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Proceed<strong>in</strong>gs <strong>of</strong> the SEM Annual Conference on Experimental and Applied Mechanics<br />

June 4-6, 2001, Portland, Oregon<br />

<strong>Ultrasonic</strong> <strong>Assessment</strong> <strong>of</strong> <strong>Impact</strong> <strong>Damage</strong><br />

<strong>in</strong> Alum<strong>in</strong>um/<strong>Acrylic</strong> Sandwich Plates<br />

B. M. Liaw, A. M. Pierides, and Y. X. Liu<br />

The City College <strong>of</strong> The City University <strong>of</strong> New York<br />

Department <strong>of</strong> Mechanical Eng<strong>in</strong>eer<strong>in</strong>g<br />

and<br />

The CUNY Graduate School and University Center<br />

Convent Avenue and 138th Street<br />

New York, NY 10031<br />

Abstract<br />

<strong>Ultrasonic</strong> studies were conducted to assess damages<br />

generated by <strong>in</strong>strumented drop-weight impact<strong>in</strong>g onto 6061-<br />

T6 alum<strong>in</strong>um/cast acrylic sandwich plates adhered by epoxy.<br />

Depend<strong>in</strong>g on several parameters, such as impact velocity,<br />

mass, temperature, sandwich construction, etc., various<br />

types <strong>of</strong> impact damage were observed, <strong>in</strong>clud<strong>in</strong>g plastic<br />

<strong>in</strong>dentation, radiat<strong>in</strong>g cracks emanat<strong>in</strong>g from the impact site,<br />

partial and full debond<strong>in</strong>g, and comb<strong>in</strong>ations <strong>of</strong> these<br />

damages. One major goal <strong>of</strong> this study is to use immersion<br />

ultrasound techniques <strong>in</strong> both pulse-echo and throughtransmission<br />

modes to detect these failure mechanisms,<br />

which were clearly visible s<strong>in</strong>ce cast acrylic is transparent.<br />

The developed NDT techniques can then be used to study<br />

damage behaviors <strong>in</strong> opaque composites, such as the fibermetal<br />

lam<strong>in</strong>ates.<br />

Introduction<br />

As part <strong>of</strong> the cont<strong>in</strong>u<strong>in</strong>g effort <strong>of</strong> a paper presented <strong>in</strong> the<br />

SEM Annual Conference last year [1], the ma<strong>in</strong> objectives <strong>of</strong><br />

this study are (i) to establish research capability <strong>in</strong> ultrasound<br />

techniques at the authors’ <strong>in</strong>stitute us<strong>in</strong>g sandwich plates<br />

made <strong>of</strong> two common commercial materials: 6061-T6<br />

alum<strong>in</strong>um and cast acrylic, and (ii) to develop prelim<strong>in</strong>ary<br />

understand<strong>in</strong>g <strong>of</strong> delam<strong>in</strong>ation and fracture caused by impact<br />

<strong>in</strong> other advanced sandwich panels (e.g., fiber-metal<br />

lam<strong>in</strong>ates [2-5]).<br />

Specimen Preparation, <strong>Impact</strong> & Ultrasound<br />

The materials for mak<strong>in</strong>g sandwich plates <strong>in</strong> this study are:<br />

(i) 6061-T6, a ductile alum<strong>in</strong>um-magnesium-silicon alloy with<br />

artificial temper<strong>in</strong>g for precipitation heat treatment (97.9 wt%<br />

Al, 1.0 Mg, 0.6 Si, 0.28 Mn, 0.2 Cr) and (ii) a brittle cast<br />

acrylic (PMMA). Typical material properties <strong>of</strong> these two<br />

materials useful for this study are listed <strong>in</strong> Table 1. Square<br />

panels with dimensions <strong>of</strong> 100 mm x 100 mm (or 4” x 4”)<br />

were then cut <strong>of</strong>f cast acrylic with a thickness <strong>of</strong> 6.3 mm (or<br />

0.25”) and 6061-T6 alum<strong>in</strong>um alloy with a thickness <strong>of</strong><br />

1.6 mm (or 1/16”). This study tested either pure acrylic<br />

panels or sandwich plates made <strong>of</strong> acrylic and alum<strong>in</strong>um<br />

panels adhered by a two-component epoxy.<br />

Table 1. Material Properties<br />

Property 6061-T6 acrylic<br />

Density, ρ<br />

g/cm 3 (ib/<strong>in</strong> 3 )<br />

2.70<br />

(0.0975)<br />

1.19<br />

(0.0430)<br />

Tensile Modulus, E<br />

GPa (Msi)<br />

69<br />

(10)<br />

3.0<br />

(0.44)<br />

Poisson Ratio, ν 0.33 0.36<br />

Longitud<strong>in</strong>al Wave Speed, c 1<br />

km/s (×10 3 <strong>in</strong>/s)<br />

6.15<br />

242<br />

2.06<br />

(81)<br />

Shear Wave Speed, c 2<br />

km/s (×10 3 <strong>in</strong>/s)<br />

3.10<br />

(122)<br />

0.96<br />

(38)<br />

⎧<br />

⎪c1<br />

=<br />

⎪<br />

Note: ⎨<br />

⎪<br />

c =<br />

⎩<br />

⎪ 2<br />

21+<br />

( 1−ν<br />

)<br />

( 1+ )( 1−2<br />

)<br />

E<br />

ρ ν ν<br />

E<br />

ν ρ<br />

( )<br />

The specimens were then clamped circumferentially along a<br />

diameter <strong>of</strong> 76 mm (or 3”) and impacted <strong>in</strong> an Instron-<br />

Dynatup 8250 drop-weight impact tester by a 16 mm- (or<br />

5/8”-) diameter spherical impactor with a weight <strong>of</strong> 6.1 kg (or<br />

13.4 lbs).<br />

The damaged specimens were first <strong>in</strong>spected visually and<br />

then C-scanned <strong>in</strong> both pulse-echo and through-transmission<br />

modes us<strong>in</strong>g a Physical Acoustics Corporation UltraPAC<br />

immersion ultrasonic imag<strong>in</strong>g system. Focused transducers<br />

(0.25”-dia., 1” focus length) <strong>of</strong> various frequencies (5 to 25<br />

MHz) were used for the pulse-echo operation whereas a pair<br />

<strong>of</strong> 0.25”-dia., 25 MHz flat transducer were used <strong>in</strong> the<br />

through-transmission mode. The schematic <strong>of</strong> a typical<br />

immersion ultrasound system is shown <strong>in</strong> Fig. 1.<br />

264


Results and Discussion<br />

The first case considered is the dropped-weight impact onto<br />

a cast acrylic plate by a 6.1 kg mass from a height <strong>of</strong> 51 mm<br />

(2”) and the test resulted <strong>in</strong> a star-shaped crack<strong>in</strong>g pattern.<br />

The ultrasound technique used here is schematically<br />

depicted <strong>in</strong> Fig. 2. As shown <strong>in</strong> Fig. 3 the optical image was<br />

reproduced fairly faithfully by the proposed ultrasound<br />

technique with the exception <strong>of</strong> a few horizontal white<br />

streaks which were mis-scanned po<strong>in</strong>ts due to the limitation<br />

<strong>of</strong> the ultrasound system. Regardless the transducer<br />

frequency (say, between 5 and 25 MHz) the ultrasound<br />

images detected the flaw pattern very accurately. In<br />

particular, the higher frequency transducer, which has a<br />

better resolution, produces more details <strong>of</strong> fracture,<br />

especially around the impact site.<br />

The ultrasound technique shown <strong>in</strong> Fig. 4 was then used to<br />

<strong>in</strong>spect the crack pattern and debond<strong>in</strong>g <strong>in</strong> a damaged<br />

alum<strong>in</strong>um/acrylic sandwich plate scanned from the acrylic<br />

side. The result<strong>in</strong>g C-scan images and the optical image are<br />

shown <strong>in</strong> Fig. 5, which aga<strong>in</strong> <strong>in</strong>dicates the high accuracy <strong>of</strong><br />

ultrasound <strong>in</strong>spection.<br />

The advantage <strong>of</strong> ultrasound technique is for flaw detection<br />

<strong>in</strong> an opaque material. We also used the technique shown <strong>in</strong><br />

Fig. 6 to scan the aforementioned damaged alum<strong>in</strong>um/<br />

acrylic sandwich plate from the alum<strong>in</strong>um side. The result<strong>in</strong>g<br />

optical and C-scan images are shown <strong>in</strong> Fig. 7. In this case<br />

only the <strong>in</strong>dentation and debond<strong>in</strong>g are detected by the<br />

ultrasound technique. Because <strong>of</strong> the presence <strong>of</strong><br />

debond<strong>in</strong>g, the back-echo signals from the cracked acrylic<br />

plate were “overshadowed” by the strong echoes from the<br />

debonded <strong>in</strong>terface. This is because ultrasound signals<br />

transmit poorly through the “air gap” with<strong>in</strong> the debonded<br />

area. The experimental evidence can be illustrated by a<br />

typical A-scan ultrasound signal shown <strong>in</strong> Fig. 8.<br />

To further verify the filter<strong>in</strong>g effect <strong>of</strong> debond<strong>in</strong>g on<br />

ultrasound signals, we adhered a pre-cracked acrylic plate to<br />

an alum<strong>in</strong>um panel; thus artificially remov<strong>in</strong>g the debond<strong>in</strong>g.<br />

The ultrasound technique shown <strong>in</strong> Fig. 9 was then used for<br />

C-scan from the alum<strong>in</strong>um side and the result<strong>in</strong>g image,<br />

along with their optical counterpart, are shown <strong>in</strong> Fig. 10. In<br />

this case, without the block<strong>in</strong>g effect from debond<strong>in</strong>g the<br />

crack<strong>in</strong>g pattern (as displayed <strong>in</strong> the optical image) was<br />

clearly detected by ultrasound. A typical A-scan signal<br />

show<strong>in</strong>g the identifiable back echo from cracked acrylic is<br />

illustrated <strong>in</strong> Fig. 11.<br />

F<strong>in</strong>ally as shown <strong>in</strong> Fig. 12, the impacted alum<strong>in</strong>um/acrylic<br />

plate studied <strong>in</strong> previously (see Fig. 5) was also scanned <strong>in</strong><br />

the through-transmission mode. Just like the case <strong>of</strong> pulseecho<br />

mode, the result<strong>in</strong>g ultrasound image, as shown <strong>in</strong> Fig.<br />

13, could only detect the debond while the crack<strong>in</strong>g was<br />

aga<strong>in</strong> shielded.<br />

Conclusions<br />

From this study one can conclude that<br />

• The ultrasound technique can detect crack and debond<br />

accurately <strong>in</strong> alum<strong>in</strong>um/acrylic sandwich plates so long<br />

as the back echo signals are not blocked by any<br />

discont<strong>in</strong>uity;<br />

• In general, all ultrasound transducers with commonly<br />

used frequencies, i.e., 5 to 25 MHz, can detect flaw<br />

accurately;<br />

• In particular, the transducers <strong>of</strong> higher frequency have<br />

better resolutions and can detect f<strong>in</strong>e details;<br />

• Both pulse-echo and through-transmission modes are<br />

workable for damage detection <strong>in</strong> relatively flat<br />

specimens.<br />

Acknowledgments<br />

This study was supported by NASA Faculty Award for<br />

Research (FAR) under Grant No. NAG3-2259 and by<br />

PSC-CUNY under Grants 61429-00 30 and 62466-00 31. Dr.<br />

Kenneth J. Bowles and Dr. John P. Gyekenyesi are the<br />

Technical Monitors <strong>of</strong> the NASA grant. Part <strong>of</strong> the equipment<br />

used <strong>in</strong> this <strong>in</strong>vestigation was acquired through Army<br />

Research Office Grant No. DAAD19-99-1-0366.<br />

References<br />

1. B.M. Liaw, G. Zeichner and Y.X. Liu, “<strong>Impact</strong><br />

delam<strong>in</strong>ation and fracture <strong>in</strong> alum<strong>in</strong>um/acrylic sandwich<br />

plates,” Proceed<strong>in</strong>gs <strong>of</strong> the SEM IX International<br />

Congress on Experimental Mechanics, Orlando, FL,<br />

June 5-8, 2000, pp. 515-518.<br />

2. A. Vlot, “<strong>Impact</strong> Properties <strong>of</strong> fiber metal lam<strong>in</strong>ates,”<br />

Composite Eng<strong>in</strong>eer<strong>in</strong>g, Vol. 3, No. 10, pp. 911-927,<br />

1993.<br />

3. C.T. Sun, A. Dicken, and H.F. Wu, “Characterization <strong>of</strong><br />

impact damage <strong>in</strong> ARALL lam<strong>in</strong>ates,” Composites<br />

Science and Technology, Vol. 49, pp. 139-144, 1993.<br />

4. H.F. Wu, “Temperature dependence <strong>of</strong> the tensile<br />

properties <strong>of</strong> ARALL-4 lam<strong>in</strong>ates,” J. <strong>of</strong> Materials<br />

Science, Vol. 25, pp. 1120-1127, 1990.<br />

5. B.M. Liaw, Y.X. Liu, and E.A. Villars, “<strong>Impact</strong> damage<br />

mechanisms <strong>in</strong> fiber-metal lam<strong>in</strong>ates,” this volume.<br />

Figure 1. Schematic <strong>of</strong> a typical immersion ultrasound<br />

system.<br />

265


Figure 2. Ultrasound technique for <strong>in</strong>spect<strong>in</strong>g a cracked<br />

acrylic plate.<br />

Figure 4. Ultrasound technique scann<strong>in</strong>g a damaged<br />

alum<strong>in</strong>um/acrylic sandwich plate from the acrylic<br />

side.<br />

Optical image<br />

C-scan (5 MHz)<br />

Optical image<br />

C-scan (5 MHz)<br />

C-scan (10 MHz)<br />

C-scan (15 MHz)<br />

C-scan (10 MHz)<br />

C-scan (15 MHz)<br />

C-scan (20 MHz)<br />

C-scan (25 MHz)<br />

Figure 3. Optical and ultrasound C-scan images <strong>of</strong> crack<strong>in</strong>g<br />

<strong>in</strong> an cast acrylic plate impacted by a dropped<br />

weight <strong>of</strong> 6.1 kg from 51 mm (2”) high.<br />

C-scan (20 MHz)<br />

C-scan (25 MHz)<br />

Figure 5. Optical and ultrasound C-scan images <strong>of</strong><br />

debond<strong>in</strong>g and crack<strong>in</strong>g scanned/photographed<br />

from the acrylic side <strong>of</strong> a n impacted<br />

alum<strong>in</strong>um/acrylic sandwich plate.<br />

266


Figure 6. Ultrasound technique scann<strong>in</strong>g a damaged<br />

alum<strong>in</strong>um/acrylic sandwich plate from the<br />

alum<strong>in</strong>um side.<br />

Figure 9. Ultrasound technique for <strong>in</strong>spect<strong>in</strong>g a<br />

pre-cracked acrylic plate shielded by an<br />

alum<strong>in</strong>um panel.<br />

Optical image<br />

C-scan (25 MHz)<br />

Figure 7. Optical and ultrasound C-scan images from the<br />

alum<strong>in</strong>um side <strong>of</strong> a damaged alum<strong>in</strong>um/acrylic<br />

sandwich plate.<br />

Optical image<br />

C-scan (25 MHz)<br />

Figure 10. Optical and ultrasound C-scan images <strong>of</strong> a<br />

pre-cracked acrylic plate shielded by an alum<strong>in</strong>um<br />

panel.<br />

Overdhadowed<br />

back echo<br />

Identifiable back echo<br />

Figure 8. An A-scan ultrasound signal show<strong>in</strong>g<br />

overshadowed back echoes.<br />

Figure 11. An A-scan ultrasound signal show<strong>in</strong>g<br />

identifiable back echoes.<br />

267


Figure 12. Through-transmission ultrasound.<br />

Figure 13. Through-transmission (0.25”-dia., 25 MHz flat<br />

transducers) ultrasound C-scan image <strong>of</strong> a<br />

damaged alum<strong>in</strong>um/acrylic sandwich plate<br />

scanned from the alum<strong>in</strong>um side.<br />

268

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