Organic micropollutants in Rhine and Meuse a - Riwa

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APPENDIX 9 LCIMS mass spectra of diethylphthalate and dibutylphthalate RIIIIVA 47
SPEC: Samp: Conun: Mode: Oper: Base: Norm: Peak: Data: 10bith 23-SEP-97 DERIVED SPECTRUM Rijn Lobith 10-9-97, 9 rn1 autosarnpler Start 13:26:01 Univ.150x3.0nun, 0.4 ml/rnin, H20+NH4dAc/ACN 95->10 ESI +DAU 147.0 @ -30eV LMR GAS Piet Sp Client: grad. 3 rnetrnieren 148.9 Inten: 790986 148.9 RIC 1578059 1000.00 mrnu +/2112>2142 - /2030>2064,2228>2262 PROG RF UP LR Inlet Masses #peaks 10 > 600 483 #9 2315 100 149 30eV E+ 05 7.91 80 60 40 20 57 I 267 I 93 i 121 1 511 483 I : l 5do Diethylphtalate SPEC: Samp: Conun: Mode: Oper: Base: Norm: Peak: Data: lobith 23-SEP-97 DERIVED SPECTRUM Rijn Lobith 10-9-97, 9 ml autosarnpler Start 13:26:01 Univ.150x3.0rnm, 0.4 rnl/rnin, H20+NH40Ac/ACN 95->10 ESI +DAU 145.0 @ -6eV LMR GAS PROG RF UP LR piet Sp Client: grad. 3 metrnieren 223.0 Inten: 1509074 223.0 RIC 2213599 1000.00 mrnu +/2115>2138 - /2049>2086,2229>2259 Inlet Masses: #peaks: 10 > 600 313 #9 2289 100 223 6eV E+ 06 1. 51 80 60 40 20 149 489 I 500 600 100 200 300 400 48 RIMI'A
Page 1 and 2: VERENIGING V A N RIVIERWATERBEDRIJV
Page 3 and 4: November 1999 Organic micropollutan
Page 5 and 6: APPENDIX? APPENDIX 8 APPENDIX 9 Ove
Page 7 and 8: 1 INTRODUCTION In the framework of
Page 9 and 10: 2 MEANING AND INTERPRETATION OF THE
Page 11 and 12: 1997). Not only can the peak patter
Page 13 and 14: 3.3 Processing of the data Peaks fr
Page 15 and 16: ------------------------ What is no
Page 17 and 18: 4.2 Individual compounds As stated
Page 19 and 20: In this study, a metabolite of diur
Page 21 and 22: Overlay at 215 nm 0,04 Meuse Octobe
Page 23 and 24: Table 3 Frequency ofoccurrence and
Page 25 and 26: 4.7.4 Notable monthly samples with
Page 27 and 28: Selection of unidentified substance
Page 29 and 30: metabolites) in the Rhine and the M
Page 31 and 32: APPENDIXl Sampling data Rhine (Lobi
Page 33 and 34: V-.l SanpleName: Rijn mrt' 97 S3IlI
Page 35 and 36: UJ ~ I SanpleNaIlIl: Haas maart' 97
Page 37 and 38: APPENDIX 5 Summed peak surface area
Page 39 and 40: 38 RllIN'A
Page 41 and 42: +:- Corrected IRhine 0 retention ti
Page 43 and 44: 42 RIMfA
Page 45 and 46: ..j::.. ..j::.. Corrected retention
Page 47: 46 RIMfA
Page 51: Colophon Publisher Cover and printi

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