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GC and GC/MS Agilent MS Certified Liners Inlet Liners - T.E.A.M.

GC and GC/MS Agilent MS Certified Liners Inlet Liners - T.E.A.M.

GC and GC/MS Agilent MS Certified Liners Inlet Liners - T.E.A.M.

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<strong>Inlet</strong> <strong>Liners</strong><br />

NEW!<br />

<strong>Agilent</strong> <strong>MS</strong> <strong>Certified</strong> <strong>Liners</strong><br />

<strong>MS</strong> certified split liner, 5188-6576<br />

<strong>Agilent</strong> <strong>MS</strong> <strong>Certified</strong> Split <strong>and</strong> Splitless <strong>Liners</strong> are manufactured <strong>and</strong> tested to our highest level<br />

of scrutiny to assure reproducibility.<br />

We have built years of experience into the <strong>MS</strong> <strong>Certified</strong> <strong>Liners</strong> to provide the quality <strong>and</strong><br />

consistency needed for critical applications, especially those using esterification agents for<br />

trace level analysis such as toxicology or drugs of abuse applications.<br />

• Geometrical dimensions <strong>and</strong> tolerances of the glass are controlled by Statistical Process<br />

Control (SPC) with 100% Go-No-Go check.<br />

• Glass wool is pre-qualified with mass spectrometry, then inserted using a unique<br />

manufacturing procedure to improve reproducibility.<br />

• Deactivated <strong>MS</strong> <strong>Certified</strong> <strong>Liners</strong> are treated with <strong>Agilent</strong>'s proven proprietary deactivation<br />

process developed to last longer than other commercially available treatment.<br />

• R<strong>and</strong>om samples of <strong>MS</strong> <strong>Certified</strong> <strong>Liners</strong> are tested using both FID <strong>and</strong> <strong>MS</strong>D analysis of<br />

challenging probes to evaluate acid/base deactivation, response linearity, peak symmetry,<br />

<strong>and</strong> bleed <strong>and</strong> background noise.<br />

• Each <strong>Agilent</strong> <strong>MS</strong> <strong>Certified</strong> Liner is traceable by the lot codes silk screened on the liner.<br />

<strong>Agilent</strong> <strong>MS</strong> <strong>Certified</strong> <strong>Liners</strong><br />

Description 1/pk 5/pk 25/pk<br />

Split <strong>Inlet</strong> <strong>Liners</strong><br />

Single taper, <strong>MS</strong> certified liner with restriction to 5188-6576<br />

hold glass wool<br />

Straight, <strong>MS</strong> certified liner with glass wool 5188-6574 5188-6569<br />

Splitless <strong>Inlet</strong> <strong>Liners</strong><br />

Single taper, <strong>MS</strong> certified liner with glass wool 5188-6568 5188-6567 5188-6566<br />

<strong>GC</strong> <strong>and</strong> <strong>GC</strong>/<strong>MS</strong><br />

For in-depth information about maintaining your <strong>GC</strong>/<strong>MS</strong>, request<br />

"Maintaining Your <strong>Agilent</strong> <strong>GC</strong> <strong>and</strong> <strong>GC</strong>/<strong>MS</strong> Systems" from your<br />

<strong>Agilent</strong> Representative (publication number 5989-7612).<br />

www.agilent.com/chem/supplies<br />

153


<strong>Inlet</strong> <strong>Liners</strong><br />

<strong>Agilent</strong> Split <strong>Liners</strong><br />

<strong>Agilent</strong> split liner<br />

<strong>Agilent</strong> Single Taper Split <strong>Liners</strong> are made to strict dimension specifications for optimal inlet<br />

performance <strong>and</strong> feature the tightest tolerances for OD, ID, taper, <strong>and</strong> glass wool placement.<br />

For ease of use <strong>and</strong> reproducibility, the liners have a positioning bead, a restriction to secure<br />

the position of the glass wool, <strong>and</strong> a feature to consistently self-position to the recommended<br />

height. The liners also feature <strong>Agilent</strong>'s proprietary deactivation.<br />

<strong>Agilent</strong> Split <strong>Liners</strong><br />

Single taper split liner<br />

Straight split liner<br />

Description 1/pk 5/pk 25/pk<br />

Single Taper Split <strong>Liners</strong><br />

Single taper, glass wool, deactivated,<br />

5183-4647 5183-4701 5183-4702<br />

low pressure drop<br />

Single taper, <strong>MS</strong> certified liner with restriction 5188-6576<br />

to hold glass wool<br />

Single taper, glass wool, deactivated 5183-4711 5183-4712 5183-4713<br />

Straight Split <strong>Liners</strong><br />

Straight, glass wool, non-deactivated 19251-60540 5183-4691 5183-4692<br />

Straight, <strong>MS</strong> certified liner with glass wool 5188-6574 5188-6569<br />

<strong>GC</strong> <strong>and</strong> <strong>GC</strong>/<strong>MS</strong><br />

Tips & Tools<br />

<strong>Agilent</strong> recommends part number 5183-4647 as the top split liner choice for:<br />

• Highest run-to-run area reproducibility<br />

• Least discrimination for wide boiling point range samples<br />

• Use with widest range of conditions <strong>and</strong> sample types<br />

• Easy self-adjusting installation<br />

154<br />

www.agilent.com/chem/supplies


<strong>Inlet</strong> <strong>Liners</strong><br />

<strong>Agilent</strong> Splitless <strong>Liners</strong><br />

<strong>Agilent</strong>'s proprietary deactivation is important for splitless liners because of the longer<br />

sample/liner contact time in splitless mode.<br />

<strong>Agilent</strong> splitless liners<br />

When deciding between a liner with or without glass wool, choose a liner without glass wool<br />

if your sample contains non-volatiles or analytes within a wide boiling range. For unknown<br />

samples, use a liner without glass wool to avoid loss of active or labile compounds. <strong>Agilent</strong><br />

recommends first trying a liner without glass wool; use glass wool as a second choice.<br />

Single taper splitless liner<br />

Single taper, glass wool splitless liner<br />

Double taper splitless liner<br />

<strong>Agilent</strong> Splitless <strong>Liners</strong><br />

Description 1/pk 5/pk 25/pk<br />

Single taper, deactivated 5181-3316 5183-4695 5183-4696<br />

Single taper, inert 5181-3316i<br />

Single taper, glass wool, deactivated 5062-3587 5183-4693 5183-4694<br />

Single taper, <strong>MS</strong> certified liner with glass wool 5188-6568<br />

Double taper, deactivated 5181-3315 5183-4705 5183-4706<br />

Straight, deactivated, quartz 5181-8818 5183-4703 5183-4704<br />

Straight, non-deactivated, quartz 18740-80220 5183-4707 5183-4708<br />

Straight, non-deactivated 210-3003 210-3003-5<br />

Direct Connect <strong>Liners</strong><br />

Direct Connect liners<br />

<strong>Agilent</strong>'s Direct Connect <strong>Liners</strong> provide maximum recovery <strong>and</strong> minimal decomposition of<br />

active compounds for methods requiring splitless injection, such as EPA 8270. They are best<br />

for relatively clean samples containing active analytes, such as water extracts. The liners<br />

directly connect with the column, similar to press-fit connectors, to aid complete transfer<br />

of sample onto the column, eliminating the problem of inlet discrimination <strong>and</strong> further<br />

increasing sensitivity.<br />

Direct Connect <strong>Liners</strong><br />

Description<br />

Part No.<br />

Single taper, <strong>Agilent</strong> proprietary deactivation G1544-80730<br />

Dual taper, <strong>Agilent</strong> proprietary deactivation G1544-80700<br />

Single taper, deactivated, inert G1544-80731<br />

<strong>GC</strong> <strong>and</strong> <strong>GC</strong>/<strong>MS</strong><br />

www.agilent.com/chem/supplies<br />

155


<strong>Inlet</strong> <strong>Liners</strong><br />

NEW!<br />

Helix <strong>Liners</strong><br />

Helix liners<br />

Helix liners approximate the benefit of glass wool without the activity. The deactivated glass<br />

spiral gives surface area without glass wool's active sites to vaporize <strong>and</strong> mix sample before<br />

getting onto the column, <strong>and</strong> prevents sample from splashing onto the bottom of liner <strong>and</strong><br />

seal. Helix liners are recommended for slower injection speeds.<br />

Helix <strong>Liners</strong><br />

Description<br />

Part No.<br />

Helix open ended, deactivated 5188-5396<br />

Helix double taper, deactivated 5188-5398<br />

Helix single taper, deactivated 5188-5397<br />

Liner O-Rings<br />

• <strong>Liners</strong> are sealed in the inlet with O-rings or graphite seals<br />

• Graphite seals are used when inlet temperatures exceed 350°C<br />

• Fluorocarbon O-ring seals are easier to replace than graphite that deforms <strong>and</strong> flakes apart<br />

Liner O-rings in dial packaging<br />

Only <strong>Agilent</strong> fluorocarbon liner O-rings are:<br />

<strong>GC</strong> <strong>and</strong> <strong>GC</strong>/<strong>MS</strong><br />

• Pre-cleaned, then conditioned to eliminate out-gassing of contaminants, especially<br />

important for trace, ECD <strong>and</strong> <strong>MS</strong>D analyses<br />

• Plasma treated for a non-stick, contaminant-free surface that won’t stick to the inlet metal<br />

surface creating unnecessary inlet maintenance<br />

• Packaged for convenience <strong>and</strong> cleanliness in a novel dial package that delivers 1 clean<br />

O-ring, ready for use<br />

Liner O-Rings<br />

Description Unit Part No.<br />

<strong>Certified</strong> non-stick fluorocarbon O-ring 10/pk 5188-5365<br />

Graphite O-ring for splitless liner 10/pk 5180-4173<br />

Graphite O-ring for split liner 10/pk 5180-4168<br />

Non-Stick fluorocarbon liner O-ring for Flip Top 10/pk 5188-5366<br />

High Temp PTV inlet liner fluorocarbon O-ring 10/pk 5188-5311<br />

156<br />

www.agilent.com/chem/supplies

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