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Proposal - The Center for Research and Learning - IUPUI

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Frequently Asked Questions re: MURI Project <strong>Proposal</strong>s<br />

Please read the answers to these “Frequently Asked Questions” be<strong>for</strong>e writing <strong>and</strong> submitting<br />

your MURI proposal.<br />

1) What is MURI<br />

MURI is an acronym <strong>for</strong> Multidisciplinary Undergraduate <strong>Research</strong> Institute.<br />

2) Who is eligible to propose a MURI project <strong>and</strong> serve as a mentor<br />

Any <strong>IUPUI</strong> faculty member from any school may propose a MURI project <strong>and</strong> serve as a principal<br />

mentor. A project may have up to three paid mentors. Preference will be given to projects that<br />

include mentors from multiple disciplines.<br />

Senior researchers, graduate students <strong>and</strong>/or post-doctoral fellows may serve as co-mentors.<br />

3) Who is able to participate as an undergraduate researcher on a MURI team<br />

<strong>IUPUI</strong> students may apply to participate on a MURI team as long as they are working on their first<br />

undergraduate degree <strong>and</strong> have a minimum 3.0 GPA.<br />

Up to six students may work on a MURI team. <strong>The</strong>re should always be two more students than<br />

mentors on a team.<br />

4) What other individuals may be involved<br />

<strong>Proposal</strong>s may also include other consultants, staff members, graduate students, <strong>and</strong><br />

postdoctoral researchers as unpaid team members. <strong>The</strong>se personnel do not need to be listed on<br />

the cover page of the proposal but their roles should be explained in the proposal where<br />

appropriate.<br />

5) For what time period are proposals being solicited<br />

<strong>Proposal</strong>s are currently being solicited <strong>for</strong> two time periods:<br />

1. Summer 2011 MURI (nine-week<br />

full-time intensive program)<br />

2. Academic Year 2011-2012 MURI<br />

(approx. 120 hours spread over fall<br />

<strong>and</strong> spring semesters)<br />

June 1, 2011 - July 29, 2011<br />

October 5, 2011 — April 30, 2012<br />

6) How many proposals may be submitted by a mentor<br />

A mentor may submit one proposal <strong>for</strong> each time period listed above <strong>for</strong> a total of two proposals.<br />

7) What is the deadline <strong>for</strong> proposals<br />

All completed proposals must be submitted electronically as a single file, preferably in pdf <strong>for</strong>mat,<br />

to CRLGrant@iupui.edu no later than midnight on March 10, 2011.<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 1


8) What <strong>for</strong>mat is required <strong>for</strong> the proposal<br />

<strong>The</strong> proposal should be <strong>for</strong>matted on 8-1/2 x 11 paper with at least 1-inch margins <strong>and</strong> a<br />

minimum of 12-pt. font size.<br />

Page Description<br />

Maximum No. of Pages<br />

Cover Page 1<br />

Request <strong>for</strong> Students 1<br />

Body of <strong>Proposal</strong> 5<br />

References/Bibliography<br />

1-2 as necessary<br />

CVs/Resumes<br />

2-pages maximum per<br />

mentor<br />

Support Letters (maximum 2) 2<br />

Appendix --1 page summary <strong>for</strong> each previous successful 5 TOTAL<br />

multidisciplinary student project (see sample template)<br />

Signature Page 1<br />

TOTAL 23<br />

*Please note that proposals that do not follow specified <strong>for</strong>mat guidelines will not be<br />

reviewed.<br />

9) When is the deadline <strong>for</strong> students to apply <strong>for</strong> summer 2011 MURI projects<br />

Students should apply to MURI by March 1, 2011 in order to be eligible to participate in summer<br />

2011 MURI projects.<br />

It is expected that winning proposals will be announced by April 11, 2011.<br />

10) If projects are not announced until April 11, 2011, how do students select a MURI project<br />

After winning proposals are announced, eligible MURI students (those who have completed the<br />

CRL Summer Program Application Form by March 1, 2011 <strong>and</strong> who have been notified of<br />

acceptance) will rank the projects they are interested in <strong>and</strong> send their choices to Elizabeth<br />

Rubens <strong>and</strong> Hazim El-Mounayri via email to crlstaff@iupui.edu by April 21, 2011. Students will<br />

then be matched to projects. Whenever possible, program leaders will attempt to match student<br />

requests to specific projects.<br />

11) When is the deadline <strong>for</strong> students to apply <strong>for</strong> AY 2011-2012 MURI projects<br />

Students wishing to participate in AY 2011-2012 projects must apply by September 9, 2011. <strong>The</strong><br />

application process <strong>for</strong> academic year projects will open on May 1, 2011.<br />

12) Do students receive a stipend<br />

Students receive a stipend of $3200 <strong>for</strong> the full-time, nine-week intensive summer program <strong>and</strong><br />

$1200 (both semesters combined) <strong>for</strong> the AY 2011-2012 program. Stipends are contingent upon<br />

students meeting the requirements of the program.<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 2


13) When do students receive their stipends<br />

Summer 2011<br />

One $3200 installment approximately the<br />

third week of June, 2011.<br />

Academic Year 2011-2012 Two $600 installments. <strong>The</strong> first $600<br />

installment is disbursed approximately the<br />

third week of January, 2012; <strong>and</strong> the<br />

second $600 installment is disbursed<br />

approximately the third week of May, 2012,<br />

<strong>for</strong> a total amount of $1200.<br />

14) Do mentors <strong>and</strong> co-mentors receive a stipend<br />

Mentors <strong>and</strong> co-mentors receive a total stipend of $500 <strong>for</strong> each MURI project they mentor.<br />

Payment is made via academic overload <strong>and</strong> disbursed in the mentors’ paychecks.<br />

15) When do mentors receive their stipends<br />

Summer 2011<br />

One $500 installment with September,<br />

2011 paycheck.<br />

Academic Year 2011-2012 One $500 installment with June, 2012<br />

paycheck.<br />

16) Is there a budgeted grant amount <strong>for</strong> MURI projects<br />

Funded MURI projects are eligible to receive up to $2000 <strong>for</strong> necessary research-related supplies<br />

<strong>and</strong> equipment. Please note that at this time MURI does not generally fund computers or travel<br />

expenses. All purchases must be cleared through the <strong>Center</strong> <strong>for</strong> <strong>Research</strong> <strong>and</strong> <strong>Learning</strong> to<br />

ensure that they are in compliance with University policies <strong>and</strong> procedures.<br />

17) How will MURI proposals be selected<br />

A MURI Project Grant Review Committee will be <strong>for</strong>med to review MURI proposals. <strong>The</strong> MURI<br />

Project Grant Review Committee will review the submitted proposals using the MURI Mentor’s<br />

<strong>Proposal</strong> Evaluation Form.<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 3


18) If I have questions regarding the proposal writing or review process, whom should I contact<br />

Questions should be directed to one of the following individuals:<br />

Elizabeth Rubens, Program Leader <strong>for</strong> MURI, UROP, <strong>and</strong> CTSI<br />

<strong>IUPUI</strong> <strong>Center</strong> <strong>for</strong> <strong>Research</strong> <strong>and</strong> <strong>Learning</strong><br />

Office of the Vice Chancellor <strong>for</strong> <strong>Research</strong><br />

erubens@iupui.edu / (317) 274-4590<br />

Hazim El-Mounayri<br />

Co-leader <strong>for</strong> MURI <strong>and</strong> Associate Professor of Mechanical Engineering<br />

Purdue School of Engineering <strong>and</strong> Technology<br />

helmouna@iupui.edu / (317) 278-3320<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 4


MURI Project <strong>Proposal</strong> Form<br />

Section I: <strong>Proposal</strong> Cover Page<br />

Date of submission: _______03/10/2011 ____________________<br />

Proposed project title: Failure warning system development <strong>for</strong> Li ion battery package<br />

Principle Mentor<br />

Name: Jian Xie<br />

Phone number: 317-274-8850<br />

Department: ME<br />

Co-mentor<br />

Name: Fan Xu<br />

Phone number: (317) 274-5934<br />

Department: ME<br />

Co-mentor<br />

Name: Hao He<br />

Phone number: (317) 274-5934<br />

Department: ME<br />

Title: Assistant Professor<br />

Email:jianxie@iupui.edu<br />

School: Engineering <strong>and</strong> Technology<br />

Title: <strong>Research</strong> Associate<br />

Email: fanxu@iupui.edu<br />

School: Engineering <strong>and</strong> Technology<br />

Title: <strong>Research</strong> Associate<br />

Email: haohe@iupui.edu<br />

School: Engineering <strong>and</strong> Technology<br />

Please note that preference will be given to projects that include mentors from multiple<br />

disciplines.<br />

<strong>The</strong> project will be carried out <strong>and</strong> completed (check only one):<br />

Summer Program<br />

Academic Year Program<br />

(June 1-July 29, 2011) (October 5, 2011-April 30, 2012)<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 5


Section II: Student Request Page<br />

Total number of students requested: _____6_________<br />

(Note: <strong>The</strong> total number of students must exceed the number of mentors by two)<br />

Total Number of freshmen <strong>and</strong>/or sophomores to be recruited: ________3_____________<br />

Disciplines or majors of students (preference will be given to projects that include at least two<br />

disciplines or majors): Mechanical Engineering, Chemistry, Physics, Industrial Engineering <strong>and</strong><br />

Technology, <strong>and</strong> Electrical Engineering<br />

Skills expected from students: _________ MatLab analysis, mechanical/electrical engineering<br />

fabrication process, instrument operation, basic knowledge of Li-ion batteries._________<br />

Names of students you request to work on this project.<br />

(Mentors are invited to recommend students that they would prefer to work on the proposed<br />

project. Please provide an email address <strong>and</strong> a rationale; <strong>for</strong> example, a student may have an<br />

essential skill, may already be working on a similar project, or may be intending to apply to<br />

graduate school to pursue the same area of research.)<br />

<strong>The</strong> <strong>Center</strong> <strong>for</strong> <strong>Research</strong> <strong>and</strong> <strong>Learning</strong> will consider the students requested below, but cannot<br />

guarantee placement of specific students on teams.<br />

Name of Student: Student’s Email: Rationale:<br />

1)_________________ ______________ ________________________<br />

2)_________________ ______________ ________________________<br />

3)_________________ ______________ ________________________<br />

4)_________________ ______________ ________________________<br />

5)_________________ ______________ ________________________<br />

6)_________________ ______________ ________________________<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 6


Section III: Body of <strong>Proposal</strong><br />

(A maximum of 5 pages is allowed <strong>for</strong> answers to questions 1-10.)<br />

1) Please list the research objectives <strong>for</strong> proposal.<br />

<strong>The</strong> objective is to build 4-cell battery cell pack <strong>and</strong> a monitoring system <strong>for</strong> measuring<br />

the inside cell temperature, which will be employed in overcharge <strong>and</strong> over discharge<br />

experiments to collect the V, I, T s <strong>and</strong> T in . Based on these data, Matlab will be employed to<br />

develop the algorithm of the four parameters, which will be used in the early warning system<br />

built.<br />

2) Please describe the significance of the research.<br />

LiFePO 4 Li ion batteries have been commercialized <strong>and</strong> adopted as one of the most<br />

promising sources <strong>for</strong> the electric vehicles <strong>and</strong> most portable electronic products, because of<br />

its good stability (85% of initial capacity at 2000 cycles <strong>for</strong> A123 18650), high temperature<br />

of releasing oxygen, rich resources <strong>and</strong> environment friendly as compared with traditional<br />

LiCoO 2 , LiNiO 2 <strong>and</strong> LiMn 2 O 4 Li ion batteries. However, it is also well known that the safety<br />

issue, like the vulnerability of thermo-chemical stability against operation under abnormal<br />

conditions, is still a big challenge <strong>for</strong> the LiFePO 4 Li ion cell, especially with regard to use of<br />

lithium-ion batteries in transportation applications. In order to exp<strong>and</strong> the application of Li<br />

ion battery on transportation, early warning system could be one of the most reliable<br />

solutions. First, the early warning system could realize real time detection to check out the<br />

state of health of every battery cells in the module. Second, the failure of single battery cell<br />

in the pack could be detected by the early warning system. In this way, the catastrophic<br />

failure could be avoided by this early warning system.<br />

3) Why does this proposal offer a good opportunity <strong>for</strong> undergraduate researchers to gain<br />

substantive research skills<br />

<strong>The</strong> proposed project is expected to promote the undergraduate research program, help the<br />

recruitment of undergraduate students, <strong>and</strong> generate interest among students from different<br />

disciplines on renewable energy. Students involved in this project will learn the “real world”<br />

R&D work experience, which will benefit their future careers.<br />

• Li-ion batteries played a prominent role in ideal electrochemical storage systems.<br />

However, the safety issue of the Li-ion battery is still a big problem in its application.<br />

• Students will be able to learn about Li-ion battery making <strong>and</strong> testing in practice.<br />

• Students will learn how to design a special battery <strong>and</strong> sample holder according to the<br />

practical experimental requirements by taking a lot of knowledge from different fields<br />

into account.<br />

• Students from different majors will collaborate with each other <strong>and</strong> learn from each other.<br />

• Students will assist in the publication of this project <strong>and</strong> following research based on this<br />

project.<br />

4) Please describe the research methodology <strong>and</strong> the specific tasks that students <strong>and</strong><br />

mentors will undertake.<br />

Student:<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 7


a) A123 18650 Li ion battery will be employed to build a 4-cell Li-ion module.<br />

b) A special design should be made to insert a temperature sensor into the<br />

commercial battery cell to monitor the temperature change by Arbin instrument.<br />

c) V, I <strong>and</strong> T s will be collected in overcharge <strong>and</strong> over discharge experiments.<br />

d) Matlab will be employed to develop the algorithm of the four parameters.<br />

Mentors:<br />

e) Dr. Jian Xie will assist students in the underst<strong>and</strong>ing of the concept <strong>and</strong> meaning<br />

of the development of the algorithm by Matlab. Dr. Jian Xie will also guide<br />

students in the analysis of experiment data <strong>and</strong> report writing.<br />

f) Mr. Fan Xu <strong>and</strong> Mr. Hao He will assist students in electrochemical measurements,<br />

4-cell battery stack buliding, <strong>and</strong> monitor system design. Mr. Fan Xu will guide<br />

the underst<strong>and</strong>ing of the fundamental theory of electrochemistry related to this<br />

project. Mr. Fan Xu will also guide the students in electrochemical data analysis.<br />

g) A multidisciplinary team of undergraduate students, one from mechanical<br />

engineering, one from Electrical Engineering <strong>and</strong> one from Mathematics will be<br />

assembled to conduct the project <strong>and</strong> analyze the results under the supervision of<br />

the MURI mentors.<br />

This team will prepare a presentation to share the results.<br />

5) What plan has been designed to ensure effective communication with all co-mentors <strong>and</strong><br />

undergraduate researchers on the MURI team<br />

A weekly oral report will be hold by Dr. Jian Xie to discuss with students <strong>and</strong> other<br />

mentors about the process of task.<br />

6) What measureable outcomes <strong>and</strong> benefits do you anticipate this research will provide<br />

A 4-cell battery system will be carried out under overcharge <strong>and</strong> over discharge condition.<br />

Three key parameters, V, I <strong>and</strong> T s will be collected. <strong>The</strong> algorithm related to these three key<br />

parameters will be developed. And a look up table <strong>for</strong> early warning system <strong>for</strong> Li ion battery<br />

pack will be developed based on this MURI work. A corresponding paper shooting <strong>for</strong> Journal<br />

of Power Source will come out <strong>for</strong> this task.<br />

7) What is the timeline <strong>for</strong> the major tasks associated with this proposal<br />

Dates Tasks<br />

June 1 st to June4 th 4-cell battery stack building<br />

June 5 th to June 12 th Real time monitor system building<br />

June 13 th to July 13 th Data collection <strong>and</strong> algorithm development<br />

July 14 th to July 29 th Preparation of academic paper(s)<br />

8) Please provide a rationale <strong>for</strong> your budget request. (NOTE: <strong>The</strong> maximum budget<br />

allowance is $2,000 <strong>for</strong> equipment <strong>and</strong>/or supplies needed <strong>for</strong> the research team. Generally<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 8


speaking, expenditures <strong>for</strong> computers <strong>and</strong>/or travel are not approved by the review<br />

committee at this time due to financial constraints.)<br />

Items<br />

Projected Expense($)<br />

Equipment 1000<br />

Materials 500<br />

Travel 500<br />

Total 2000<br />

9) Please describe your plan <strong>for</strong> sustaining your research beyond the funding that MURI is<br />

able to provide. (For example, please list other external grants that will be submitted as a<br />

follow-up to your MURI funding.)<br />

“Development of Early Warning System <strong>for</strong> Li Ion Battery System”, Navy.<br />

10) Risk Management<br />

All university policies with respect to research must be followed. Thus, the usual risk management<br />

assurances must be provided where appropriate (animal use, radiation safety, DNA, human<br />

subjects protocols) in accordance with the university policies. No funds may be released without<br />

risk-management assurances, where needed. Project proposals without required compliance<br />

approvals will be reviewed but the funds will not be released until approval is given by the<br />

university.<br />

Further in<strong>for</strong>mation on risk management is available from http://researchadmin.iu.edu/cs.html<br />

Please check any risk assurances that apply to this proposal:<br />

Animals (IACUC Study #): _________________<br />

Human Subjects (IRB Study #): ____________________<br />

r-DNA (IBC Study #): _____________________<br />

Human Pathogens, Blood, Fluids, or Tissues must be identified if used: ______<br />

Section IV: References/Bibliography (insert 1-2 pages as needed)<br />

Dr. Jian Xie<br />

1. Jian Xie*, David Wood, Karren More, Palmen. Atanassov <strong>and</strong> Rodney Borup, “Micro-<br />

Structural Changes of Membrane Electrode Assembly During PEFC Durability Testing at High<br />

Humidity Conditions,” J. Electrochem. Soc. 152, A1011 (2005).<br />

2. Jian Xie*, David Wood, David Wayne, Thomas Zawodzinski, Palmen. Atanassov <strong>and</strong> Rodney<br />

Borup “Durability of PEFCs at High Humidity Conditions,” J. Electrochem. Soc.152, A47<br />

(2005).<br />

3. Y. Lin, J. Xie, H. Wang, Y. Li, Sang Yoel Lee, S. R. Foltyn, S. A. Crooker, Q. X. Jia, A. K.<br />

Burrell, <strong>and</strong> T. M. McCleskey, “Green Luminescent Zinc Oxide Films Prepared By Polymer-<br />

Assisted Deposition With Rapid <strong>The</strong>rmal Process”, Thin Solid Films, 492 (2005) 101-104.<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 9


4. Jian Xie*, Karren More, Thomas Zawodzinski <strong>and</strong> Wayne Smith, “Porosimetry of MEAs<br />

Made by ``Thin Film Decal'' Method <strong>and</strong> Its Effect on Per<strong>for</strong>mance of PEFCs,” J. Electrochem.<br />

Soc. 151, A1841 (2004).<br />

5. Jian Xie*, Fern<strong>and</strong>o Garzon <strong>and</strong> Thomas Zawodzinski, <strong>and</strong> Wayne Smith “Ionomer<br />

Segregation in Composite MEAs <strong>and</strong> Its Effect on Polymer Electrolyte Fuel Cell Per<strong>for</strong>mance,”<br />

J. Electrochem. Soc. 151, A1084 (2004).<br />

Fan Xu<br />

1. Fan Xu, Mei-xian Wang, Qi Liu, Hong-fang Sun, Seth Simonson, Noma Ogbeifun, Eric A.<br />

Stach, <strong>and</strong> Jian Xie; “Investigation of the Carbon Corrosion Process <strong>for</strong> Polymer Electrolyte Fuel<br />

Cells Using a Rotating Disk Electrode Technique”, Journal of <strong>The</strong> Electrochemical Society, 157<br />

(8) B1138-B1145, 2010.<br />

2. Fan Xu, Hang-Yu Zhang, Jan Ilavsky, Derek Ho, Matthew J. Justice, Horia I. Petrache,<br />

Stanciu, <strong>and</strong> Jian Xie; “Investigation of Catalyst Ink Dispersion Using Both Ultra Small Angle<br />

X-Ray Scattering <strong>and</strong> Cryogenic TEM”, Langmuir 2010, 26(24), 19199–19208.<br />

3. Jian Xie, Fan Xu, David Wood, Karren Moore <strong>and</strong> Thomas Zawodzinski; “Influence of<br />

Nafion Ionomer Content in the Catalyst Layer on the Per<strong>for</strong>mance of PEM Fuel Cell”,<br />

Electrochimica Acta, 55 (2010) 7404–7412.<br />

4. Mei-xian Wang, Fan Xu, Hong-fang Sun, Qi Liu, Kateryna Artyushkova, Eric A.Stach, <strong>and</strong><br />

Jian Xie; “Nanoscale graphite-supported Pt catalysts <strong>for</strong> oxygen reduction reactions in fuel cells”,<br />

Electrochimica Acta (in press).<br />

5. Mei-xian Wang, Fan Xu, Qi Liu, Hong-fang Sun, Rui-hua Cheng, Hao He, Eric A.Stach, Jian<br />

Xie; “Enhancing the catalytic per<strong>for</strong>mance of Pt/C catalysts using steam-etched carbon blacks as<br />

a catalyst support”, Carbon, 49 (2011) 256 –265.<br />

6. Fan Xu, Xuan Cheng, Ying Zhang <strong>and</strong> Qinbai Fan; “Influence of Assembly Force in a<br />

PEMFC under a Lifetime Test”, Electrochemistry, Vol.14, No.2, (2008).<br />

Section V: CVs/Resumes (insert 2 pages per mentor <strong>for</strong> a maximum of 6 pages)<br />

Jian Xie<br />

Education<br />

1999 Ph.D. Miami University, Chemistry/Electrochemistry.<br />

1996 M.S. University of South Dakota, Chemistry/Electrochemistry.<br />

1982 B.S. Tianjin University, Chemical/Electrochemical Engineering.<br />

Professional Experience<br />

2007-present, Assistant Professor, Department of Mechanical Engineering, Indiana<br />

University Purdue University Indianapolis (<strong>IUPUI</strong>)<br />

2007, Principal <strong>Research</strong> Scientist, Battelle Memorial Institute, Columbus, Ohio<br />

2005-2006, Senior Electrochemist, Cabot Corp, Albuquerque, New Mexico<br />

2001-2004, <strong>Research</strong>er, Los Alamos National Laboratory, Los Alamos, New Mexico<br />

1999-2000, System Engineer, General Motors Advanced Technology Vehicles (GMATV)<br />

Division, Indianapolis Technical <strong>Center</strong><br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 10


Publications<br />

Authors of ~20 journal publications, ~30 conference papers <strong>and</strong> 1 book chapter<br />

Five Significant Publications<br />

1. Jian Xie*, David Wood, Karren More, Palmen. Atanassov <strong>and</strong> Rodney Borup , “Micro-<br />

Structural Changes of Membrane Electrode Assembly During PEFC Durability Testing at<br />

High Humidity Conditions,” J. Electrochem. Soc. 152, A1011 (2005).<br />

2. Jian Xie*, Jose-Marie, Sansinena, Junbo Gao, Hsing-Lin Wang*, “Fabrication <strong>and</strong><br />

Characterization of Solid State Conducting Polymer Actuators” Proc. SPIE Int. Soc. Opt.<br />

Eng. 5385, 406 (2004)<br />

3. Jian Xie <strong>and</strong> Thomas L. Riechel*, “Room Temperature Molten Salts Buffered with<br />

Magnesium Metal,” J. Electrochem. Soc., 147, 4247 (2000).<br />

4. Jian Xie <strong>and</strong> Thomas L. Riechel*, “Electrochemistry of 1-Ethyl-3-Methylimidazolium in<br />

Acetonitrile,” J. Electrochem. Soc., 145, 2660 (1998).<br />

5. Walter J. Bowyer, Jian Xie <strong>and</strong> Royce C. Engstrom*, “Fluorescence Imaging of the<br />

Heterogeneous Reduction of Oxygen,” Anal. Chem., 68, 2005 (1996).<br />

Synergistic Activities<br />

1. Served as the panelist <strong>for</strong> the National Science Foundation (NSF) to conduct the panel<br />

review of Renewable Energy (Fuel Cells) proposals <strong>for</strong> the Energy <strong>for</strong> Sustainability<br />

Program (PD07-7644) in the Chemical, Bioengineering, Environmental <strong>and</strong> Transport<br />

Systems (CBET) Program of the Directorate <strong>for</strong> Engineering.<br />

2. Served as review board member <strong>for</strong> the Journal of Electrochemical Society,<br />

Electrochemical <strong>and</strong> Solid-State Letters, Journal of Power Sources, Electrochim. Acta <strong>and</strong><br />

Topics in Catalysis.<br />

3. Served as a Technical Council Member of Battelle Memorial Institute.<br />

4. Member of Electrochemical Society<br />

Education<br />

Fan Xu<br />

• M.S. Mechanical Engineering, Purdue University, Indianapolis, 2008- Present; (I have<br />

applied to the ME Ph.D. program at <strong>IUPUI</strong> in Aug 2010). GPA: 3.7<br />

• M.S. Electrochemistry, Xiamen University, China, 2005-2008 GPA: 3.6<br />

• B.S. Chemistry , Xiamen University, China, 2001-2005 GPA: 3.4<br />

<strong>Research</strong> Experience:<br />

1. <strong>Research</strong> Assistant & Lab manager, Mechanical Engineering Department, Purdue<br />

University, Indianapolis.<br />

2008-present;<br />

Investigated the process-structure-property relationships of membrane electrode assembly<br />

(MEAs) of polymer electrolyte fuel cells (PEMFCs).<br />

Improved <strong>and</strong> optimized per<strong>for</strong>mance of the PEMFC catalyst layer.<br />

Developed high per<strong>for</strong>mance <strong>and</strong> high stability Pt/C catalysts (using modified carbons).<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 11


Investigated durability of catalysts, Nafion ionomer, <strong>and</strong> MEAs of PEMFCs.<br />

Developed corrosion-resistant carbon as a fuel cell catalyst support.<br />

Per<strong>for</strong>med fuel cell test station maintenance <strong>and</strong> repair.<br />

Per<strong>for</strong>med Lithium ion battery safety tests.<br />

Designed a CO 2 electrochemical diversion system.<br />

2. Co-mentor of Multidisciplinary Undergraduate <strong>Research</strong> Institute project, Mechanical<br />

Engineering Department, Purdue University, Indianapolis 2008-2009;<br />

Assembled a testing lab <strong>for</strong> fuel cell research.<br />

Designed a water treatment system by “smart carbon” system design.<br />

Determined the sulfur content in functionalized carbon black <strong>for</strong> fuel cell catalysts.<br />

Supervised undergraduate student’s research work on the above mentioned projects.<br />

3. <strong>Research</strong> Assistant, <strong>The</strong> China National Key Laboratory, Department of Chemistry <strong>and</strong><br />

Chemical engineering, Xiamen University, China 2004-2008;<br />

Investigated the effects of the assembly <strong>for</strong>ce on lifetime <strong>and</strong> per<strong>for</strong>mance of PEMFCs.<br />

Set up an in situ characterization system to analyze hydrogen oxidation in a PEMFC under<br />

harsh conditions.<br />

Publications, Patent <strong>and</strong> presentations<br />

I. Journal Articles<br />

1. Fan Xu, Mei-xian Wang, Qi Liu, Hong-fang Sun, Seth Simonson, Noma Ogbeifun, Eric<br />

A. Stach, <strong>and</strong> Jian Xie; Investigation of the Carbon Corrosion Process <strong>for</strong> Polymer<br />

Electrolyte Fuel Cells Using a Rotating Disk Electrode Technique; Journal of <strong>The</strong><br />

Electrochemical Society, 157 (8) B1138-B1145, 2010.<br />

2. Jian Xiea, Fan Xu, David L. Wood, III, Karren L. More, Thomas A. Zawodzinski, <strong>and</strong><br />

Wayne H. Smith; Influence of Ionomer Content on the Structure <strong>and</strong> Per<strong>for</strong>mance of PEFC<br />

Membrane Electrode Assemblies, Electrochimica Acta, 2010, in press;<br />

3. Investigation of Catalyst Ink Dispersion Using Ultra Small Angle X-Ray <strong>and</strong> Croyenic<br />

TEM: Xu, Fan; Zhang, Hang-Yu; Ilavsky, Jan; Ho, Derek; Justice, Matthew; Petrache, Horia;<br />

Stanciu, Lia; Xie, Jian; under review of Langmuir;<br />

4. Fan Xu, Xuan Cheng, Ying Zhang, Qinbai Fan Influence of Assembly Force in a<br />

PEMFC under a Lifetime Test, Electrochemistry, Vol.14, No.2, May 2008;<br />

5. Fan Xu, Xuan Cheng, Ying Zhang, <strong>and</strong> Qinbai Fan In Situ AC Impedance Diagnosis of<br />

Hydrogen Oxidation in a PEMFC full text 212th ECS Meeting, held in Washington, DC,<br />

October 7 - 12, 2007;<br />

6. Mei-xian Wang, Fan Xu, Qi Liu, Hao He, Jian Xie; Enhanced Catalytic Per<strong>for</strong>mance of<br />

Pt/C Catalysts Using Steam Etching Carbon Blacks as Support, under review of Carbon.<br />

7. Mei-xian Wang, Fan Xu, Hong-fang Sun, Qi Liu, Kateryna Artyushkova, Eric A. Stach,<br />

Jian Xie; Highly Hydrophilic Nanoscale Graphite Particles as Support <strong>for</strong> Polymer<br />

Electrolyte Fuel Cell Catalysts; under review of <strong>The</strong> Journal of Physical Chemistry C;<br />

8. Fan Xu, Afzaal Hassan, Jian Xie; Degradation of Ionomer Network in a Catalyst layer of<br />

PEFC MEA; Currently in draft;<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 12


9. Fan Xu, Afzaal Hassan, Jian Xie; Effect of Fabrication process on the per<strong>for</strong>mance <strong>and</strong><br />

structure of MEA; Currently in draft;<br />

II. Patents<br />

1. Jian Cie, Fan Xu New Electrochemical Method of Carbon Dioxide Processing (10080)<br />

01/01/2010;<br />

Ⅲ. Presentations<br />

1. Fundamental Investigation of Effect of Ink Formulation on Per<strong>for</strong>mance of PEFC MEA;<br />

Fan Xu, Derek Ho, Jan Ilavsky, Matt Justics, Horia Petrache <strong>and</strong> Jian Xie; 216th ECS<br />

Meeting in Vienna, Austria; 2009;<br />

2. Development of High Durability <strong>and</strong> High Per<strong>for</strong>mance Catalysts Utilizing<br />

Functionalized Carbons <strong>for</strong> Polymer Electrolyte Fuel Cells; J. Xie, M. Wang, F. Xu <strong>and</strong> A.<br />

Saab; 216th ECS Meeting in Vienna, Austria; 2009;<br />

3. Investigation of Pt-C Interaction on Stability of Pt/C Catalysts in Polymer Electrolyte<br />

Fuel Cells; M. Wang, F. Xu, R. Cheng <strong>and</strong> J. Xie; 216th ECS Meeting in Vienna, Austria;<br />

2009;<br />

4. Impedance Study of Anode Per<strong>for</strong>mance <strong>and</strong> Durability in a Working PEM Fuel Cell by<br />

F. Xu, L. Zhang, X. Cheng, Y. Zhang <strong>and</strong> Q.B. Fan, 215th ECS Meeting in Hawaii,<br />

American, 2008;<br />

5. In Situ AC Impedance Diagnosis of Hydrogen Oxidation in a PEMFC by Fan Xu, Xuan<br />

Cheng, Ying Zhang, <strong>and</strong> Qinbai Fan, 215th ECS Meeting in Hawaii, American, 2008;<br />

In situ investigation of hydrogen absorption in anode of PMFCs by Fan Xu, Xuan Cheng,<br />

Ying Zhang, <strong>and</strong> Qinbai Fan, 8th National Electrochemical Conference in Yang Zhou, P.R.<br />

China, 2007;<br />

Hao He<br />

Education<br />

2009- present Joint Ph.D. student in <strong>IUPUI</strong><br />

2008-2009 Ph.D. student Chemical Engineering, Hunan University, China<br />

2006-2008 Master student, Chemical Engineering, Hunan University, China<br />

2002-2006 B.S. Applied Chemistry, Hunan University, Changsha, China<br />

<strong>Research</strong> interests<br />

Zeolite membranes <strong>and</strong> their application<br />

Synthesis of zeolites (Y, X, A, MFI), mesoporous materials, <strong>and</strong> zeolite membranes<br />

Application of zeolite membranes in gas seperation <strong>and</strong> green chemistry by zeolite<br />

catalysts<br />

Dehydration of glycerol to high valued acrolein<br />

Synthesis of the catalysts (zeolite, transition metal oxide)<br />

Trans<strong>for</strong>mation of bio-mass such as dehydration of ethanol, glycerol, <strong>and</strong> latic acid<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 13


Materials characterization (XRD, SEM, TGA/DSC, BET, AAS, FTIR, UVs), analysis<br />

instruments (GC, GC-MS), thermal modeling.<br />

Li-ion battery safety project<br />

Synthesis of cathode materials (LiFePO 4 ), <strong>and</strong> anode materials (SnO 2 /C composite);<br />

Failure mechanisms of Li-ion batteries at overcharge/overdischarge conditions<br />

Li metal deposit in the Li-ion battery<br />

<strong>Research</strong> experience<br />

1. 2009-present Li-ion battery safety<br />

2. 2007-2009 Dehydration of glycerol to produce acrogenic<br />

3. 2006-2007 Synthesis of the Silicate-1 membrane <strong>and</strong> its application in separation of waste<br />

acid<br />

Publications<br />

4. Mei-xian Wang, Fan Xu, Qi Liu, Hao He, Jian Xie; Enhanced Catalytic Per<strong>for</strong>mance of Pt/C<br />

Catalysts Using Steam Etching Carbon Blacks as Support, under review of Carbon.<br />

5. <strong>The</strong> application of In-situ High Energy XRD in Li ion battery failure mechanism<br />

development (finished), Hao He, Fan Xu, Yang Ren, Jian Xie<br />

6. Failure mechanism of Li ion battery under over-discharging condition. Hao He, Fan Xu,<br />

Yang Ren, Jian Xie<br />

Section VI: Support Letters (insert 1- 2 pages as needed)<br />

Section VII: Appendix (Title of <strong>and</strong> in<strong>for</strong>mation on the status <strong>and</strong> outcomes of past MURI<br />

projects received by the Principal Mentor. Please insert 1 page summary per previous MURI<br />

project as needed according to template below. Maximum - 5 pages.)<br />

Title of Past MURI Project: Study of the Failure Mechanism of Li-Ion Batteries<br />

Date Awarded: 12/30/2010<br />

Date Completed: 07/30/2010<br />

Brief Description:<br />

Synchronal X-Ray Diffraction technology was employed to investigate the failure mechanism of<br />

LiFePO4 cell under overcharge <strong>and</strong> over discharge condition<br />

Outcomes:<br />

All the work had been finished. Two manuscripts had been finished <strong>for</strong> this task:<br />

1. Investigation of the failure of A123 18650 LiFePO4 cell under overcharge condition; Fan Xu,<br />

Hao He, YaDong Liu, Qi Liu, Mei-xian Wang, Clif Dun, Jian Xie ,under review of Journal of<br />

power source<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 14


2. Failure mechanism of LiFePO4 battery under over discharge condition; Hao He, Fan Xu,<br />

YaDong Liu, Qi Liu, Mei-xian Wang, Clif Dun, Jian Xie , , under review of Journal of power<br />

source;<br />

Poster presentations:<br />

Title: Muri final poster presentation<br />

Date:<br />

Students Involved: Upeksha Mahanama, Cemil Cihan Ozalevli, Philip Jamerson, Leon Charles<br />

Shagoury, Teoh, ShaoChen;<br />

Conference presentations:<br />

Title: Symposium on <strong>Research</strong> Opportunities in Electrochemical Energy Storage<br />

Date: Oct 7 to 8<br />

Students Involved: Hao He, Leon Charles Shagoury<br />

Publications:<br />

Title:<br />

Date:<br />

Students Involved:<br />

Section VIII: Signature<br />

Name <strong>and</strong> Signature of the Principal Mentor:<br />

(typing the full name suffices as signature <strong>for</strong> electronic copies)<br />

Jian Xie 3/10/2011<br />

______________________________________________________________________<br />

Name Signature Date<br />

MURI Mentor’s Project <strong>Proposal</strong> Form, Updated: 1-25-2011 15

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