112.6805(3)º � = 98.1609(4)º � = 105.4338(4)º
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Crystal En
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Applications: - Laquers & paints -
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Example 1: Colours of quinacridones
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H N O H N O Isolated molecule Weak
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Polymorphs of quinacridone: A real
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Described polymorphs � Polymorphs
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Described polymorphs � � B I Po
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Described polymorphs � � B I
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Polymorphs of quinacridones � I
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� phase Quinacridone: Synthesis N
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Crystal En
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Crystal En
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Polymorph screening without knowled
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Polymorphism of Pigment Red 53:2 Na
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Page 71 and 72: � Polymorphism of Pigment Red 53:
Page 73 and 74: Example 2: Weather fastness of Pigm
Page 75 and 76: N H 2 N N Pigment Red 170 O H O O H
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Page 80 and 81: Extraction of reliable reflection i
Page 82 and 83: Determination of crystal structures
Page 84 and 85: Lattice energy minimizations (CRYSC
Page 86 and 87: Pigment Red 170 P2 1 /n, Z = 4, a =
Page 88 and 89: Pigment Red 170: New derivatives an
Page 90 and 91: O Violet pigment Example 3: Methyl-
Page 92 and 93: Methyl-dioxazine: Structure solutio
Page 98 and 99: Crystal structure
Page 104 and 105: Methyl - ethyl compound O C H 3 H N
Page 106 and 107: H N O N H3C N O O C H 3 Cl Cl Methy
Page 108 and 109: Solid solution Solid solution (�
Page 112 and 113: Example 4: Diaryl Pigments CH 3 O C
Page 114 and 115: Example 4: Diaryl Pigments CH 3 O C
Page 118 and 119: Pigment Yellow 14: Structure soluti
Page 120 and 121: Pigment Yellow 14: Structure soluti
Page 126 and 127: Diaryl pigments: Understanding the
Page 128 and 129: Diaryl pigments: Understanding the
Page 130 and 131: Diaryl pigments: Crystal</s
Page 142: Diaryl pigments: Crystal</s
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Crystal Engineering on Organic Pigments

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