EPA Method 1600 Series Dioxins and Furans 1600 Method Description 199-210 1613 Dioxins & Furans (HRGC/HRMS) 199 1614 Polybrominated Diphenyl Ethers 200 1618 Organochloride & Phosphorus Pesticides 201 1653 Chlorinated Phenolics in Pulp & Paper 202 1656 Organo Halide Pesticides 202-203 1657 Organo Phosphorus Pesticides 204 1658 Phenoxy - acid Herbicides 205 1659 Dazomet 205 1664 Oil and Grease 205 1665 PMI Semi-Volatiles (GC/MS) 206 1666A PMIVolatiles (GC/MS) 206 1667A PMI Polutants (HPLC) 207 1668 209 PCB Congeners (GC) 208-209 1671 PMI Semi-Volatiles (GC/FID) 210 1673 PEG-600 (HPLC) 210 5041 VOCs from Stack Gas Effluents 210 Method 1613 Method 1613 Dioxins & Furans by HRGC/HRMS Precision and Recovery Standard M-1613-PAR Bold (-04) $ 525 / 1 x 1 mL M-1613-PAR-PAK $ 2,100 / 5 x 1 mL All units in ng/mL in Nonane 17 comps. M-1613-CAL -01 -02 -03 -04 -05 2,3,7,8-Tetrachlorodibenzo-p-dioxin 0.5 2 10 40 200 2,3,7,8-Tetrachlorodibenzofuran 0.5 2 10 40 200 1,2,3,7,8-Pentachlorodibenzo-p-dioxin 2.5 10 50 200 1000 1,2,3,7,8-Pentachlorodibenzofuran 2.5 10 50 200 1000 2,3,4,7,8-Pentachlorodibenzofuran 2.5 10 50 200 1000 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin 2.5 10 50 200 1000 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin 2.5 10 50 200 1000 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin 2.5 10 50 200 1000 1,2,3,4,7,8-Hexachlorodibenzofuran 2.5 10 50 200 1000 1,2,3,6,7,8-Hexachlorodibenzofuran 2.5 10 50 200 1000 1,2,3,7,8,9-Hexachlorodibenzofuran 2.5 10 50 200 1000 2,3,4,6,7,8-Hexachlorodibenzofuran 2.5 10 50 200 1000 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin 2.5 10 50 200 1000 1,2,3,4,6,7,8-Heptachlorodibenzofuran 2.5 10 50 200 1000 1,2,3,4,7,8,9-Heptachlorodibenzofuran 2.5 10 50 200 1000 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin 5 20 100 400 2000 1,2,3,4,6,7,8,9-Octachlorodibenzofuran 5 20 100 400 2000 2,3,7,8 Isomers only Mix This solution is for those labs only determining the concentration of the two most toxic isomers. M-1613-DF $ 75 / 1 x 1 mL 40 ng/mL each in Nonane 2 comps. 2,3,7,8-Tetrachlorodibenzo-p-dioxin 2,3,7,8-Tetrachlorodibenzofuran Technical Note Native Solutions of the USEPA Method 1613 analytes can also be used for USEPA Method 23, 8280, 8290, EU Method EN-1948 and Japanese Methods JIS-K0311 and JIS-K0312. Calibration Set M-1613-CAL-SET (-01,-02,-03,-04,-05) All in ng/mL in Nonane $ 2,100 / 5 x 1 mL 17 comps. Over 40,000 <strong>Standards</strong>, just a click away (Over 10,000 Listed and over 30,000 formulated custom standards) AccuStandard.com Tel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • Web AccuStandard.com 199
1600 EPA Method 1600 Series Bromodiphenyl Ethers Method 1614 Bromodiphenyl Ether Mixtures Responding to the need for the analysis of polybrominated diphenyl ether (PBDE) congeners, the EPA has developed Method 1614. Method 1614 is recommended for analysis of aqueous, solid, tissue, and multi-phase environmental samples. AccuStandard has the largest offering of synthesized PBDEs, see Flame Retardant section for complete listing. Method 1614 PBDEs Standard Solution for Accuracy & Precision At stated conc.in Isooctane 39 comps. BDE-AAP-A BDE-AAP-A-15X Component $ 195 / 1 mL $ 750 / 1 mL ng/mL µg/mL 2-Bromodiphenyl ether (#1) 100 1.5 3-Bromodiphenyl ether (#2) 100 1.5 4-Bromodiphenyl ether (#3) 100 1.5 2,4-Dibromodiphenyl ether (#7) 100 1.5 2,4'-Dibromodiphenyl ether (#8) 100 1.5 2,6-Dibromodiphenyl ether (#10) 100 1.5 3,3'-Dibromodiphenyl ether (#11) 100 1.5 3,4-Dibromodiphenyl ether (#12) 100 1.5 3,4'-Dibromodiphenyl ether (#13) 100 1.5 4,4'-Dibromodiphenyl ether (#15) 100 1.5 2,2',4-Tribromodiphenyl ether (#17) 100 1.5 2,3',4-Tribromodiphenyl ether (#25) 100 1.5 2,4,4'-Tribromodiphenyl ether (#28) 100 1.5 2,4,6-Tribromodiphenyl ether (#30) 100 1.5 2,4',6-Tribromodiphenyl ether (#32) 100 1.5 2',3,4-Tribromodiphenyl ether (#33) 100 1.5 3,3',4-Tribromodiphenyl ether (#35) 100 1.5 3,4,4'-Tribromodiphenyl ether (#37) 100 1.5 2,2',4,4’-Tetrabromodiphenyl ether (#47) 100 1.5 2,2',4,5'-Tetrabromodiphenyl ether (#49) 100 1.5 2,3',4,4'-Tetrabromodiphenyl ether (#66) 100 1.5 2,3',4',6-Tetrabromodiphenyl ether (#71) 100 1.5 2,4,4',6-Tetrabromodiphenyl ether (#75) 100 1.5 3,3',4,4'-Tetrabromodiphenyl ether (#77) 100 1.5 2,2',3,4,4'-Pentabromodiphenyl ether (#85) 150 2.25 2,2',4,4',5-Pentabromodiphenyl ether (#99) 150 2.25 2,2',4,4',6-Pentabromodiphenyl ether (#100) 150 2.25 2,3,4,5,6-Pentabromodiphenyl ether (#116) 150 2.25 2,3',4,4',5-Pentabromodiphenyl ether (#118) 150 2.25 2,3',4,4',6-Pentabromodiphenyl ether (#119) 150 2.25 3,3',4,4',5-Pentabromodiphenyl ether (#126) 150 2.25 2,2',3,4,4',5'-Hexabromodiphenyl ether (#138) 200 3.0 2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 200 3.0 2,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 200 3.0 2,2',4,4',6,6'-Hexabromodiphenyl ether (#155) 200 3.0 2,3,4,4',5,6-Hexabromodiphenyl ether (#166) 200 3.0 2,2',3,4,4',5,6-Heptabromodiphenyl ether (#181) 250 3.75 2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 250 3.75 2,3,3',4,4',5,6-Heptabromodiphenyl ether (#190) 250 3.75 Br Br Commonly Occurring PBDE Congeners for Precision and Recovery BDE-COC $ 600 / 1 x 1 mL At stated conc.in Isooctane 14 comps. µg/mL 2,2',4-Tribromodiphenyl ether (#17) 5 2,4,4'-Tribromodiphenyl ether (#28) 5 2,2',4,4'-Tetrabromodiphenyl ether (#47) 5 2,3',4,4'-Tetrabromodiphenyl ether (#66) 5 2,3',4',6-Tetrabromodiphenyl ether (#71) 5 2,2',3,4,4’-Pentabromodiphenyl ether (#85) 5 2,2',4,4',5-Pentabromodiphenyl ether (#99) 5 2,2',4,4',6-Pentabromodiphenyl ether (#100) 5 2,2',3,4,4',5'-Hexabromodiphenyl ether (#138) 5 2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 5 2,2',4,4’,5,6'-Hexabromodiphenyl ether (#154) 5 2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 5 2,3,3',4,4’,5,6-Heptabromodiphenyl ether (#190) 5 Decabromodiphenyl ether (#209) 25 PBDE Congeners of <strong>Primary</strong> Interest BDE-CSM $ 225 / 1 x 1 mL At stated conc.in Isooctane:Toluene 8 comps. µg/mL 2,4,4'-Tribromodiphenyl ether (#28) 20 2,2',4,4'-Tetrabromodiphenyl ether (#47) 20 2,2',4,4',5-Pentabromodiphenyl ether (#99) 20 2,2',4,4',6-Pentabromodiphenyl ether (#100) 20 2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 20 2,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 20 2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 20 Decabromodiphenyl ether (#209) 200 Calibration Mix BDE-CM At stated conc.in Isooctane Matrix Spiking Solution BDE-MS At stated conc.in Isooctane $ 65 / 1 x 1 mL 8 comps. $ 40 / 1 x 1 mL 8 comps. BDE-CM BDE-MS µg/mL ng/mL 2,4,4'-Tribromodiphenyl ether (#28) 2.5 1 2,2',4,4'-Tetrabromodiphenyl ether (#47) 2.5 1 2,2',4,4',5-Pentabromodiphenyl ether (#99) 2.5 1 2,2',4,4',6-Pentabromodiphenyl ether (#100) 2.5 1 2,2',4,4',5,5'-Hexabromodiphenyl ether (#153) 2.5 1 2,2',4,4',5,6'-Hexabromodiphenyl ether (#154) 2.5 1 2,2',3,4,4',5',6-Heptabromodiphenyl ether (#183) 2.5 1 Decabromodiphenyl ether (#209) 25 10 Br O Br 200 AccuStandard is accredited to ISO/IEC 17025 and certified to ISO 9001