EPA Method 8000 Series

EPA Method 8000 Series 

Method 8270C/D Semi-Volatile by GC/MS as core mixtures 

Method 8270 

The primary analytes typically analyzed in Method 8270 version C and D have been formulated based on one of the following considerations: large 

core mixes, analyte retention time association to ISTD’s, similar functional groups, Third Party Certified Standards or as working level Ready-to-Inject 

standards 

Use of these Method 8270C/D components in 5 mixtures can save you time and money in preparing your calibration curves. Four high concentration 

solutions CLP-HC-BN-SET, CLP-HC-A-R, CLP-HC-X1 and Z-014E can be combined to give you the 92 typical analytes needed for Method 8270C/D. 

Product Z-014E-R can be used in lieu of Z-014E for those labs interested in adding pyridine to their target list. 

These mixtures can also serve as your second source requirements since they are independently prepared from product M-8270 (7 x 1 mL). 

Base-Neutral Mixture (44 components) 

CLP-HC-BN-R 

Acenaphthene 

Acenaphthylene 

Anthracene 

Azobenzene 

Benz[a]anthracene 

Benzo[b]fluoranthene 

Benzo[k]fluoranthene 

Benzo[g,h,i]perylene 

Benzo[a]pyrene 

4-Bromophenyl phenyl ether 

Butyl benzyl phthalate 

bis(2-Chloroethoxy)methane 

bis(2-Chloroethyl)ether 

bis(2-Chloro-1-methylethyl)ether 

2-Chloronaphthalene 

4-Chlorophenyl phenyl ether 

Chrysene 

Dibenz[a,h]anthracene 

Di-n-butyl phthalate 

1,2-Dichlorobenzene 



Diethyl phthalate 

Dimethyl phthalate 

2,4-Dinitrotoluene 


Di-n-octyl phthalate 

bis(2-Ethylhexyl)phthalate 

Fluoranthene 

Fluorene 

Hexachlorobenzene 

Hexachlorobutadiene 

Hexachlorocyclopentadiene 

Hexachloroethane 

Indeno[1,2,3-cd]pyrene 

Isophorone 

Naphthalene 

Nitrobenzene 

N-Nitrosodimethylamine 

N-Nitrosodiphenylamine 

N-Nitrosodi-n-propylamine 

Phenanthrene 

Pyrene 

1,2,4-Trichlorobenzene 

Benzidine Mixture (2 comps.) 

Z-014F 

Benzidine 

3,3'-Dichlorobenzidine 

Alternate Source Line (ASL) 

For complete listing of competitive 8270 

see the QC Section 

Technical Note 

Azobenzene was substituted for 1,2-diphenylhydrazine 

since it oxidizes to azobenzene under GC operating 

conditions. 

Base-Neutrals 

CLP-HC-BN-R 

$ 160 / 1 x 1 mL 

2.0 mg/mL each in Benzene :CH 2 Cl 2 :AcCN (2:2:1) 44 comps. 

CLP-HC-BN-R-PAK 

SAVE 20% $ 640 / 5 x 1 mL 

2.0 mg/mL each in Benzene :CH 2 Cl 2 :AcCN (2:2:1) 44 comps. 

Benzidine 

Z-014F 

$ 30 / 1 x 1 mL 

2.0 mg/mL each in MeOH 2 comps. 

Base-Neutral and Benzidine Sets 

CLP-HC-BN-SET 

CLP-HC-BN-SET-PAK 

$ 190 / 2 x 1 mL 

(CLP-HC-BN-R, Z-014F) 

SAVE 20% $ 760 / 5 x (2 x 1 mL) 

5 x (CLP-HC-BN-R, Z-014F) 

Acid Composite Mixture 

CLP-HC-A-R $ 55 / 1 x 1 mL 

2.0 mg/mL each in CH 2 Cl 2 19 comps. 

Benzoic acid 

4-Chloro-3-methylphenol 

2-Chlorophenol 

o-Cresol 

p-Cresol 

2,4-Dichlorophenol 


2,4-Dimethylphenol 

4,6-Dinitro-2-methylphenol 

2,4-Dinitrophenol 

Ethyl methanesulfonate 

Methyl methanesulfonate 

2-Nitrophenol 

4-Nitrophenol 

Pentachlorophenol 

Phenol 

2,3,4,6-Tetrachlorophenol 

2,4,5-Trichlorophenol 


Additional Analyte Solutions 

Composite #1 

Z-014E 

$ 30 / 1 x 1 mL 


Aniline 

Benzyl alcohol 

4-Chloroaniline 

Dibenzofuran 

Composite #2 

2-Methylnaphthalene 

2-Nitroaniline 



Z-014E-R 

$ 32 / 1 x 1 mL 


Aniline 



Dibenzofuran 





Pyridine 

Composite #3A 

CLP-HC-X1 $ 85 / 1 x 1 mL 


Acetophenone 

4-Aminobiphenyl 


Dibenz[a,j]acridine 

p-Dimethylaminoazobenzene 

7,12-Dimethylbenz[a]anthracene 

α,α-Dimethylphenethylamine 

Diphenylamine 

3-Methylcholanthrene 

1-Naphthylamine 


N-Nitrosodi-n-butylamine 

N-Nitrosopiperidine 

Pentachlorobenzene 

Pentachloronitrobenzene 

Phenacetin 

2-Picoline 

Pronamide 

1,2,4,5-Tetrachlorobenzene 

M-8270-07 $ 160 / 1 x 1 mL 


Aramite 

Chlorobenzilate 

Diallate 

2,4-D 

Dimethoate 

Dinoseb 

Disulfoton 

Famphur 

Kepone 

Methyl parathion 

Parathion 

Phorate 

Silvex (2,4,5-TP) 

Sulfotep 

Thionazin 

M-8270-08 

$ 65 / 1 x 1 mL 


3,3'-Dimethyl benzidine 

4-Nitroquinoline-1-oxide 

N-Nitrosodiethylamine 

N-Nitrosomethylethylamine 

N-Nitrosomorpholine 

N-Nitrosopyrrolidine 

5-Nitro-o-toluidine 

p-Phenylenediamine 

o-Toluidine 

M-8270-09 

$ 65 / 1 x 1 mL 


2-Acetyl aminofluorene 

m-Dinitrobenzene 

Hexachlorophene 

Hexachloropropene 

Isodrin 

Isosafrole 

Methapyrilene 

1,4-Naphthoquinone 

Safrole 

0,0,0-Triethyl phosphorothioate 

242 AccuStandard is accredited to ISO/IEC 17025 and certified to ISO 9001


Method 8270C/D (Continued) Auxiliary Standards 

Internal Standard 

Z-014J 

$ 80 / 1 x 1 mL 

Z-014J-PAK 

SAVE 37% $ 250 / 5 x 1 mL 


Naphthalene-d Acenaphthene-d 10 

1,4-Dichlorobenzene-d 4 Phenanthrene-d 10 

Chrysene-d 12 

8 

Perylene-d 12 

Surrogate Standards 

M-8270-SS 

$ 80 / 1 x 1 mL 

M-8270-SS-PAK 

SAVE 20% $ 320 / 5 x 1 mL 


Phenol-d 2-Fluorobiphenyl 

Nitrobenzene-d 5 2,4,6-Tribromophenol 

2-Fluorophenol 

5 

p-Terphenyl-d 14 

M-8270-SS-R 

M-8270-SS-R-PAK 

At stated conc.each in CH 2 Cl 2 :MeOH (4:1) 

2-Fluorobiphenyl (1.0 mg/mL) 

2-Fluorophenol (2.0 mg/mL) 

Nitrobenzene-d 5 (1.0 mg/mL) 

Base/Neutrals & Acids - Matrix Standard Spiking 

Solutions 

CLP-007-SET 

CLP-007-SET-PAK 

Base/Neutrals 

$ 75 / 1 x 1 mL 

SAVE 20% $ 300 / 5 x 1 mL 

6 comps. 

Phenol-d 5 (2.0 mg/mL) 

Terphenyl-d 14 (1.0 mg/mL) 

2,4,6-Tribromophenol (2.0 mg/mL) 

$ 35 / 2 x 1 mL 

SAVE 20% $ 140 / 5 x (2 x 1 mL) 

(CLP-007A, CLP-007B) 

CLP-007A 

$ 20 / 1 x 1 mL 


GC/MSTuning Standard 

M-625-TS-20X 

$ 40 / 1 x 1 mL 


Benzidine 

p,p'-DDT 

Calibration Check Compounds (CCC) 

CLP-011-SET 

Base/Neutrals 

$ 35 / set of 2 x 1 mL 

(includes CLP-011A and CLP-011B) 

CLP-011A 

$ 20 / 1 x 1 mL 


Acenaphthene 



Di-n-octylphthalate 

Acids 

DFTPP 


CLP-011B 

$ 20 / 1 x 1 mL 




2-Nitrophenol 

System Performance Check Compounds (SPCC) 

CLP-010 

$ 25 / 1 x 1 mL 


CLP-010-10X 

$ 25 / 1 x 1 mL 





Fluoranthene 

N-nitroso-diphenylamine 


Phenol 


4-Nitrophenol 

N-nitroso-di-n-propylamine 


Acenaphthene 



Acids 

N-nitroso-di-n-propylamine 

Pyrene 


CLP-007B 

$ 20 / 1 x 1 mL 




4-Nitrophenol 


Phenol 

Multi-Component Analytes 

Polychlorinated Biphenyls, Chlordane &Toxaphene 

Each at 1,000 µg/mL in Hexane 

AccuPAK (5 x 1 mL) 

SAVE 20% 

Aroclors# Cat. No. 1 mL Cat. No. PAK 

Aroclor 1016 C-216S-H-10X $ 20 C-216S-H-10X-PAK $ 80 

Aroclor 1221 C-221S-H-10X 20 C-221S-H-10X-PAK 80 








Pesticides 

Chlordane P-017S-H-10X $ 15 P-017S-H-10X-PAK $ 80 

Toxaphene P-093S-H-10X 15 P-093S-H-10X-PAK 80 

Tel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • Web AccuStandard.com 243


Method 8270C/D (Continued) Semi-Volatiles by Capillary Column GC/MS 


These Method 8270C/D formulations are designed based on the association of the analyte to a specific internal standard. These formulations allow 

for easy preparation of the typical analytes in the calibration curve. In addition, instrument/method problems can be rapidly diagnosed by examining 

those specific analytes and the associated internal standard in the affected part of the analysis. Save 

when ordering a complete set over 

individual solutions 

Complete 8270 Method Mixture Set 

M-8270-SET 

M-8270-R-SET 

M-8270-01 

$ 80 / 1 x 1 mL 


Aniline 








Ethylmethanesulfonate 


Methylmethanesulfonate 

2-Methylphenol 




Phenol 

2-Picoline 

M-8270-04A $ 45 / 1 x 1 mL 


4-Aminobiphenyl 

Anthracene 




Fluoranthene 



Phenanthrene 


$ 505 / 7 x 1 mL (M-8270-01,M-8270-02,M-8270-03,M-8270-04A,M-8270-04B,M-8270-05,M-8270-06) 

$ 480 / 7 x 1 mL (M-8270-01,M-8270-02,M-8270-03,M-8270-04A,M-8270-04B-R1,M-8270-05,M-8270-06) 

M-8270-02 

$ 80 / 1 x 1 mL 


Acetophenone 

Benzoic acid 






α,α-Dimethylphenethylamine 



Isophorone 


Naphthalene 

Nitrobenzene 

2-Nitrophenol 

N-Nitroso-di-n-butylamine 

N-Nitrosopiperidine 


M-8270-04B $ 35 / 1 x 1 mL 


Diphenylamine 

1,2-Diphenylhydrazine 



Phenacetin 

Pronamide 

Under EPA recommended GC conditions (Method 8270) the analyte 1,2-Diphenylhydrazine is converted in 

varying degrees to Azobenzene and breakdown products. According to our study, the use of an injection 

port temperature range (240°C - 300°C) will cause the 1,2-Diphenylhydrazine to break down. 

Substituting Azobenzene for 1,2-Diphenylhydrazine will allow analysis yielding a single peak regardless of 

the EPA recommended injection port temperature range used. 

Alternate Formulation 

M-8270-04B-R1 $ 35 / 1 x 1 mL 


Azobenzene 

Diphenylamine 



Phenacetin 

Pronamide 

M-8270-03 $ 120 / 1 x 1 mL 


Acenaphthene 





Dibenzofuran 






Fluorene 







4-Nitrophenol 

Pentachlorobenzene 

1,2,4,5-Tetrachlorobenzene 

2,3,4,6-Tetrachlorophenol 



M-8270-05 

$ 80 / 1 x 1 mL 


Benzidine 

Benzo[a]anthracene 


Butylbenzylphthalate 

Chrysene 


p-Dimethylaminoazobenzene 

Pyrene 

M-8270-06 $ 120 / 1 x 1 mL 






Dibenz[a,j]acridine 


7,12-Dimethylbenz[a]anthracene 

Di-n-octylphthalate 


3-Methylcholanthrene 

M-8270-07 $ 160 / 1 x 1 mL 


Aramite 

Chlorobenzilate 

Diallate 

2,4-D 

Dimethoate 

Dinoseb 

Disulfoton 

Famphur 

Kepone 


Parathion 

Phorate 


Sulfotep 

Thionazin 

M-8270-08 

$ 65 / 1 x 1 mL 


3,3'-Dimethyl benzidine 

4-Nitroquinoline-1-oxide 

N-Nitrosodiethylamine 

N-Nitrosomethylethylamine 

N-Nitrosomorpholine 

N-Nitrosopyrrolidine 

5-Nitro-o-toluidine 

p-Phenylenediamine 

o-Toluidine 

M-8270-09 

$ 65 / 1 x 1 mL 


2-Acetyl aminofluorene 

1,3-Dinitrobenzene 

Hexachlorophene 

Hexachloropropene 

Isodrin 

Isosafrole 

Methapyrilene 

1,4-Naphthoquinone 

Safrole 

O,O,O-Triethylphosphorothioate 



Method 8270C/D (Continued) Appendix IX Semi-Volatiles Analyzed by Method 8270 

M-8270-10 

2.0 mg/mL in MeOH 

sym-Trinitrobenzene 

M-8270-13-SET 

4-Aminoazobenzene 

3-Amino-9-ethylcarbazole 

o-Anisidine 

5-Chloro-2-methylaniline 

p-Cresidine 

2,4-Diaminotoluene 

$ 15 / 1 x 1 mL 

M-8270-10-R 

$ 15 / 1 x 1 mL 


Pyridine 

Additions to Method 8270 

sym-Trinitrobenzene 

$ 95 / 2 x 1 mL 

(M-8270-13A-R, M-8270-13B-R) 

M-8270-13A-R 

$ 85 / 1 x 1 mL 


4,4'-Methylenebis(N,N-dimethylaniline) 

4,4'-Methylene bis(2-chloroaniline) 

4,4'-Oxydianiline 

2-Picoline 

Pyridine 

2,4,5-Trimethylaniline 

Pesticides 

M-8270-16 

$ 50 / 1 x 1 mL 

1000 µg/mL each in CH 2 Cl 2 10 comps. 

Anilazine 

Azinphos methyl 

Barbamate 

Demeton (mixed isomers) 

Dichlone 

Dioxathion 

Mirex 

Sulfoxide 

Sulfallate 

Trifluralin 

M-8270-17 

$ 50 / 1 x 1 mL 


Brominal 

Captafol 

Captan 

Dinex 

Carbamates/Pesticides 

Dinocap 

Fluchloralin 

Nitrofen 

M-8270-18 

$ 75 / 1 x 1 mL 


Carbaryl 

Carbofuran 

Ethyl carbamate 

Mexacarbate 

Schradan (Octamethylpyrophosphoramide) 

Phenobarbital 


M-8270-13B-R 

$ 25 / 1 x 1 mL 

2.0 mg/mL each inTHF 3 comps. 

2-Aminoanthraquinone 

4-Chloro-1,2-phenylenediamine 

M-8270-14-SET 

M-8270-14A 

$ 35 / 1 x 1 mL 


m-Cresol 

o-Cresol 

Resorcinol 

Thiophenol 

tris(2,3-Dibromopropyl)phosphate 

Tri-p-tolyl phosphate 

M-8270-14B 

$ 35 / 1 x 1 mL 

2.0 mg/mL each inTHF 5 comps. 

p-Benzoquinone 

Hydroquinone 

Maleic anhydride 

Phthalic anhydride 

Trimethyl phosphate 

M-8270-14C 

$ 35 / 1 x 1 mL 

2.0 mg/mL each in CH 2 Cl 2 :MeOH (3:1) 5 comps. 

1-Acetyl-2-thiourea 

Diethyl sulfate 

Hexamethylphosphoramide 

4-Chloro-1,3-phenylenediamine 

3-Picolyl chloride HCL 

Toluene diisocyanate 

M-8270-15 

$ 95 / 1 x 1 mL 

1.0 mg/mL each in CH 2 Cl 2 :MeOH (19:1) 13 comps. 

Dibenzo[a,e]pyrene 

1,2-Dibromo-3-chloropropane 

Diethyl stilbestrol 



5,5-Diphenylhydantoin 

Mestranol 

$ 95 / 3 x 1 mL 

(M-8270-14A, M-8270-14B, M-8270-14C) 

Nicotine 

5-Nitroacenapthene 

5-Nitro-o-anisidine 

4-Nitrobiphenyl 

Propylthiouracil 

Strychnine 

Pesticides 

M-8270-19 

$ 50 / 1 x 1 mL 


Carbophenothion 

Coumaphos 

EPN 

Ethion 

Fensulfothion 

Fenthion 

Pesticide Mix 

Z-014C-R 

$ 95 / 1 x 1 mL 

Z-014C-R-PAK 

SAVE 20% $ 380 / 5 x 1 mL 

2.0 mg/mL each inToluene :Hexane (1:1) 20 comps. 

Aldrin 

α-BHC 

β-BHC 

γ-BHC 

δ-BHC 

α-Chlordane 

γ-Chlordane 

4,4'-DDD 

4,4'-DDE 

4,4'-DDT 

Leptophos 

Malathion 

Phosalone 

Imidan (Phosmet) 

Terbufos 

Tetrachlorvinphos 

M-8270-20 

$ 50 / 1 x 1 mL 


Chlorfenvinphos 

Ciodrin (Crotoxyphos) 

Dichlorvos 

Dicrotophos 

Mevinphos 

Azo Dye 

RAC-12-10X 

1.0 mg/mL in CH 2 Cl 2 

3,3'-Dimethoxylbenzidine 

Monocrotophos 

Naled 

Phosphamidon 

TEPP (Tetraethyl pyrophosphate) 

Dieldrin 

Endosulfan I 

Endosulfan II 

Endosulfan sulfate 

Endrin 

Endrin aldehyde 

Endrin ketone 

Heptachlor 

Heptachlor epoxide 

Methoxychlor 

$ 35 / 1 x 1 mL 

Alternate Source Line 

For complete listing of 

competitive 8270 see the QC Section 


Method 8270C/D 5 point Semi-Volatile Calibration Curve 


Ready-to-Inject Working Level Semi-Volatile Standards 

AccuStandard provides a 5 point semi-volatile calibration curve in 2 formats. One calibration curve already incorporates the internal standards in 

each level of the curve. To begin analysis, the chemist just cracks the ampule open and transfers the content to the autosampler vial. The second 

semi-volatile curve does not contain the internal standard. 

The analytical chemist will need to add 10 µL of internal standard to each level of the curve and the environmental samples as the vials are placed 

on the GC/MS. AccuStandard offers both types of curves to meet your laboratory's preference regarding the addition of internal standards. 


Target Analytes (Semi-Volatiles) 

Acenaphthene 


Aniline 

Anthracene 

Azobenzene 


Benzidine 



Benzoic acid 





Butyl benzyl phthalate 

Carbazole 









Chrysene 

o-Cresol 

p-Cresol 


Dibenzofuran 














Di-n-octyl phthalate 


Fluoranthene 

Fluorene 






Isophorone 


Naphthalene 




Nitrobenzene 

2-Nitrophenol 

4-Nitrophenol 





Phenanthrene 

Phenol 

Pyrene 

Pyridine 




Surrogates Analytes 

Phenol-d 2-Fluorobiphenyl 

Nitrobenzene-d 5 2,4,6-Tribromophenol 

2-Fluorophenol 

5 

p-Terphenyl-d 14 


AccuStandard has prepared both Semi-Volatile 

curves from special high concentration stocks. The 

useful shelf life for these 5 point curves is similar to 

the shelf life experienced at the environmental 

laboratory when the standard is prepared from 

previously used high concentrate stocks. 

Internal Standard Analytes 

Acenaphthene-d 10 

Chrysene-d 12 

1,4-Dichlorobenzene-d 4 

Naphthalene-d 8 

Perylene-d 12 

Phenanthrene-d 10 

Working Level Semi-Volatiles Curve 

With Internal Standards 

M-8270-CAL-IS-SET 

All solutions in CH 2 Cl 2 

$ 275 / 5 x 1 mL 

83 comps. 

Components Level 1 Level 2 Level 3 Level 4 Level 5 

(units in µg/mL) ( 2.5X ) ( 4X ) ( 6X ) ( 8X ) 

Target Analytes 20 50 80 120 160 

Surrogate Analytes 20 50 80 120 160 

Internal Analytes 40 40 40 40 40 

Level 2 Daily QCWorking Level 

CCC (with Internal Standard) 

M-8270-IS-WL-2.5X-5ML $ 275 / 1 x 5 mL 

M-8270-IS-WL-2.5X-10ML $ 425 / 1 x 10 mL 

At stated conc.in CH 2 Cl 2 

Working Level Semi-Volatiles Curve 

Without Internal Standards 

M-8270-CAL-SET 

All solutions in CH 2 Cl 2 

$ 250 / 5 x 1 mL 

77 comps. 

Level 2 Daily QCWorking Level 

CCC (without Internal Standard) 

M-8270-WL-2.5X-5ML $ 250 / 1 x 5 mL 

M-8270-WL-2.5X-10ML $ 400 / 1 x 10 mL 

Components Level 1 Level 2 Level 3 Level 4 Level 5 

(units in µg/mL) ( 2.5X ) ( 4X ) ( 6X ) ( 8X ) 

Target Analytes 20 50 80 120 160 

Surrogate Analytes 20 50 80 120 160 

At stated conc.in CH 2 Cl 2 



Ready-to-Inject Working Level Semi-Volatile Standards 

Method 8270C/D (Continued) 

Matrix Spike (SW 846) 

CLP-007-WL-50ML 

At stated conc.in MeOH 

4-Chloro-3-methyl phenol (200 µg/mL) 

2-Chlorophenol (200 µg/mL) 

4-Nitrophenol (200 µg/mL) 

Pentachlorophenol (200 µg/mL) 

Phenol (200 µg/mL) 

Acenaphthene (100 µg/mL) 


Prep Note 

$ 115 / 1 x 50 mL 

11 comps. 

1,4-Dichlorobenzene (100 µg/mL) 

2,4-Dinitrotoluene (100 µg/mL) 

N-Nitrosodi-n-propylamine (100 µg/mL) 

Pyrene (100 µg/mL) 

1,2,4-Trichlorobenzene (100 µg/mL) 

To help maximize instrument performance, add 10 µL of internal standard to 

a 1 mL sample extract. 

Z-014J 

$ 80 / 1 x 1 mL 

Z-014J-PAK 

SAVE 37% $ 250 / 5 x 1 mL 


Method 8270 Surrogate Spiking Solution 

M-8270-SS-R-WL-PAK 

M-8270-SS-R-WL-VAP 

At stated conc.in CH 2 Cl 2 :MeOH (4:1) 

2-Fluorobiphenyl (100 µg/mL) 

2-Fluorophenol (200 µg/mL) 

Nitrobenzene-d 5 (100 µg/mL) 

M-8270-SS-R 

M-8270-SS-R-PAK 

At stated conc.in CH 2 Cl 2 :MeOH (4:1) 

2-Fluorobiphenyl (1000 µg/mL) 

2-Fluorophenol (2000 µg/mL) 

Nitrobenzene-d 5 (1000 µg/mL) 

Prep Note 

$ 190 / 5 x 10 mL 

$ 300 / 10 x 10 mL 

6 comps. 

Phenol-d 5 (200 µg/mL) 

Terphenyl-d 14 (100 µg/mL) 

2,4,6-Tribromophenol (200 µg/mL) 

$ 75 / 1 x 1 mL 

SAVE 20% $ 300 / 5 x 1 mL 

6 comps. 

Phenol-d 5 (2000 µg/mL) 

Terphenyl-d 14 (1000 µg/mL) 

2,4,6-Tribromophenol (2000 µg/mL) 

To ensure extraction efficiency add, 1 mL of Surrogate to the sample. 

Method 8270-8275 



Chrysene-d 12 

8 

Perylene-d 12 

Benzidine Solution 

M-625C-1-40X 

2.0 mg/mL in CH 2 Cl 2 

Benzidine 

$ 20 / 1 x 1 mL 

CLP Surrogate Spiking Solution 

CLP-031-R-WL-25ML 

$ 110 / 1 x 25 mL 

CLP-031-R-WL-50ML 

$ 190 / 1 x 50 mL 


8 comps. 

2-Chlorophenol-d 4 (150 µg/mL) Nitrobenzene-d 5 (100 µg/mL) 

1,2-Dichlorobenzene-d 4 (100 µg/mL) Phenol-d 6 (150 µg/mL) 

2-Fluorobiphenyl (100 µg/mL) p-Terphenyl-d 14 (100 µg/mL) 

2-Fluorophenol (150 µg/mL) 2,4,6-Tribromophenol (150 µg/mL) 

GC/MSTuning Solution 

M-625-TS 

$ 40 / 1 x 1 mL 

M-625-TS-PAK 

SAVE 20% $ 160 / 5 x 1 mL 


Benzidine 

p,p'-DDT 

DFTPP GC/MSTuning Solution 

M-625C-3 

M-625C-3-PAK 

25 µg/mL in CH 2 Cl 2 

Decafluorotriphenylphosphine (DFTPP) 

Matrix Spike (3/90 SOW) 

CLP-007R-WL-50ML 


4-Chloro-3-methyl phenol (150 µg/mL) 

2-Chlorophenol (150 µg/mL) 

4-Nitrophenol (150 µg/mL) 

Pentachlorophenol (150 µg/mL) 

Phenol (150 µg/mL) 



DFTPP 


$ 20 / 1 x 1 mL 

SAVE 20% $ 80 / 5 x 1 mL 

$ 115 / 1 x 50 mL 

11 comps. 

1,4-Dichlorobenzene (100 µg/mL) 

2,4-Dinitrotoluene (100 µg/mL) 

N-Nitrosodi-n-propylamine (100 µg/mL) 


1,2,4-Trichlorobenzene (100 µg/mL) 

AccuStandard has found that benzidine degrades in multi-component semivolatile 

solutions. For this reason, the benzidine in any calibration curve 

should be used as a qualitative retention time marker. Reported hits for 

benzidine should be quantitatively determined by analyzing a single benzidine 

solution or by using the benzidine response observed in the Daily GC/MS 

tuning solution. 

Method 8275A (Thermal Extraction/GC/FID/MS) 

Semi-Volatiles by Thermal Chromatography 

Semi-Volatiles 

M-8275 $ 60 / 1 x 1 mL 

1.0 mg/mL each inAcetone 17 comps. 

Aldrin 



Carbazole 




Dibenzothiophene 




Diphenylamine 

Fluorene 



Naphthalene 

Phenanthrene 

Pyrene 

Z-014J 

$ 80 / 1 x 1 mL 

Z-014J-PAK 

SAVE 37% $ 250 / 5 x 1 mL 




Chrysene-d 12 

8 

Perylene-d 12 

Alternate Source Line 

For complete listing of 

competitive 8270 see the QC Section 



Method 8280-8310, Canadian, FL 

Method 8280A Dioxins & Furans by HRGC/LRMS 

Dioxin Mixture 

M-8280A 

$ 150 / 1 x 1 mL 

M-8280A-PAK 

SAVE 20% $ 600 / 5 x 1 mL 

5 µg/mL each inToluene 5 comps. 

2,3,7,8-Tetrachlorodibenzo-p-dioxin 

1,2,3,7,8-Pentachlorodibenzo-p-dioxin 

1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin 

Furan Mixture 

M-8280B 

$ 150 / 1 x 1 mL 

M-8280B-PAK 

SAVE 20% $ 600 / 5 x 1 mL 


2,3,7,8-Tetrachlorodibenzofuran 

1,2,3,7,8-Pentachlorodibenzofuran 

1,2,3,4,7,8-Hexachlorodibenzofuran 

Column Performance Check 

M-8280-CPC 

$ 200 / 1 x 1 mL 






1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin 

Octachlorodibenzo-p-dioxin 

1,2,3,4,6,7,8-Heptachlorodibenzofuran 

Octachlorodibenzofuran 


1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin 


Canadian Environmental Method Multi-Component 

Dioxin Mixtures 

CustomWindow Defining Mixture 

D-WD 20,000 ng/mL in Toluene $ 1,100 / 1 x 1 mL 

D-WD-2.5X 50,000 ng/mL in Toluene $ 2,000 / 1 x 1 mL 

7 comps. 

1,2,4,6,8/1,2,4,7,9-Pentachlorodibenzo-p-dioxin (Isomer pair) 


1,2,4,6,7,9/1,2,4,6,8,9-Hexachlorodibenzo-p-dioxin (Isomer pair) 





Custom Calibration Mixture 

D-CAL 20,000 ng/mL in Toluene $ 900 / 1 x 1 mL 

D-CAL-2.5X 50,000 ng/mL in Toluene $ 1,600 / 1 x 1 mL 

6 comps. 







Column Performance Check 

M-8280-CPC 

$ 200 / 1 x 1 mL 

5.0 µg/mL each inToluene 7 comps. 






1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin 


Formulations 

atHighest Concentration for 

Economical Prices 

Method 8310 PAHs by HPLC 

PAH Mixture 

M-8310 $ 75 / 1 x 1 mL 

M-8310-PAK 

SAVE 20% $ 300 / 5 x 1 mL 

0.5 mg/mL each inAcCN 16 comps. 

Acenaphthene 


Anthracene 






Surrogate Standard 

M-8310-SS 

M-8310-SS-PAK 

0.1 mg/mL inAcetonitrile 

Decafluorobiphenyl 

Chrysene 


Fluoranthene 

Fluorene 


Naphthalene 

Phenanthrene 

Pyrene 

PAH Quality Control Calibration Mixture 

M-610-QC 

At stated conc.inAcCN 

Acenaphthene (0.1 mg/mL) 

Acenaphthylene (0.1 mg/mL) 

Anthracene (0.1 mg/mL) 

Benzo[a]anthracene (0.01 mg/mL) 

Benzo[a]pyrene (0.01 mg/mL) 

Benzo[b]fluoranthene (0.01 mg/mL) 

Benzo[g,h,i]perylene (0.01 mg/mL) 

Benzo[k]fluoranthene (0.005 mg/mL) 

$ 10 / 1 x 1 mL 

SAVE 20% $ 40 / 5 x 1 mL 

Internal Standard Post Supercritical Fluid Extraction 

M-8310-SFE-IS-100X 

M-8310-SFE-IS-100X-PAK 

20,000 µg/mL inAcCN:THF (1:1) 

Biphenyl 

Florida Method PAH Mixture 

$ 35 / 1 x 1 mL 

16 comps. 

Chrysene (0.01 mg/mL) 

Dibenz[a,h]anthracene (0.01 mg/mL) 

Fluoranthene (0.01 mg/mL) 

Fluorene (0.1 mg/mL) 

Indeno[1,2,3-cd]pyrene (0.01 mg/mL) 

Naphthalene (0.1 mg/mL) 

Phenanthrene (0.1 mg/mL) 

Pyrene (0.01 mg/mL) 

$ 10 / 1 x 1 mL 

SAVE 20% $ 40 / 5 x 1 mL 

Z-014G-FL 

$ 85 / 1 x 1 mL 

2.0 mg/mL each in CH 2 Cl 2 :Benzene 18 comps. 

Acenaphthene 


Anthracene 






Chrysene 


Fluoranthene 

Fluorene 


Naphthalene 

Phenanthrene 

Pyrene 



Standards of Interest 

For more Canadian Methods see the Regional Section of this catalog, pages 

256-258. 



Florida Administrative Code (continued) PAHs by HPLC 

Performance Check Solution 

M-610-QC-FL 

M-610-QC-FL-PAK 


Acenaphthene (0.1 mg/mL) 

Acenaphthylene (0.1 mg/mL) 

Anthracene (0.1 mg/mL) 

Benz[a]anthracene (0.01 mg/mL) 

Benzo[a]pyrene (0.01 mg/mL) 

Benzo[b]fluoranthene (0.01 mg/mL) 

Benzo[g,h,i]perylene (0.01 mg/mL) 

Benzo[k]fluoranthene (0.005 mg/mL) 


Matrix Spiking Solution 

M-610-MS 

M-610-MS-PAK 


$ 35 / 1 x 1 mL 

SAVE 20% $ 140 / 5 x 1 mL 

18 comps. 

Dibenz[a,h]anthracene (0.01 mg/mL) 

Fluoranthene (0.01 mg/mL) 

Fluorene (0.1 mg/mL) 

Indeno[1,2,3-cd]pyrene (0.01 mg/mL) 

1-Methyl naphthalene (0.1 mg/mL) 

2-Methyl naphthalene (0.1 mg/mL) 

Naphthalene (0.1 mg/mL) 



$ 30 / 1 x 1 mL 

SAVE 20% $ 120 / 5 x 1 mL 

6 comps. 

Buy AccuPaks 

Save 20-40% 5 x 1 mL 

Florida Method 

Benz[a]pyrene (0.5 mg/mL) 


1-Methylnaphthalene (5.0 mg/mL) 

2-Methylnaphthalene (5.0 mg/mL) 



PAH Mix Additions 

H-001S/002S-M-20X 

$ 30 / 1 x 1 mL 


1-Methyl naphthalene 

2-Methyl naphthalene 

Polynuclear Aromatic Hydrocarbons (HPLC) 

M-8310-FL 

$ 50 / 1 x 1 mL 

M-8310-FL-PAK 

SAVE 20% $ 200 / 5 x 1 mL 


M-8310-FL-SET 

$ 360 / 18 x 1 mL 

Acenaphthene M-8310-FL-01 $ 20 

Acenaphthylene M-8310-FL-02 20 

Anthracene M-8310-FL-03 20 

Benz[a]anthracene M-8310-FL-04 25 

Benzo[a]pyrene M-8310-FL-05 25 

Benzo[b]fluoranthene M-8310-FL-06 30 

Benzo[g,h,i]perylene M-8310-FL-07 30 

Benzo[k]fluoranthene M-8310-FL-08 30 

Chrysene M-8310-FL-09 25 

Dibenz[a,h]anthracene M-8310-FL-10 20 

Fluoranthene M-8310-FL-11 20 

Fluorene M-8310-FL-12 20 

Indeno[1,2,3-cd]pyrene M-8310-FL-13 35 

1-Methylnaphthalene M-8310-FL-14 20 

2-Methylnaphthalene M-8310-FL-15 20 

Naphthalene M-8310-FL-16 20 

Phenanthrene M-8310-FL-17 20 

Pyrene M-8310-FL-18 20 

Polynuclear Aromatic Hydrocarbons (HPLC) 

M-8310-QC-ATI 

M-8310-QC-ATI-PAK 



Acenaphthylene (2000 µg/mL) 

Anthracene (100 µg/mL) 

Benz[a]anthracene (100 µg/mL) 

Benzo[a]pyrene (100 µg/mL) 

Benzo[b]fluoranthene (200 µg/mL) 

Benzo[g,h,i]perylene (200 µg/mL) 

Benzo[k]fluoranthene (100 µg/mL) 

Chrysene (100 µg/mL) 

$ 55 / 1 x 1 mL 

SAVE 20% $ 220 / 5 x 1 mL 

18 comps. 

Dibenz[a,h]anthracene (200 µg/mL) 

Fluoranthene (200 µg/mL) 

Fluorene (200 µg/mL) 

Indeno[1,2,3-cd]pyrene (100 µg/mL) 

1-Methylnaphthalene (1000 µg/mL) 

2-Methylnaphthalene (1000 µg/mL) 

Naphthalene (1000 µg/mL) 

Phenanthrene (100 µg/mL) 


AccuStandard's Environmental Efforts 

1.As part of a recent facility expansion, and in cooperation with 

the local utilities, AccuStandard invested almost $100,000 on 

energy conservation and controls.The estimated impact on the 

environment is similar to that of planting 19 acres of trees. 

2.Many customers avoid the environmental impact and cost of 

disposing of unused standards.One of the only standards 

manufacturers to offer this, Accustandard's "On-Going Stability 

Program" allows us to extend the expiration date on a standard if 

our testing over time on a specific lot warrants it. 

3.Many every day steps such as using recycled paper for the 

tens of thousands of catalogs every year, educating customers 

on the value of using standards as pre-made solutions rather 

than buying large quantities of neats. 



Method 8315/8315A Ketones/Aldehydes by HPLC 


Aldehyde Mixture 

M-8315 $ 20 / 1 x 1 mL 

M-8315-PAK 

SAVE 20% $ 80 / 5 x 1 mL 

1.0 mg/mL each in H 2 O 2 comps. 

Acetaldehyde 

Formaldehyde 

Aldehyde Individuals 

Acetaldehyde (1.0 mg/mL in H 2 O) M-8315-01 $ 20 / 1 x 1 mL 

Formaldehyde (1.0 mg/mL in H 2 O) M-8315-02 $ 20 / 1 x 1 mL 

Aldehyde as DNPH Derivatives 

M-8315-DNPH-10ML 

$ 30 / 1 x 10 mL 

1.0 mg/mL each in MeOH 2 comps.as DNPH Derivatives 

Acetaldehyde 

Formaldehyde 

Option 1 (Samples Collected fromWater,Air, Soil, 

Waste or Stacks by Method 0011) 

Carbonyl Mixture 

M-8315-R1 

$ 65 / 1 x 1 mL 


Acetaldehyde 

Butanal (Butyraldehyde) 

Crotonaldehyde 

Cyclohexanone 

Decanal 

Formaldehyde 

Heptanal 

Hexanal (Hexaldehyde) 

Nonanal 

Octanal 

Pentanal (Valeraldehyde) 

Propanal (Propionaldehyde) 

Carbonyl DNPH Derivative Mixture 

M-8315-R2-DNPH 

$ 120 / 1 x 1 mL 

0.1 mg/mL each inAcCN 15 comps.as DNPH derivatives 

Acetaldehyde 

Acetone 

Acrolein 

Benzaldehyde 



2,5-Dimethylbenzaldehyde 

Formaldehyde 

Carbonyl Compound Set 

M-8315-R3-10X-SET 

Each at 1.0 mg/mL inAcCN 

Acetaldehyde (01) 

Acetone (02) 

Acrolein (03) 

Benzaldehyde (04) 

Butanal (05) 

Crotonaldehyde (06) 

Cyclohexanone (07) 

Decanal (08) 

2,5-Dimethylbenzaldehyde (09) 

Formaldehyde (10) 

Carbonyl DNPH Derivative Set 

M-8315-R-DNPH-SET 

Each at 0.1 mg/mL inAcCN 


Isovaleraldehyde 



m-Tolualdehyde 

o-Tolualdehyde 

p-Tolualdehyde 

Heptanal (11) 

Hexanal (12) 

Isovaleraldehyde (13) 

Nonanal (14) 

Octanal (15) 

Pentanal (16) 

Propanal (17) 

m-Tolualdehyde (18) 

o-Tolualdehyde (19) 

p-Tolualdehyde (20) 

$ 200 / 20 x 1 mL 

$ 250 / 20 x 1 mL 

20 comps.as DNPH Derivatives 

Carbonyl DNPH Derivative Mixture 

M-8315-R1-DNPH 

$ 90 / 1 x 1 mL 

0.1 mg/mL each inAcCN 12 comps.as DNPH derivatives 

Acetaldehyde 



Cyclohexanone 

Decanal 

Formaldehyde 

Heptanal 


Nonanal 

Octanal 



Acetaldehyde (01) 

Acetone (02) 

Acrolein (03) 

Benzaldehyde (04) 

Butanal (Butyraldehyde) (05) 

Crotonaldehyde (06) 

Cyclohexanone (07) 

Decanal (08) 

2,5-Dimethylbenzaldehyde (09) 

Formaldehyde (10) 

Heptanal (11) 

Hexanal (Hexaldehyde) (12) 

Isovaleraldehyde (13) 

Nonanal (14) 

Octanal (15) 

Pentanal (Valeraldehyde) (16) 

Propanal (Propionaldehyde) (17) 

m-Tolualdehyde (18) 

o-Tolualdehyde (19) 

p-Tolualdehyde (20) 

Option 2 (Samples Collected from Indoor Air by 

Method 0100) 

Carbonyl Mixture 

M-8315-R2 

$ 75 / 1 x 1 mL 


Acetaldehyde 

Acetone 

Acrolein 

Benzaldehyde 



2,5-Dimethylbenzaldehyde 

Formaldehyde 


Isovaleraldehyde 



m-Tolualdehyde 

o-Tolualdehyde 

p-Tolualdehyde 

Method 8316 Acrolein, Acrylamide, Acrylonitrile by HPLC 


For initial Method 8315 development, AccuStandard offers individual analyte 

sets (20 x 1 mL) for both the Carbonyl compounds and their corresponding 

DNPH derivatives. Use of these sets will allow the analytical chemist to 

rapidly establish individual analyte retention times and to troubleshoot 

possible extraction recovery problems. 

Method 8318 N-Methylcarbamates by HPLC 

M-8316 $ 20 / 1 x 1 mL 

1.0 mg/mL each inWater 3 comps. 

Acrolein 

Acrylamide 

Acrylonitrile 

N-Methylcarbamates 

M-8318-SET 

Each at 0.1 mg/mL in MeOH 

M-8318M 

Mixture,0.1 mg/mL each in MeOH 

Aldicarb (01) 

Aldicarb sulfone (02) 

Carbaryl (03) 

Carbofuran (04) 

Dioxacarb (05) 

3-Hydroxycarbofuran (06) 

Methiocarb (07) 

Methomyl (08) 

Promecarb (09) 

Propoxur (10) 

$ 140 / 10 x 1 mL 

$ 60 / 1 x 1 mL 

10 comps. 



Method 8321 Non-Volatile Compounds by HPLC/TSP/MS or 

UV Solvent Extractable 

Chlorinated Phenoxyacid Herbicide Mix 

M-8321-HERB 

$ 75 / 1 x 1 mL 


Dalapon 

Dicamba 

2,4-D 

2,4-D, butoxyethanol ester 

2,4-D, ethylhexyl ester 

2,4-DB 

Dichlorprop 

Organophosphorus Pesticide Mix 

Dinoseb 

MCPA 

MCPP 


2,4,5-T 

2,4,5-T, butyl ester 

2,4,5-T, butoxyethanol ester 

M-8321-OP 

$ 75 / 1 x 1 mL 


Asulam 

Dichlorvos 

Dimethoate 

Disulfoton 

Famphur 

Fensulfothion 

Merphos 

Methomyl 


Monocrotophos 

Naled 

Phorate 

Thiofanox 

Trichlorfon 

Tris(2,3-Dibromopropyl)phosphate 

Method 8325 Benzidines & Nitrogen containing Pesticides 

by L-L or L-S Extraction & RP HPLC/Particle Beam/MS 

Benzidine/Pesticide Mix 

M-553 $ 95 / 1 x 1 mL 

At stated conc.inAcCN :MeOH (1:1) 

13 comps. 

Benzidine (250 µg/mL) 

Benzoylprop ethyl (350 µg/mL) 

Caffeine (300 µg/mL) 

Carbaryl (1,000 µg/mL) 

o-Chlorophenyl thiourea (750 µg/mL) 

3,3'-Dichlorobenzidine (250 µg/mL) 

3,3'-Dimethoxybenzidine (750 µg/mL) 

Performance Check Solution 

M-553-PC 

0.1 mg/mL inAcCN 

DFTPPO (Decafluorotriphenylphosphine oxide) 

3,3'-Dimethylbenzidine (350 µg/mL) 

Diuron (450 µg/mL) 

Linuron (1,300 µg/mL) 

Monuron (400 µg/mL) 

Rotenone (3,200 µg/mL) 

Siduron (450 µg/mL) 

$ 20 / 1 x 1 mL 

‡ To delay premature breakdown of thermally labile products in transit we 

suggest shipping with a “Cold Pack” 


Method 8323 Organometallic Tin Analysis by Electrospray Ion Trap Mass Spectrometry 

The following Organo-Tin standards were originally formulated to meet custom applications for a number of our customers. AccuStandard has 

introduced the below set of standards as regular catalog items to meet the increased requests for Organo-Tin standards. The environmental interest 

in these compounds stems from their addition to the list of endocrine disrupters. Organo-Tin compounds such as Tributyl-Tin were used as marine 

antifouling agents and Triphenyl-Tin as a crop pesticide. 

Organometallic Butyltin Chloride 

Standard 

OMT-001 

$ 40 / 1 x 1 mL 

OMT-001-PAK SAVE 20% $ 160 / 5 x 1 mL 


Tri-n-propyltin 


OMT-003 

$ 30 / 1 x 1 mL 



Tetra-n-propyl tin 


OMT-005 

$ 40 / 1 x 1 mL 



Butyltin trichloride 

Dibutyltin dichloride 

Tetrabutyltin 

Tributyltin chloride 

Tri-n-propyltin chloride 

Tetra-n-propyl tin 

Organometallic Phenyltin 

Chloride Standard 

OMT-002 

$ 40 / 1 x 1 mL 



Diphenyltin dichloride 

Phenyltin trichloride 

Tetraphenyltin 

Triphenyltin chloride 

Tripentyltin Chloride 


OMT-004 

$ 30 / 1 x 1 mL 



Tripentyltin chloride 

Tetrapentyltin 


OMT-006 

$ 30 / 1 x 1 mL 



Tetrapentyltin 

Over 40,000 Standards, 

just a click away 

(Over 10,000 Listed and over 30,000 formulated 

custom standards) 

AccuStandard.com 



Explosives 


Method 8330 TNT Metabolites 

Analyte Concentration Solvent Cat. No. Price 

(µg/mL) 

(1 mL) 

1,3-Dinitrobenzene 100 AcCN : MeOH (1:1) M-8330-01-0.1X $ 20 

2,4-Dinitrotoluene 100 AcCN : MeOH (1:1) M-8330-02-0.1X 20 

2,6-Dinitrotoluene 100 AcCN : MeOH (1:1) M-8330-03-0.1X 20 

Nitrobenzene 100 AcCN : MeOH (1:1) M-8330-06-0.1X 20 

2-Nitrotoluene 100 AcCN : MeOH (1:1) M-8330-07-0.1X 15 



TNT 100 AcCN : MeOH (1:1) M-8330-11-0.1X 20 

1,3,5-Trinitrobenzene 100 AcCN : MeOH (1:1) M-8330-12-0.1X 20 

2-Amino-4,6-dinitrotoluene 100 AcCN : MeOH (1:1) M-8330-13-0.1X 20 

4-Amino-2,6-dinitrotoluene 100 AcCN : MeOH (1:1) M-8330-14-0.1X 20 

2,4-Diamino-6-nitrotoluene 100 AcCN M-8330-ADD-12 40 

2,4-Diamino-4-nitrotoluene 100 AcCN M-8330-ADD-13 40 

2,2',6,6'-Tetranitro-4,4'-azoxytoluene 100 AcCN : MeOH (1:1) M-8330-ADD-15 75 

2,2',6,6'-Tetranitro-4,4'-azotoluene 100 AcCN M-8330-ADD-17 100 

4,4',6,6'-Tetranitro-2,2'-azotoluene 100 AcCN M-8330-ADD-19 100 

2-Hydroxylamino-4,6-dinitrotoluene * 100 AcCN M-8330-ADD-18 115 

4-Hydroxylamino-2,6-dinitrotoluene * 100 AcCN M-8330-ADD-20 100 

Hexanitrostilbene (HNS) NEW 100 AcCN M-8330-ADD-26 60 

3,5-Dinitrotoluene NEW 100 AcCN : MeOH (1:1) M-8330-ADD-39 75 

* (3 month stability) 

Explosives by HPLC Set 

M-8330-R-SET ‡ $ 175 / 14 x 1 mL 

Each at 100 µg/mL inAcCN :MeOH (1:1) 

M-8330-R-10X-SET ‡ $ 210 / 14 x 1 mL 

Each at 1000 µg/mL inAcCN :MeOH (1:1) 

1,3-Dinitrobenzene (01) 

2,4-Dinitrotoluene (02) 

2,6-Dinitrotoluene (03) 

HMX (04) 

RDX (05) 

Nitrobenzene (06) 

2-Nitrotoluene (07) 



Tetryl (10) 

TNT (11) 

1,3,5-Trinitrobenzene (12) 

2-Amino-4,6-dinitrotoluene (13) 

4-Amino-2,6-dinitrotoluene (14) 

Method 8330 Additional Explosives by HPLC 

Analyte Concentration Solvent Cat. No. Price 

(µg/mL) 

(1 mL) 

1,3-Dinitrobenzene 100 AcCN : MeOH (1:1) M-8330-01-0.1X $ 20 

HMX 100 AcCN : MeOH (1:1) M-8330-04-0.1X 20 

RDX 100 AcCN : MeOH (1:1) M-8330-05-0.1X 20 

Tetryl 100 AcCN : MeOH (1:1) M-8330-10-0.1X 20 

Nitroglycerin 100 EtOH M-8330-ADD-1 20 

1000 EtOH M-8330-ADD-1-10X 30 

PETN 100 MeOH M-8330-ADD-2 20 

1000 MeOH M-8330-ADD-2-10X 30 

Picric acid 100 AcCN : MeOH (1:1) M-8330-ADD-3 20 

3,5-Dinitroaniline 100 AcCN : MeOH (1:1) M-8330-ADD-4 30 

EGDN 100 AcCN M-8330-ADD-5 20 

Nitroguanidine 100 MeOH M-8330-ADD-6 20 

Nitromethane 100 MeOH M-8330-ADD-7 20 

Hydrazine 100 MeOH M-8330-ADD-8 20 

1,2-Diaminopropane 100 MeOH M-8330-ADD-9 20 

Guanidine nitrate 100 MeOH M-8330-ADD-10 20 

PYX(2,6-bis,bis-(pricrylamine)-3,5-dinitropyridine 100 AcCN M-8330-ADD-11 20 

1,3,5-Triamino-2,4,6-trinitrobenzene (TATB) 40 Dimethyl formamide M-8330-ADD-14-DMF 40 

2,3-Dimethyl-2,3-dinitrobutane (DMNB) 100 AcCN M-8330-ADD-21 30 

Picramic acid 100 AcCN : MeOH (1:1) M-8330-ADD-22 30 

2,4,6-Triaminotoluene trihydrochloride N/A 10 mg M-8330-ADD-23N 25 

Triacetone triperoxide (TATP) 100 AcCN M-8330-ADD-24 75 

Hexamethylenetriperoxide diamine (HMTD) 100 AcCN M-8330-ADD-25 75 

Hexanitrostilbene (HNS) 100 AcCN M-8330-ADD-26 60 

Ammonium picrate 100 AcCN M-8330-ADD-27 25 

Trimethylolethane trinitrate 100 AcCN : MeOH (1:1) M-8330-ADD-28 30 

2,4,6-Trinitroresorcinol NEW 100 AcCN : MeOH (1:1) M-8330-ADD-29 60 

1-Nitroglycerin NEW 100 AcCN : MeOH (1:1) M-8330-ADD-31 20 

2-Nitroglycerin NEW 100 AcCN : MeOH (1:1) M-8330-ADD-32 20 

1,2-Dinitroglycerin NEW 100 AcCN : MeOH (1:1) M-8330-ADD-33 20 

1,3-Dinitroglycerin NEW 100 AcCN : MeOH (1:1) M-8330-ADD-34 20 

DEGDN NEW 100 AcCN : MeOH (1:1) M-8330-ADD-36 30 

Hexanitrodiphenylamine NEW 100 AcCN : MeOH (1:1) M-8330-ADD-37 40 

N-Nitrodimethylamine NEW 100 AcCN M-8330-ADD-40 75 

TEGDN NEW 100 AcCN M-8330-ADD-41 30 


AccuStandard complies with ATF and other 

regulations for manufacuring and shipping 

explosives. 


DMNB (M-8330-ADD-21) is a required taggant 

added to commercially manufactured plastic 

explosives. 

Additional Explosive Standards 


Explosive & Related Compounds by 

SPE & Capillary Column GC/MS 


Also see Explosive Intermediate 

(GC/ECD) 

‡ To delay premature breakdown of thermally labile products in 

transit we suggest shipping with a “Cold Pack” 



Method 8330 Multi-Component Formulations for Explosive Analysis 

The following A and B mixes provide better resolution between possible coeluting analytes, assisting the chemist to optimize the HPLC system. 

We suggest, when first performing Method 8330 development, to purchase the high concentration 14 x 1 mL set “M-8330-R-10X-SET”. 

M-8330A ‡ 

$ 40 / 1 x 1 mL 

0.1 mg/mL each inAcCN:MeOH (1:1) 

M-8330A-10X ‡ 

$ 50 / 1 x 1 mL 

1.0 mg/mL each inAcCN:MeOH (1:1) 7 comps. 



HMX 

Nitrobenzene 

RDX 

1,3,5-Trinitrobenzene 

TNT 

M-8330A-R ‡ 

$ 45 / 1 x 1 mL 


M-8330A-R-10X ‡ 

$ 55 / 1 x 1 mL 


2-Amino-4,6-dinitrotoluene 



HMX 

Composite Explosive Mixture 


M-8330-IS 

M-8330-IS-PAK 



Nitrobenzene 

RDX 


TNT 

M-8330-R 

$ 110 / 1 x 1 mL 

M-8330-R-PAK 

SAVE 20% $ 440 / 5 x 1 mL 

1.0 mg/mL each in MeOH:AcCN (1:1) 14 comps. 




HMX 

RDX 

Nitrobenzene 

2-Nitrotoluene 



Tetryl 

TNT 




$ 15 / 1 x 1 mL 

SAVE 20% $ 60 / 5 x 1 mL 

M-8330B ‡ 

$ 25 / 1 x 1 mL 


M-8330B-10X ‡ 

$ 40 / 1 x 1 mL 


Tetryl 





M-8330B-R ‡ 

$ 30 / 1 x 1 mL 


M-8330B-R-10X ‡ 

$ 45 / 1 x 1 mL 




Tetryl 





M-8330B-R2 ‡ 

$ 30 / 1 x 1 mL 


M-8330B-R2-10X ‡ 

$ 40 / 1 x 1 mL 



Tetryl 



M-8330-SS 






‡ To delay premature breakdown of thermally labile products in 

transit we suggest shipping with a “Cold Pack” 

$ 20 / 1 x 1 mL 


Method 8410 Semi-Volatiles by GC/FTIR 


M-8410-IS 

$ 30 / 1 x 1 mL 

M-8410-IS-PAK 

SAVE 20% $ 120 / 5 x 1 mL 


Method 8440 Total Petroleum Hydrocarbon 

Total Recoverable Petroleum Hydrocarbon Mix 

M-8440 $ 20 / 1 x 1 mL 

M-8440-PAK 

SAVE 20% $ 80 / 5 x 1 mL 

At stated conc.inTetrachloroethene 

3 comps. 

1-Fluoronaphthalene p-Terphenyl-d 14 

Chlorobenzene (0.10 w/w %) 

n-Hexadecane (0.15 w/w %) 

Isooctane (0.15 w/w %) 

Method 8430 bis(2-Chloroethyl)ether & Hydrolysis Products 

M-8430 $ 20 / 1 x 1 mL 

1.0 mg/mL each inWater 5 comps. 


2-Chloroethanol 

2-(2-Chloroethoxy)-ethanol 

Diethylene glycol 

Ethylene glycol 

Silica Gel Cleanup Calibration Solution 

M-8440-SGC 

M-8440-SGC-PAK 

10.0 mg/mL inTetrachloroethene 

Corn Oil 

$ 10 / 1 x 1 mL 

SAVE 20% $ 40 / 5 x 1 mL 

Total Petroleum Hydrocarbon Concentrate Mix 

M-8440-CON 

M-8440-CON-PAK 

Chlorobenzene (25.0 vol %) 

n-Hexadecane (37.5 vol %) 

$ 30 / 1 x 1 mL 

SAVE 20% $ 120 / 5 x 1 mL 

3 comps. 

Isooctane (37.5 vol %)

EPA Method 8000 Series

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