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Radio Age - 1944, January - 36 Pages, 3.3 MB ... - VacuumTubeEra

Radio Age - 1944, January - 36 Pages, 3.3 MB ... - VacuumTubeEra

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Iili. JAMES HILI.IKK (LEFT) ANDDK. V. K.<br />

ZWORYKIN DEMONSTRATE THE NEW<br />

ELECTRON MICRO-ANALYZER. DR. HIL-<br />

LIER PREPARES TO INSERT A SPECIMEN,<br />

WHILE DR. ZWORYKIN HOLDS THE PHO-<br />

TOGRAPHIC PLATE.<br />

DEVICE IDENTIFIES<br />

ATOMS<br />

Electron Micrc-aimlyzer Deoehped by Dr. Hillier in RCA Laboratories<br />

Reveals Chemical Composition of<br />

IDENTIFICATION of atoms in<br />

ultra-microscopic particles of<br />

matter no larger than 1/100,000 of<br />

an inch in diameter can be accomplished<br />

quickly and accurately for<br />

the first time by a revolutionary<br />

new tool of science—the electron<br />

Tnicro-analyzer — developed experimentally<br />

by Dr. James Hillier of<br />

RCA Laboratories.<br />

Revealed by Dr. Hillier in a letter<br />

published in the current issue of<br />

the magazine Physical Review, the<br />

new instrument — like the RCA<br />

Electron Microscope-— promises to<br />

go far toward overcoming one of<br />

the great barriers to the accumulation<br />

of knowledge about the infinitesimally<br />

small particles of matter<br />

of which all things are made. Information<br />

vital to the solution of<br />

many practical problems in the<br />

physical, chemical, and biological<br />

sciences, according to Dr. Hillier,<br />

can be obtained.<br />

"The chemical elements constituting<br />

such unimaginably tiny objects<br />

as the head or tail of a bacterium<br />

or virus," he said in an interview<br />

today, "can be identified within a<br />

few minutes by this new instrument."<br />

Ultra-microscopic Matter.<br />

Supplementing the electron microscope,<br />

the micro-analyzer comes<br />

ever closer to observing the building<br />

blocks of nature, Dr. Hillier explained.<br />

Scientists in recent years<br />

have been turning up invaluable information<br />

as to the size, shape, and<br />

internal structure of microscopic<br />

particles of matter, and now they<br />

can identify the atoms of which<br />

they are made.<br />

"The vital question : "Of what<br />

particular atoms, or chemical elements,<br />

are these different particles<br />

of matter constructed' can be answered<br />

by the electron micro-analyzer,"<br />

he continued. "For the first<br />

time, the scientist, using this new<br />

instrument, will be able to determine<br />

the chemical constituents of a<br />

particle weighing only 10"^^, or<br />

1/1,000,000,000,000,000, grams.<br />

And, more imi)ortant still, he will be<br />

able to see the relationship of the<br />

particles to the rest of the specimen<br />

under examination."<br />

In operation, the micro-analyzer<br />

uses an "electron needle" of extraordinary<br />

fine focus to knock<br />

other electrons loose from their<br />

parent atoms in the specimen, measures<br />

the amount rf energy lost by<br />

tile incident electrons in the process,<br />

and thereby reveals the specimen's<br />

chemical content.<br />

"With the new instrument, the<br />

image of the specimen may be observed<br />

by means of an electron microscope,<br />

which is incorporated as<br />

a part of the micro-analyzer, and a<br />

selection made by the exact portion<br />

to be analyzed," Dr. Hillier said.<br />

"Then by manipulation of a few<br />

controls, a photographic exposure<br />

is made of what we call the 'electron<br />

velocity distribution.'<br />

"This results in a series of small<br />

marks on the photographic plate,<br />

each one of which indicates by its<br />

position the presence of a chemical<br />

element in the specimen. Thus, with<br />

one exposure, information is obtained<br />

that would have required<br />

weeks or months to obtain by present<br />

indirect methods, which too<br />

often result in failure."<br />

In explaining how the instrument<br />

works. Dr. Hillier pointed out that<br />

in the table of chemical elements<br />

each atom, or element, is differentiated<br />

from another by the number<br />

of electrons surrounding the atom's<br />

nucleus. The electrons are arranged<br />

around the nucleus in "shells," he<br />

added, and it is known how much<br />

energy, or voltage, is required to<br />

knock holes in the shells of different<br />

atoms.<br />

"In the micro-analyzer," he continued,<br />

"the electi'ons of the 'needle'<br />

that strike the selected area of the<br />

specimen are all moving with the<br />

same velocity, say 50,000 volts.<br />

After they have passed through the<br />

specimen area, some of the electrons—the<br />

ones that struck atoms<br />

—are traveling with less velocity,<br />

or energy.<br />

"The next thing of importance in<br />

micro-analysis is the fact that the<br />

energy loss suffered by the speeding<br />

electron is different for each<br />

chemical elements. What's more,<br />

the differences are large enough to<br />

be easily distinguished by a method<br />

of measuring electron velocities. If,<br />

[RADIO AGE 13]

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