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FREEZE DRYER(LYOPHILIZER) - Daintree Scientific

FREEZE DRYER(LYOPHILIZER) - Daintree Scientific

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<strong>FREEZE</strong> <strong>DRYER</strong>(<strong>LYOPHILIZER</strong>)<br />

Bulk Tray type<br />

Compact construction squared tray chamber<br />

reduce about 30% of space for installation than the<br />

circular type of chamber<br />

● Squard tray chamber<br />

● Powerful cold trap<br />

● Programmable controller<br />

Fast cooling & defrosting<br />

systems applied. International<br />

Patented the Cryogenic technology<br />

Squared tray chamber<br />

Construction<br />

Programmable Microprocessor<br />

Control<br />

Optional Vacuum<br />

system & others<br />

● International Patents Registered Operon's<br />

the cryogenic auto cascade system.<br />

● Fast cooling & defrosting systems applied<br />

the Cryogenic Technology.<br />

● Lowest temperature -120℃ of Cold trap<br />

Collect for almost kinds of vapors even<br />

ethanol and protect vacuum pump.<br />

● Automatic/Manual or 8mode<br />

programmable shelf temperature range<br />

between -40 ~ +70℃.<br />

● Ice holding capacity from 111L ~ 6L<br />

● Automatic defrosting system by hot gas<br />

bypass.<br />

● Mixed CFC-free Refrigerants.<br />

● Exclusive LBP Hermetic Compressor<br />

● Lifeguard Compressor Thermal protector,<br />

extending LBP Compressor<br />

Freeze Dryer Bulk tray type<br />

● Compact construction with square type of<br />

drying chamber available to reduce about<br />

30% of the space for installation than<br />

circular type of chamber.<br />

● Squared type of drying chamber allows<br />

easy cleaning and maximum shelf area<br />

without space loss.<br />

● Anti corrosion stainless steel for inner<br />

chamber,Cold trap condenser, Shelves,<br />

and tray.<br />

● 40mm of Clear acrylic door for chamber<br />

and trap enables monitoring throughout<br />

freeze drying process.<br />

● N2 back-filling systems(N2-port)<br />

● Optional 6port of manifold allows freeze<br />

drying process simultaneously without<br />

disturbing the drying chamber.<br />

● Automatic / Manual and Programmable<br />

microprocessor controller(8mode / 9step<br />

/ 999cycle)<br />

● One-touch automatic operation key for<br />

cooling, vacuum and drying process.<br />

● Function selection for the Automatic/<br />

Manual drying process.<br />

● Digital temperature(Cold trap & 3<br />

samples) and vacuum(2000 ~ 0 mtorr)<br />

display.<br />

● Temperature limitation setting function for<br />

automatic start up and stop to protect<br />

the vacuum pump.<br />

● Printer set (Temperature/Vacuum/time/<br />

Archieved or real time printing)<br />

● Vacuum control set<br />

● Selectable the double stage oil rotary<br />

vane Vacuum pumps(600LPM ~<br />

200LPM)<br />

● Ultimate vacuum pressure 5 x 10<br />

-4<br />

torr<br />

● Digital vacuum gauge measurable from<br />

atm. to 1 x 10 -3 torr.<br />

● Automatic gas ballasting function allows<br />

circulating fresh air , automatically.<br />

● Vacuum control valve allows maintaining<br />

the set-point vacuum level between<br />

1950 ~ 0 mtorr.<br />

● Vacuum break valve that bleeds air into<br />

the system when power to the<br />

main body or vacuum pump is shot off.<br />

● Printing system available output data for<br />

temperature, Vacuum pressure(2000 ~<br />

0mtorr), time in real time or archieved<br />

data.<br />

● Rear-mounted RS-232 port to transmit<br />

data to a user’s Computer.<br />

Main<br />

Body<br />

Model<br />

Bulk Tray Type<br />

FDT-86111 FDT-55111 FDT-12050 FDT-8650 FDT-12032 FDT-8632 FDT-12012 FDT-8612 FDT-12006 FDT-8606<br />

Cold Trap Temp -86℃ -55℃ -120℃ -90℃ -120℃ -90℃ -120℃ -90℃ -120℃ -90℃<br />

Capacity 111L<br />

50L 32L 12L 6L<br />

Shelf Temp<br />

-20,-40,-55℃ ~ +70℃,(OPTION)<br />

Dimension (Out)(W1200×D1100×H1850)×2EA<br />

(Out)W1200×D1100×H1850 (Out)W1000×D1000×H1850<br />

Chamber Size (In)W500×D900×H1300 (In)W500×D900×H650 (In)W500×D900×H500 (In)W360×D700×H400 (In)W330×D550×H330<br />

Trap Size Ø 840×L850<br />

Ø 420×L750 Ø 350×L750 Ø 315×L450<br />

Ø 315×L300<br />

Tray<br />

16ea<br />

6ea 4ea 4ea 3ea<br />

W470×D740×H40<br />

W470×D740×H40 W470×D740×H40 W320×D450×H40 W280×D280×H40<br />

Progranmmable Controller 8mode 9step 999cycle programmable controller, Auto/Manual start-up controller, Display cold trap temp. & vacuum pressure(2000~0 mtorr), Vacuum maintenance set<br />

Sample Sensor<br />

3 port of display sensor & 1 printer sensor<br />

Pump Protection System<br />

Built-in(Automatic pump start & stop control system for vacuum pump)<br />

Defrost<br />

Auto<br />

Electric 220V/440V 3ph<br />

220V/440V 3ph 220V/440V 3ph 220V/1ph 220V/440V 3ph 220V/1ph<br />

Weight 450kg×2 430kg×2 780kg 750kg 730kg 700kg 580kg 550kg 480kg 450kg


<strong>FREEZE</strong> <strong>DRYER</strong> (<strong>LYOPHILIZER</strong>)<br />

Chemical-Free Up-Right Type<br />

Only Operon ! -120℃ of Chemical-free Freeze dryer !<br />

Why -120℃<br />

- Collectable almost kinds of Vapors and protect a Vacuum pump<br />

- Convenient(All-in-one type)- No need inconvenient double process(Concentration-Freezing by L.N2-Drying)<br />

- Rapid & Available to reach up to ultimate Vacuum pressure 5 x 10 -4 torr<br />

- Smaller Vacuum pump is required Compare to other -80℃ of freeze dryers.<br />

0<br />

Freezing Points<br />

-10<br />

-20<br />

-40<br />

-15.25℃ Trifluoroacetic Acid<br />

-17.01℃ O-Dichlorobenzene<br />

-35.66℃ Ethylene Dichloride<br />

-60<br />

-70<br />

-63.55℃ Chloroform<br />

-73.9℃ Methyl Isoamyl Ketone<br />

● Down for pre-freezing<br />

● Up for drying<br />

-80<br />

-90<br />

-95<br />

-100<br />

-110<br />

-115<br />

-120<br />

-83.97℃ Acetate<br />

-88.62℃ n-Butyl Alcohol<br />

-94.7℃ Acetone<br />

-94.99℃ Toluene<br />

-95.14℃ Dichloromethane<br />

-95.3℃ Hexane<br />

-97.68℃ Methyl Alcohol<br />

-107.39℃ Iso-Octane<br />

-108℃ Isobutyl Alcohol<br />

-114.1℃ Ethyl Alcohol<br />

-117.4℃ Ethyl Ether<br />

International Patented the<br />

Cryogenic Cooling System<br />

Up-right Construction<br />

One-touch operation<br />

Microprocessor Control<br />

Optional Vacuum<br />

system & others<br />

● Lowest temperature -120 ℃ of Cold trap<br />

Collect for almost kinds of vapors,<br />

organic solvent and protect vacuum<br />

pump<br />

● Operon’s innovative chemical-free freeze<br />

dryer for Organic solvent enables 99%<br />

collection of methanol and ethanol by<br />

utilizing a poweful -120 ℃ of Cold trap.<br />

● Excellent Anti corrosion Teflon coated<br />

stainless steel for trap chamber, Cold<br />

trap condenser and cold rolled steel with<br />

powder coated outer frame.<br />

● Only Operon offers Chemical-free freeze<br />

dryer (12L)model available with -120 ℃<br />

of pre-freezing coil attachment(Ø315 x<br />

L380mm/30L Volume).<br />

● Optional drying chamber & D-type manifold<br />

or T-type manifold available drying,<br />

simultaneously.<br />

● One-touch automatic operation key for<br />

cooling, vacuum and drying process.<br />

● Digital temperature and vacuum(2000 ~<br />

0 mtorr) display<br />

● Temperature limitation setting function for<br />

automatic start up and stop to protect the<br />

vacuum pump.<br />

● Printer set (Temperature/Vacuum/time/<br />

Archieved or real time printing)<br />

● Vacuum control set<br />

● Selectable the double stage oil rotary<br />

vane Vacuum pumps(600LPM ~<br />

100LPM)<br />

● Ultimate vacuum pressure 5 x 10<br />

-4<br />

torr<br />

● Digital vacuum gauge measurable from<br />

atm to 1 x 10 -3 torr.<br />

● Automatic gas ballasting function allows<br />

circulating fresh air , automatically.<br />

● Vacuum control valve allows maintaining<br />

the set-point vacuum level between<br />

1950 ~ 0 mtorr.<br />

● Vacuum break valve that bleeds air into<br />

the system when power to the main<br />

body or vacuum pump is shot off.<br />

● Printing system available output data for<br />

temperature, Vacuum pressure(2000 ~<br />

0mtorr), time in real time or archieved<br />

data.<br />

● Rear-mounted RS-232 port to transmit<br />

data to a user’s Computer.<br />

Freeze Dryer-Chemical-Free Model<br />

Main<br />

Body<br />

MODEL<br />

Chemical Free<br />

FDCF-12012 FDCF-12006 FDCF-12003<br />

Cold Trap Temp -120℃ -120℃ -120℃<br />

Capacity 12L 6L<br />

3L<br />

Dimension<br />

(Out)W850×D800×H950<br />

Trap Size Ø 345×L380<br />

Ø 315×L300 Ø 315×L180<br />

Ccontroller<br />

Auto/Manual start-up controller, Display cold trap, Temperature & vacuum pressure, printer set, Vacuum maintenance set<br />

Pump Protecteion System<br />

(Automatic vacuum pump start & Stop controller system)<br />

Defrost<br />

Auto<br />

Electric<br />

220V/1Ph<br />

Weight<br />

210kg 190kg 180kg


Up-right type & Bench top type<br />

Various types , Capacities and Combinations of<br />

Operon’s Freeze dryer !!<br />

-90℃ ~ -55℃ / 24L ~ 3L Capacity<br />

Cooling Systems<br />

Up-right & Bench top<br />

Construction<br />

One-touch operation<br />

Microprocessor Control<br />

Optional Vacuum<br />

system & others<br />

● Lowest temperature -90 ℃ of Cold trap<br />

Collect for almost kinds of humidiity &<br />

vapor effectively and protects vacuum<br />

pump.<br />

● Ice holding capacity from 24L ~ 3L<br />

● Average evacuation time of 16 ~<br />

30minutes to reach acceptable vacuum<br />

level.<br />

● Automatic defrosting system by hot gas<br />

bypass(24L/12L).<br />

● Mixed CFC-free Refrigerants.<br />

● Specially designed large capacity air-cold<br />

condenser and aero-dynamic fan.<br />

● Exclusive LBP Hermetic Compressor<br />

● Lifeguard Compressor Thermal protector,<br />

extending LBP Compressor.<br />

● Anti corrosion stainless steel for trap<br />

chamber , Cold trap condenser and high<br />

impact coating finished outer frame.<br />

● Operon’s freeze dryer (12L)model<br />

available sample pre-freezing with -90/-<br />

70 ℃ of pre-freezing coil attachment(Ø315<br />

x L380mm/30L Volume).<br />

● Selective installation of manifold type or<br />

drying chamber type.<br />

● 40mm of clear acrylic lid.<br />

● Heavy duty swivel casters.<br />

● Washable filter.<br />

● One-touch automatic operation key for<br />

cooling, vacuum and drying process.<br />

● Digital temperature and vacuum(2000 ~<br />

0mtorr) display .<br />

● Temperature limitation setting function for<br />

automatic start up and stop to protect the<br />

vacuum pump.<br />

● Printer set (Temperature/Vacuum/time/<br />

Archieved or real time printing)<br />

● Vacuum control set<br />

● Selectable the double stage oil rotary vane<br />

Vacuum pumps(600LPM ~ 100LPM)<br />

● Ultimate vacuum pressure 5 x 10<br />

-4<br />

torr<br />

● Digital vacuum gauge measurable from<br />

atm. to 1 x 10 -3 torr.<br />

● Automatic gas ballasting function allows<br />

circulating fresh air , automatically.<br />

● Vacuum control valve allows maintaining<br />

the set-point vacuum level between 1950<br />

~ 0 mtorr.<br />

● Vacuum break valve that bleeds air into<br />

the system when power to the main body<br />

or vacuum pump is shot off.<br />

● Printing system available output data for<br />

temperature, Vacuum pressure(2000 ~<br />

0mtorr), time in real time or archieved<br />

data.<br />

● Rear-mounted RS-232 port to transmit<br />

data to a user’s Computer.<br />

Freeze Dryer-up-Right & Bench Top Model<br />

Main<br />

Body<br />

Model<br />

UP-Right Type<br />

Bench Top<br />

FDU-8624 FDU-7024 FDU-8612 FDU-8612/7012 FDU-7012 FDU-8606 FDU-8606/7006 FDU-7006 FDU-8603 FDU-7003 FDB-5503<br />

Cold Trap Temp -90℃ -70℃ -90℃ -70℃ -90℃ -70℃ -90℃ -70℃ -55℃<br />

Capacity<br />

24L<br />

12L<br />

6L<br />

3L<br />

3L<br />

Dimension<br />

(OUT)W850×D800×H950<br />

(OUT)W500×D650×H950<br />

(OUT)W480×D580×H480<br />

Trap Size<br />

Ø 315×L680 Ø 315×L380<br />

Ø 315×L300 Ø 315×L180 Ø 315×L180<br />

Controller<br />

Auto/Manual Start-up Controller, Display Cold Trap,Vacuum Pressure, Printer Set, Vacuum maintenance set<br />

Pump Protecteion System<br />

(Automatic Vacuum Pump Start & Stop Control System)<br />

Defrost<br />

Auto<br />

Manual<br />

Electric<br />

220V/1ph<br />

Weight<br />

180kg<br />

155kg<br />

115kg<br />

110kg<br />

50kg


<strong>FREEZE</strong> <strong>DRYER</strong> (<strong>LYOPHILIZER</strong>)<br />

With Stoppering System Up-right type & Bench top type<br />

Various types , Capacities and Combinations of<br />

the Operon Freeze dryer !!<br />

120℃ ~ -55℃ / 24L ~ 3L Capacity<br />

Compatible Stoppering System allows to seal cap of the vials<br />

under vacuum status after freeze drying.<br />

● Vials<br />

● Stoppering device + Drying chamber<br />

+ D-type manifold<br />

Main<br />

Body<br />

Stoppering Type<br />

Model FDS-12012 FDS-8612 FDS-7012 FDS-12006 FDS-8606 FDS-7006 FDS-12003 FDS-8603 FDS-7003 FDS-5503<br />

Cold trap temp.<br />

Dimension<br />

Capacity<br />

Drying chamber<br />

Trap Size<br />

Controller<br />

Stoppering System<br />

Pump Protection<br />

System<br />

Defrost<br />

Electric<br />

Weight<br />

Overall<br />

-120℃<br />

230kg<br />

W850×D800×H1410<br />

Ø 345xL380<br />

#.The lift for stoppering device is not included in the 3L, 6L Model<br />

#.The lift shown above is optional item<br />

-90℃ -70℃ -120℃ -90℃ -70℃ -120℃ -90℃ -70℃<br />

12L 6L 3L 3L<br />

Ø 315xL300<br />

Ø 300 x L330<br />

Auto/Manual start-up controller, Display cold trap temperature & vacuum pressure(2000~0mtorr)<br />

printer set, Vacuum maintenance set<br />

Clear acrylic chamber+3shelves+stoppering device<br />

(Automatic vacuum pump start & Stop control system)<br />

Auto<br />

220V/1ph , 60hz/50hz<br />

W500×D650×H1410<br />

Ø 315xL180<br />

Manual<br />

W480×D580×H880<br />

175kg 175kg 210kg 135kg 135kg 200kg 130kg 130kg 70kg<br />

-55℃


Acid freeze dryer Up-right type - Glass type<br />

Only Operon ! Acid Freeze dryer !!<br />

Safe from an Acid !!!<br />

Borosilicate Glass A3.3 and-120℃ of powerful cold trap protectable the<br />

Vacuum pump & Products from sulfuric Acid, Hydro - chloric acid, Acetetic acid<br />

International Patented the<br />

Cryogenic Cooling System<br />

Borosilicate Glass allin-one<br />

Construction<br />

● Operon’s innovative chemical-free freeze<br />

dryer for Acid enables collection of Acid<br />

by utilizing a poweful -120 ℃ of Cold<br />

trap.<br />

● Borosilicate Glass A3.3 for trap chamber<br />

& Cold trap condenser and cold rolled<br />

steel with powder coated outer frame.<br />

● Special designed drain device required<br />

● Teflon materials of a disk to divide the<br />

drying chamber & cold trap condenser.<br />

● Built-in a special designed vacuum fitting<br />

device.<br />

● Glass type cold trap<br />

● Glass type drying chamber<br />

● Teflon disc<br />

Freeze Dryer Glass Type<br />

Model FDG-120 FDG-105 FDG-90<br />

Main<br />

Body<br />

Application<br />

Dimension(mm)<br />

Materials<br />

Cold Trap Temp -120℃ -105℃ -90℃<br />

Cold Trap Capacity<br />

Controller<br />

Drying Chamber<br />

Cold Trap<br />

Overall<br />

12L<br />

Ø 300xL230<br />

Ø 300xL250<br />

W850xD800xH1410(Included drying chamber)<br />

Drying Chamber Borosilicate Glass A3.3<br />

Cold Trap Borosilicate Glass A3.3<br />

External<br />

Insulation<br />

Pump Protection System<br />

Defrost<br />

Electric<br />

Weight<br />

·Freeze drying for Sulfuric acid, Hydrochloric acid, Acetic acid, Organic lvent<br />

Cold rolled steel with powder coated<br />

High density urethane foam<br />

Auto/Manual start-up controller, Display cold trap temperature & vacuum<br />

pressure(2000~0mtorr), printer set, Vacuum maintenance set<br />

(Automatic vacuum pump start & Stop control system)<br />

Manual defrost<br />

220V, 1ph, 60hz/50hz<br />

230kg

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