EPA Method 8000 Series

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EPA Method 8000 Series Method 8270C/D (Continued) Appendix IX Semi-Volatiles Analyzed by Method 8270 M-8270-10 2.0 mg/mL in MeOH sym-Trinitrobenzene M-8270-13-SET 4-Aminoazobenzene 3-Amino-9-ethylcarbazole o-Anisidine 5-Chloro-2-methylaniline p-Cresidine 2,4-Diaminotoluene $ 15 / 1 x 1 mL M-8270-10-R $ 15 / 1 x 1 mL 2.0 mg/mL each in MeOH 2 comps. Pyridine Additions to Method 8270 sym-Trinitrobenzene $ 95 / 2 x 1 mL (M-8270-13A-R, M-8270-13B-R) M-8270-13A-R $ 85 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 12 comps. 4,4'-Methylenebis(N,N-dimethylaniline) 4,4'-Methylene bis(2-chloroaniline) 4,4'-Oxydianiline 2-Picoline Pyridine 2,4,5-Trimethylaniline Pesticides M-8270-16 $ 50 / 1 x 1 mL 1000 µg/mL each in CH 2 Cl 2 10 comps. Anilazine Azinphos methyl Barbamate Demeton (mixed isomers) Dichlone Dioxathion Mirex Sulfoxide Sulfallate Trifluralin M-8270-17 $ 50 / 1 x 1 mL 1000 µg/mL each in CH 2 Cl 2 7 comps. Brominal Captafol Captan Dinex Carbamates/Pesticides Dinocap Fluchloralin Nitrofen M-8270-18 $ 75 / 1 x 1 mL 1000 µg/mL each in CH 2 Cl 2 6 comps. Carbaryl Carbofuran Ethyl carbamate Mexacarbate Schradan (Octamethylpyrophosphoramide) Phenobarbital Method 8270 M-8270-13B-R $ 25 / 1 x 1 mL 2.0 mg/mL each inTHF 3 comps. 2-Aminoanthraquinone 4-Chloro-1,2-phenylenediamine M-8270-14-SET M-8270-14A $ 35 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 6 comps. m-Cresol o-Cresol Resorcinol Thiophenol tris(2,3-Dibromopropyl)phosphate Tri-p-tolyl phosphate M-8270-14B $ 35 / 1 x 1 mL 2.0 mg/mL each inTHF 5 comps. p-Benzoquinone Hydroquinone Maleic anhydride Phthalic anhydride Trimethyl phosphate M-8270-14C $ 35 / 1 x 1 mL 2.0 mg/mL each in CH 2 Cl 2 :MeOH (3:1) 5 comps. 1-Acetyl-2-thiourea Diethyl sulfate Hexamethylphosphoramide 4-Chloro-1,3-phenylenediamine 3-Picolyl chloride HCL Toluene diisocyanate M-8270-15 $ 95 / 1 x 1 mL 1.0 mg/mL each in CH 2 Cl 2 :MeOH (19:1) 13 comps. Dibenzo[a,e]pyrene 1,2-Dibromo-3-chloropropane Diethyl stilbestrol 1,2-Dinitrobenzene 1,4-Dinitrobenzene 5,5-Diphenylhydantoin Mestranol $ 95 / 3 x 1 mL (M-8270-14A, M-8270-14B, M-8270-14C) Nicotine 5-Nitroacenapthene 5-Nitro-o-anisidine 4-Nitrobiphenyl Propylthiouracil Strychnine Pesticides M-8270-19 $ 50 / 1 x 1 mL 1000 µg/mL each in CH 2 Cl 2 12 comps. Carbophenothion Coumaphos EPN Ethion Fensulfothion Fenthion Pesticide Mix Z-014C-R $ 95 / 1 x 1 mL Z-014C-R-PAK SAVE 20% $ 380 / 5 x 1 mL 2.0 mg/mL each inToluene :Hexane (1:1) 20 comps. Aldrin α-BHC β-BHC γ-BHC δ-BHC α-Chlordane γ-Chlordane 4,4'-DDD 4,4'-DDE 4,4'-DDT Leptophos Malathion Phosalone Imidan (Phosmet) Terbufos Tetrachlorvinphos M-8270-20 $ 50 / 1 x 1 mL 1000 µg/mL each in CH 2 Cl 2 9 comps. Chlorfenvinphos Ciodrin (Crotoxyphos) Dichlorvos Dicrotophos Mevinphos Azo Dye RAC-12-10X 1.0 mg/mL in CH 2 Cl 2 3,3'-Dimethoxylbenzidine Monocrotophos Naled Phosphamidon TEPP (Tetraethyl pyrophosphate) Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Methoxychlor $ 35 / 1 x 1 mL Alternate Source Line For complete listing of competitive 8270 see the QC Section Tel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • Web AccuStandard.com 245
Method 8270C/D 5 point Semi-Volatile Calibration Curve EPA Method 8000 Series Ready-to-Inject Working Level Semi-Volatile Standards AccuStandard provides a 5 point semi-volatile calibration curve in 2 formats. One calibration curve already incorporates the internal standards in each level of the curve. To begin analysis, the chemist just cracks the ampule open and transfers the content to the autosampler vial. The second semi-volatile curve does not contain the internal standard. The analytical chemist will need to add 10 µL of internal standard to each level of the curve and the environmental samples as the vials are placed on the GC/MS. AccuStandard offers both types of curves to meet your laboratory's preference regarding the addition of internal standards. Method 8270 Target Analytes (Semi-Volatiles) Acenaphthene Acenaphthylene Aniline Anthracene Azobenzene Benz[a]anthracene Benzidine Benzo[b]fluoranthene Benzo[k]fluoranthene Benzoic acid Benzo[g,h,i]perylene Benzo[a]pyrene Benzyl alcohol 4-Bromophenyl phenyl ether Butyl benzyl phthalate Carbazole 4-Chloroaniline bis(2-Chloroethoxy)methane bis(2-Chloroethyl)ether bis(2-Chloro-1-methylethyl)ether 4-Chloro-3-methylphenol 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenyl phenyl ether Chrysene o-Cresol p-Cresol Dibenz[a,h]anthracene Dibenzofuran Di-n-butyl phthalate 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Diethyl phthalate 2,4-Dimethylphenol Dimethyl phthalate 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octyl phthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno[1,2,3-cd]pyrene Isophorone 2-Methylnaphthalene Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitrosodimethylamine N-Nitrosodiphenylamine N-Nitrosodi-n-propylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Surrogates Analytes Phenol-d 2-Fluorobiphenyl Nitrobenzene-d 5 2,4,6-Tribromophenol 2-Fluorophenol 5 p-Terphenyl-d 14 Technical Note AccuStandard has prepared both Semi-Volatile curves from special high concentration stocks. The useful shelf life for these 5 point curves is similar to the shelf life experienced at the environmental laboratory when the standard is prepared from previously used high concentrate stocks. Internal Standard Analytes Acenaphthene-d 10 Chrysene-d 12 1,4-Dichlorobenzene-d 4 Naphthalene-d 8 Perylene-d 12 Phenanthrene-d 10 Working Level Semi-Volatiles Curve With Internal Standards M-8270-CAL-IS-SET All solutions in CH 2 Cl 2 $ 275 / 5 x 1 mL 83 comps. Components Level 1 Level 2 Level 3 Level 4 Level 5 (units in µg/mL) ( 2.5X ) ( 4X ) ( 6X ) ( 8X ) Target Analytes 20 50 80 120 160 Surrogate Analytes 20 50 80 120 160 Internal Analytes 40 40 40 40 40 Level 2 Daily QCWorking Level CCC (with Internal Standard) M-8270-IS-WL-2.5X-5ML $ 275 / 1 x 5 mL M-8270-IS-WL-2.5X-10ML $ 425 / 1 x 10 mL At stated conc.in CH 2 Cl 2 Working Level Semi-Volatiles Curve Without Internal Standards M-8270-CAL-SET All solutions in CH 2 Cl 2 $ 250 / 5 x 1 mL 77 comps. Level 2 Daily QCWorking Level CCC (without Internal Standard) M-8270-WL-2.5X-5ML $ 250 / 1 x 5 mL M-8270-WL-2.5X-10ML $ 400 / 1 x 10 mL Components Level 1 Level 2 Level 3 Level 4 Level 5 (units in µg/mL) ( 2.5X ) ( 4X ) ( 6X ) ( 8X ) Target Analytes 20 50 80 120 160 Surrogate Analytes 20 50 80 120 160 At stated conc.in CH 2 Cl 2 246 AccuStandard is accredited to ISO/IEC 17025 and certified to ISO 9001
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